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Sample records for acoustic chemometrics monitoring

  1. Near infrared and acoustic chemometrics monitoring of volatile fatty acids and dry matter during co-digestion of manure and maize silage

    Lomborg, Carina J.; Holm-Nielsen, Jens Bo; Oleskowicz-Popiel, Piotr; Esbensen, Kim H.

    2009-01-01

    accuracy) and RPD between 2.8 and 3.6 (acceptable precision). A second experiment employed at-line monitoring with both near infrared spectroscopy and acoustic chemometrics. A larger calibration span was obtained for total solids by spiking. Both process analytical modalities were validated with respect to......In this study, two process analytical technologies, near infrared spectroscopy and acoustic chemometrics, were investigated as means of monitoring a maize silage spiked biogas process. A reactor recirculation loop which enables sampling concomitant with on-line near infrared characterisation was...... applied. Near infrared models resulted in multivariate models for total and volatile solids with ratio of standard error of performance to standard deviation (RPD) values of 5 and 5.1. indicating good on-line monitoring prospects. The volatile fatty acid models had slopes between 0.83 and 0.92 (good...

  2. Acoustic chemometric prediction of total solids in bioslurry

    Ihunegbo, Felicia; Madsen, Michael; Esbensen, Kim;

    2012-01-01

    several earlier dedicated attempts. A full-scale feasibility study based on standard addition experiments involving natural plant biomass was conducted using multivariate calibration (Partial Least Squares Regression, PLS-R) of acoustic signatures against dry matter content (total solids, TS). Prediction...... range of 5.8–10.8% w/w dry matter. Based on these excellent prediction performance measures, it is concluded that acoustic chemometrics has come of age as a full grown PAT approach for on-line monitoring of dry matter (TS) in complex bioslurry, with a promising application potential in other biomass...

  3. Acoustic multivariate condition monitoring - AMCM

    Rosenhave, P.E. [Vestfold College, Maritime Dept., Toensberg (Norway)

    1997-12-31

    In Norway, Vestfold College, Maritime Department presents new opportunities for non-invasive, on- or off-line acoustic monitoring of rotating machinery such as off-shore pumps and diesel engines. New developments within acoustic sensor technology coupled with chemometric data analysis of complex signals now allow condition monitoring of hitherto unavailable flexibility and diagnostic specificity. Chemometrics paired with existing knowledge yields a new and powerful tool for condition monitoring. By the use of multivariate techniques and acoustics it is possible to quantify wear and tear as well as predict the performance of working components in complex machinery. This presentation describes the AMCM method and one result of a feasibility study conducted onboard the LPG/C `Norgas Mariner` owned by Norwegian Gas Carriers as (NGC), Oslo. (orig.) 6 refs.

  4. Acoustic monitoring method and device

    The present invention provides a method of eliminating resonance noises upon acoustically monitoring the operation state of power plants and plant equipments whether they are normal or not, to improve sensitivity for detecting abnormalities. Namely, a microphone detects acoustic signals including leaking sounds and converts them into electric signals. An amplifier amplifies the electric signals to an appropriate level. A noise eliminating section eliminates resonance noises other than the leaking sounds. An abnormality judging section judges presence of abnormality based on the level of the acoustic signals of the leaking sounds. With such a constitution, a plurality of resonance noises generated also during normal plant operation are automatically eliminated. Since resonance noises as a factor of lowering the sensitivity for abnormal sound detection are not included in the acoustic signals, the sensitivity for the abnormal sound detection is improved. Accordingly, the performance of the acoustic monitoring device is improved. (I.S.)

  5. PORTABLE ACOUSTIC MONITORING PACKAGE (PAMP)

    John L. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Patrick Browning

    2004-07-20

    The Portable Acoustic Monitoring Package (PAMP) has been designed to record and monitor the acoustic signal in natural gas transmission lines. In particular the three acoustic signals associated with a line leak. The system is portable ({approx}30 lbs) and is designed for line pressures up to 1000 psi. It has become apparent that cataloging of the various background acoustic signals in natural gas transmission line is very important if a system to identify leak signals is to be developed. The low-pressure (0-200 psig) laboratory test phase has been completed and a number of field trials have been conducted. Before the cataloging phase could begin, a few problems identified in field trials identified had to be corrected such as: (1) Decreased microphone sensitivity at line pressures above 250 psig. (2) The inability to deal with large data sets collected when cataloging the variety of signals in a transmission line. (3) The lack of an available online acoustic calibration system. These problems have been solved and the WVU PAMP is now fully functional over the entire pressure range found in the Natural Gas transmission lines in this region. Field portability and reliability have been greatly improved. Data collection and storage have also improved to the point were the full acoustic spectrum of acoustic signals can be accurately cataloged, recorded and described.

  6. PORTABLE ACOUSTIC MONITORING PACKAGE (PAMP)

    John l. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Deepak Mehra

    2003-07-01

    The 1st generation acoustic monitoring package was designed to detect and analyze weak acoustic signals inside natural gas transmission lines. Besides a microphone it housed a three-inch diameter aerodynamic acoustic signal amplifier to maximize sensitivity to leak induced {Delta}p type signals. The theory and test results of this aerodynamic signal amplifier was described in the master's degree thesis of our Research Assistant Deepak Mehra who is about to graduate. To house such a large three-inch diameter sensor required the use of a steel 300-psi rated 4 inch weld neck flange, which itself weighed already 29 pounds. The completed 1st generation Acoustic Monitoring Package weighed almost 100 pounds. This was too cumbersome to mount in the field, on an access port at a pipeline shut-off valve. Therefore a 2nd generation and truly Portable Acoustic Monitor was built. It incorporated a fully self-contained {Delta}p type signal sensor, rated for line pressures up to 1000 psi with a base weight of only 6 pounds. This is the Rosemont Inc. Model 3051CD-Range 0, software driven sensor, which is believed to have industries best total performance. Its most sensitive unit was purchased with a {Delta}p range from 0 to 3 inch water. This resulted in the herein described 2nd generation: Portable Acoustic Monitoring Package (PAMP) for pipelines up to 1000 psi. Its 32-pound total weight includes an 18-volt battery. Together with a 3 pound laptop with its 4-channel data acquisition card, completes the equipment needed for field acoustic monitoring of natural gas transmission pipelines.

  7. Acoustic emission leak monitoring system LMS-96

    On-line acoustic emission leak monitoring under industrial conditions of nuclear power plants is a problem with specific features setting specific demands on the leak monitoring system. The paper briefly reviews those problems (attenuation pattern of a real structure, acoustic background, alarm system, etc.) and the solution of some of them is discussed. Information is presented on the Acoustic Emission Leak Monitoring System LMS-96 by SKODA NUCLEAR MACHINERY and the system's function is briefly described. (author)

  8. Acoustic transducer for nuclear reactor monitoring

    Disclosed is a transducer to monitor a parameter and produce an acoustic signal from which the monitored parameter can be recovered. The transducer comprises a modified Galton whistle which emits a narrow band acoustic signal having a frequency dependent upon the parameter being monitored, such as the temperature of the cooling media of a nuclear reactor. Multiple locations within a reactor are monitored simultaneously by a remote acoustic receiver by providing a plurality of transducers each designed so that the acoustic signal it emits has a frequency distinct from the frequencies of signals emitted by the other transducers, whereby each signal can be unambiguously related to a particular transducer. 8 claims, 1 figure

  9. Chemometrics and visible-near infrared spectroscopic monitoring of red wine fermentation in a pilot scale.

    Cozzolino, Daniel; Parker, Mango; Dambergs, Robert G; Herderich, Markus; Gishen, Mark

    2006-12-20

    The modern wine industry needs tools for process control and quality assessment in order to better manage fermentation or bottling processes. During wine fermentation it is important to measure both substrate and product concentrations (e.g. sugars, phenolic compounds), however, the analysis of these compounds by traditional means requires sample preparation and in some cases several steps of purification are needed. The combination of visible/near-infrared (Vis/NIR) spectroscopy and chemometrics potentially provides an ideal solution to accurately and rapidly monitor physical or chemical changes in wine during processing without the need for chemical analysis. The aim of this study was to assess the possibility of combining spectral and multivariate techniques, such as principal component analysis (PCA), discriminant partial least squares (DPLS), or linear discriminant analysis (LDA), to monitor time-related changes that occur during red wine fermentation. Samples (n = 652) were collected at various times from several pilot scale fermentations with grapes from either Cabernet Sauvignon or Shiraz varieties, over three vintages (2001-2003) and scanned using a monochromator instrument (Foss-NIRSystems 6500, Silver Spring, MD) in transmission mode (400-2,500 nm). PCA was used to demonstrate consistent progressive spectral changes that occur through the time course of the fermentation. LDA using PCA scores showed that regardless of variety or vintage, samples belonging to a particular time point in fermentation could be correctly classified. This study demonstrates the potential of Vis/NIR spectroscopy combined with chemometrics, as a tool for the rapid monitoring of red wine fermentation. PMID:16817241

  10. An acoustical model based monitoring network

    Wessels, P.W.; Basten, T.G.H.; Eerden, F.J.M. van der

    2010-01-01

    In this paper the approach for an acoustical model based monitoring network is demonstrated. This network is capable of reconstructing a noise map, based on the combination of measured sound levels and an acoustic model of the area. By pre-calculating the sound attenuation within the network the noi

  11. Acoustic Monitoring for Spaceflight Vehicle Applications Project

    National Aeronautics and Space Administration — This SBIR will develop and demonstrate acoustic sensor technology enabling real-time, remotely performed measuring and monitoring of sound pressure levels and noise...

  12. Prototype acoustic resonance spectroscopy monitor

    This report reports on work performed for the International Atomic Energy Agency (IAEA) through the Program Office for Technical Assistance (POTAS). In this work, we investigate possible applications of nondestructive acoustics measurements to facilitate IAEA safeguards at bulk processing facilities. Two different acoustic techniques for verifying the internal structure of a processing tank were investigated. During this effort we also examined two acoustic techniques for assessing the fill level within a processing tank. The fill-level measurements could be made highly portable and have an added safeguards advantage that they can also detect stratification of fill material. This later application may be particularly useful in confirming the absence of stratification in plutonium processing tanks before accountability samples are withdrawn

  13. Chemometrical exploration of the wet precipitation chemistry from the Austrian Monitoring Network (1988-1999).

    Stanimirova, I; Daszykowski, M; Massart, D L; Questier, F; Simeonov, V; Puxbaum, H

    2005-03-01

    The present paper deals with the application of different chemometric methods to an environmental data set derived from the monitoring of wet precipitation in Austria (1988-1999). These methods are: principal component analysis (PCA); projection pursuit (PP); density-based spatial clustering of application with noise (DBSCAN); ordering points to identify the clustering structures (OPTICS); self-organizing maps (SOM), also called the Kohonen network; and the neural gas (NG) network. The aim of the study is to introduce some new approaches into environmetrics and to compare their usefulness with already existing techniques for the classification and interpretation of environmental data. The density-based approaches give information about the occurrence of natural clusters in the studied data set, which, however, do not occur in the case presented here; information about high-density zones (very similar samples) and extreme samples is also obtained. The partitioning techniques (clustering, but also neural gas and Kohonen networks) offer an opportunity to classify the objects of interest into several defined groups, the patterns of ionic concentration of which can be studied in detail. The visual aids, such as the color map and the Kohonen map, for each site are very helpful in understanding the relationships between samples and between samples and variables. All methods, and in particular projection pursuit, give information about samples with extreme characteristics. PMID:15737459

  14. Distributed acoustic sensing: towards partial discharge monitoring

    Rohwetter, Philipp; Eisermann, René; Krebber, Katerina

    2015-09-01

    We report on the successful application of distributed acoustic sensing (DAS) to the detection of partial discharge (PD). A detection limit of about 1 nC discharge magnitude was achieved for PD in a real-scale model of a high voltage termination. Dedicated ultrasonic fibre-optic transducers were interrogated using coherent optical time-domain Rayleigh backscatter reflectometry (C-OTDR). Random quadrature demodulation was employed for retrieving relevant acoustic information from the raw C-OTDR backscatter traces. To our knowledge, our results are a first-time demonstration that quasi-distributed fibre-optic acoustic sensing is a candidate technology for the acoustic partial discharge monitoring of power cable joints and terminations.

  15. Ultrasonic wavequide sensor for NPP acoustic monitoring

    Design of a waveguide sensor for NPP equipment acoustic testing is considered taking as an example a water coolant steam content monitor designed for application in an active emission-receipt regime. The sensor comprises an acoustic transducer, a waveguide with a suspension and a sensitive element. The transducer includes a disk piezoelement of TsTS-19 ceramics. A longitudinal wave waveguide, produced of a steel wire 0.8-1.2 mm in diameter, can transmit signals within the 50-1000 kHz range. A capillar tube 1.6x0.2 mm in diameter and 200 mm long with sealed ends is used as a sensitive element. The sensor operation is based on determining ultrasonic pulse attennuation in the capillar, which changes depending on acoustic wave resistance of the following-round coolant and depends on steam content. In passive regime the sensor may be applied for acoustic-emission monitoring of various equipment. In this case a matching device, providing for emission signal transmission from the monitored object surface to the waveguide, should be introduced instead of the sensitive element

  16. Sensor combination and chemometric modelling for improved process monitoring in recombinant E. coli fed-batch cultivations.

    Clementschitsch, Franz; Jürgen, Kern; Florentina, Pötschacher; Karl, Bayer

    2005-11-01

    The key objective for the optimisation of recombinant protein production in bacteria is to optimize the exploitation of the host cell's synthesis potential. Recent studies show that the novel concept of transcription rate control allows the tuning of recombinant gene expression in relation to the metabolic capacity of the host cell. To adjust the inducer-biomass ratio to a tolerable level, real-time knowledge about key process variables is paramount. Since there are no reliable online-sensors for key variables such as biomass or recombinant product, it is necessary to relate available online signals to process variables by mathematical models. To improve chemometric modelling of process variables, dielectric spectroscopy and a multi-wavelength online fluorescence sensor for two-dimensional fluorescence spectroscopy were applied in a series of recombinant Escherichia coli fed-batch cultivations applying two different process operation states. Dielectric spectroscopy signals were closely correlated to biomass, while two-dimensional fluorescence spectroscopy allowed the monitoring of fluorescent biogenic components. Chemometric modelling of key process variables with two different modelling techniques showed that this sensor combination greatly improved the estimation (i.e. reduce error magnitude) of process variables in recombinant E. coli cultivations, thereby enhancing process monitoring capabilities. PMID:16139381

  17. Acoustic Emission Health Monitoring of Steel Bridges

    Pahlavan, Pooria Lotfollah; Paulissen, Joep; Pijpers, Richard; Hakkesteegt, Henk; Jansen, Rob

    2014-01-01

    Despite extensive developments in the field of Acoustic Emission (AE) for monitoring fatigue cracks in steel structures, the implementation of AE systems for large-scale bridges is hindered by limitations associated with instrumentation costs and signal processing complexities. This paper sheds light on some of the most important challenges in the utilization of AE systems for steel bridge decks. These challenges are mainly related to the multi-modal character of guided waves, and the expensi...

  18. Acoustic emission monitoring of composite containment systems

    This paper considers two different types of composite containment system, and two different types of acoustic emission (AE) monitoring approach. The first system is a composite reinforced pressure vessel (CRPV) which is monitored both during construction and in-service using a broadband modal acoustic emission (MAE) technique. The second system is a membrane cargo containment system which is monitored using both a global as well as a local AE technique. For the CRPV, the damage assessment is concerned mainly with the integrity of the composite outer layer at the construction stage, and possible fatigue cracking of the inner steel liner at the in-service stage. For the membrane tank, the damage assessment is concerned with locating and quantifying any abnormal porosities that might develop in-service. By comparing and contrasting the different types of structural system and different monitoring approaches inferences are drawn as to what role AE monitoring could take in the damage assessment of other types of composite containment system. (Detailed technical data have not been included, due to client confidentiality constraints.)

  19. Distributed acoustic sensing for pipeline monitoring

    Hill, David; McEwen-King, Magnus [OptaSense, QinetiQ Ltd., London (United Kingdom)

    2009-07-01

    Optical fibre is deployed widely across the oil and gas industry. As well as being deployed regularly to provide high bandwidth telecommunications and infrastructure for SCADA it is increasingly being used to sense pressure, temperature and strain along buried pipelines, on subsea pipelines and downhole. In this paper we present results from the latest sensing capability using standard optical fibre to detect acoustic signals along the entire length of a pipeline. In Distributed Acoustic Sensing (DAS) an optical fibre is used for both sensing and telemetry. In this paper we present results from the OptaSense{sup TM} system which has been used to detect third party intervention (TPI) along buried pipelines. In a typical deployment the system is connected to an existing standard single-mode fibre, up to 50km in length, and was used to independently listen to the acoustic / seismic activity at every 10 meter interval. We will show that through the use of advanced array processing of the independent, simultaneously sampled channels it is possible to detect and locate activity within the vicinity of the pipeline and through sophisticated acoustic signal processing to obtain the acoustic signature to classify the type of activity. By combining spare fibre capacity in existing buried fibre optic cables; processing and display techniques commonly found in sonar; and state-of-the-art in fibre-optic distributed acoustic sensing, we will describe the new monitoring capabilities that are available to the pipeline operator. Without the expense of retrofitting sensors to the pipeline, this technology can provide a high performance, rapidly deployable and cost effective method of providing gapless and persistent monitoring of a pipeline. We will show how this approach can be used to detect, classify and locate activity such as; third party interference (including activity indicative of illegal hot tapping); real time tracking of pigs; and leak detection. We will also show how an

  20. Multipurpose Acoustic Sensor for Downhole Fluid Monitoring

    Pantea, Cristian [Los Alamos National Laboratory

    2012-05-04

    The projects objectives and purpose are to: (1) development a multipurpose acoustic sensor for downhole fluid monitoring in Enhanced Geothermal Systems (EGS) reservoirs over typical ranges of pressures and temperatures and demonstrate its capabilities and performance for different EGS systems; (2) determine in real-time and in a single sensor package several parameters - temperature, pressure, fluid flow and fluid properties; (3) needed in nearly every phase of an EGS project, including Testing of Injection and Production Wells, Reservoir Validation, Inter-well Connectivity, Reservoir Scale Up and Reservoir Sustainability. (4) Current sensors are limited to operating at lower temperatures, but the need is for logging at high temperatures. The present project deals with the development of a novel acoustic-based sensor that can work at temperatures up to 374 C, in inhospitable environments.

  1. Condition Monitoring and Management from Acoustic Emissions

    Pontoppidan, Niels Henrik Bohl

    2005-01-01

    In the following, I will use technical terms without explanation as it gives the freedom to describe the project in a shorter form for those who already know. The thesis is about condition monitoring of large diesel engines from acoustic emission signals. The experiments have been focused on a...... this work is the analysis of the angular position changes of the engine related events such as fuel injection and valve openings, caused by operational load changes. With inspiration from speech recognition and voice effects the angular timing changes have been inverted with the event alignment...

  2. Detection of respiratory compromise by acoustic monitoring, capnography, and brain function monitoring during monitored anesthesia care.

    Tanaka, Pedro P; Tanaka, Maria; Drover, David R

    2014-12-01

    Episodes of apnea in sedated patients represent a risk of respiratory compromise. We hypothesized that acoustic monitoring would be equivalent to capnography for detection of respiratory pauses, with fewer false alarms. In addition, we hypothesized that the patient state index (PSI) would be correlated with the frequency of respiratory pauses and therefore could provide information about the risk of apnea during sedation. Patients undergoing sedation for surgical procedures were monitored for respiration rate using acoustic monitoring and capnography and for depth of sedation using the PSI. A clinician blinded to the acoustic and sedation monitor observed the capnograph and patient to assess sedation and episodes of apnea. Another clinician retrospectively reviewed the capnography and acoustic waveform and sound files to identify true positive and false positive respiratory pauses by each method (reference method). Sensitivity, specificity, and likelihood ratio for detection of respiratory pause was calculated for acoustic monitoring and capnography. The correlation of PSI with respiratory pause events was determined. For the 51 respiratory pauses validated by retrospective analysis, the sensitivity, specificity, and likelihood ratio positive for detection were 16, 96 %, and 3.5 for clinician observation; 88, 7 %, and 1.0 for capnography; and 55, 87 %, and 4.1 for acoustic monitoring. There was no correlation between PSI and respiratory pause events. Acoustic monitoring had the highest likelihood ratio positive for detection of respiratory pause events compared with capnography and clinician observation and, therefore, may provide the best method for respiration rate monitoring during these procedures. PMID:24420342

  3. Acoustic monitoring techniques for corrosion degradation in cemented waste canisters

    This report describes work carried out to investigate acoustic emission as a monitor of corrosion and degradation of wasteforms where the waste is potentially reactive metal. Electronic monitoring equipment has been designed, built and tested to allow long-term monitoring of a number of waste packages simultaneously. Acoustic monitoring experiments were made on a range of 1 litre cemented Magnox and aluminium samples cast into canisters comparing the acoustic events with hydrogen gas evolution rates and electrochemical corrosion rates. The attenuation of the acoustic signals by the cement grout under a range of conditions has been studied to determine the volume of wasteform that can be satisfactorily monitored by one transducer. The final phase of the programme monitored the acoustic events from full size (200 litre) cemented, inactive, simulated aluminium swarf wastepackages prepared at the AEA waste cementation plant at Winfrith. (Author)

  4. Introducing passive acoustic filter in acoustic based condition monitoring: Motor bike piston-bore fault identification

    Jena, D. P.; Panigrahi, S. N.

    2016-03-01

    Requirement of designing a sophisticated digital band-pass filter in acoustic based condition monitoring has been eliminated by introducing a passive acoustic filter in the present work. So far, no one has attempted to explore the possibility of implementing passive acoustic filters in acoustic based condition monitoring as a pre-conditioner. In order to enhance the acoustic based condition monitoring, a passive acoustic band-pass filter has been designed and deployed. Towards achieving an efficient band-pass acoustic filter, a generalized design methodology has been proposed to design and optimize the desired acoustic filter using multiple filter components in series. An appropriate objective function has been identified for genetic algorithm (GA) based optimization technique with multiple design constraints. In addition, the sturdiness of the proposed method has been demonstrated in designing a band-pass filter by using an n-branch Quincke tube, a high pass filter and multiple Helmholtz resonators. The performance of the designed acoustic band-pass filter has been shown by investigating the piston-bore defect of a motor-bike using engine noise signature. On the introducing a passive acoustic filter in acoustic based condition monitoring reveals the enhancement in machine learning based fault identification practice significantly. This is also a first attempt of its own kind.

  5. Acoustic emission monitoring of HFIR vessel during hydrostatic testing

    This report discusses the results and conclusions reached from applying acoustic emission monitoring to surveillance of the High Flux Isotope Reactor vessel during pressure testing. The objective of the monitoring was to detect crack growth and/or fluid leakage should it occur during the pressure test. The report addresses the approach, acoustic emission instrumentation, installation, calibration, and test results

  6. Acoustic Emission Monitoring of Cementitious Wasteforms

    A summary is presented of the potential of non-destructive acoustic emission (AE) method to be applied for structures immobilising nuclear wastes. The use and limitations of the method are discussed with given examples of experimental configurations and results obtained from AE monitoring and data analysis of two different processes addressing particular issues related to the nuclear waste immobilisation. These are (a) corrosion of aluminium, classified as intermediate level waste (ILW) in the UK, encapsulated in cementitious structures and (b) partial melting and solidification during cooling of granite at a pressure of 0.15 GPa which simulates the conditions in a deep borehole disposal of canisters of vitrified high level waste (HLW). Methodology for analysis of the collected data and characterisation of the potential AE sources is performed at different steps including simple signals count and more complex signal parameter-based approach and advanced signal processing. The AE method has been shown as a potential tool for monitoring and inspection of structures immobilising nuclear wastes in relation to the time progress of different interactions of the waste with the encapsulating matrix or the wasteform with the hosting environment for permanent disposal. (author)

  7. Acoustic Monitoring of the Arctic Ice Cap

    Porter, D. L.; Goemmer, S. A.; Chayes, D. N.

    2012-12-01

    Introduction The monitoring of the Arctic Ice Cap is important economically, tactically, and strategically. In the scenario of ice cap retreat, new paths of commerce open, e.g. waterways from Northern Europe to the Far East. Where ship-going commerce is conducted, the U.S. Navy and U.S. Coast Guard have always stood guard and been prepared to assist from acts of nature and of man. It is imperative that in addition to measuring the ice from satellites, e.g. Icesat, that we have an ability to measure the ice extent, its thickness, and roughness. These parameters play an important part in the modeling of the ice and the processes that control its growth or shrinking and its thickness. The proposed system consists of three subsystems. The first subsystem is an acoustic source, the second is an array of geophones and the third is a system to supply energy and transmit the results back to the analysis laboratory. The subsystems are described below. We conclude with a plan on how to tackle this project and the payoff to the ice cap modeler and hence the users, i.e. commerce and defense. System Two historically tested methods to generate a large amplitude multi-frequency sound source include explosives and air guns. A new method developed and tested by the University of Texas, ARL is a combustive Sound Source [Wilson, et al., 1995]. The combustive sound source is a submerged combustion chamber that is filled with the byproducts of the electrolysis of sea water, i.e. Hydrogen and Oxygen, an explosive mixture which is ignited via a spark. Thus, no additional compressors, gases, or explosives need to be transported to the Arctic to generate an acoustic pulse capable of the sediment and the ice. The second subsystem would be geophones capable of listening in the O(10 Hz) range and transmitting that data back to the laboratory. Thus two single arrays of geophones arranged orthogonal to each other with a range of 1000's of kilometers and a combustive sound source where the two

  8. In-situ monitoring of Saccharomyces cerevisiae ITV01 bioethanol process using near-infrared spectroscopy NIRS and chemometrics.

    Corro-Herrera, Víctor Abel; Gómez-Rodríguez, Javier; Hayward-Jones, Patricia Margaret; Barradas-Dermitz, Dulce María; Aguilar-Uscanga, María Guadalupe; Gschaedler-Mathis, Anne Christine

    2016-03-01

    The application feasibility of in-situ or in-line monitoring of S. cerevisiae ITV01 alcoholic fermentation process, employing Near-Infrared Spectroscopy (NIRS) and Chemometrics, was investigated. During the process in a bioreactor, in the complex analytical matrix, biomass, glucose, ethanol and glycerol determinations were performed by a transflection fiber optic probe immersed in the culture broth and connected to a Near-Infrared (NIR) process analyzer. The NIR spectra recorded between 800 and 2,200 nm were pretreated using Savitzky-Golay smoothing and second derivative in order to perform a partial least squares regression (PLSR) and generate the calibration models. These calibration models were tested by external validation and then used to predict concentrations in batch alcoholic fermentations. The standard errors of calibration (SEC) for biomass, ethanol, glucose and glycerol were 0.212, 0.287, 0.532, and 0.296 g/L and standard errors of prediction (SEP) were 0.323, 0.369, 0.794, and 0.507 g/L, respectively. Calibration and validation criteria were defined and evaluated in order to generate robust and reliable models for an alcoholic fermentation process matrix. © 2016 American Institute of Chemical Engineers Biotechnol. Prog., 32:510-517, 2016. PMID:26743160

  9. Acoustic Signature Monitoring and Management of Naval Platforms

    Basten, T.G.H.; Jong, C.A.F. de; Graafland, F.; Hof, J. van 't

    2015-01-01

    Acoustic signatures make naval platforms susceptible to detection by threat sensors. The variable operational conditions and lifespan of a platform cause variations in the acoustic signature. To deal with these variations, a real time signature monitoring capability is being developed, with advisory

  10. Time Reversal Processing in Acoustic Emission Monitoring

    Převorovský, Zdeněk; Krofta, Josef; Farová, Zuzana; Chlada, Milan; Dos Santos, S.

    Singapore, 2013. s. 65-65. [International Congress on ULTRASONICS. 02.05.2013-05.05.2013, Singapore] Institutional support: RVO:61388998 Keywords : time reveresal * acoustic emission * deconvolution * source identification Subject RIV: JS - Reliability ; Quality Management, Testing

  11. Acoustic monitoring of BWR main steam safety relief valves

    Main steam safety relief valves (SRVs) are important equipment in boiling water reactor plants, so monitoring of leakage and valve opening of SRVs is also important. To detect leakage and valve opening, thermocouples are installed on exhaust pipes and limit switches or position sensors on valve stems. The acoustic detection technique with AE sensors and accelerometers is adopted not only to increase the accuracy and response speed of leak detection, but also to estimate leak rate and to detect valve opening. The acoustic leak detection technique was found effective by the mock-up experiment in which an actual SRV and steam under the same condition as the actual use were used to measure the signals from AE sensors and accelerometers attached to the SRV with artificial cuttings on its thermal disk. The acoustic monitoring tests of SRVs have been carried out at a nuclear power plant to prove the acoustic leak detection technique to be effective. The results of the acoustic monitoring tests at the plant are discussed. As a result of the on-site test, the acoustic leak monitoring system was found effective in the plant

  12. OPERATING PROCEDURE FOR THE PORTABLE ACOUSTIC MONITORING PACKAGE (PAMP)

    John L. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Patrick Browning

    2004-08-29

    The Portable Acoustic Monitoring Package (PAMP) has been designed to record and monitor acoustic signals in high-pressure natural gas (NG) transmission lines. Of particular interest are the three acoustic signals associated with a pipeline fracture. The system is portable (less than 30 lbm) and can be used at all line pressures up to 1000 psig. The PAMP requires a shut-off valve equipped 1/2 inch NPT access port in the pipeline. It is fully functional over the typical pressure range found in the natural gas transmission pipelines in the West Virginia, Virginia, Pennsylvania, and Ohio areas. With the use of the PAMP, a full spectrum of acoustic signals can be recorded and defined in terms of acoustic energy in decibels. To detect natural gas pipeline infringements and leaks, the acoustic energy generated inside the line is monitored with a sensitive pressure-equalized microphone and a step function type {Delta}p transducer. The assembly is mounted on a 1000 psig pipe fitting-tree called the PAMP. The electronics required to record, store and analyze the data are described within this report in the format of an operating manual.

  13. Ultrasonic waveguide sensor for acoustic monitoring of nuclear power plants

    Waveguide sensors are being increasingly used for acoustic emission monitoring of equipment in nuclear power plants and in systems for acoustic diagnostics of the coolant. In this paper we examine the construction of a waveguide sensor for acoustic monitoring for the example of an impedance sensor for the steam content of water coolant, intended for use in the active emission-reception mode. The dynamic properties of the sensor are determined by the construction and the dimensions of the transducer, and are usually represented by its amplitude-frequency characteristic, which, as a rule, is of the resonance type. The longitudinal-wave waveguide, made from steel wire 0.8-1.2 mm in diameter, can transmit signals in the band 50-1000 kHz. To increase the reliability and the ease of maintenance of the monitoring system the transducer and the waveguide are connected in a detachable manner

  14. Urban air quality assessment using monitoring data of fractionized aerosol samples, chemometrics and meteorological conditions.

    Yotova, Galina I; Tsitouridou, Roxani; Tsakovski, Stefan L; Simeonov, Vasil D

    2016-06-01

    The present article deals with assessment of urban air by using monitoring data for 10 different aerosol fractions (0.015-16 μm) collected at a typical urban site in City of Thessaloniki, Greece. The data set was subject to multivariate statistical analysis (cluster analysis and principal components analysis) and, additionally, to HYSPLIT back trajectory modeling in order to assess in a better way the impact of the weather conditions on the pollution sources identified. A specific element of the study is the effort to clarify the role of outliers in the data set. The reason for the appearance of outliers is strongly related to the atmospheric condition on the particular sampling days leading to enhanced concentration of pollutants (secondary emissions, sea sprays, road and soil dust, combustion processes) especially for ultra fine and coarse particles. It is also shown that three major sources affect the urban air quality of the location studied-sea sprays, mineral dust and anthropogenic influences (agricultural activity, combustion processes, and industrial sources). The level of impact is related to certain extent to the aerosol fraction size. The assessment of the meteorological conditions leads to defining of four downwind patterns affecting the air quality (Pelagic, Western and Central Europe, Eastern and Northeastern Europe and Africa and Southern Europe). Thus, the present study offers a complete urban air assessment taking into account the weather conditions, pollution sources and aerosol fractioning. PMID:26942452

  15. Acoustic monitoring of a fluidized bed coating process

    Naelapaa, Kaisa; Veski, Peep; Pedersen, Joan G.; Anov, Dan; Jørgensen, Pia; Kristensen, Henning Gjelstrup; Bertelsen, Poul

      The aim of the study was to investigate the potential of acoustic monitoring of a production scale fluidized bed coating process. The correlation between sensor signals and the estimated amount of film applied and percentage release, respectively, were investigated in coating potassium chloride...

  16. Monitoring of rapid sand filters using an acoustic imaging technique

    Allouche, N.; Simons, D.G.; Rietveld, L.C.

    2012-01-01

    A novel instrument is developed to acoustically image sand filters used for water treatment and monitor their performance. The instrument consists of an omnidirectional transmitter that generates a chirp with a frequency range between 10 and 110 kHz, and an array of hydrophones. The instrument was e

  17. Acoustic monitoring of safety/relief valves for leak detection

    The results presented here indicate that there is a high probability of confidentially detecting pilot stage leakage in safety/relief valves through the use of acoustic monitoring, especially in the frequency range 30-60 kHz. This should be particularly true if the sensors and signal processing equipment are designed for sensitivity to this range, and if routine or continuous monitoring is performed so that trends can be recognized

  18. Monitoring of rapid sand filters using an acoustic imaging technique

    Allouche, N.; Simons, D.G.; Rietveld, L. C.

    2012-01-01

    A novel instrument is developed to acoustically image sand filters used for water treatment and monitor their performance. The instrument consists of an omnidirectional transmitter that generates a chirp with a frequency range between 10 and 110 kHz, and an array of hydrophones. The instrument was extensively tested in a lab before being deployed in an industrial rapid sand filter, made available by a Dutch drinking water company. This filter was monitored over a period of 10 days. We perform...

  19. Acoustic monitoring systems tests at Indian Point Unit 1. Final report

    This report describes the results of a program to test acoustic monitoring systems on Indian Point Unit No. 1 under actual plant operating conditions, less the reactor core. The two types of systems evaluated were the monitoring of acoustic emissions generated by growing flaws and the monitoring of acoustic signals from leaks

  20. Acoustic emission/flaw relationships for inservice monitoring of LWRs

    The program concerning Acoustic Emission/Flaw Relationships for Inservice Monitoring of LWRs was initiated in FY76 with the objective of validating the application of acoustic emission (AE) to monitor nuclear reactor pressure-containing components during operation to detect cracking. The program has been supported by the US Nuclear Regulatory Commission, Office of Nuclear Regulatory Research. Research and development has been performed by Pacific Northwest Laboratory, operated for the Department of Energy by Battelle Memorial Institute. The program has shown the feasibility of continuous, on-line AE monitoring to detect crack growth and produced validated methods for applying the technology. Included are relationships for estimating flaw severity from AE data and field applications at Watts Bar Unit 1 Reactor, Limerick Unit 1 Reactor, and the High Flux Isotope Reactor. This report discusses the program scope and organization, the three program phases and the results obtained, standard and code activities, and instrumentation and software developed under this program

  1. Monitoring of hard turning using acoustic emission signal

    Bhaskaran, J.; Murugan, M. [B.S. Abdur Rahman University, Chennai (India); Balashanmugam, N.; Chellamalai, M. [Central Manufacturing Technology Institute, Bangalore (India)

    2012-02-15

    Monitoring of tool wear during hard turning is essential. Many investigators have analyzed the acoustic emission (AE) signals generated during machining to understand the metal cutting process and for monitoring tool wear and failure. In the current study on hard turning, the skew and kurtosis parameters of the root mean square values of AE signal (AERMS) are used to monitor tool wear. The rubbing between the tool and the workpiece increases as the tool wear crosses a threshold, thereby shifting the mass of AERMS distribution to right, leading to a negative skew. The increased rubbing also led to a high kurtosis value in the AERMS distribution curve.

  2. Smart acoustic emission system for wireless monitoring of concrete structures

    Yoon, Dong-Jin; Kim, Young-Gil; Kim, Chi-Yeop; Seo, Dae-Cheol

    2008-03-01

    Acoustic emission (AE) has emerged as a powerful nondestructive tool to detect preexisting defects or to characterize failure mechanisms. Recently, this technique or this kind of principle, that is an in-situ monitoring of inside damages of materials or structures, becomes increasingly popular for monitoring the integrity of large structures. Concrete is one of the most widely used materials for constructing civil structures. In the nondestructive evaluation point of view, a lot of AE signals are generated in concrete structures under loading whether the crack development is active or not. Also, it was required to find a symptom of damage propagation before catastrophic failure through a continuous monitoring. Therefore we have done a practical study in this work to fabricate compact wireless AE sensor and to develop diagnosis system. First, this study aims to identify the differences of AE event patterns caused by both real damage sources and the other normal sources. Secondly, it was focused to develop acoustic emission diagnosis system for assessing the deterioration of concrete structures such as a bridge, dame, building slab, tunnel etc. Thirdly, the wireless acoustic emission system was developed for the application of monitoring concrete structures. From the previous laboratory study such as AE event patterns analysis under various loading conditions, we confirmed that AE analysis provided a promising approach for estimating the condition of damage and distress in concrete structures. In this work, the algorithm for determining the damage status of concrete structures was developed and typical criteria for decision making was also suggested. For the future application of wireless monitoring, a low energy consumable, compact, and robust wireless acoustic emission sensor module was developed and applied to the concrete beam for performance test. Finally, based on the self-developed diagnosis algorithm and compact wireless AE sensor, new AE system for practical

  3. Signal processing methodologies for an acoustic fetal heart rate monitor

    Pretlow, Robert A., III; Stoughton, John W.

    1992-01-01

    Research and development is presented of real time signal processing methodologies for the detection of fetal heart tones within a noise-contaminated signal from a passive acoustic sensor. A linear predictor algorithm is utilized for detection of the heart tone event and additional processing derives heart rate. The linear predictor is adaptively 'trained' in a least mean square error sense on generic fetal heart tones recorded from patients. A real time monitor system is described which outputs to a strip chart recorder for plotting the time history of the fetal heart rate. The system is validated in the context of the fetal nonstress test. Comparisons are made with ultrasonic nonstress tests on a series of patients. Comparative data provides favorable indications of the feasibility of the acoustic monitor for clinical use.

  4. Nonintrusive Monitoring and Control of Metallurgical Processes by Acoustic Measurements

    Yu, Hao-Ling; Khajavi, Leili Tafaghodi; Barati, Mansoor

    2011-06-01

    The feasibility of developing a new online monitoring technique based on the characteristic acoustic response of gas bubbles in a liquid has been investigated. The method is intended to monitor the chemistry of the liquid through its relation to the bubble sound frequency. A low-temperature model consisting of water and alcohol mixtures was established, and the frequency of bubbles rising under varying concentrations of methanol was measured. It was shown that the frequency of the sound created by bubble pulsation varies with the percentage of alcohol in water. The frequency drops sharply with the increase in methanol content up to 20 wt pct, after which the decreases is gradual. Surface tension seems to be a critical liquid property affecting the sound frequency through its two-fold effects on the bubble size and the pulsation domain. The dependence between the frequency and the liquid composition suggests the feasibility of developing an acoustic-based technique for process control purposes.

  5. Acoustic emission monitoring for assessment of steel bridge details

    Acoustic emission (AE) testing was deployed on details of two large steel Interstate Highway bridges: one cantilever through-truss and one trapezoidal box girder bridge. Quantitative measurements of activity levels at known and suspected crack locations were made by monitoring AE under normal service loads (e.g., live traffic and wind). AE indications were used to direct application of radiography, resulting in identification of a previously unknown flaw, and to inform selection of a retrofit detail.

  6. Acoustic module of the Acquabona (Italy debris flow monitoring system

    A. Galgaro

    2005-01-01

    Full Text Available Monitoring of debris flows aimed to the assessment of their physical parameters is very important both for theoretical and practical purposes. Peak discharge and total volume of debris flows are crucial for designing effective countermeasures in many populated mountain areas where losses of lives and property damage could be avoided. This study quantifies the relationship between flow depth, acoustic amplitude of debris flow induced ground vibrations and front velocity in the experimental catchment of Acquabona, Eastern Dolomites, Italy. The analysis of data brought about the results described in the following. Debris flow depth and amplitude of the flow-induced ground vibrations show a good positive correlation. Estimation of both mean front velocity and peak discharge can be simply obtained monitoring the ground vibrations, through geophones installed close to the flow channel; the total volume of debris flow can be so directly estimated from the integral of the ground vibrations using a regression line. The application of acoustic technique to debris flow monitoring seems to be of the outmost relevance in risk reduction policies and in the correct management of the territory. Moreover this estimation is possible in other catchments producing debris flows of similar characteristics by means of their acoustic characterisation through quick and simple field tests (Standard Penetration Tests and seismic refraction surveys.

  7. Acoustic module of the Acquabona (Italy) debris flow monitoring system

    Galgaro, A.; Tecca, P. R.; Genevois, R.; Deganutti, A. M.

    2005-02-01

    Monitoring of debris flows aimed to the assessment of their physical parameters is very important both for theoretical and practical purposes. Peak discharge and total volume of debris flows are crucial for designing effective countermeasures in many populated mountain areas where losses of lives and property damage could be avoided. This study quantifies the relationship between flow depth, acoustic amplitude of debris flow induced ground vibrations and front velocity in the experimental catchment of Acquabona, Eastern Dolomites, Italy. The analysis of data brought about the results described in the following. Debris flow depth and amplitude of the flow-induced ground vibrations show a good positive correlation. Estimation of both mean front velocity and peak discharge can be simply obtained monitoring the ground vibrations, through geophones installed close to the flow channel; the total volume of debris flow can be so directly estimated from the integral of the ground vibrations using a regression line. The application of acoustic technique to debris flow monitoring seems to be of the outmost relevance in risk reduction policies and in the correct management of the territory. Moreover this estimation is possible in other catchments producing debris flows of similar characteristics by means of their acoustic characterisation through quick and simple field tests (Standard Penetration Tests and seismic refraction surveys).

  8. SAMARUC a Programmable system for Passive acoustic monitoring of cetaceans

    Miralles Ricós, Ramón; Lara Martínez, Guillermo-Fernan; CARRIÓN GARCÍA, ALICIA; Esteban, José Antonio

    2013-01-01

    This paper reports the work carried out by iTEAM researchers in Passive Acoustic Monitoring (PAM) for underwater monitoring of cetaceans. It includes a description of novel signal processing algorithms for detection and classification of aquatic mammal species as well as a hardware system called SAMARUC specially designed in collaboration with marine biologists. Ministerio de Ciencia e Innovación within the Project number TEC2011-23403 Miralles Ricós, R.; Lara Martínez, G.; Carrión Gar...

  9. A passive acoustic monitor of treatment effectiveness during extracorporeal lithotripsy

    Fedele, F; Coleman, A J [Medical Physics Department, Guy' s and St Thomas NHS Foundation Trust, Westminster Bridge Road, SE1 7EH, London (United Kingdom); Thomas, K; Ryves, S; Phillips, D [Urology Department, Guy' s and St Thomas NHS Foundation Trust, Great Maze Pond, SE1 9RT, London (United Kingdom); Leighton, T G, E-mail: fiammetta.fedele@gstt.nhs.uk [Institute of Sound and Vibration Research, University of Southampton, Highfield, S017 1BJ, Southampton (United Kingdom)

    2011-02-01

    Although extracorporeal shockwave lithotripsy (ESWL) has now been in the clinic for at least three decades, there has been little advance in efforts (i) to estimate the efficacy of the treatment whilst it is in progress, or (ii) to determine the end-point of a treatment session in terms of the degree of stone fragmentation achieved. Previous in vitro experimentation and clinical trials have shown that a passive acoustic monitor has the potential to provide evidence of the effectiveness and end-point of lithotripsy. The system exploits secondary emissions generated during shock-tissue interaction, whose features depend on the quality of tissue at the beam focus. This prototype was developed into the first commercially available clinical ESWL treatment monitor (Precision Acoustic Ltd, Dorchester, UK), and a unit has been acquired and tested in the clinical routine by urologists at Guy's and St Thomas NHS Trust in March 2009. This paper critically assesses the performance of the new system for the first 25 treatments monitored. The ESWL monitor correctly predicted the treatment outcome of 15 of the 18 treatments that were followed-up clinically. In addition, it was noted that the measure of treatment effectiveness provided by the monitor after 500 shocks was predictive of the final treatment outcome (p < 0.001). This suggests that the system could be used in pre-assessment; indicating if the stone is susceptible to ESWL or if the patient should be sent for surgery.

  10. Acoustical monitoring of diesel engines in reverberant environment

    The feed-back knowledge of emergency diesel generators in nuclear power plants shows that some malfunctions, mainly affecting fuel-injection or distribution system of the engine can be heard and detected by experienced maintenance agents. This study consists in the feasibility,v of acoustical monitoring of those diesel engines, taking into account the reverberant environment of the machine. The operating cycle of the diesel is composed of transient events (injection, combustion, valve closure...) which generate highly non stationary acoustical signals. The detection of a malfunction appearing on such transients requires the use of adapted signal processing techniques. Visual analysis of the phenomena is first proceeded using time-frequency and time-scale representations. The second step will be parametric modeling of acoustical signatures for the extraction of characteristic parameters, in order to characterize the fault and to use an automatic classification system. The lest part of the study will concern the evaluation of the robustness of the detection methods in regard to acoustical reverberation. (author). 10 refs., 6 figs

  11. Employing Acoustic Emission for Monitoring Oil Film Regimes

    David Mba

    2013-07-01

    Full Text Available The major purpose of a gear lubricant is to provide adequate oil film thickness to reduce and prevent gear tooth surface failures. Real time monitoring for gear failures is important in order to predict and prevent unexpected failures which would have a negative impact on the efficiency, performance and safety of the gearbox. This paper presents experimental results on the influence of specific oil film thickness on Acoustic Emission (AE activity for operational helical gears. Variation in film thickness during operations was achieved by spraying liquid nitrogen onto the rotating gear wheel. The experimental results demonstrated a clear relationship between the root mean square (r.m.s value of the AE signal and the specific film thickness. The findings demonstrate the potential of Acoustic Emission technology to quantify lubrication regimes on operational gears.

  12. Application of acoustic emission technique for check valve monitoring

    Very limited choice is available in monitoring the health of check valves during service. Ultrasonics, magnetic flux leakage and acoustic emission (AE) monitoring are three methods, of which AE is the prominent. The paper describes work done on swing check valves in the ECCS circuit of Cirus using AE. It indicates that the valves can be monitored for any abnormal behaviour during their stable operation and during opening and closing. AE can also sense any abnormality at the hinge pin, hinge arm, disc etc., if they give AE emission. However, many of these may require background data from a spare valve of similar design or a working stand by. In absence of such a valve, data from the present study will be used as a baseline data for comparison with signatures taken during future inspections. (author). 3 refs., 5 figs., 1 tab

  13. Monitoring of Robot Assisted Polishing through parameters of acoustic emission

    Lazarev, Ruslan; Top, Søren; Bilberg, Arne

    duration of each process stage and predict the end of process in a precise and unmanned way. This paper presents and analyses the utilization of acoustic emission for generation of control signals in the stone polishing process for achieving these control objectives in an industrial set-up prototype....... determination of the point in time to change a polishing media or stop the process is needed for computer controlled functional surface generation. During the last years, several research works have been done in order to build grinding/polishing monitoring systems to determine process characteristics, the...

  14. Use of acoustic monitoring system for debris flow discharge evaluation

    Galgaro, A. G.; Tecca, P. R.; Genevois, R.; Deganutti, A. M.

    2003-04-01

    In 1997 an automated system for monitoring of debris flows has been installed in the Acquabona channel Dolomites, Italy. Induction geophones, with a specific frequency of 10 Hz, measure the amplitude of vertical ground vibrations generated by the passage of a flowing mass along the channel. Continuous acoustic logs and ultrasonic hydrograph recorded at the lower-channel measurement station for the debris flow of August 17, 1998, show a striking correspondence. This correspondence, already observed in different flow sites, is represented by the best fit between flow depth and flow sensor amplitude. Average front velocity for surges, calculated from the signal peak time shift and the distance between the sensors along the flow path, range between 2.00 and 7.7 m/s. As the ultrasonic sensor provides a way to measure the variation of the flow section area with the flow depth, the debris flow peak discharge may be estimated; obtained values of debris flow peak discharge range from 4 and 30 m3/s. Volumes were calculated by integrating instantaneous discharges through the hydrograph and by integrating the geophone log (acoustic flux). Volumes of 13700 m3 and 15500 m3 have been respectively obtained. The slight difference between the two values may result from the fact that acoustic records: i) are sensitive to the high frequencies, typical of the debris flow tails; ii) sum up the contributions sent by the whole flowing mass, while the ecometer detect the flow depth at every time at only one section. As a consequence the rising of the whole geophone log gives a higher value at the integration result. This only acoustic system can give a reasonably proxy for discharge and total volumes involved, which are among the most important parameters for debris flow hazard assessment and planning countermeasures. This methodology can be used in other debris flow sites if they are calibrated by the acoustic characterization of debris, obtained by both seismic surveys and SPT tests, and

  15. Aero-acoustic Measurement and Monitoring of Dynamic Pressure Fields Project

    National Aeronautics and Space Administration — This innovative and practical measurement and monitoring system optimally defines dynamic pressure fields, including sound fields. It is based on passive acoustic...

  16. SensIs - Underwater acoustic network for ice-monitoring

    Reinen, Tor Arne; Knudsen, Finn Tore

    2016-01-01

    Routing for low latency underwater acoustic network-communication is investigated. The application is monitoring of ice-threats to offshore operations in the Arctic - to provide warnings that enable operators to react to such threats. The scenario produces relatively high traffic load, and the network should favour low delay and adequate reliability rather than energy usage minimization. The ICRP (Information-Carrying based Routing Protocol), originally proposed by Wei Liang et al. in 2007, is chosen as basis. ICRP obtains unicast routing paths by sending data payload as broadcast packets when no route information is available. Thus, data can be delivered without the cost of reactive signalling latency. In this paper we explore the capabilities of a slightly enhanced/adapted ICRP, tailored to the ice monitoring application. By simulations and experiments at sea it is demonstrated that the protocol performs well and can manage the applications high traffic load - this provided that the point-to-point links pro...

  17. Acoustics

    Goodman, Jerry R.; Grosveld, Ferdinand

    2007-01-01

    The acoustics environment in space operations is important to maintain at manageable levels so that the crewperson can remain safe, functional, effective, and reasonably comfortable. High acoustic levels can produce temporary or permanent hearing loss, or cause other physiological symptoms such as auditory pain, headaches, discomfort, strain in the vocal cords, or fatigue. Noise is defined as undesirable sound. Excessive noise may result in psychological effects such as irritability, inability to concentrate, decrease in productivity, annoyance, errors in judgment, and distraction. A noisy environment can also result in the inability to sleep, or sleep well. Elevated noise levels can affect the ability to communicate, understand what is being said, hear what is going on in the environment, degrade crew performance and operations, and create habitability concerns. Superfluous noise emissions can also create the inability to hear alarms or other important auditory cues such as an equipment malfunctioning. Recent space flight experience, evaluations of the requirements in crew habitable areas, and lessons learned (Goodman 2003; Allen and Goodman 2003; Pilkinton 2003; Grosveld et al. 2003) show the importance of maintaining an acceptable acoustics environment. This is best accomplished by having a high-quality set of limits/requirements early in the program, the "designing in" of acoustics in the development of hardware and systems, and by monitoring, testing and verifying the levels to ensure that they are acceptable.

  18. Overview of chemometrics

    Schlager, Kenneth J.; Ruchti, Timothy L.

    1995-04-01

    Chemometrics is a broad field concerned with the application of mathematical and statistical methods to problems in chemistry. Biotronics Technologies has applied chemometrics to demanding chemical applications involving noninvasive medical diagnostic measurement instrumentation using advanced signal processing and calibration techniques. The chemometrics methods have also been extended to quantitative analysis in microbiology. Signal processing transforms data measurements to enhance the extraction of physically significant information. Examples include the Fourier Transform, first and second derivatives, and digital and adaptive filtering. Calibration is the process of relating data measurements to a chemical concentration for the purpose of estimation. Standard methods of calibration include linear regression, multiple-linear regression, partial linear regression, and principal components regression. For more demanding applications, novel techniques involving artificial neural networks, genetic algorithms, and rotated principal components have been developed. This paper summarizes the chemometric experience of Biotronics Technologies including relevant theoretical background.

  19. Intraoperative monitoring during surgery for acoustic neuroma: benefits of an extratympanic intrameatal electrode

    Mullatti, N; Coakham, H; Maw, A; Butler, S; Morgan, M.

    1999-01-01

    OBJECTIVES—To assess the utility of an extratympanic intrameatal electrode for intraoperative monitoring during acoustic neuroma and other cerebellopontine angle tumour surgery and to define the neurophysiological and surgical factors which influence hearing preservation.
METHODS—Twenty two patients, 18 with acoustic neuromas and four with other cerebellopontine angle tumours, underwent intraoperative monitoring during tumour excision. The extratympanic intrameatal electrode...

  20. Remote Acoustic Monitoring of North Atlantic Right Whales (Eubalaena glacialis) Reveals Seasonal and Diel Variations in Acoustic Behavior

    Matthews, Leanna P.; Jessica A McCordic; Susan E Parks

    2014-01-01

    Remote acoustic monitoring is a non-invasive tool that can be used to study the distribution, behavior, and habitat use of sound-producing species. The North Atlantic right whale (Eubalaena glacialis) is an endangered baleen whale species that produces a variety of stereotyped acoustic signals. One of these signals, the "gunshot" sound, has only been recorded from adult male North Atlantic right whales and is thought to function for reproduction, either as reproductive advertisement for femal...

  1. A multi-channel acoustics monitor for perioperative respiratory monitoring: preliminary data.

    Jafarian, Kamal; Amineslami, Majid; Hassani, Kamran; Navidbakhsh, Mahdi; Lahiji, Mohammad Niakan; Doyle, D John

    2016-02-01

    This study pertains to a six-channel acoustic monitoring system for use in patient monitoring during or after surgery. The base hardware consists of a USB data acquisition system, a custom-built six-channel amplification system, and a series of microphones of various designs. The software is based on the MATLAB platform with data acquisition drivers installed. The displayed information includes: time domain signals, frequency domain signals, and tools to aid in the detection of endobronchial intubation. We hypothesize that the above mentioned arrangement may be helpful to the anesthesiologist in recognizing clinical conditions like wheezing, bronchospasm, endobronchial intubation, and apnea. The study also evaluated various types of microphone designs used to transduce breath sounds. The system also features selectable band-pass filtering using MATLAB algorithms as well as a collection of recordings obtained with the system to establish what respiratory acoustic signals look like under various conditions. PMID:25869899

  2. Acoustic emission monitoring of recycled aggregate concrete under bending

    Tsoumani, A. A.; Barkoula, N.-M.; Matikas, T. E.

    2015-03-01

    The amount of construction and demolition waste has increased considerably over the last few years, making desirable the reuse of this waste in the concrete industry. In the present study concrete specimens are subjected at the age of 28 days to four-point bending with concurrent monitoring of their acoustic emission (AE) activity. Several concrete mixtures prepared using recycled aggregates at various percentages of the total coarse aggregate and also a reference mix using natural aggregates, were included to investigate their influence of the recycled aggregates on the load bearing capacity, as well as on the fracture mechanisms. The results reveal that for low levels of substitution the influence of using recycled aggregates on the flexural strength is negligible while higher levels of substitution lead into its deterioration. The total AE activity, as well as the AE signals emitted during failure, was related to flexural strength. The results obtained during test processing were found to be in agreement with visual observation.

  3. Operational Performance Analysis of Passive Acoustic Monitoring for Killer Whales

    Matzner, Shari; Fu, Tao; Ren, Huiying; Deng, Zhiqun; Sun, Yannan; Carlson, Thomas J.

    2011-09-30

    For the planned tidal turbine site in Puget Sound, WA, the main concern is to protect Southern Resident Killer Whales (SRKW) due to their Endangered Species Act status. A passive acoustic monitoring system is proposed because the whales emit vocalizations that can be detected by a passive system. The algorithm for detection is implemented in two stages. The first stage is an energy detector designed to detect candidate signals. The second stage is a spectral classifier that is designed to reduce false alarms. The evaluation presented here of the detection algorithm incorporates behavioral models of the species of interest, environmental models of noise levels and potential false alarm sources to provide a realistic characterization of expected operational performance.

  4. Surface Acoustic Wave (SAW Resonators for Monitoring Conditioning Film Formation

    Siegfried Hohmann

    2015-05-01

    Full Text Available We propose surface acoustic wave (SAW resonators as a complementary tool for conditioning film monitoring. Conditioning films are formed by adsorption of inorganic and organic substances on a substrate the moment this substrate comes into contact with a liquid phase. In the case of implant insertion, for instance, initial protein adsorption is required to start wound healing, but it will also trigger immune reactions leading to inflammatory responses. The control of the initial protein adsorption would allow to promote the healing process and to suppress adverse immune reactions. Methods to investigate these adsorption processes are available, but it remains difficult to translate measurement results into actual protein binding events. Biosensor transducers allow user-friendly investigation of protein adsorption on different surfaces. The combination of several transduction principles leads to complementary results, allowing a more comprehensive characterization of the adsorbing layer. We introduce SAW resonators as a novel complementary tool for time-resolved conditioning film monitoring. SAW resonators were coated with polymers. The adsorption of the plasma proteins human serum albumin (HSA and fibrinogen onto the polymer-coated surfaces were monitored. Frequency results were compared with quartz crystal microbalance (QCM sensor measurements, which confirmed the suitability of the SAW resonators for this application.

  5. Chemometric Methods in Plant Metabolomics

    Isomaa, Keijo

    2013-01-01

    This study focuses on chemometric analysis of instrumental data that has been obtained from chemical analysis of plant extracts. Chemometric analysis applies statistical and mathematical tools on chemical data, aiming to find new information or classifying samples in categories defined by the analyst. Chemometric analysis is based on computational pattern recognition and reveals any features that studied samples may have in common. In the literature part of this study, chemometrics and r...

  6. Passive acoustic monitoring of human physiology during activity indicates health and performance of soldiers and firefighters

    Scanlon, Michael V.

    2003-04-01

    The Army Research Laboratory has developed a unique gel-coupled acoustic physiological monitoring sensor that has acoustic impedance properties similar to the skin. This facilitates the transmission of body sounds into the sensor pad, yet significantly repels ambient airborne noises due to an impedance mismatch. The sensor's sensitivity and bandwidth produce excellent signatures for detection and spectral analysis of diverse physiological events. Acoustic signal processing detects heartbeats, breaths, wheezes, coughs, blood pressure, activity, motion, and voice for communication and automatic speech recognition. The health and performance of soldiers, firefighters, and other first responders in strenuous and hazardous environments can be continuously and remotely monitored with body-worn acoustic sensors. Comfortable acoustic sensors can be in a helmet or in a strap around the neck, chest, and wrist. Noise-canceling sensor arrays help remove out-of-phase motion noise and enhance covariant physiology by using two acoustic sensors on the front sides of the neck and two additional acoustic sensors on each wrist. Pulse wave transit time between neck and wrist acoustic sensors will indicate systolic blood pressure. Larger torso-sized arrays can be used to acoustically inspect the lungs and heart, or built into beds for sleep monitoring. Acoustics is an excellent input for sensor fusion.

  7. ONKALO POSE experiment. Phase 3: acoustic and ultrasonic monitoring

    Reyes-Montes, J.; Flynn, W.; Huang, J. [Applied Seismology Consultants, Shrewsbury (United Kingdom)

    2014-01-15

    The objectives of the third phase of the POSE experiment are to determine the in situ state of stress at Olkiluoto and the spalling strength of Olkiluoto rock, by internal heating of the experimental hole (ONK-EH3) using 8 vertically installed heaters. This report presents the results from the Acoustic and ultrasonic monitoring carried out around the third experimental hole of the POSE niche between November 2012 and May 2013. The experiment was monitored using an array of 24 transducers installed along 4 monitoring drillholes and data was automatically acquired and processed using the system installed at the niche by Applied Seismology Consultants in May 2012. Daily ultrasonic surveys were carried out between 14{sup th} November 2012 and 21{sup st} May 2013, monitoring the changes in transmission velocities of P and S-waves with an estimated error of ±2 m x s{sup -1} (ASC, 2013). Changes in transmission velocities closely follow the evolution of the temperature profile in the hole wall. An increase in both P-and S-wave transmission velocities is observed at all depth levels and surveyed raypaths during the heating phase, with the highest changes observed in raypaths skimming the hole surface and depths between 2.33 m and 3.7 m. This observation indicates the closure of in situ and excavation-induced microcracks due to thermal stress. After the heaters were switched off, P-wave velocities show a marked decrease, in all raypaths reaching values below those measured at the start of the monitoring approximately 4 weeks after the heaters were switched off. The highest decrease was observed along raypaths surveying the region skimming the hole wall. This decrease below original background values indicates the induction of rock degradation as microcracking induced through the heating-cooling cycle. Changes in P- and S-wave transmission velocity were used to calculate changes in Young's modulus and Poisson's ratio along the different raypaths and depth levels

  8. ONKALO POSE experiment. Phase 3: acoustic and ultrasonic monitoring

    The objectives of the third phase of the POSE experiment are to determine the in situ state of stress at Olkiluoto and the spalling strength of Olkiluoto rock, by internal heating of the experimental hole (ONK-EH3) using 8 vertically installed heaters. This report presents the results from the Acoustic and ultrasonic monitoring carried out around the third experimental hole of the POSE niche between November 2012 and May 2013. The experiment was monitored using an array of 24 transducers installed along 4 monitoring drillholes and data was automatically acquired and processed using the system installed at the niche by Applied Seismology Consultants in May 2012. Daily ultrasonic surveys were carried out between 14th November 2012 and 21st May 2013, monitoring the changes in transmission velocities of P and S-waves with an estimated error of ±2 m x s-1 (ASC, 2013). Changes in transmission velocities closely follow the evolution of the temperature profile in the hole wall. An increase in both P-and S-wave transmission velocities is observed at all depth levels and surveyed raypaths during the heating phase, with the highest changes observed in raypaths skimming the hole surface and depths between 2.33 m and 3.7 m. This observation indicates the closure of in situ and excavation-induced microcracks due to thermal stress. After the heaters were switched off, P-wave velocities show a marked decrease, in all raypaths reaching values below those measured at the start of the monitoring approximately 4 weeks after the heaters were switched off. The highest decrease was observed along raypaths surveying the region skimming the hole wall. This decrease below original background values indicates the induction of rock degradation as microcracking induced through the heating-cooling cycle. Changes in P- and S-wave transmission velocity were used to calculate changes in Young's modulus and Poisson's ratio along the different raypaths and depth levels. An overall

  9. Continuous acoustic emission monitoring of reinforced concrete under accelerated corrosion

    Di Benedetti, M.; Loreto, G.; Nanni, A.; Matta, F.; Gonzalez-Nunez, M. A.

    2011-04-01

    The development of techniques capable of evaluating deterioration of reinforced concrete (RC) structures is instrumental to the advancement of techniques for the structural health monitoring (SHM) and service life estimate for constructed facilities. One of the main causes leading to degradation of RC is the corrosion of the steel reinforcement. This process can be modeled phenomenologically, while laboratory tests aimed at studying durability responses are typically accelerated in order to provide useful results within a realistic period of time. To assess the condition of damage in RC, a number of nondestructive methods have been recently studied. Acoustic emission (AE) is emerging as a nondestructive tool to detect the onset and progression of deterioration mechanisms. In this paper, the development of accelerated corrosion and continuous AE monitoring test set-up for RC specimens are presented. Relevant information are provided with regard to the characteristics of the corrosion circuit, continuous measurement and acquisition of corrosion potential, selection of AE sensors and AE parameter setting. The effectiveness of the setup in detecting and characterizing the initiation and progression of the corrosion phenomenon is discussed on the basis of preliminary results from small-scale, pre-cracked RC specimens, which are representative of areas near the clear cover in typical RC bridge members.

  10. Early corrosion monitoring of prestressed concrete piles using acoustic emission

    Vélez, William; Matta, Fabio; Ziehl, Paul H.

    2013-04-01

    The depassivation and corrosion of bonded prestressing steel strands in concrete bridge members may lead to major damage or collapse before visual inspections uncover evident signs of damage, and well before the end of the design life. Recognizing corrosion in its early stage is desirable to plan and prioritize remediation strategies. The Acoustic Emission (AE) technique is a rational means to develop structural health monitoring and prognosis systems for the early detection and location of corrosion in concrete. Compelling features are the sensitivity to events related to micro- and macrodamage, non-intrusiveness, and suitability for remote and wireless applications. There is little understanding of the correlation between AE and the morphology and extent of early damage on the steel surface. In this paper, the evidence collected from prestressed concrete (PC) specimens that are exposed to salt water is discussed vis-à-vis AE data from continuous monitoring. The specimens consist of PC strips that are subjected to wet/dry salt water cycles, representing portions of bridge piles that are exposed to tidal action. Evidence collected from the specimens includes: (a) values of half-cell potential and linear polarization resistance to recognize active corrosion in its early stage; and (b) scanning electron microscopy micrographs of steel areas from two specimens that were decommissioned once the electrochemical measurements indicated a high probability of active corrosion. These results are used to evaluate the AE activity resulting from early corrosion.

  11. Oxidação de glicerol sobre nanopartículas de ouro suportadas em carvão ativado: monitoramento quimiométrico da reação por ESI-MS e MIR Glycerol oxidation over gold nanoparticles supported on activated carbon: chemometric monitoring of the reaction by ESI-MS and MIR

    Cleiton A. Nunes

    2013-01-01

    Full Text Available A study on the monitoring of glycerol oxidation catalyzed by gold nanoparticles supported on activated carbon under mild conditions by chemometric methods is presented. The reaction was monitored by mass spectrometry-electrospray ionization (ESI-MS and comparatively by mid infrared spectroscopy (MIR. Concentration profiles of reagent and products were determined by chemometric tools such as Principal Component Analysis (PCA, Evolving Factor Analysis (EFA and Multivariate Curve Resolution (MCR. The gold nanoparticle catalyst was relatively active in glycerol oxidation, favoring formation of high added value products. It was found that the reaction stabilization was reached at four hours, with approximately 70% glycerol conversion and high selectivity for glycerate.

  12. Passive acoustic monitoring of Cook Inlet beluga whales (Delphinapterus leucas).

    Lammers, Marc O; Castellote, Manuel; Small, Robert J; Atkinson, Shannon; Jenniges, Justin; Rosinski, Anne; Oswald, Julie N; Garner, Chris

    2013-09-01

    The endangered beluga whale (Delphinapterus leucas) population in Cook Inlet, AK faces threats from a variety of anthropogenic factors, including coastal development, oil and gas exploration, vessel traffic, and military activities. To address existing gaps in understanding about the occurrence of belugas in Cook Inlet, a project was developed to use passive acoustic monitoring to document the year-round distribution of belugas, as well as killer whales (Orcinus orca), which prey on belugas. Beginning in June 2009, ten moorings were deployed throughout the Inlet and refurbished every two to eight months. Despite challenging conditions consisting of strong tidal currents carrying debris and seasonal ice cover, 83% of mooring deployments were successfully recovered. Noise from water flow, vessel traffic, and/or industrial activities was present at several sites, potentially masking some signals. However, belugas were successfully detected at multiple locations. Detections were relatively common in the upper inlet and less common or absent at middle and lower inlet locations. Killer whale signals were also recorded. Some seasonal variability in the occurrence of both belugas and killer whales was evident. PMID:23968047

  13. Hydraulic Fracturing of Heterogeneous Rock Monitored by Acoustic Emission

    Stanchits, Sergey; Burghardt, Jeffrey; Surdi, Aniket

    2015-11-01

    In this paper, the results of laboratory studies of hydraulic fracture in homogeneous sandstone blocks with man-made interfaces and heterogeneous shale blocks with weak natural interfaces are reported. Tests were conducted under similar stress conditions, with fluids of different viscosity and at different injection rates. The measurements and analysis allows the identification of fracture initiation and behavior. Fracturing with high-viscosity fluids resulted in stable fracture propagation initiated before breakdown, while fracturing with low-viscosity fluids resulted in unstable fracture propagation initiated almost simultaneously with breakdown. Analysis also allows us to measure the fluid volume entering the fracture and the fracture volume. Monitoring of acoustic emission hypocenter localizations, indicates the development of created fractured area including the intersection with interfaces, fluid propagation along interfaces, crossing interfaces, and approaching the boundaries of the block. We observe strong differences in hydraulic fracture behavior, fracture geometry and fracture propagation speed, when fracturing with water and high-viscosity fluids. We also observed distinct differences between sandstone blocks and shale blocks, when a certain P-wave velocity ray path is intersected by the hydraulic fracture. The velocity increases in sandstones and decreases in shale.

  14. Acoustical method of whole-body hydration status monitoring

    Sarvazyan, A. P.; Tsyuryupa, S. N.; Calhoun, M.; Utter, A.

    2016-07-01

    An acoustical handheld hydration monitor (HM) for assessing the water balance of the human body was developed. Dehydration is a critical public health problem. Many elderly over age of 65 are particularly vulnerable as are infants and young children. Given that dehydration is both preventable and reversible, the need for an easy-to-perform method for the detection of water imbalance is of the utmost clinical importance. The HM is based on an experimental fact that ultrasound velocity in muscle is a linear function of water content and can be referenced to the hydration status of the body. Studies on the validity of HM for the assessment of whole-body hydration status were conducted in the Appalachian State University, USA, on healthy young adults and on elderly subjects residing at an assisted living facility. The HM was able to track changes in total body water during periods of acute dehydration and rehydration in athletes and day-to-day and diurnal variability of hydration in elderly. Results of human studies indicate that HM has a potential to become an efficient tool for detecting abnormal changes in the body hydration status.

  15. Acoustic Emissions (AE) Electrical Systems' Health Monitoring Project

    National Aeronautics and Space Administration — Acoustic Emissions (AE) are associated with physical events, such as thermal activity, dielectric breakdown, discharge inception, as well as crack nucleation and...

  16. Time Reversal Acoustic Structural Health Monitoring Using Array of Embedded Sensors Project

    National Aeronautics and Space Administration — Time Reversal Acoustic (TRA) structural health monitoring with an embedded sensor array represents a new approach to in-situ nondestructive evaluation of air-space...

  17. Automatic classification of urban traffic noise onboard an acoustic monitoring system

    Wessels, P.W.; Zon, A.T. van; Basten, T.G.H.

    2013-01-01

    Recent developments in acoustic monitoring systems make it possible to measure complex noise situations, like urban traffic noise, continuously. Monitoring provides more insight in the noise situation, from which more specific and (cost) effective measures can be taken. Monitoring also allows direct

  18. A stationary acoustic system for monitoring undisturbed and vessel affected fish behaviour

    Godø, Olav Rune; Totland, Atle

    1996-01-01

    Thorough knowledge of the dynamics of natural fish behaviour and distribution within a survey and among surveys is fundamental for reliability of time series of abundance indices. Further, vessel/trawl affected avoidance may greatly affect density estimates from trawl and acoustic surveys. Means for monitoring behaviour of fish during surveys or in special experiments have been limited, time consuming and expensive. This paper describes an acoustic buoy system for monitoring...

  19. Listening to the Deep: Live monitoring of ocean noise and cetacean acoustic signals

    André, Michel; Van der Schaar, Mike Connor Roger Malcolm; Zaugg, Serge Alain; Houégnigan, Ludwig; A..M. Sánchez; Castell, Joan

    2011-01-01

    The development and broad use of passive acoustic monitoring techniques have the potential to help assessing the large-scale influence of artificial noise on marine organisms and ecosystems. Deep-sea observatories have the potential to play a key role in understanding these recent acoustic changes. LIDO(Listening to the Deep Ocean Environment) is an international project that is allowing the real-time longterm monitoring of marine ambient noise as well as marine mammal sounds at cabled and...

  20. Surface Acoustic Wave Monitor for Deposition and Analysis of Ultra-Thin Films

    Hines, Jacqueline H. (Inventor)

    2015-01-01

    A surface acoustic wave (SAW) based thin film deposition monitor device and system for monitoring the deposition of ultra-thin films and nanomaterials and the analysis thereof is characterized by acoustic wave device embodiments that include differential delay line device designs, and which can optionally have integral reference devices fabricated on the same substrate as the sensing device, or on a separate device in thermal contact with the film monitoring/analysis device, in order to provide inherently temperature compensated measurements. These deposition monitor and analysis devices can include inherent temperature compensation, higher sensitivity to surface interactions than quartz crystal microbalance (QCM) devices, and the ability to operate at extreme temperatures.

  1. Aespoe Pillar Stability Experiment. Acoustic emission and ultrasonic monitoring

    Haycox, Jon; Pettitt, Will; Young, R. Paul [Applied Seismology Consultants Ltd., Shrewsbury (United Kingdom)

    2005-12-15

    This report describes the results from acoustic emission (AE) and ultrasonic monitoring of the Aespoe Pillar Stability Experiment (APSE) at SKB's Hard Rock Laboratory (HRL), Sweden. The APSE is being undertaken to demonstrate the current capability to predict spalling in a fractured rock mass using numerical modelling techniques, and to demonstrate the effect of backfill and confining pressure on the propagation of micro-cracks in rock adjacent to deposition holes within a repository. An ultrasonic acquisition system has provided acoustic emission and ultrasonic survey monitoring throughout the various phases of the experiment. Results from the entire data set are provided with this document so that they can be effectively compared to several numerical modelling studies, and to mechanical and thermal measurements conducted around the pillar volume, in an 'integrated analysis' performed by SKB staff. This document provides an in-depth summary of the AE and ultrasonic survey results for future reference. The pillar has been produced by excavating two 1.8 m diameter deposition holes 1 m apart. These were bored in 0.8 m steps using a Tunnel Boring Machine specially adapted for vertical drilling. The first deposition hole was drilled in December 2003. Preceding this a period of background monitoring was performed so as to obtain a datum for the results. The hole was then confined to 0.7 MPa internal over pressure using a specially designed water-filled bladder. The second deposition hole was excavated in March 2004. Heating of the pillar was performed over a two month period between ending in July 2004, when the confined deposition hole was slowly depressurised. Immediately after depressurisation the pillar was allowed to cool with cessation of monitoring occurring a month later. A total of 36,676 AE triggers were recorded over the reporting period between 13th October 2003 and 14th July 2004. Of these 15,198 have produced AE locations. The AE data set

  2. Aespoe Pillar Stability Experiment. Acoustic emission and ultrasonic monitoring

    This report describes the results from acoustic emission (AE) and ultrasonic monitoring of the Aespoe Pillar Stability Experiment (APSE) at SKB's Hard Rock Laboratory (HRL), Sweden. The APSE is being undertaken to demonstrate the current capability to predict spalling in a fractured rock mass using numerical modelling techniques, and to demonstrate the effect of backfill and confining pressure on the propagation of micro-cracks in rock adjacent to deposition holes within a repository. An ultrasonic acquisition system has provided acoustic emission and ultrasonic survey monitoring throughout the various phases of the experiment. Results from the entire data set are provided with this document so that they can be effectively compared to several numerical modelling studies, and to mechanical and thermal measurements conducted around the pillar volume, in an 'integrated analysis' performed by SKB staff. This document provides an in-depth summary of the AE and ultrasonic survey results for future reference. The pillar has been produced by excavating two 1.8 m diameter deposition holes 1 m apart. These were bored in 0.8 m steps using a Tunnel Boring Machine specially adapted for vertical drilling. The first deposition hole was drilled in December 2003. Preceding this a period of background monitoring was performed so as to obtain a datum for the results. The hole was then confined to 0.7 MPa internal over pressure using a specially designed water-filled bladder. The second deposition hole was excavated in March 2004. Heating of the pillar was performed over a two month period between ending in July 2004, when the confined deposition hole was slowly depressurised. Immediately after depressurisation the pillar was allowed to cool with cessation of monitoring occurring a month later. A total of 36,676 AE triggers were recorded over the reporting period between 13th October 2003 and 14th July 2004. Of these 15,198 have produced AE locations. The AE data set shows an intense

  3. Remote acoustic monitoring of North Atlantic right whales (Eubalaena glacialis reveals seasonal and diel variations in acoustic behavior.

    Leanna P Matthews

    Full Text Available Remote acoustic monitoring is a non-invasive tool that can be used to study the distribution, behavior, and habitat use of sound-producing species. The North Atlantic right whale (Eubalaena glacialis is an endangered baleen whale species that produces a variety of stereotyped acoustic signals. One of these signals, the "gunshot" sound, has only been recorded from adult male North Atlantic right whales and is thought to function for reproduction, either as reproductive advertisement for females or as an agonistic signal toward other males. This study uses remote acoustic monitoring to analyze the presence of gunshots over a two-year period at two sites on the Scotian Shelf to determine if there is evidence that North Atlantic right whales may use these locations for breeding activities. Seasonal analyses at both locations indicate that gunshot sound production is highly seasonal, with an increase in the autumn. One site, Roseway West, had significantly more gunshot sounds overall and exhibited a clear diel trend in production of these signals at night. The other site, Emerald South, also showed a seasonal increase in gunshot production during the autumn, but did not show any significant diel trend. This difference in gunshot signal production at the two sites indicates variation either in the number or the behavior of whales at each location. The timing of the observed seasonal increase in gunshot sound production is consistent with the current understanding of the right whale breeding season, and our results demonstrate that detection of gunshots with remote acoustic monitoring can be a reliable way to track shifts in distribution and changes in acoustic behavior including possible mating activities.

  4. Remote acoustic monitoring of North Atlantic right whales (Eubalaena glacialis) reveals seasonal and diel variations in acoustic behavior.

    Matthews, Leanna P; McCordic, Jessica A; Parks, Susan E

    2014-01-01

    Remote acoustic monitoring is a non-invasive tool that can be used to study the distribution, behavior, and habitat use of sound-producing species. The North Atlantic right whale (Eubalaena glacialis) is an endangered baleen whale species that produces a variety of stereotyped acoustic signals. One of these signals, the "gunshot" sound, has only been recorded from adult male North Atlantic right whales and is thought to function for reproduction, either as reproductive advertisement for females or as an agonistic signal toward other males. This study uses remote acoustic monitoring to analyze the presence of gunshots over a two-year period at two sites on the Scotian Shelf to determine if there is evidence that North Atlantic right whales may use these locations for breeding activities. Seasonal analyses at both locations indicate that gunshot sound production is highly seasonal, with an increase in the autumn. One site, Roseway West, had significantly more gunshot sounds overall and exhibited a clear diel trend in production of these signals at night. The other site, Emerald South, also showed a seasonal increase in gunshot production during the autumn, but did not show any significant diel trend. This difference in gunshot signal production at the two sites indicates variation either in the number or the behavior of whales at each location. The timing of the observed seasonal increase in gunshot sound production is consistent with the current understanding of the right whale breeding season, and our results demonstrate that detection of gunshots with remote acoustic monitoring can be a reliable way to track shifts in distribution and changes in acoustic behavior including possible mating activities. PMID:24646524

  5. MONITORING OF THE METAL STRUCTURAL STATE BY ACOUSTICAL STRUCTURAL NOISE

    V. V. Muraviev

    2015-03-01

    Full Text Available To determine the structural state of the metal as an informative parameter the structural acoustic noise is proposed. The paper represents the experimental results of the use at acoustical structural noise for the determination at the structural state of carbon pipe steels exposed by heat treatment, corrosion and tensile loads. The effect of grain size, corrosion and tensile loads on the level of structural noise is discussed.

  6. Real Time Monitoring of Containerless Microreactions in Acoustically Levitated Droplets via Ambient Ionization Mass Spectrometry.

    Crawford, Elizabeth A; Esen, Cemal; Volmer, Dietrich A

    2016-09-01

    Direct in-droplet (in stillo) microreaction monitoring using acoustically levitated micro droplets has been achieved by combining acoustic (ultrasonic) levitation for the first time with real time ambient tandem mass spectrometry (MS/MS). The acoustic levitation and inherent mixing of microliter volumes of reactants (3 μL droplets), yielding total reaction volumes of 6 μL, supported monitoring the acid-catalyzed degradation reaction of erythromycin A. This reaction was chosen to demonstrate the proof-of-principle of directly monitoring in stillo microreactions via hyphenated acoustic levitation and ambient ionization mass spectrometry. The microreactions took place completely in stillo over 30, 60, and 120 s within the containerless stable central pressure node of an acoustic levitator, thus readily promoting reaction miniaturization. For the evaluation of the miniaturized in stillo reactions, the degradation reactions were also carried out in vials (in vitro) with a total reaction volume of 400 μL. The reacted in vitro mixtures (6 μL total) were similarly introduced into the acoustic levitator prior to ambient ionization MS/MS analysis. The in stillo miniaturized reactions provided immediate real-time snap-shots of the degradation process for more accurate reaction monitoring and used a fraction of the reactants, while the larger scale in vitro reactions only yielded general reaction information. PMID:27505037

  7. Acoustic emission (AT) monitoring of metallic Ariane 5 boostervessel from MAN Technologie AG

    The Ariane 5 comprises high-grade products and components, including those qualified and tested by acoustic emission: The steel boostervessel, the SPELTRA structure consisting of a CFRP/aluminium honeycomb and the GAT/GAM high-pressure vessel of CFRP/steel. Classic nondestructive test methods like X-ray and ultrasound cannot be applied, so acoustic emission testing was used instead. It was applied for detecting and localizing active acoustic sources in order to monitor the test stand and initiate pressure reduction if necessary. (orig.)

  8. Real-time monitoring of acoustic linear and nonlinear behavior of titanium alloys during cyclic loading

    Frouin, J.; Maurer, J.; Sathish, S.; Eylon, D.; Na, J.K.; Matikas, T.E.

    2000-07-01

    Variation in acoustic nonlinearity has been monitored in real time during fatigue, on four dog-bone specimens of Ti-6Al-4V, under low cycle fatigue conditions, from the virgin state all the way to fracture. The results of these experiments show that the acoustic nonlinearity undergoes large changes during the fatigue and follows a similar trend for the material under given fatigue test conditions. Transmission electron microscopic (TEM) examination of the samples with similar composition fatigues to different stages indicates a gradual change in the microstructure and dislocation density, which correlates with the changes in acoustic nonlinearity.

  9. A novel sensor for monitoring acoustic cavitation. Part I: Concept, theory, and prototype development.

    Zeqiri, Bajram; Gélat, Pierre N; Hodnett, Mark; Lee, Nigel D

    2003-10-01

    This paper describes a new concept for an ultrasonic cavitation sensor designed specifically for monitoring acoustic emissions generated by small microbubbles when driven by an applied acoustic field. Its novel features include a hollow, open-ended, cylindrical shape, with the sensor being a right circular cylinder of height 32 mm and external diameter 38 mm. The internal diameter of the sensor is 30 mm; its inner surface is fabricated from a 110-microm layer of piezoelectrically active film whose measurement bandwidth is sufficient to enable acoustic emissions up to and beyond 10 MHz to be monitored. When in use, the sensor is immersed within the liquid test medium and high frequency (megahertz) acoustic emissions occurring within the hollow body of the sensor are monitored. In order to shield the sensor response from events occurring outside the cylinder, the outer surface of the sensor cylinder is encapsulated within a special 4-mm thick polyurethane-based cavitation shield with acoustic properties specifically developed to be minimally perturbing to the 40 kHz applied acoustic field but attenuating to ultrasound generated at megahertz frequencies (plane-wave transmission loss > 30 dB at 1 MHz). This paper introduces the rationale behind the new sensor, describing details of its construction and the materials formulation program undertaken to develop the cavitation shield. PMID:14609074

  10. An effective sensor for tool wear monitoring in face milling : acoustic emmision

    Mathew, M. T.; P S Pai; Rocha, L A

    2008-01-01

    Acoustic Emission (AE) has been widely used for monitoring manufacturing processes particularly those involving metal cutting. Monitoring the condition of the cutting tool in the machining process is very important since tool condition will affect the part size, quality and an unexpected tool failure may damage the tool, work-piece and sometimes the machine tool itself. AE can be effectively used for tool condition monitoring applications because the emissions from process c...

  11. LOCAL TO BASIN SCALE ARRAYS FOR PASSIVE ACOUSTIC MONITORING IN THE ATLANTIC SECTOR OF THE SOUTHERN OCEAN

    Rettig, Stefanie; Boebel, Olaf; Menze, Sebastian; Kindermann, Lars; Thomisch, Karolin; Van Opzeeland, Ilse

    2013-01-01

    Passive acoustic data provide a prime source of information on marine mammal distribution and behaviour. Particularly in the Southern Ocean, where ship-based data collection can be severely hampered by weather and ice conditions, passive acoustic monitoring (PAM) of marine mammals forms an important source of year-round information on acoustic presence. Array data can be used to obtain directional information on the species present in the recordings to derive movement patterns. Acoustic array...

  12. Acoustic emission monitoring of fracturing process of migmatite samples

    Petružálek, Matěj; Lokajíček, Tomáš; Svitek, Tomáš

    Montréal: Canadian Institute of Mining , Metallurgy and Petroleum, 2015. ISBN 978-1-926872-25-4. [International Congress of Rock Mechanics /13./. Montréal (CA), 10.05.2015-13.05.2015] R&D Projects: GA ČR(CZ) GAP104/12/0915; GA MŠk LH13102 Institutional support: RVO:67985831 Keywords : anisotropy * fracturing process * acoustic emission * ultrasonic sounding Subject RIV: DC - Siesmology, Volcanology, Earth Structure

  13. Monitoring and Analysis of In-Pile Phenomena in Advanced Test Reactor using Acoustic Telemetry

    The interior of a nuclear reactor presents a particularly harsh and challenging environment for both sensors and telemetry due to high temperatures and high fluxes of energetic and ionizing particles among the radioactive decay products. A number of research programs are developing acoustic-based sensing approach to take advantage of the acoustic transmission properties of reactor cores. Idaho National Laboratory has installed vibroacoustic receivers on and around the Advanced Test Reactor (ATR) containment vessel to take advantage of acoustically telemetered sensors such as thermoacoustic (TAC) transducers. The installation represents the first step in developing an acoustic telemetry infrastructure. This paper presents the theory of TAC, application of installed vibroacoustic receivers in monitoring the in-pile phenomena inside the ATR, and preliminary data processing results.

  14. Monitoring and Analysis of In-Pile Phenomena in Advanced Test Reactor using Acoustic Telemetry

    Agarwal, Vivek [Idaho National Lab. (INL), Idaho Falls, ID (United States). Dept. of Human Factors, Controls, and Statistics; Smith, James A. [Idaho National Lab. (INL), Idaho Falls, ID (United States). Dept. of Fuel Performance and Design; Jewell, James Keith [Idaho National Lab. (INL), Idaho Falls, ID (United States). Dept. of Fuel Performance and Design

    2015-02-01

    The interior of a nuclear reactor presents a particularly harsh and challenging environment for both sensors and telemetry due to high temperatures and high fluxes of energetic and ionizing particles among the radioactive decay products. A number of research programs are developing acoustic-based sensing approach to take advantage of the acoustic transmission properties of reactor cores. Idaho National Laboratory has installed vibroacoustic receivers on and around the Advanced Test Reactor (ATR) containment vessel to take advantage of acoustically telemetered sensors such as thermoacoustic (TAC) transducers. The installation represents the first step in developing an acoustic telemetry infrastructure. This paper presents the theory of TAC, application of installed vibroacoustic receivers in monitoring the in-pile phenomena inside the ATR, and preliminary data processing results.

  15. Ultrasonic acoustic health monitoring of ball bearings using neural network pattern classification of power spectral density

    Kirchner, William; Southward, Steve; Ahmadian, Mehdi

    2010-03-01

    This paper presents a generic passive non-contact based approach using ultrasonic acoustic emissions (UAE) to facilitate the neural network classification of bearing health, and more specifically the bearing operating condition. The acoustic emission signals used in this study are in the ultrasonic range (20-120 kHz). A direct benefit of microphones capable of measurements in this frequency range is their inherent directionality. Using selected bands from the UAE power spectrum signature, it is possible to pose the health monitoring problem as a multi-class classification problem, and make use of a single neural network to classify the ultrasonic acoustic emission signatures. Artificial training data, based on statistical properties of a significantly smaller experimental data set is used to train the neural network. This specific approach is generic enough to suggest that it is applicable to a variety of systems and components where periodic acoustic emissions exist.

  16. Chemometrics review for chemical sensor development, task 7 report

    NONE

    1994-05-01

    This report, the seventh in a series on the evaluation of several chemical sensors for use in the U.S. Department of Energy`s (DOE`s) site characterization and monitoring programs, concentrates on the potential use of chemometrics techniques in analysis of sensor data. Chemometrics is the chemical discipline that uses mathematical, statistical, and other methods that employ formal logic to: design or select optimal measurement procedures and experiments and provide maximum relevant chemical information by analyzing chemical data. The report emphasizes the latter aspect. In a formal sense, two distinct phases are in chemometrics applications to analytical chemistry problems: (1) the exploratory data analysis phase and (2) the calibration and prediction phase. For use in real-world problems, it is wise to add a third aspect - the independent validation and verification phase. In practical applications, such as the ERWM work, and in order of decreasing difficulties, the most difficult tasks in chemometrics are: establishing the necessary infrastructure (to manage sampling records, data handling, and data storage and related aspects), exploring data analysis, and solving calibration problems, especially for nonlinear models. Chemometrics techniques are different for what are called zeroth-, first-, and second-order systems, and the details depend on the form of the assumed functional relationship between the measured response and the concentrations of components in mixtures. In general, linear relationships can be handled relatively easily, but nonlinear relationships can be difficult.

  17. Chemometrics review for chemical sensor development, task 7 report

    This report, the seventh in a series on the evaluation of several chemical sensors for use in the U.S. Department of Energy's (DOE's) site characterization and monitoring programs, concentrates on the potential use of chemometrics techniques in analysis of sensor data. Chemometrics is the chemical discipline that uses mathematical, statistical, and other methods that employ formal logic to: design or select optimal measurement procedures and experiments and provide maximum relevant chemical information by analyzing chemical data. The report emphasizes the latter aspect. In a formal sense, two distinct phases are in chemometrics applications to analytical chemistry problems: (1) the exploratory data analysis phase and (2) the calibration and prediction phase. For use in real-world problems, it is wise to add a third aspect - the independent validation and verification phase. In practical applications, such as the ERWM work, and in order of decreasing difficulties, the most difficult tasks in chemometrics are: establishing the necessary infrastructure (to manage sampling records, data handling, and data storage and related aspects), exploring data analysis, and solving calibration problems, especially for nonlinear models. Chemometrics techniques are different for what are called zeroth-, first-, and second-order systems, and the details depend on the form of the assumed functional relationship between the measured response and the concentrations of components in mixtures. In general, linear relationships can be handled relatively easily, but nonlinear relationships can be difficult

  18. Experimental study of advanced continuous acoustic-emission monitoring of BWR components. Final report

    This report presents the results of a four year research program on the utilization of acoustic emission techniques on light water reactor component applications. Two techniques of the acoustic emission technology were applied to specific problems occurring within the light water reactor system. Crack detection AE monitoring was applied to thermal cycle fatigue cracking problems and stress corrosion cracking problems. Leak detection AE monitoring was applied to valve leakage in the main steam safety relief valves and incontainment packing gland valves. The report provides AE data showing how AE crack detection can be used as an on-line diagnostic monitoring tool. By having an active monitor on light water reactor components, the inservice inspection of the components is being performed during operation rather than refueling periods, thereby reducing critical path time during outages. The resultant benefit is increased plant availability and a reduction in accumulated radiation exposure

  19. Statistical fracture of E-glass fibres using a bundle tensile test and acoustic emission monitoring

    R'Mili, M.; Moevus, M.; Godin, N.

    2009-01-01

    Statistical fracture of E-glass fibres using a bundle tensile test and acoustic emission monitoring correspondance: Corresponding author.Tel.: +33472436127; fax: +33472438528. (R?Mili, M.) (R?Mili, M.) Universite de Lyon--> , INSA-Lyon--> , MATEIS--> , 7 Avenue Jean Capelle--> , 69621 Villeurbanne Cedex--> - FRANCE (R?Mili, M.) Universite de Lyon--> , INSA-Lyo...

  20. A scalable acoustic sensor network for model based monitoring of urban traffic noise

    Basten, T.G.H.; Wessels, P.W.; Eerden, F.J.M. van der

    2012-01-01

    A good understanding of the acoustic environment due to traffic in urban areas is very important. Long term monitoring within large areas provides a clear insight in the actual noise situation. This is needed to take appropriate and cost efficient measures; to asses the effect of measures by compari

  1. An integrated vision for environmental monitoring and the role of acoustic communication networks

    Jesus, S.M.

    2012-01-01

    Current pace of ocean resources exploitation have set the alarm for tighter environmental monitoring. Recent European legislation requires very accurate measurements of reference values for all types of ocean pollution, including acoustic noise. For near shore or offshore construction, platforms or infrastructures extensive measurements should be carried out before during and after exploitation activities have taken place. Environmental monitoring requires the deployment of sensors with speci...

  2. Acoustic impedance rhinometry (AIR): a technique for monitoring dynamic changes in nasal congestion

    We describe a simple and inexpensive method for monitoring nasal air flow resistance using measurement of the small-signal acoustic input impedance of the nasal passage, similar to the audiological measurement of ear drum compliance with acoustic tympanometry. The method requires generation of a fixed sinusoidal volume–velocity stimulus using ear-bud speakers, and an electret microphone to monitor the resultant pressure fluctuation in the nasal passage. Both are coupled to the nose via high impedance silastic tubing and a small plastic nose insert. The acoustic impedance is monitored in real-time using a laptop soundcard and custom-written software developed in LabView 7.0 (National Instruments). The compact, lightweight equipment and fast time resolution lends the technique to research into the small and rapid reflexive changes in nasal resistance caused by environmental and local neurological influences. The acoustic impedance rhinometry technique has the potential to be developed for use in a clinical setting, where the need exists for a simple and inexpensive objective nasal resistance measurement technique. (paper)

  3. Acoustic emission monitoring of preservice testing at Watts Bar Unit 1 Nuclear Reactor

    Acoustic emission (AE) monitoring of selected pressure boundary areas at TVA's Watts Bar, Unit 1 Nuclear Plant in the US during hot functional preservice testing is described. Background, methodology, and results are included. The work discussed here is a major milestone in a program supported by the US NRC to develop and demonstrate application of AE monitoring for continuous surveillance of reactor pressure boundaries to detect and evaluate growing flaws. The subject work demonstrated that anticipated problem areas can be overcome. Work is continuing to AE monitoring during reactor operation. 3 refs., 6 figs

  4. Distributed feedback fiber laser acoustic emission sensor for concrete structure health monitoring

    Hao, Gengjie; Huang, Wenzhu; Zhang, Wentao; Sun, Baochen; Li, Fang

    2014-05-01

    This paper introduces a highly-sensitive fiber optical acoustic emission (AE) sensor and a parameter analysis method aiming at concrete structure health monitoring. Distributed feedback fiber-laser (DFB-FL), which is encapsulated to have a high acoustic sensitivity, is used for sensor unit of the AE sensor. The AE signal of concrete beam in different work stages, based on the four-point bending experiment of the concrete beam, is picked up, and the relationship between the concrete beam work stages and the AE parameter is found. The results indicate that DFB-FLAES can be used as sensitive transducers for recording acoustic events and forecasting the imminent failure of the concrete beam.

  5. Acoustic emission analysis for structural health monitoring of hot metal components

    For the application of acoustic emission analysis on hot components such as pipes special application techniques are necessary to protect the sensor from the heat. The Fraunhofer IKTS-MD has developed a waveguide solution that meets these requirements. Major challenges in the application of acoustic emission analysis in an industrial environment is the strong ambient noise. This requirement meets the developed acoustic measurement system at the Fraunhofer Institute by a high measurement dynamics, storage and assessment of the complete waveforms and by special algorithms. The attractiveness of the method lies in the relatively low number of sensors with which the integrity of large plant areas (e.g. several meters under high alternating load standing superheated steam pipe) can be permanently monitored.

  6. An Automated Acoustic System to Monitor and Classify Birds

    Ho KC

    2006-01-01

    Full Text Available This paper presents a novel bird monitoring and recognition system in noisy environments. The project objective is to avoid bird strikes to aircraft. First, a cost-effective microphone dish concept (microphone array with many concentric rings is presented that can provide directional and accurate acquisition of bird sounds and can simultaneously pick up bird sounds from different directions. Second, direction-of-arrival (DOA and beamforming algorithms have been developed for the circular array. Third, an efficient recognition algorithm is proposed which uses Gaussian mixture models (GMMs. The overall system is suitable for monitoring and recognition for a large number of birds. Fourth, a hardware prototype has been built and initial experiments demonstrated that the array can acquire and classify birds accurately.

  7. An Automated Acoustic System to Monitor and Classify Birds

    Ho KC; Li Y.; Stanford V; Rochet C; Kwan C; Mei G; Ren Z; Xu R; Zhang Y; Lao D; Stevenson M.

    2006-01-01

    This paper presents a novel bird monitoring and recognition system in noisy environments. The project objective is to avoid bird strikes to aircraft. First, a cost-effective microphone dish concept (microphone array with many concentric rings) is presented that can provide directional and accurate acquisition of bird sounds and can simultaneously pick up bird sounds from different directions. Second, direction-of-arrival (DOA) and beamforming algorithms have been developed for the circular a...

  8. The Doppler Effect based acoustic source separation for a wayside train bearing monitoring system

    Zhang, Haibin; Zhang, Shangbin; He, Qingbo; Kong, Fanrang

    2016-01-01

    Wayside acoustic condition monitoring and fault diagnosis for train bearings depend on acquired acoustic signals, which consist of mixed signals from different train bearings with obvious Doppler distortion as well as background noises. This study proposes a novel scheme to overcome the difficulties, especially the multi-source problem in wayside acoustic diagnosis system. In the method, a time-frequency data fusion (TFDF) strategy is applied to weaken the Heisenberg's uncertainty limit for a signal's time-frequency distribution (TFD) of high resolution. Due to the Doppler Effect, the signals from different bearings have different time centers even with the same frequency. A Doppler feature matching search (DFMS) algorithm is then put forward to locate the time centers of different bearings in the TFD spectrogram. With the determined time centers, time-frequency filters (TFF) are designed with thresholds to separate the acoustic signals in the time-frequency domain. Then the inverse STFT (ISTFT) is taken and the signals are recovered and filtered aiming at each sound source. Subsequently, a dynamical resampling method is utilized to remove the Doppler Effect. Finally, accurate diagnosis for train bearing faults can be achieved by applying conventional spectrum analysis techniques to the resampled data. The performance of the proposed method is verified by both simulated and experimental cases. It shows that it is effective to detect and diagnose multiple defective bearings even though they produce multi-source acoustic signals.

  9. Acoustic emission monitoring and ultrasonic examination correlation on a reactor pressure vessel. Final report

    The acoustic emission monitoring and corroborative ultrasonic examination of the acoustic emission (AE) locations established during the hydrostatic pressure test of a BWR primary pressure vessel is described. Descriptive information regarding AE is provided as a background and details of the AE and ultrasonic instrumentation, procedures, problems encountered, and test results are discussed. In total, 42 acoustic emission locations were detected, located, and ultrasonically examined during this project. At all 42 AE locations ultrasonic indications were obtained. Of the AE locations, 76% (or 32 of the 42) were confirmed at amplitudes greater than or equal to 2.5% Distance Amplitude Correction (DAC) by either L-wave or shear wave ultrasonic examination, the largest of these being 18% DAC. The remainder of the AE locations were confirmed at amplitudes less than 2.5% DAC. ASME Code requires that ultrasonic examination record for permanent reference indications of 50% DAC or greater. As is to be expected ultrasonic examination detected examinations which were not located by AE monitoring since AE locates only active flaws. Results show the complementary value of AE monitoring to ultrasonic examination in two primary uses: determining the existence and the location of active discontinuities; and assuring that active discontinuities are not overlooked. Results reflect the position that AE monitoring and ultrasonics are supplementary to each other, not replacements for one another

  10. A fully automatic wildlife acoustic monitor and survey system

    Boucher, Neil; Jinnai, Michihiro; Smolders, Andrew

    2012-01-01

    International audience We describe a fully automated, PC based wildlife monitoring and survey system that is used for diverse species studies. The system uses a wide-area recorder that can record over areas of up to several square kilometres. The recorder can run, unattended for more than a month. The recordings can either be analysed in real time to produce a particular response (e.g. send an SMS if a rare parrot is detected), or can be analysed later on a PC. Any number of different spec...

  11. Wireless surface acoustic wave sensors for displacement and crack monitoring in concrete structures

    Perry, M.; McKeeman, I.; Saafi, M.; Niewczas, P.

    2016-03-01

    In this work, we demonstrate that wireless surface acoustic wave devices can be used to monitor millimetre displacements in crack opening during the cyclic and static loading of reinforced concrete structures. Sensors were packaged to extend their gauge length and to protect them against brittle fracture, before being surface-mounted onto the tensioned surface of a concrete beam. The accuracy of measurements was verified using computational methods and optical-fibre strain sensors. After packaging, the displacement and temperature resolutions of the surface acoustic wave sensors were 10 μ {{m}} and 2 °C respectively. With some further work, these devices could be retrofitted to existing concrete structures to facilitate wireless structural health monitoring.

  12. Monitoring suspended sediment transport in an ice-affected river using acoustic Doppler current profilers

    Moore, S. A.; Ghareh Aghaji Zare, S.; Rennie, C. D.; Ahmari, H.; Seidou, O.

    2013-12-01

    Quantifying sediment budgets and understanding the processes which control fluvial sediment transport is paramount to monitoring river geomorphology and ecological habitat. In regions that are subject to freezing there is the added complexity of ice. River ice processes impact flow distribution, water stage and sediment transport. Ice processes typically have the largest impact on sediment transport and channel morphodynamics when ice jams occur during ice cover formation and breakup. Ice jams may restrict flow and cause local acceleration when released. Additionally, ice can mechanically scour river bed and banks. Under-ice sediment transport measurements are lacking due to obvious safety and logistical reasons, in addition to a lack of adequate measurement techniques. Since some rivers can be covered in ice during six months of the year, the lack of data in winter months leads to large uncertainty in annual sediment load calculations. To address this problem, acoustic profilers are being used to monitor flow velocity, suspended sediment and ice processes in the Lower Nelson River, Manitoba, Canada. Acoustic profilers are ideal for under-ice sediment flux measurements since they can be operated autonomously and continuously, they do not disturb the flow in the zone of measurement and acoustic backscatter can be related to sediment size and concentration. In March 2012 two upward-facing profilers (1200 kHz acoustic Doppler current profiler, 546 KHz acoustic backscatter profiler) were installed through a hole in the ice on the Nelson River, 50 km downstream of the Limestone Generating Station. Data were recorded for four months, including both stable cover and breakup periods. This paper presents suspended sediment fluxes calculated from the acoustic measurements. Velocity data were used to infer the vertical distribution of sediment sizes and concentrations; this information was then used in the interpretation of the backscattered intensity data. It was found that

  13. The use of acoustic monitoring to manage concrete structures in the nuclear industry

    Concrete and steel are widely used in containment vessels within the nuclear industry. Both are excellent acoustic transmitters. In many structures tensioned wire elements are used within containment structures. However, tensioned wire can be vulnerable to corrosion. To reduce the probability of corrosion sophisticated protection systems are used. To confirm that the design strength is available through time, extensive inspection and maintenance regimes are implemented. These regimes include tests to confirm the condition of the post-tensioning, and pressure tests (leak tests) to verify the performance of vessel. This paper presents an acoustic monitoring technology which uses widely distributed sensors to detect and locate wire failures using the energy released at failure. The technology has been used on a range of structures including post-tensioned concrete bridges, suspension bridges, buildings, pre-cast concrete cylinder pipelines (PCCP) and prestressed concrete containment vessels (PCCV), where it has increased confidence in structures and reduced maintenance costs. Where the level of ambient noise is low then SoundPrint acoustic monitoring can detect concrete cracking. This has been shown in PCCP pipelines, on laboratory test structures and also in nuclear structures. The programme has shown that distributed sensors can locate internal cracking well before there is any external evidence. Several projects have been completed on nuclear vessels. The first has been completed on an Electricite de France (EDF) concrete test pressure vessel at Civaux in France. The second at the Sandia PCCV Test Vessel in Albuquerque, New Mexico, USA, which involved the testing of a steel lined concrete vessel. The third was on a PCCV in Maryland, USA. Acoustic monitoring is also able to monitor the deterioration of post-tensioned concrete structures as a result of seismic activity. Summary details of a case history are presented. (authors)

  14. Acoustic Telemetry Validates a Citizen Science Approach for Monitoring Sharks on Coral Reefs

    Vianna, Gabriel M. S.; Meekan, Mark G; Bornovski, Tova H.; Jessica J Meeuwig

    2014-01-01

    Citizen science is promoted as a simple and cost-effective alternative to traditional approaches for the monitoring of populations of marine megafauna. However, the reliability of datasets collected by these initiatives often remains poorly quantified. We compared datasets of shark counts collected by professional dive guides with acoustic telemetry data from tagged sharks collected at the same coral reef sites over a period of five years. There was a strong correlation between the number of ...

  15. The use of acoustic monitoring to manage concrete structures in the nuclear industry

    Concrete and steel are widely used in containment vessels within the nuclear industry. Both are excellent acoustic transmitters. In many structures tensioned wire elements are used within containment structures. However, tensioned wire can be vulnerable to corrosion. To reduce the probability of corrosion sophisticated protection systems are used. To confirm that the design strength is available through time, extensive inspection and maintenance regimes are implemented. These regimes include tests to confirm the condition of the post-tensioning, and pressure tests (leak tests) to verify the performance of vessel. This paper presents an acoustic monitoring technology which uses widely distributed sensors to detect and locate wire failures using the energy released at failure. The technology has been used on a range of structures including post-tensioned concrete bridges, suspension bridges, buildings, pre-cast concrete cylinder pipelines (PCCP) and prestressed concrete containment vessels (PCCV), where it has increased confidence in structures and reduced maintenance costs. Where the level of ambient noise is low then SoundPrint acoustic monitoring can detect concrete cracking. This has been shown in PCCP pipelines, on laboratory test structures and also in nuclear structures. The programme has shown that distributed sensors can locate internal cracking well before there is any external evidence. Several projects have been completed on nuclear vessels. The first has been completed on an Electricite de France (EDF) concrete test pressure vessel at Civaux in France. The second at the Sandia PCCV Test Vessel in Albuquerque, New Mexico, USA, which involved the testing of a steel lined concrete vessel. The third was on a PCCV in Maryland, USA. Acoustic monitoring is also able to monitor the deterioration of post-tensioned concrete structures as a result of seismic activity. Summary details of a case history are presented. (author)

  16. EDP-assisted system solutions in machine monitoring and quality assurance based on acoustic signals

    In many fields of engineering and technology, experienced staff are able to assess the condition of machines, plants and production processes by changes in both noise and vibrations ('old hand's touch'). Similar to these subjective methods based on mental expertise, complete EDP-assisted system solutions are needed to implement reliable and objective monitoring based on acoustic signals. The author describes such a system including its mature hardware components, problem-oriented software and engineering people ware. (orig./DG)

  17. Monitoring of firmness evolution of peaches during storage by combining acoustic and impact methods

    Diezma Iglesias, Belen; Valero Ubierna, Constantino; García Ramos, Francisco Javier; Ruiz-Altisent, Margarita

    2006-01-01

    Firmness is a very important quality property in peach. The storage of peach affects its subsequent softening process and shelf life. The temperature and duration of storage mainly influence the firmness of stored fruit, and monitoring the evolution of fruits enables producers to manage its commercial life. The objective of the present study was to use non-destructive acoustic and impact tests to estimate firmness of peaches and to elucidate the influence of storage temperature and of time on...

  18. Development of Acoustic Emission Technology for Condition Monitoring and Diagnosis of Rotating Machines; Bearings, Pumps, Gearboxes, Engines and Rotating Structures.

    Mba, David; Rao, Raj B. K. N.

    2006-01-01

    One of the earliest documented applications of Acoustic Emission Technology (AET) to rotating machinery monitoring was in the late 1960s. Since then there has been an explosion in research and application based studies covering bearings, pumps, gearboxes, engines and rotating structures. This paper presents a comprehensive and critical review to date on the application of Acoustic Emission Technology to condition monitoring and diagnostics of rotating machinery.

  19. STUDY ON STABILITY OF UNDERGROUND STRUCTURAL ENGINEERING BY ACOUSTIC EMISSION MONITORING SYSTEM

    来兴平; 张冰川; 蔡美峰

    2000-01-01

    A simulation acoustic emission (AE) signal was processed. And an effective algorithm was presented to obtain the useful signal about the place information from the simulation signal. This paper introduces the artificial monitoring system, its application at underground roadway and its monitoring results, and tries to explore theoretically analyzing method of stability of underground concrete roadway by AE parameters. A simulation AE signal was processed. And an effective algorithm was presented to obtain the useful signal about the place information from the simulation signal It shows the nice future of the application in the active damage detection of composite material.

  20. Field trials of a tactile acoustic monitor for the profoundly deaf.

    Summers, I R; Peake, M A; Martin, M C

    1981-08-01

    Profoundly deaf subjects were given information about sound level in their environment by means of a body-worn unit coupled to a small vibrator worn on the finger. Results of trials on 19 adults are discussed. The Tactile Acoustic Monitor was found to be useful for identifying domestic sounds by means of their distinctive timing patterns. No significant overall improvement in subject's control of voice level was observed, although some subjects found that having a voice level monitor gave them greater confidence to join conversations. Various design improvements were suggested by the trials. Modifications which have been incorporated into an improved unit are described. PMID:7296098

  1. Acoustic emission-based in-process monitoring of surface generation in robot-assisted polishing

    Pilny, Lukas; Bissacco, Giuliano; De Chiffre, Leonardo;

    2015-01-01

    The applicability of acoustic emission (AE) measurements for in-process monitoring of surface generation in the robot-assisted polishing (RAP) was investigated. Surface roughness measurements require interruption of the process, proper surface cleaning and measurements that sometimes necessitate...... removal of the part from the machine tool. In this study, stabilisation of surface roughness during polishing rotational symmetric surfaces by the RAP process was monitored by AE measurements. An AE sensor was placed on a polishing arm in direct contact with a bonded abrasive polishing tool...

  2. Assessment of Groundwater Quality by Chemometrics.

    Papaioannou, Agelos; Rigas, George; Kella, Sotiria; Lokkas, Filotheos; Dinouli, Dimitra; Papakonstantinou, Argiris; Spiliotis, Xenofon; Plageras, Panagiotis

    2016-07-01

    Chemometric methods were used to analyze large data sets of groundwater quality from 18 wells supplying the central drinking water system of Larissa city (Greece) during the period 2001 to 2007 (8.064 observations) to determine temporal and spatial variations in groundwater quality and to identify pollution sources. Cluster analysis grouped each year into three temporal periods (January-April (first), May-August (second) and September-December (third). Furthermore, spatial cluster analysis was conducted for each period and for all samples, and grouped the 28 monitoring Units HJI (HJI=represent the observations of the monitoring site H, the J-year and the period I) into three groups (A, B and C). Discriminant Analysis used only 16 from the 24 parameters to correctly assign 97.3% of the cases. In addition, Factor Analysis identified 7, 9 and 8 latent factors for groups A, B and C, respectively. PMID:27329059

  3. Volatile organic compound monitoring by photo acoustic radiometry

    Two methods for sampling and analyzing volatile organics in subsurface pore gas were developed for use at the Hazardous Waste Disposal Site at Los Alamos National Laboratory. One is Thermal Desorption Gas Chromatography Mass Spectrometry (TDGCMS), the other is Photoacoustic Radiometry (PAR). Presented here are two years worth of experience and lessons learned as both techniques matured. The sampling technique is equally as important as the analysis method. PAR is a nondispersive infrared technique utilizing band pass filters in the region from 1 to 15 μm. A commercial instrument, the Model 1302 Multigas Analyzer, made by Bruel and Kjaer, was adapted for field use. To use the PAR there must be some a priori knowledge of the constellation of analytes to be measured. The TDGCMS method is sensitive to 50 analytes. Hence TDGCMS is used in an initial survey of the site to determine what compounds are present and at what concentration. Once the major constituents of the soil-gas vapor plume are known the PAR can be configured to monitor for the five analytes of most interest. The PAR can analyse a sample in minutes, while in the field. The PAR is also quite precise in controlled situations

  4. A Device for Fetal Monitoring by Means of Control Over Cardiovascular Parameters Based on Acoustic Data

    Khokhlova, L. A.; Seleznev, A. I.; Zhdanov, D. S.; Zemlyakov, I. Yu; Kiseleva, E. Yu

    2016-01-01

    The problem of monitoring fetal health is topical at the moment taking into account a reduction in the level of fertile-age women's health and changes in the concept of perinatal medicine with reconsideration of live birth criteria. Fetal heart rate monitoring is a valuable means of assessing fetal health during pregnancy. The routine clinical measurements are usually carried out by the means of ultrasound cardiotocography. Although the cardiotocography monitoring provides valuable information on the fetal health status, the high quality ultrasound devices are expensive, they are not available for home care use. The recommended number of measurement is also limited. The passive and fully non-invasive acoustic recording provides an alternative low-cost measurement method. The article describes a device for fetal and maternal health monitoring by analyzing the frequency and periodicity of heart beats by means of acoustic signal received on the maternal abdomen. Based on the usage of this device a phonocardiographic fetal telemedicine system, which will allow to reduce the antenatal fetal mortality rate significantly due to continuous monitoring over the state of fetus regardless of mother's location, can be built.

  5. Online monitoring of the two-dimensional temperature field in a boiler furnace based on acoustic computed tomography

    Online monitoring of the temperature field is crucial to optimally adjust combustion within a boiler. In this paper, acoustic computed tomography (CT) technology was used to obtain the temperature profile of a furnace cross-section. The physical principles behind acoustic CT, acoustic signals and time delay estimation were studied. Then, the technique was applied to a domestic 600-MW coal-fired boiler. Acoustic CT technology was used to monitor the temperature field of the cross-section in the boiler furnace, and the temperature profile was reconstructed through ART iteration. The linear sweeping frequency signal was adopted as the sound source signal, whose sweeping frequency ranged from 500 to 3000 Hz with a sweeping cycle of 0.1 s. The generalized cross-correlation techniques with PHAT and ML were used as the time delay estimation method when the boiler was in different states. Its actual operation indicated that the monitored images accurately represented the combustion state of the boiler, and the acoustic CT system was determined to be accurate and reliable. - Highlights: • An online monitoring approach to monitor temperature field in a boiler furnace. • The paper provides acoustic CT technology to obtain the temperature profile of a furnace cross-section. • The temperature profile was reconstructed through ART iteration. • The technique is applied to a domestic 600-MW coal-fired boiler. • The monitored images accurately represent the combustion state of the boiler

  6. An acoustic-array based structural health monitoring technique for wind turbine blades

    Aizawa, Kai; Poozesh, Peyman; Niezrecki, Christopher; Baqersad, Javad; Inalpolat, Murat; Heilmann, Gunnar

    2015-04-01

    This paper proposes a non-contact measurement technique for health monitoring of wind turbine blades using acoustic beamforming techniques. The technique works by mounting an audio speaker inside a wind turbine blade and observing the sound radiated from the blade to identify damage within the structure. The main hypothesis for the structural damage detection is that the structural damage (cracks, edge splits, holes etc.) on the surface of a composite wind turbine blade results in changes in the sound radiation characteristics of the structure. Preliminary measurements were carried out on two separate test specimens, namely a composite box and a section of a wind turbine blade to validate the methodology. The rectangular shaped composite box and the turbine blade contained holes with different dimensions and line cracks. An acoustic microphone array with 62 microphones was used to measure the sound radiation from both structures when the speaker was located inside the box and also inside the blade segment. A phased array beamforming technique and CLEAN-based subtraction of point spread function from a reference (CLSPR) were employed to locate the different damage types on both the composite box and the wind turbine blade. The same experiment was repeated by using a commercially available 48-channel acoustic ring array to compare the test results. It was shown that both the acoustic beamforming and the CLSPR techniques can be used to identify the damage in the test structures with sufficiently high fidelity.

  7. Effects of different analysis techniques and recording duty cycles on passive acoustic monitoring of killer whales.

    Riera, Amalis; Ford, John K; Ross Chapman, N

    2013-09-01

    Killer whales in British Columbia are at risk, and little is known about their winter distribution. Passive acoustic monitoring of their year-round habitat is a valuable supplemental method to traditional visual and photographic surveys. However, long-term acoustic studies of odontocetes have some limitations, including the generation of large amounts of data that require highly time-consuming processing. There is a need to develop tools and protocols to maximize the efficiency of such studies. Here, two types of analysis, real-time and long term spectral averages, were compared to assess their performance at detecting killer whale calls in long-term acoustic recordings. In addition, two different duty cycles, 1/3 and 2/3, were tested. Both the use of long term spectral averages and a lower duty cycle resulted in a decrease in call detection and positive pod identification, leading to underestimations of the amount of time the whales were present. The impact of these limitations should be considered in future killer whale acoustic surveys. A compromise between a lower resolution data processing method and a higher duty cycle is suggested for maximum methodological efficiency. PMID:23968036

  8. Acoustic remote monitoring of rock and concrete structures for nuclear waste repositories

    Excavation and thermally induced damage is of significance for many types of engineering structures but no more so than in the case of nuclear waste repository design. My research and that of my group, formally at Queen's University Canada and Keele University UK and now at the University of Liverpool UK, has focused on the development of acoustic techniques for the in situ detection and quantification of induced damage and fracturing. The application of earthquake seismology to this problem has provided the opportunity to study the micro mechanics of damage mechanisms in situ and provide validation data for predictive geomechanical models used for engineering design. Since 1987 I have been a principal investigator at Atomic Energy of Canada's Underground Research Laboratory (URL), responsible for the development of acoustic emission techniques (AE). In the last twelve years, the application of acoustic techniques to rock damage assessment has been pioneered by my group at the URL and successfully applied in several other major international projects including the ZEDEX, Retrieval and Prototype repository experiments at the Aspo Hard Rock Laboratory (HRL) of SKB Sweden. In this paper I describe what information is available by remote acoustic monitoring of rock and concrete structures and demonstrate this with reference to two international scientific experiments carried out at the URL Canada and the HRL Sweden. (author)

  9. Dual instrument passive acoustic monitoring of belugas in Cook Inlet, Alaska.

    Castellote, Manuel; Small, Robert J; Lammers, Marc O; Jenniges, Justin J; Mondragon, Jeff; Atkinson, Shannon

    2016-05-01

    As part of a long-term research program, Cook Inlet beluga (Delphinapterus leucas) presence was acoustically monitored with two types of acoustic sensors utilized in tandem in moorings deployed year-round: an ecological acoustic recorder (EAR) and a cetacean and porpoise detector (C-POD). The EAR was used primarily to record the calls, whistles, and buzzes produced by belugas and killer whales (Orcinus orca). The C-POD was used to log and classify echolocation clicks from belugas, killer whales, and porpoises. This paper describes mooring packages that maximized the chances of successful long-term data collection in the particularly challenging Cook Inlet environment, and presents an analytical comparison of odontocete detections obtained by the collocated EAR and C-POD instruments from two mooring locations in the upper inlet. Results from this study illustrate a significant improvement in detecting beluga and killer whale presence when the different acoustic signals detected by EARs and C-PODs are considered together. Further, results from concurrent porpoise detections indicating prey competition and feeding interference with beluga, and porpoise displacement due to ice formation are described. PMID:27250163

  10. Acoustic emission for on-line reactor monitoring: results of intermediate vessel test monitoring and reactor hot functional testing

    The objective of the acoustic emission (AE)/flaw characterization program is to provide an experimental feasibility evaluation of using the AE method on a continuous basis (during operation and during hydrotest) to detect and analyze flaw growth in reactor pressure vessels and primary piping. This effort is based on earlier results showing that AE has potential for being a valuable addition to nondestructive evaluation (NDE) methods with the added unique capability for continuous monitoring, high sensitivity and remote flaw location. Results are reported for the ZB-1 vessel test and the Watts Bar-1 hot functional test

  11. Development of acoustic emission monitoring system for fault detection of thermal reduction reactor

    The research on the development of the fault monitoring system for the thermal reduction reactor has been performed preliminarily in order to support the successful operation of the thermal reduction reactor. The final task of the development of the fault monitoring system is to assure the integrity of the thermal reduction reactor by the Acoustic Emission (AE) method. The objectives of this paper are to identify and characterize the fault-induced signals for the discrimination of the various AE signals acquired during the reactor operation. The AE data acquisition and analysis system was constructed and applied to the fault monitoring of the small-scale reduction reactor. Through the series of experiments, the various signals such as background noise, operating signals, and fault-induced signals were measured and their characteristics were identified, which will be used in the signal discrimination for further application to full-scale thermal reduction reactor

  12. On-line Acoustic Emission monitoring of nuclear reactor systems - Status and future

    Development of Acoustic Emission (AE) technology for on-line monitoring of nuclear reactors has been going on to one degree or another for the past 20 years. The concept has received a wide variety of support and condemnation. Initially, it suffered from over enthusiasm on the part of proponents which resulted in some disappointing application efforts and a premature effort to gain ASME Code acceptance. Some very pessimistic assessments of AE for continuous monitoring grew out of all this. These critical reviews, however, served a valuable function because they helped focus what had to be accomplished to make the technology useful. The topic of this paper is, ''Where do we stand on achieving the needed accomplishments, and what is the future direction to implement effective on-line AE monitoring of nuclear reactor systems?''

  13. Monitoring the viscosity of diesel engine lubricating oil by using acoustic emission technique, the selection of measurement parameters

    Acoustic emission technique has been developed through years of monitoring and diagnosis of bearing, but it is still new in the diagnosis and monitoring of lubrication oil to bearings drive. The propagation of acoustic emission signal is generated when the signal piston on the cylinder liner lubricating oil which is a par. The signal is analyzed in time domain to obtain the parameters of root mean squared, amplitude, energy and courtesy. Lubricant viscosity will undergo changes due to temperature, pressure and useful. This study focuses on the appropriate parameters for the diagnosis and monitoring of lubricating oil viscosity. Studies were conducted at a constant rotational speed and temperature, but use a different age. The results showed that the energy parameter is the best parameter used in this monitoring. However, this parameter cannot be used directly and it should be analyzed using mathematical formulas. This mathematical formula is a relationship between acoustic emission energy with the viscosity of lubricating oil. (author)

  14. Damage Accumulation in Cyclically-Loaded Glass-Ceramic Matrix Composites Monitored by Acoustic Emission

    Aggelis, D. G.; Dassios, K. G.; Kordatos, E. Z.; Matikas, T. E.

    2013-01-01

    Barium osumilite (BMAS) ceramic matrix composites reinforced with SiC-Tyranno fibers are tested in a cyclic loading protocol. Broadband acoustic emission (AE) sensors are used for monitoring the occurrence of different possible damage mechanisms. Improved use of AE indices is proposed by excluding low-severity signals based on waveform parameters, rather than only threshold criteria. The application of such improvements enhances the accuracy of the indices as accumulated damage descriptors. RA-value, duration, and signal energy follow the extension cycles indicating moments of maximum or minimum strain, while the frequency content of the AE signals proves very sensitive to the pull-out mechanism. PMID:24381524

  15. On-line acoustic emission monitoring for crack growth in LWRs

    Program activities to develop Acoustic Emission/Flaw Relationships for Inservice Monitoring of LWRs are discussed in this paper. The program is supported by the NRC Research Office with supplemental funding provided by the TVA. Accomplishments for FY87 and plans for FY88 are presented under the topics of technology development, validation on a reactor, standard and code acceptance, and dissemination of the technology. Subjects include detection of very slow crack growth, pattern recognition, on-reactor AE system performance testing, ASTM Standard, ASME Code item, and technology dissemination through application. The current program work continues to emphasize technology transfer. (author)

  16. Laser ablation of absorbing liquids under transparent cover: acoustical and optical monitoring

    Samokhin, A. A.; Il'ichev, N. N.; Pivovarov, P. A.; Sidorin, A. V.

    2016-06-01

    Phase transition induced with infrared (λ = 2920 nm and λ = 2940 nm) nanosecond laser pulses in strongly absorbing liquids (water, ethanol) under transparent solid cover is investigated with the help of acoustical and optical monitoring. LiNbO3 transducer is used for registration of pressure pulses generated in irradiated liquids. Optical signals due to scattering and specular reflection of probing optical beams are explored with the schemes involving total internal reflection and interference effects. Combination of these two optical diagnostic methods permits for the first time to show that irradiation of covered liquids leads to vapor cavity formation which is divided from the cover with thin (submicron) liquid film despite the fact that radiation intensity maximum is located just at the liquid-plate boundary. The cavity formation is due to explosive boiling which occurs when the superheated liquid reaches its superheating limit in near critical region. After the first acoustical signal, the second signal is observed with several hundreds microseconds time delay which is caused by the vapor cavity collapse. Some results of optical and acoustical diagnostics in the case of free liquid surface are also presented.

  17. Acoustic monitoring method and system in laser-induced optical breakdown (LIOB)

    O' Donnell, Matthew (Ann Arbor, MI); Ye, Jing Yong (Ann Arbor, MI); Norris, Theodore B. (Dexter, MI); Baker, Jr., James R. (Ann Arbor, MI); Balogh, Lajos P. (Ann Arbor, MI); Milas, Susanne M. (Ann Arbor, MI); Emelianov, Stanislav Y. (Ann Arbor, MI); Hollman, Kyle W. (Fenton, MI)

    2008-05-06

    An acoustic monitoring method and system in laser-induced optical breakdown (LIOB) provides information which characterize material which is broken down, microbubbles in the material, and/or the microenvironment of the microbubbles. In one embodiment of the invention, femtosecond laser pulses are focused just inside the surface of a volume of aqueous solution which may include dendrimer nanocomposite (DNC) particles. A tightly focused, high frequency, single-element ultrasonic transducer is positioned such that its focus coincides axially and laterally with this laser focus. When optical breakdown occurs, a microbubble forms and a shock or pressure wave is emitted (i.e., acoustic emission). In addition to this acoustic signal, the microbubble may be actively probed with pulse-echo measurements from the same transducer. After the microbubble forms, received pulse-echo signals have an extra pulse, describing the microbubble location and providing a measure of axial microbubble size. Wavefield plots of successive recordings illustrate the generation, growth, and collapse of microbubbles due to optical breakdown. These same plots can also be used to quantify LIOB thresholds.

  18. Experimental study of advanced continuous acoustic emission monitoring of BWR components. Final report

    The program consisted of installing, maintaining, and monitoring AE sensors located on primary piping, nozzles, and valves in the BWR system. Analysis of the AE data was correlated to the results of supplementary nondestructive testing techniques used during the in-service inspection, performed at refueling outages. Purpose of the program was to develop the on-line surveillance acoustic emission technique in order to identify areas of possible structural degradation. Result of reducing inspection time was to reduce accumulated radiation exposure to inspecting personnel and to reduce the amount of critical plant outage time by identifying the critical inspection areas during operation. The program demonstrated the capability of acoustic emission instrumentation to endure the nuclear reactor environment. The acoustic emission sensors withstood 12 months of reactor operation at temperatures of 4000F and greater in high radiation fields. The preamplifiers, also mounted in the reactor environment, operated for the 12-month period in 100% humidity, 2500F conditions. The remaining cable and AE instrumentation were operated in controlled environments

  19. Health monitoring of Ceramic Matrix Composites from waveform-based analysis of Acoustic Emission

    Maillet Emmanuel

    2015-01-01

    Full Text Available Ceramic Matrix Composites (CMCs are anticipated for use in the hot section of aircraft engines. Their implementation requires the understanding of the various damage modes that are involved and their relation to life expectancy. Acoustic Emission (AE has been shown to be an efficient technique for monitoring damage evolution in CMCs. However, only a waveform-based analysis of AE can offer the possibility to validate and precisely examine the recorded AE data with a view to damage localization and identification. The present work fully integrates wave initiation, propagation and acquisition in the analysis of Acoustic Emission waveforms recorded at various sensors, therefore providing more reliable information to assess the relation between Acoustic Emission and damage modes. The procedure allows selecting AE events originating from damage, accurate determination of their location as well as the characterization of effects of propagation on the recorded waveforms. This approach was developed using AE data recorded during tensile tests on carbon/carbon composites. It was then applied to melt-infiltrated SiC/SiC composites.

  20. Impact-acoustics-based health monitoring of tile-wall bonding integrity using principal component analysis

    Tong, F.; Tso, S. K.; Hung, M. Y. Y.

    2006-06-01

    The use of the acoustic features extracted from the impact sounds for bonding integrity assessment has been extensively investigated. Nonetheless, considering the practical implementation of tile-wall non-destructive evaluation (NDE), the traditional defects classification method based directly on frequency-domain features has been of limited application because of the overlapping feature patterns corresponding to different classes whenever there is physical surface irregularity. The purpose of this paper is to explore the clustering and classification ability of principal component analysis (PCA) as applied to the impact-acoustics signature in tile-wall inspection with a view to mitigating the adverse influence of surface non-uniformity. A clustering analysis with signature acquired on sample slabs shows that impact-acoustics signatures of different bonding quality and different surface roughness are well separated into different clusters when using the first two principal components obtained. By adopting as inputs the feature vectors extracted with PCA applied, a multilayer back-propagation artificial neural network (ANN) classifier is developed for automatic health monitoring and defects classification of tile-walls. The inspection results obtained experimentally on the prepared sample slabs are presented and discussed, confirming the utility of the proposed method, particularly in dealing with tile surface irregularity.

  1. Experimental study of advanced continuous acoustic emission monitoring of BWR components. Final report

    McElroy, J W; Hartman, W F

    1980-09-01

    The program consisted of installing, maintaining, and monitoring AE sensors located on primary piping, nozzles, and valves in the BWR system. Analysis of the AE data was correlated to the results of supplementary nondestructive testing techniques used during the in-service inspection, performed at refueling outages. Purpose of the program was to develop the on-line surveillance acoustic emission technique in order to identify areas of possible structural degradation. Result of reducing inspection time was to reduce accumulated radiation exposure to inspecting personnel and to reduce the amount of critical plant outage time by identifying the critical inspection areas during operation. The program demonstrated the capability of acoustic emission instrumentation to endure the nuclear reactor environment. The acoustic emission sensors withstood 12 months of reactor operation at temperatures of 400/sup 0/F and greater in high radiation fields. The preamplifiers, also mounted in the reactor environment, operated for the 12-month period in 100% humidity, 250/sup 0/F conditions. The remaining cable and AE instrumentation were operated in controlled environments.

  2. Acoustic monitoring of laboratory faults: locating the origin of unstable slip events

    Korkolis, Evangelos; Niemeijer, André; Spiers, Christopher

    2015-04-01

    Over the past several decades, much work has been done on studying the frictional properties of fault gouges at earthquake nucleation velocities. In addition, post-experiment microstructural analyses have been performed in an attempt to link microphysical mechanisms to the observed mechanical data. However, all observations are necessarily post-mortem and it is thus difficult to directly link transients to microstructural characteristics. We are developing an acoustic monitoring system to be used in sliding experiments using a ring shear apparatus. The goal is to locate acoustic emission sources in sheared granular assemblages and link them to processes that act on microstructures responsible for the frictional stability of the simulated fault gouge. The results will be used to develop and constrain microphysical models that explain the relation of these processes to empirical friction laws, such as rate- and state-dependent friction. The acoustic monitoring setup is comprised of an array of 16 piezo-electric sensors installed on the top and bottom sides of an annular sample, at 45 degree intervals. Acoustic emissions associated with slip events can be recorded at sampling rates of up to 50 MHz, in triggered mode. Initial experiments on 0.1 to 0.2 mm and 0.4 to 0.5 mm diameter glass beads, at 1 to 5 MPa normal stress and 1 to 30 um/s load point velocity, have been conducted to estimate the sensitivity of the sensor array. Preliminary results reveal that the intensity of the audible signal is not necessarily proportional to the magnitude of the associated stress drop for constant loading conditions, and that acoustic emissions precede slip events by a small amount of time, in the order of a few milliseconds. Currently, our efforts are focused on developing a suitable source location algorithm with the aim to identify differences in the mode of (unstable) sliding for different types of materials. This will help to identify the micromechanical mechanisms operating

  3. Near-real-time acoustic monitoring of beaked whales and other cetaceans using a Seaglider™.

    Klinck, Holger; Mellinger, David K; Klinck, Karolin; Bogue, Neil M; Luby, James C; Jump, William A; Shilling, Geoffrey B; Litchendorf, Trina; Wood, Angela S; Schorr, Gregory S; Baird, Robin W

    2012-01-01

    In most areas, estimating the presence and distribution of cryptic marine mammal species, such as beaked whales, is extremely difficult using traditional observational techniques such as ship-based visual line transect surveys. Because acoustic methods permit detection of animals underwater, at night, and in poor weather conditions, passive acoustic observation has been used increasingly often over the last decade to study marine mammal distribution, abundance, and movements, as well as for mitigation of potentially harmful anthropogenic effects. However, there is demand for new, cost-effective tools that allow scientists to monitor areas of interest autonomously with high temporal and spatial resolution in near-real time. Here we describe an autonomous underwater vehicle--a glider--equipped with an acoustic sensor and onboard data processing capabilities to passively scan an area for marine mammals in near-real time. The glider was tested extensively off the west coast of the Island of Hawai'i, USA. The instrument covered approximately 390 km during three weeks at sea and collected a total of 194 h of acoustic data. Detections of beaked whales were successfully reported to shore in near-real time. Manual analysis of the recorded data revealed a high number of vocalizations of delphinids and sperm whales. Furthermore, the glider collected vocalizations of unknown origin very similar to those made by known species of beaked whales. The instrument developed here can be used to cost-effectively screen areas of interest for marine mammals for several months at a time. The near-real-time detection and reporting capabilities of the glider can help to protect marine mammals during potentially harmful anthropogenic activities such as seismic exploration for sub-sea fossil fuels or naval sonar exercises. Furthermore, the glider is capable of under-ice operation, allowing investigation of otherwise inaccessible polar environments that are critical habitats for many

  4. Near-real-time acoustic monitoring of beaked whales and other cetaceans using a Seaglider™.

    Holger Klinck

    Full Text Available In most areas, estimating the presence and distribution of cryptic marine mammal species, such as beaked whales, is extremely difficult using traditional observational techniques such as ship-based visual line transect surveys. Because acoustic methods permit detection of animals underwater, at night, and in poor weather conditions, passive acoustic observation has been used increasingly often over the last decade to study marine mammal distribution, abundance, and movements, as well as for mitigation of potentially harmful anthropogenic effects. However, there is demand for new, cost-effective tools that allow scientists to monitor areas of interest autonomously with high temporal and spatial resolution in near-real time. Here we describe an autonomous underwater vehicle--a glider--equipped with an acoustic sensor and onboard data processing capabilities to passively scan an area for marine mammals in near-real time. The glider was tested extensively off the west coast of the Island of Hawai'i, USA. The instrument covered approximately 390 km during three weeks at sea and collected a total of 194 h of acoustic data. Detections of beaked whales were successfully reported to shore in near-real time. Manual analysis of the recorded data revealed a high number of vocalizations of delphinids and sperm whales. Furthermore, the glider collected vocalizations of unknown origin very similar to those made by known species of beaked whales. The instrument developed here can be used to cost-effectively screen areas of interest for marine mammals for several months at a time. The near-real-time detection and reporting capabilities of the glider can help to protect marine mammals during potentially harmful anthropogenic activities such as seismic exploration for sub-sea fossil fuels or naval sonar exercises. Furthermore, the glider is capable of under-ice operation, allowing investigation of otherwise inaccessible polar environments that are critical

  5. Laser tattoo removal as an ablation process monitored by acoustical and optical methods

    Cencič, Boris; Gregorčič, Peter; Možina, Janez; Jezeršek, Matija

    2013-07-01

    Strength of the laser-tissue interaction varies even within a single tattoo because of the inhomogeneous distribution of the tattoo pigment embedded in the skin. A monitoring system is therefore developed for simultaneous monitoring of the laser tattoo removal process based on acoustical and optical techniques. A laser-beam-deflection probe is used for measuring the acoustical signals accompanying the breakdown, and a CCD camera captures the level and the spatial distribution of the plasma radiation. Using these methods we examine the degree of excitation-pulse absorption within the pigment and the degree of the structural changes of the skin. A Nd:YAG laser with a top-hat beam profile, designed for tattoo removal, is used as the excitation source in our experiments. Special attention is given to structural changes in the skin, which depend on the applied fluence. Tattoo removal with multiple pulses is also analyzed. Experiments are made in vitro (skin phantoms) and ex vivo (marking tattoos on the pig skin). The presented results are important for the understanding and optimization of the process used in medical therapies.

  6. Monitoring accelerated carbonation on standard Portland cement mortar by nonlinear resonance acoustic test

    Eiras, J. N.; Kundu, T.; Popovics, J. S.; Monzó, J.; Borrachero, M. V.; Payá, J.

    2015-03-01

    Carbonation is an important deleterious process for concrete structures. Carbonation begins when carbon dioxide (CO2) present in the atmosphere reacts with portlandite producing calcium carbonate (CaCO3). In severe carbonation conditions, C-S-H gel is decomposed into silica gel (SiO2.nH2O) and CaCO3. As a result, concrete pore water pH decreases (usually below 10) and eventually steel reinforcing bars become unprotected from corrosion agents. Usually, the carbonation of the cementing matrix reduces the porosity, because CaCO3 crystals (calcite and vaterite) occupy more volume than portlandite. In this study, an accelerated carbonation-ageing process is conducted on Portland cement mortar samples with water to cement ratio of 0.5. The evolution of the carbonation process on mortar is monitored at different levels of ageing until the mortar is almost fully carbonated. A nondestructive technique based on nonlinear acoustic resonance is used to monitor the variation of the constitutive properties upon carbonation. At selected levels of ageing, the compressive strength is obtained. From fractured surfaces the depth of carbonation is determined with phenolphthalein solution. An image analysis of the fractured surfaces is used to quantify the depth of carbonation. The results from resonant acoustic tests revealed a progressive increase of stiffness and a decrease of material nonlinearity.

  7. Preliminary studies for monitoring erosion in pipelines by the acoustic emission technique

    Tiboni, G.B. [Universidade Tecnologica Federal do Parana (UTFPR), Curitiba, PR (Brazil). Programa de Pos-graduacao em Engenharia Mecanica e de Materiais; Marquardt, T.A.S; SantaMaria, V.A.R.; Silva, C.H. [Universidade Tecnologica Federal do Parana (UTFPR), Curitiba, PR (Brazil)

    2009-07-01

    The aim of this work is to present some applications of Acoustic Emission (AE), which is a powerful technique for nondestructive testing in Tribology, treated here as tests of friction, wear by contact fatigue, wear by slip and wear by erosion. In this work a special attention is given to solid particle erosion and hydro-abrasive erosion, problems found in almost every pipeline that lead to local loss of material and eventually rupture of the line. The technique of AE can be used as an efficient online tool when, primarily, to monitor tribological aspects such as the rate of wear of materials, as well as detect the spread of flaws in them. In wear by erosion, specifically, the parameters of RMS and acoustic energy are capable of correlation with the type of mechanism for removal of material. As a preliminary goal, erosive tests were performed with gas (air) without erosive particles, monitored by AE, varying the surface of the samples and the internal diameter the nozzle, taking the differences in signs of AE. Correlation between parameters of RMS and amplitude were noticed with the variables of the tests, such as roughness and fluid velocity. The RMS parameter showed a exponential correction with the fluid velocity, however the amplitude signals had a linear behavior. The knowledge of these parameters is essential for the development of a system that is able to quantify the wear rate of a pipeline without taking it out of operation. (author)

  8. A portable Raman acoustic levitation spectroscopic system for the identification and environmental monitoring of algal cells.

    Wood, Bayden R; Heraud, Philip; Stojkovic, Slobodanka; Morrison, Danielle; Beardall, John; McNaughton, Don

    2005-08-01

    We report the coupling of a portable Raman spectrometer to an acoustic levitation device to enable environmental monitoring and the potential taxonomic identification of microalgae. Spectra of living cells were recorded at 785 nm using a fiber-optic probe coupled to a portable Raman spectrometer. The spectra exhibit an excellent signal-to-noise ratio and clearly show bands from chlorophyll a and beta-carotene. Spectra of levitated photobleached microalgae clearly show a reduction in chlorophyll a concentration relative to beta-carotene after 10 min of exposure to a quartz halogen lamp. Spectra recorded from levitated nitrogen-limited cells also show a significant reduction in bands associated with chlorophyll a, as compared to nitrogen-replete cells. To investigate the diagnostic capability of the technique, four species of microalgae were analyzed. Good quality spectra of all four species were obtained showing varying ratios of beta-carotene to chlorophyll. The combination of an acoustic levitation device and a portable Raman spectrometer shows potential as a taxonomic and environmental monitoring tool with direct application to field studies in remote environments. PMID:16053309

  9. Structural Health Monitoring of Wind Turbine Blades: Acoustic Source Localization Using Wireless Sensor Networks

    Omar Mabrok Bouzid

    2015-01-01

    Full Text Available Structural health monitoring (SHM is important for reducing the maintenance and operation cost of safety-critical components and systems in offshore wind turbines. This paper proposes an in situ wireless SHM system based on an acoustic emission (AE technique. By using this technique a number of challenges are introduced due to high sampling rate requirements, limitations in the communication bandwidth, memory space, and power resources. To overcome these challenges, this paper focused on two elements: (1 the use of an in situ wireless SHM technique in conjunction with the utilization of low sampling rates; (2 localization of acoustic sources which could emulate impact damage or audible cracks caused by different objects, such as tools, bird strikes, or strong hail, all of which represent abrupt AE events and could affect the structural health of a monitored wind turbine blade. The localization process is performed using features extracted from aliased AE signals based on a developed constraint localization model. To validate the performance of these elements, the proposed system was tested by testing the localization of the emulated AE sources acquired in the field.

  10. Acoustic emission-based condition monitoring methods: Review and application for low speed slew bearing

    Caesarendra, Wahyu; Kosasih, Buyung; Tieu, Anh Kiet; Zhu, Hongtao; Moodie, Craig A. S.; Zhu, Qiang

    2016-05-01

    This paper presents an acoustic emission-based method for the condition monitoring of low speed reversible slew bearings. Several acoustic emission (AE) hit parameters as the monitoring parameters for the detection of impending failure of slew bearings are reviewed first. The review focuses on: (1) the application of AE in typical rolling element bearings running at different speed classifications, i.e. high speed (>600 rpm), low speed (10-600 rpm) and very low speed (<10 rpm); (2) the commonly used AE hit parameters in rolling element bearings and (3) AE signal processing, feature extraction and pattern recognition methods. In the experiment, impending failure of the slew bearing was detected by the AE hit parameters after the new bearing had run continuously for approximately 15 months. The slew bearing was then dismantled and the evidence of the early defect was analysed. Based on the result, we propose a feature extraction method of the AE waveform signal using the largest Lyapunov exponent (LLE) algorithm and demonstrate that the LLE feature can detect the sign of failure earlier than the AE hit parameters with improved prediction of the progressive trend of the defect.

  11. Monitoring of the deformation and fracture process of dual phase steels employing acoustic emission techniques

    Highlights: ► Acoustic emission (AE) signals from a tensile test of dual phase steels (DPS)s with various morphologies were captured. ► By utilizing sentry function we tried to relate the AE signals and micromechanisms of fracture of these steels. ► SEM observations for verification of results, indicate that AE monitoring is an efficient tool to detect micromechanisms identifying failure in DPSs. - Abstract: In this paper, continuing our previous works, a new approach for detection of fracture micro mechanisms of ferrite–martensite dual-phase steels (DPSs) with various microstructures was investigated. For this purpose, dual phase steels with different volume fractions of martensite (VM) were produced by various heat treatment methods on a low carbon steel (0.1% C), and acoustic emission (AE) monitoring was then used during tensile testing of these DPSs. The AE signals from a tensile test using DPS in the range of 12–73% VM and various morphologies, like equiaxed or fibrous martensite phase, were captured. Principally, to understand the AE response and behavior of the martensite or ferrite phase separately, some samples of martensite and heat treated ferrite were tested. After the tests, by utilizing a new function named “sentry function”, we tried to relate the AE signals to various failure mechanisms of these steels. In confirmation of our earlier works, the results show that AE monitoring and sentry function are efficient tools to detect failure micromechanisms, consisting of ferrite–martensite interface decohesion and/or martensite phase fracture, identifying the correlation of failure mechanisms to microstructure in DPS. The results were verified with scanning electron microscopic observations and they indicate that AE monitoring is an efficient tool to detect micromechanisms identifying failure in DPSs.

  12. Acoustic emission (AE) health monitoring of diaphragm type couplings using neural network analysis

    Godinez-Azcuaga, Valery F.; Shu, Fong; Finlayson, Richard D.; O'Donnell, Bruce

    2005-05-01

    This paper presents the latest results obtained from Acoustic Emission (AE) monitoring and detection of cracks and/or damage in diaphragm couplings, which are used in some aircraft and engine drive systems. Early detection of mechanical failure in aircraft drive train components is a key safety and economical issue with both military and civil sectors of aviation. One of these components is the diaphragm-type coupling, which has been evaluated as the ideal drive coupling for many application requirements such as high speed, high torque, and non-lubrication. Its flexible axial and angular displacement capabilities have made it indispensable for aircraft drive systems. However, diaphragm-type couplings may develop cracks during their operation. The ability to monitor, detect, identify, and isolate coupling cracks on an operational aircraft system is required in order to provide sufficient advance warning to preclude catastrophic failure. It is known that metallic structures generate characteristic Acoustic Emission (AE) during crack growth/propagation cycles. This phenomenon makes AE very attractive among various monitoring techniques for fault detection in diaphragm-type couplings. However, commercially available systems capable of automatic discrimination between signals from crack growth and normal mechanical noise are not readily available. Positive classification of signals requires experienced personnel and post-test data analysis, which tend to be a time-consuming, laborious, and expensive process. With further development of automated classifiers, AE can become a fully autonomous fault detection technique requiring no human intervention after implementation. AE has the potential to be fully integrated with automated query and response mechanisms for system/process monitoring and control.

  13. Passive acoustic monitoring of coastally associated Hawaiian spinner dolphins, Stenella longirostris, ground-truthed through visual surveys.

    Heenehan, Heather L; Tyne, Julian A; Bejder, Lars; Van Parijs, Sofie M; Johnston, David W

    2016-07-01

    Effective decision making to protect coastally associated dolphins relies on monitoring the presence of animals in areas that are critical to their survival. Hawaiian spinner dolphins forage at night and rest during the day in shallow bays. Due to their predictable presence, they are targeted by dolphin-tourism. In this study, comparisons of presence were made between passive acoustic monitoring (PAM) and vessel-based visual surveys in Hawaiian spinner dolphin resting bays. DSG-Ocean passive acoustic recording devices were deployed in four bays along the Kona Coast of Hawai'i Island between January 8, 2011 and August 30, 2012. The devices sampled at 80 kHz, making 30-s recordings every four minutes. Overall, dolphins were acoustically detected on 37.1% to 89.6% of recording days depending on the bay. Vessel-based visual surveys overlapped with the PAM surveys on 202 days across the four bays. No significant differences were found between visual and acoustic detections suggesting acoustic surveys can be used as a proxy for visual surveys. Given the need to monitor dolphin presence across sites, PAM is the most suitable and efficient tool for monitoring long-term presence/absence. Concomitant photo-identification surveys are necessary to address changes in abundance over time. PMID:27475147

  14. Acoustic emission for on-line reactor monitoring: results of intermediate vessel test monitoring and reactor hot functional

    The objective of the acoustic emission (AE)/flaw characterization program presented is to develop use of the AE method on a continuous basis during operation and during hydrotest, to detect and analyze flow growth in reactor pressure vessels and primary piping. The program scope is described by three primary areas of effort: develop a method to identify crack growth AE signals; develop a relationship between measured AE and crack growth; demonstrate the total concept through off-reactor vessel tests; and, on-reactor monitoring. The laboratory speciments used to determine fundamental feasibility of program objectives were ASTM A533 B, Class 1 steel. The ZB-1 vessel test is described, and the results are presented. Reactor hot functional testing was done on the Watts Bar Unit 1. Evidence shows that AE from cracking in inaccessible parts of the reactor system such as the vessel beltline should be detectable

  15. Chemometrics and in-line near infrared spectroscopic monitoring of a biopharmaceutical Chinese hamster ovary cell culture: prediction of multiple cultivation variables.

    Clavaud, Matthieu; Roggo, Yves; Von Daeniken, Ralph; Liebler, André; Schwabe, Jan-Oliver

    2013-07-15

    In the present study near infrared (NIR) spectroscopy was used to monitor the cultivation of mammalian Chinese hamster ovary (CHO) cells producing a monoclonal antibody in a fed-batch cell culture process. A temperature shift was applied during the cultivation. The cells were incubated at 37 °C and 33 °C. The Fourier transform near infrared (FT-NIR) multiplex process analyzer spectroscopy was investigated to monitor cultivation variables of the CHO cell culture from 10 independent batches using two channels of the FT-NIR. The measurements were performed on production scale bioreactors of 12,500 L. The cell cultures were analyzed with the spectrometer coupled to a transflection sterilizable fiber optic probe inserted into the bioreactors. Multivariate data analysis (MVDA) employing unsupervised principal component analysis (PCA) and partial least squares regression methods (PLS) were applied. PCA demonstrated that 96% of the observed variability was explained by the process trajectory and the inter-batch variability. PCA was found to be a significant tool in identifying batch homogeneity between lots and in detecting abnormal fermentation runs. Seven different cell culture parameters such as osmolality, glucose concentration, product titer, packed cell volume (PCV), integrated viable packed cell volume (ivPCV), viable cell density (VCD), and integrated viable cell count (iVCC) were monitored inline and predicted by NIR. NIR spectra and reference analytics data were computed using control charts to evaluate the monitoring abilities. Control charts of each media component were under control by NIR spectroscopy. The PLS calibration plots offered accurate predictive capabilities for each media. This paper underlines the capability for inline prediction of multiple cultivation variables during bioprocess monitoring. PMID:23622522

  16. An effective sensor for tool wear monitoring in face milling: Acoustic emission

    M T Mathew; P Srinivasa Pai; L A Rocha

    2008-06-01

    Acoustic Emission (AE) has been widely used for monitoring manufacturing processes particularly those involving metal cutting. Monitoring the condition of the cutting tool in the machining process is very important since tool condition will affect the part size, quality and an unexpected tool failure may damage the tool, work-piece and sometimes the machine tool itself. AE can be effectively used for tool condition monitoring applications because the emissions from process changes like tool wear, chip formation i.e. plastic deformation, etc. can be directly related to the mechanics of the process. Also AE can very effectively respond to changes like tool fracture, tool chipping, etc. when compared to cutting force and since the frequency range is much higher than that of machine vibrations and environmental noises, a relatively uncontaminated signal can be obtained. AE signal analysis was applied for sensing tool wear in face milling operations. Cutting tests were carried out on a vertical milling machine. Tests were carried out for a given cutting condition, using single insert, two inserts (adjacent and opposite) and three inserts in the cutter. AE signal parameters like ring down count and rms voltage were measured and were correlated with flank wear values (VB max). The results of this investigation indicate that AE can be effectively used for monitoring tool wear in face milling operations.

  17. Estimating population size of a nocturnal burrow-nesting seabird using acoustic monitoring and habitat mapping

    Steffen Oppel

    2014-04-01

    Full Text Available Population size assessments for nocturnal burrow-nesting seabirds are logistically challenging because these species are active in colonies only during darkness and often nest on remote islands where manual inspections of breeding burrows are not feasible. Many seabird species are highly vocal, and recent technological innovations now make it possible to record and quantify vocal activity in seabird colonies. Here we test the hypothesis that remotely recorded vocal activity in Cory’s shearwater (Calonectris borealis breeding colonies in the North Atlantic increases with nest density, and combined this relationship with cliff habitat mapping to estimate the population size of Cory’s shearwaters on the island of Corvo (Azores. We deployed acoustic recording devices in 9 Cory’s shearwater colonies of known size to establish a relationship between vocal activity and local nest density (slope = 1.07, R2 = 0.86, p < 0.001. We used this relationship to predict the nest density in various cliff habitat types and produced a habitat map of breeding cliffs to extrapolate nest density around the island of Corvo. The mean predicted nest density on Corvo ranged from 6.6 (2.1–16.2 to 27.8 (19.5–36.4 nests/ha. Extrapolation of habitat-specific nest densities across the cliff area of Corvo resulted in an estimate of 6326 Cory’s shearwater nests (95% confidence interval: 3735–10,524. This population size estimate is similar to previous assessments, but is too imprecise to detect moderate changes in population size over time. While estimating absolute population size from acoustic recordings may not be sufficiently precise, the strong positive relationship that we found between local nest density and recorded calling rate indicates that passive acoustic monitoring may be useful to document relative changes in seabird populations over time.

  18. Monitoring and failure analysis of corroded bridge cables under fatigue loading using acoustic emission sensors.

    Li, Dongsheng; Ou, Jinping; Lan, Chengming; Li, Hui

    2012-01-01

    Cables play an important role in cable-stayed systems, but are vulnerable to corrosion and fatigue damage. There is a dearth of studies on the fatigue damage evolution of corroded cable. In the present study, the acoustic emission (AE) technology is adopted to monitor the fatigue damage evolution process. First, the relationship between stress and strain is determined through a tensile test for corroded and non-corroded steel wires. Results show that the mechanical performance of corroded cables is changed considerably. The AE characteristic parameters for fatigue damage are then established. AE energy cumulative parameters can accurately describe the fatigue damage evolution of corroded cables. The failure modes in each phase as well as the type of acoustic emission source are determined based on the results of scanning electron microscopy. The waveform characteristics, damage types, and frequency distribution of the corroded cable at different damage phases are collected. Finally, the number of broken wires and breakage time of the cables are determined according to the variation in the margin index. PMID:22666009

  19. Monitoring and Failure Analysis of Corroded Bridge Cables under Fatigue Loading Using Acoustic Emission Sensors

    Hui Li

    2012-03-01

    Full Text Available Cables play an important role in cable-stayed systems, but are vulnerable to corrosion and fatigue damage. There is a dearth of studies on the fatigue damage evolution of corroded cable. In the present study, the acoustic emission (AE technology is adopted to monitor the fatigue damage evolution process. First, the relationship between stress and strain is determined through a tensile test for corroded and non-corroded steel wires. Results show that the mechanical performance of corroded cables is changed considerably. The AE characteristic parameters for fatigue damage are then established. AE energy cumulative parameters can accurately describe the fatigue damage evolution of corroded cables. The failure modes in each phase as well as the type of acoustic emission source are determined based on the results of scanning electron microscopy. The waveform characteristics, damage types, and frequency distribution of the corroded cable at different damage phases are collected. Finally, the number of broken wires and breakage time of the cables are determined according to the variation in the margin index.

  20. Stress-Induced Fracturing of Reservoir Rocks: Acoustic Monitoring and μCT Image Analysis

    Pradhan, Srutarshi; Stroisz, Anna M.; Fjær, Erling; Stenebråten, Jørn F.; Lund, Hans K.; Sønstebø, Eyvind F.

    2015-11-01

    Stress-induced fracturing in reservoir rocks is an important issue for the petroleum industry. While productivity can be enhanced by a controlled fracturing operation, it can trigger borehole instability problems by reactivating existing fractures/faults in a reservoir. However, safe fracturing can improve the quality of operations during CO2 storage, geothermal installation and gas production at and from the reservoir rocks. Therefore, understanding the fracturing behavior of different types of reservoir rocks is a basic need for planning field operations toward these activities. In our study, stress-induced fracturing of rock samples has been monitored by acoustic emission (AE) and post-experiment computer tomography (CT) scans. We have used hollow cylinder cores of sandstones and chalks, which are representatives of reservoir rocks. The fracture-triggering stress has been measured for different rocks and compared with theoretical estimates. The population of AE events shows the location of main fracture arms which is in a good agreement with post-test CT image analysis, and the fracture patterns inside the samples are visualized through 3D image reconstructions. The amplitudes and energies of acoustic events clearly indicate initiation and propagation of the main fractures. Time evolution of the radial strain measured in the fracturing tests will later be compared to model predictions of fracture size.

  1. Passive wireless surface acoustic wave sensors for monitoring sequestration sites CO2 emission

    Wang, Yizhong [Univ. of Pittsburgh, PA (United States); Chyu, Minking [Univ. of Pittsburgh, PA (United States); Wang, Qing-Ming [Univ. of Pittsburgh, PA (United States)

    2013-02-14

    University of Pittsburgh’s Transducer lab has teamed with the U.S. Department of Energy’s National Energy Technology Laboratory (DOE NETL) to conduct a comprehensive study to develop/evaluate low-cost, efficient CO2 measuring technologies for geological sequestration sites leakage monitoring. A passive wireless CO2 sensing system based on surface acoustic wave technology and carbon nanotube nanocomposite was developed. Surface acoustic wave device was studied to determine the optimum parameters. Delay line structure was adopted as basic sensor structure. CNT polymer nanocomposite was fabricated and tested under different temperature and strain condition for natural environment impact evaluation. Nanocomposite resistance increased for 5 times under pure strain, while the temperature dependence of resistance for CNT solely was -1375ppm/°C. The overall effect of temperature on nanocomposite resistance was -1000ppm/°C. The gas response of the nanocomposite was about 10% resistance increase under pure CO2 . The sensor frequency change was around 300ppm for pure CO2 . With paralyne packaging, the sensor frequency change from relative humidity of 0% to 100% at room temperature decreased from over 1000ppm to less than 100ppm. The lowest detection limit of the sensor is 1% gas concentration, with 36ppm frequency change. Wireless module was tested and showed over one foot transmission distance at preferred parallel orientation.

  2. Electrical Resistance and Acoustic Emission Measurements for Monitoring the Structural Behavior of CFRP Laminate

    Zhou, Wei

    2015-07-12

    Electrical resistance and acoustic emission (AE) measurement are jointly used to monitor the degradation in CFRP laminates subjected to tensile tests. The objective of this thesis is to perform a synergertic analysis between a passive and an active methods to better access how these perform when used for Structural Health Moni- toring (SHM). Laminates with three different stacking sequences: [0]4, [02/902]s and [+45/ − 45]2s are subjected to monotonic and cyclic tensile tests. In each laminate, we carefully investigate which mechanisms of degradation can or cannot be detect- ed by each technique. It is shown that most often, that acoustic emission signals start before any electrical detection is possible. This is is explained based on the redundance of the electrical network that makes it less sensitive to localized damages. Based on in depth study of AE signals clustering, a new classification is proposed to recognize the different damage mechanims based on only two parameters: the RA (rise time/amplitude) and the duration of the signal.

  3. Fatigue damage monitoring for basalt fiber reinforced polymer composites using acoustic emission technique

    Wang, Wentao; Li, Hui; Qu, Zhi

    2012-04-01

    Basalt fiber reinforced polymer (BFRP) is a structural material with superior mechanical properties. In this study, unidirectional BFRP laminates with 14 layers are made with the hand lay-up method. Then, the acoustic emission technique (AE) combined with the scanning electronic microscope (SEM) technique is employed to monitor the fatigue damage evolution of the BFRP plates in the fatigue loading tests. Time-frequency analysis using the wavelet transform technique is proposed to analyze the received AE signal instead of the peak frequency method. A comparison between AE signals and SEM images indicates that the multi-frequency peaks picked from the time-frequency curves of AE signals reflect the accumulated fatigue damage evolution and fatigue damage patterns. Furthermore, seven damage patterns, that is, matrix cracking, delamination, fiber fracture and their combinations, are identified from the time-frequency curves of the AE signals.

  4. A study of condition monitoring of check valve using acoustic emission and neural network technique

    The check valve is one of typical component being extensively used in safety systems of nuclear power plants. The failures of check valves have resulted in significant maintenance efforts, on occasion, have resulted in water hammer, over-pressurization of low-pressure systems, and damage to flow system components. The objective of this research is to demonstrate condition-monitoring system based on acoustic emission, AE detection that can provide timely detection of check valve degradation and service aging so that maintenance/ replacement could be preformed prior to loss of safety function. This work is also focused on the capability of neural network technique to provide diagnostic information useful in determining check valve aging and degradation, check valve failures and undesirable operating modes

  5. Passive acoustic monitoring of toothed whales with implications for mitigation, management and biology

    Kyhn, Line Anker

    Toothed whales are vocal animals and their social life as well as successful orientation and feeding depends on emission and reception of sound. Such sounds may e.g. be clicks used for echolocation or whistles used for communication and they can be monitored in time and space by means of passive......-recapture design to describe the detection function. From the detection function we then calculated the effective detection radius, which we then used to estimate the density of porpoises in the area. As cue for the acoustic detections we tested different durations with click trains. We obtained the cue production...... is in accordance with new molecular phylogenies. In chapter I use the information I have gathered on spectral source properties as well as on source levels and directionality and use this information to challenge the theories for the evolution of the NBHF click type. I conclude that the NBHF signals likely evolved...

  6. Acoustic emission condition monitoring of a nuclear power plant check valve using artificial neural networks

    Lee, Joon Hyun; Lee, Min Rae [Pusan National University, Pusan (Korea, Republic of); Kim, Jung Teak [Korea Atomic Energy Research Institute, Taejeon (Korea, Republic of)

    2005-11-15

    In this study, an advanced condition monitoring technique based on acoustic emission (AE) detection and artificial neural networks was applied to a check valve, one of the components being used extensively in a safety system of a nuclear power plant (Npp). AE testing for a check valve under controlled flow loop conditions was performed to detect and evaluate disk movement for valve degradation such as wear and leakage due to foreign object interference in a check valve. It is clearly demonstrated that the evaluation of different types of failure modes such as disk wear and check valve leakage were successful by systematically analyzing the characteristics of various AE parameters. It is also shown that the leak size can be determined with an artificial neural network.

  7. Acoustic emission condition monitoring of a nuclear power plant check valve using artificial neural networks

    In this study, an advanced condition monitoring technique based on acoustic emission (AE) detection and artificial neural networks was applied to a check valve, one of the components being used extensively in a safety system of a nuclear power plant (Npp). AE testing for a check valve under controlled flow loop conditions was performed to detect and evaluate disk movement for valve degradation such as wear and leakage due to foreign object interference in a check valve. It is clearly demonstrated that the evaluation of different types of failure modes such as disk wear and check valve leakage were successful by systematically analyzing the characteristics of various AE parameters. It is also shown that the leak size can be determined with an artificial neural network

  8. Acoustic Monitoring of a Previously Unstudied Whale Shark Aggregation in the Red Sea

    Cochran, Jesse

    2012-01-01

    The whale shark (Rhincodon, typus), is a large, pelagic, filter feeder for which the available information is limited. The Red Sea populations in particular are practically unstudied. An aggregation site was recently discovered off the western coast of Saudi Arabia. We report the use of passive acoustic monitoring to assess the spatial and temporal behavior patterns of whale sharks in this new site. The aggregation occurs in the spring and peaks in April/ May. Whale sharks showed a preference for a single near shore reef and even a specific area within it. There is no evidence of sexual segregation as the genders were present in roughly equal proportion and used the same habitat at similar times. This information can be used to guide future studies in the area and to inform local management. Continued study will add to the collective knowledge on Red Sea whale sharks, including the population dynamics within the region and how they interact with the global whale shark community.

  9. Nuclear safeguards for an underground final repository - Research for acoustic-seismic monitoring

    Final repositories for spent nuclear fuel need to be put under safeguards of the International Atomic Energy Agency (IAEA) to detect potential access, during and after the emplacement phase. Tasked by the German Support Programme for the IAEA we have measured acoustic and seismic signals from various mining activities in the Gorleben exploratory mine. Geophone spectra show excitation up to several kHz, often with considerable broad-band content. With periodic machinery harmonic series appear. Seismic signal strengths from different sources vary by three (including blast shots by six) orders of magnitude, in power-law fits the decrease with distance is with exponents -2 to -0.8. Many sources could be detected by amplitude at several 100 m distance, blasts at several km. By a ring of underground geophones around a repository in salt monitoring for undeclared activities seems principally possible.

  10. A Methodological Review of Piezoelectric Based Acoustic Wave Generation and Detection Techniques for Structural Health Monitoring

    Zhigang Sun

    2013-01-01

    Full Text Available Piezoelectric transducers have a long history of applications in nondestructive evaluation of material and structure integrity owing to their ability of transforming mechanical energy to electrical energy and vice versa. As condition based maintenance has emerged as a valuable approach to enhancing continued aircraft airworthiness while reducing the life cycle cost, its enabling structural health monitoring (SHM technologies capable of providing on-demand diagnosis of the structure without interrupting the aircraft operation are attracting increasing R&D efforts. Piezoelectric transducers play an essential role in these endeavors. This paper is set forth to review a variety of ingenious ways in which piezoelectric transducers are used in today’s SHM technologies as a means of generation and/or detection of diagnostic acoustic waves.

  11. Gaussian mixture modeling of acoustic emissions for structural health monitoring of reinforced concrete structures

    Farhidzadeh, Alireza; Dehghan-Niri, Ehsan; Salamone, Salvatore

    2013-04-01

    Reinforced Concrete (RC) has been widely used in construction of infrastructures for many decades. The cracking behavior in concrete is crucial due to the harmful effects on structural performance such as serviceability and durability requirements. In general, in loading such structures until failure, tensile cracks develop at the initial stages of loading, while shear cracks dominate later. Therefore, monitoring the cracking modes is of paramount importance as it can lead to the prediction of the structural performance. In the past two decades, significant efforts have been made toward the development of automated structural health monitoring (SHM) systems. Among them, a technique that shows promises for monitoring RC structures is the acoustic emission (AE). This paper introduces a novel probabilistic approach based on Gaussian Mixture Modeling (GMM) to classify AE signals related to each crack mode. The system provides an early warning by recognizing nucleation of numerous critical shear cracks. The algorithm is validated through an experimental study on a full-scale reinforced concrete shear wall subjected to a reversed cyclic loading. A modified conventional classification scheme and a new criterion for crack classification are also proposed.

  12. Acoustic telemetry validates a citizen science approach for monitoring sharks on coral reefs.

    Vianna, Gabriel M S; Meekan, Mark G; Bornovski, Tova H; Meeuwig, Jessica J

    2014-01-01

    Citizen science is promoted as a simple and cost-effective alternative to traditional approaches for the monitoring of populations of marine megafauna. However, the reliability of datasets collected by these initiatives often remains poorly quantified. We compared datasets of shark counts collected by professional dive guides with acoustic telemetry data from tagged sharks collected at the same coral reef sites over a period of five years. There was a strong correlation between the number of grey reef sharks (Carcharhinus amblyrhynchos) observed by dive guides and the telemetry data at both daily and monthly intervals, suggesting that variation in relative abundance of sharks was detectable in datasets collected by dive guides in a similar manner to data derived from telemetry at these time scales. There was no correlation between the number or mean depth of sharks recorded by telemetry and the presence of tourist divers, suggesting that the behaviour of sharks was not affected by the presence of divers during our study. Data recorded by dive guides showed that current strength and temperature were important drivers of the relative abundance of sharks at monitored sites. Our study validates the use of datasets of shark abundance collected by professional dive guides in frequently-visited dive sites in Palau, and supports the participation of experienced recreational divers as contributors to long-term monitoring programs of shark populations. PMID:24760081

  13. Acoustic telemetry validates a citizen science approach for monitoring sharks on coral reefs.

    Gabriel M S Vianna

    Full Text Available Citizen science is promoted as a simple and cost-effective alternative to traditional approaches for the monitoring of populations of marine megafauna. However, the reliability of datasets collected by these initiatives often remains poorly quantified. We compared datasets of shark counts collected by professional dive guides with acoustic telemetry data from tagged sharks collected at the same coral reef sites over a period of five years. There was a strong correlation between the number of grey reef sharks (Carcharhinus amblyrhynchos observed by dive guides and the telemetry data at both daily and monthly intervals, suggesting that variation in relative abundance of sharks was detectable in datasets collected by dive guides in a similar manner to data derived from telemetry at these time scales. There was no correlation between the number or mean depth of sharks recorded by telemetry and the presence of tourist divers, suggesting that the behaviour of sharks was not affected by the presence of divers during our study. Data recorded by dive guides showed that current strength and temperature were important drivers of the relative abundance of sharks at monitored sites. Our study validates the use of datasets of shark abundance collected by professional dive guides in frequently-visited dive sites in Palau, and supports the participation of experienced recreational divers as contributors to long-term monitoring programs of shark populations.

  14. On-line quantitative monitoring of liquid-liquid extraction of Lonicera japonica and Artemisia annua using near-infrared spectroscopy and chemometrics

    Sha Wu

    2015-01-01

    Full Text Available Background: Liquid liquid extraction of Lonicera japonica and Artemisia annua (JQ plays a significant role in manufacturing Reduning injection. Many process parameters may influence liquid liquid extraction and cause fluctuations in product quality. Objective: To develop a near infrared (NIR spectroscopy method for on line monitoring of liquid liquid extraction of JQ. Materials and Methods: Eleven batches of JQ extraction solution were obtained, ten for building quantitative models and one for assessing the predictive accuracy of established models. Neochlorogenic acid (NCA, chlorogenic acid (CA, cryptochlorogenic acid (CCA, isochlorogenic acid B (ICAB, isochlorogenic acid A (ICAA, isochlorogenic acid C (ICAC and soluble solid content (SSC were selected as quality control indicators, and measured by reference methods. NIR spectra were collected in transmittance mode. After selecting the spectral sub ranges, optimizing the spectral pretreatment and neglecting outliers, partial least squares regression models were built to predict the content of indicators. The model performance was evaluated by the coefficients of determination (R2, the root mean square errors of prediction (RMSEP and the relative standard error of prediction (RSEP. Results: For NCA, CA, CCA, ICAB, ICAA, ICAC and SSC, R2 was 0.9674, 0.9704, 0.9641, 0.9514, 0.9436, 0.9640, 0.9809, RMSEP was 0.0280, 0.2913, 0.0710, 0.0590, 0.0815, 0.1506, 1.167, and RSEP was 2.32%, 4.14%, 3.86%, 5.65%, 7.29%, 6.95% and 4.18%, respectively. Conclusion: This study demonstrated that NIR spectroscopy could provide good predictive ability in monitoring of the content of quality control indicators in liquid liquid extraction of JQ.

  15. Validation of an acoustic location system to monitor Bornean orangutan (Pongo pygmaeus wurmbii) long calls.

    Spillmann, Brigitte; van Noordwijk, Maria A; Willems, Erik P; Mitra Setia, Tatang; Wipfli, Urs; van Schaik, Carel P

    2015-07-01

    The long call is an important vocal communication signal in the widely dispersed, semi-solitary orangutan. Long calls affect individuals' ranging behavior and mediate social relationships and regulate encounters between dispersed individuals in a dense rainforest. The aim of this study was to test the utility of an Acoustic Location System (ALS) for recording and triangulating the loud calls of free-living primates. We developed and validated a data extraction protocol for an ALS used to record wild orangutan males' long calls at the Tuanan field site (Central Kalimantan). We installed an ALS in a grid of 300 ha, containing 20 SM2+ recorders placed in a regular lattice at 500 m intervals, to monitor the distribution of calling males in the area. The validated system had the following main features: (i) a user-trained software algorithm (Song Scope) that reliably recognized orangutan long calls from sound files at distances up to 700 m from the nearest recorder, resulting in a total area of approximately 900 ha that could be monitored continuously; (ii) acoustic location of calling males up to 200 m outside the microphone grid, which meant that within an area of approximately 450 ha, call locations could be calculated through triangulation. The mean accuracy was 58 m, an error that is modest relative to orangutan mobility and average inter-individual distances. We conclude that an ALS is a highly effective method for detecting long-distance calls of wild primates and triangulating their position. In combination with conventional individual focal follow data, an ALS can greatly improve our knowledge of orangutans' social organization, and is readily adaptable for studying other highly vocal animals. PMID:25773926

  16. The application of acoustic emission measurements on laboratory testpieces to large scale pressure vessel monitoring

    A test pressure vessel containing 4 artificial defects was monitored for emission whilst pressure cycling to failure. Testpieces cut from both the failed vessel and from as-rolled plate material were tested in the laboratory. A marked difference in emission characteristics was observed between plate and vessel testpieces. Activity from vessel material was virtually constant after general yield and emission amplitudes were low. Plate testpieces showed maximum activity at general yield and more frequent high amplitude emissions. An attempt has been made to compare the system sensitivities between the pressure vessel test and laboratory tests. In the absence of an absolute calibration device, system sensitivities were estimated using dummy signals generated by the excitation of an emission sensor. The measurements have shown an overall difference in sensitivity between vessel and laboratory tests of approximately 25db. The reduced sensitivity in the vessel test is attributed to a combination of differences in sensors, acoustic couplant, attenuation, and dispersion relative to laboratory tests and the relative significance of these factors is discussed. Signal amplitude analysis of the emissions monitored from laboratory testpieces showed that, whith losses of the order of 25 to 30db, few emissions would be detected from the pressure vessel test. It is concluded that no reliable prediction of acoustic behaviour of a structure may be made from laboratory test unless testpieces of the actual structural material are used. A considerable improvement in detection sensitivity, is also required for reliable detection of defects in low strength ductile materials and an absolute method of system calibration is required between tests

  17. Monitoring the quality consistency of Fufang Danshen Pills using micellar electrokinetic chromatography fingerprint coupled with prediction of antioxidant activity and chemometrics.

    Ji, Zhengchao; Sun, Wanyang; Sun, Guoxiang; Zhang, Jin

    2016-08-01

    A fast micellar electrokinetic chromatography fingerprint method combined with quantification was developed and validated to evaluate the quality of Fufang Danshen Pills, a traditional Chinese Medicine, which has been used in the treatment of cardiovascular system diseases, in which the tetrahedron optimization method was first used to optimize the background electrolyte solution. Subsequently, the index of the fingerprint information amount of I was performed as an excellent objective indictor to investigate the experimental conditions. In addition, a systematical quantified fingerprint method was constructed for evaluating the quality consistency of 20 batches of test samples obtained from the same drug manufacturer. The fingerprint analysis combined with quantitative determination of two components showed that the quality consistency of the test samples was quite good within the same commercial brand. Furthermore, the partial least squares model analysis was used to explore the fingerprint-efficacy relationship between active components and antioxidant activity in vitro, which can be applied for the assessment of anti-oxidant activity of Fufang Danshen pills and provide valuable medicinal information for quality control. The result illustrated that the present study provided a reliable and reasonable method for monitoring the quality consistency of Fufang Danshen pills. PMID:27279557

  18. Remote erosion and corrosion monitoring of subsea pipelines using acoustic telemetry and wet-mate connector technology

    Painter, Howard; Barlow, Stewart [Teledyne ODI, Thousand Oaks, CA (United States); Clarke, Daniel [Teledyne Cormon, Thousand Oaks, CA (United States); Green, Dale [Teledyne Benthos, North Falmouth, MA (United States)

    2009-07-01

    This paper will present a novel approach for monitoring erosion and corrosion using proven sub sea technologies: intrusive erosion and corrosion monitoring, acoustic telemetry and wet-mateable connector technology. Intrusive metal loss based monitoring systems on sub sea pipelines are increasingly being used because of their ability to directly measure erosion and corrosion. These systems are integrated with the sub sea production control system or located close to the platform and hard-wired. However, locations remote from a sub sea control system or platform requires a dedicated communication system and long lengths of cable that can be cost prohibitive to procure and install. The system presented consists of an intrusive erosion or corrosion monitor with pressure and temperature transmitters, a retrievable electronics module with an acoustic modem, a data storage module, and a replaceable power module. Time-stamped erosion and corrosion data can be transmitted via an acoustic link to a surface platform, a vessel of opportunity or to a relaying modem. Acoustic signals can be transmitted up to 6 km from the monitoring location. The power module along with data module and acoustic modem are mounted on the erosion and corrosion module using wet-mateable connectors, allowing retrieval by remotely operated vehicles. The collected data can be used to assess the cumulative erosion and corrosion as well as use the real-time metal loss rate data to correlate with operational parameters. Benefits include optimization of corrosion inhibitor dosage rates, mitigation of damage caused by solids production, and increased flow assurance. (author)

  19. MONITORING POWER PLANT EFFICIENCY USING THE MICROWAVE-EXCITED THERMAL-ACOUSTIC EFFECT TO MEASURE UNBURNED CARBON

    Robert C. Brown; Robert J. Weber; Jeffrey J. Swetelitsch

    2005-01-01

    The objective of this project is to explore microwave-excited thermal-acoustic (META) phenomena for quantitative analysis of granular and powdered materials, with the culmination of the research to be an on-line carbon-in-ash monitor for coal-fired power plants. This technique of analyzing unburned carbon in fly ash could be a less tedious and time consuming method as compared to the traditional LOI manual procedure. Phase 1 of the research focused on off-line single-frequency thermal-acoustic measurements where an off-line fly ash monitor was constructed that could operate as analytical tool to explore instrument and methodology parameters for quantifying the microwave-excited thermal-acoustic effect of carbon in fly ash, and it was determined that the off-line thermal-acoustic technique could predict the carbon content of a random collection of fly ashes with a linear correlation constant of R{sup 2} = 0.778. Much higher correlations are expected for fly ashes generated from a single boiler. Phase 2 of the research developing a methodology to generate microwave spectra of various powders, including fly ash, coal, and inorganic minerals, and to determine if these microwave spectra could be used for chemical analyses. Although different minerals produced different responses, higher resolution microwave spectra would be required to be able to distinguish among minerals. Phase 3 of the research focused on the development of an on-line fly ash monitor that could be adapted to measure either a thermal-acoustic or thermal-elastic response to due microwave excitation of fly ash. The thermal-acoustic response was successfully employed for this purpose but the thermal-elastic response was too weak to yield a useful on-line device.

  20. Calibrating passive acoustic monitoring: correcting humpback whale call detections for site-specific and time-dependent environmental characteristics.

    Helble, Tyler A; D'Spain, Gerald L; Campbell, Greg S; Hildebrand, John A

    2013-11-01

    This paper demonstrates the importance of accounting for environmental effects on passive underwater acoustic monitoring results. The situation considered is the reduction in shipping off the California coast between 2008-2010 due to the recession and environmental legislation. The resulting variations in ocean noise change the probability of detecting marine mammal vocalizations. An acoustic model was used to calculate the time-varying probability of detecting humpback whale vocalizations under best-guess environmental conditions and varying noise. The uncorrected call counts suggest a diel pattern and an increase in calling over a two-year period; the corrected call counts show minimal evidence of these features. PMID:24181982

  1. Clinical Studies of Real-Time Monitoring of Lithotripter Performance Using Passive Acoustic Sensors

    Leighton, T. G.; Fedele, F.; Coleman, A. J.; McCarthy, C.; Ryves, S.; Hurrell, A. M.; De Stefano, A.; White, P. R.

    2008-09-01

    This paper describes the development and clinical testing of a passive device which monitors the passive acoustic emissions generated within the patient's body during Extracorporeal Shock Wave Lithotripsy (ESWL). Designed and clinically tested so that it can be operated by a nurse, the device analyses the echoes generated in the body in response to each ESWL shock, and so gives real time shock-by-shock feedback on whether the stone was at the focus of the lithotripter, and if so whether the previous shock contributed to stone fragmentation when that shock reached the focus. A shock is defined as being `effective' if these two conditions are satisfied. Not only can the device provide real-time feedback to the operator, but the trends in shock `effectiveness' can inform treatment. In particular, at any time during the treatment (once a statistically significant number of shocks have been delivered), the percentage of shocks which were `effective' provides a treatment score TS(t) which reflects the effectiveness of the treatment up to that point. The TS(t) figure is automatically delivered by the device without user intervention. Two clinical studies of the device were conducted, the ethics guidelines permitting only use of the value of TS(t) obtained at the end of treatment (this value is termed the treatment score TS0). The acoustically-derived treatment score was compared with the treatment score CTS2 given by the consultant urologist at the three-week patient's follow-up appointment. In the first clinical study (phase 1), records could be compared for 30 out of the 118 patients originally recruited, and the results of phase 1 were used to refine the parameter values (the `rules') with which the acoustic device provides its treatment score. These rules were tested in phase 2, for which records were compared for 49 of the 85 patients recruited. Considering just the phase 2 results (since the phase 1 data were used to draw up the `rules' under which phase 2 operated

  2. Acoustic emission monitoring of medieval towers considered as sensitive earthquake receptors

    A. Carpinteri

    2007-01-01

    Full Text Available Many ancient masonry towers are present in Italian territory. In some cases these structures are at risk on account of the intensity of the stresses they are subjected to due to the high level of regional seismicity. In order to preserve this inestimable cultural heritage, a sound safety assessment should take into account the evolution of damage phenomena. In this connection, acoustic emission (AE monitoring can be highly effective. This study concerns the structural stability of three medieval towers rising in the centre of Alba, a characteristic town in Piedmont (Italy. During the monitoring period a correlation between peaks of AE activity in the masonry of these towers and regional seismicity was found. Earthquakes always affect structural stability. Besides that, the towers behaved as sensitive earthquake receptors. Here a method to correlate bursts of AE activity in a masonry building and regional seismicity is proposed. In particular, this method permits to identify the premonitory signals that precede a catastrophic event on a structure, since, in most cases, these warning signs can be captured well in advance.

  3. Environmental influences on the spatial ecology of juvenile smalltooth sawfish (Pristis pectinata: results from acoustic monitoring.

    Colin A Simpfendorfer

    Full Text Available To aid recovery efforts of smalltooth sawfish (Pristis pectinata populations in U.S. waters a research project was developed to assess how changes in environmental conditions within estuarine areas affected the presence, movements, and activity space of this endangered species. Forty juvenile P. pectinata were fitted with acoustic tags and monitored within the lower 27 km of the Caloosahatchee River estuary, Florida, between 2005 and 2007. Sawfish were monitored within the study site from 1 to 473 days, and the number of consecutive days present ranged from 1 to 125. Residency index values for individuals varied considerably, with annual means highest in 2005 (0.95 and lowest in 2007 (0.73 when several P. pectinata moved upriver beyond detection range during drier conditions. Mean daily activity space was 1.42 km of river distance. The distance between 30-minute centers of activity was typically <0.1 km, suggesting limited movement over short time scales. Salinity electivity analysis demonstrated an affinity for salinities between 18 and at least 24 psu, suggesting movements are likely made in part, to remain within this range. Thus, freshwater flow from Lake Okeechobee (and its effect on salinity affects the location of individuals within the estuary, although it remains unclear whether or not these movements are threatening recovery.

  4. Acoustic emission detection with fiber optical sensors for dry cask storage health monitoring

    Lin, Bin; Bao, Jingjing; Yu, Lingyu; Giurgiutiu, Victor

    2016-04-01

    The increasing number, size, and complexity of nuclear facilities deployed worldwide are increasing the need to maintain readiness and develop innovative sensing materials to monitor important to safety structures (ITS). In the past two decades, an extensive sensor technology development has been used for structural health monitoring (SHM). Technologies for the diagnosis and prognosis of a nuclear system, such as dry cask storage system (DCSS), can improve verification of the health of the structure that can eventually reduce the likelihood of inadvertently failure of a component. Fiber optical sensors have emerged as one of the major SHM technologies developed particularly for temperature and strain measurements. This paper presents the development of optical equipment that is suitable for ultrasonic guided wave detection for active SHM in the MHz range. An experimental study of using fiber Bragg grating (FBG) as acoustic emission (AE) sensors was performed on steel blocks. FBG have the advantage of being durable, lightweight, and easily embeddable into composite structures as well as being immune to electromagnetic interference and optically multiplexed. The temperature effect on the FBG sensors was also studied. A multi-channel FBG system was developed and compared with piezoelectric based AE system. The paper ends with conclusions and suggestions for further work.

  5. Acoustic Emission Monitoring of Lightning-Damaged CFRP Laminates during Compression-after-Impact Test

    Carbon-fiber reinforced plastic(CFRP) laminates made of nano-particle-coated carbon fibers and damaged by a simulated lightning strike were tested under compression-after-impact(CAI) mode, during which the damage progress due to compressive loading has been monitored by acoustic emission(AE). The impact damage was induced not by mechanical loading but by a simulated lightning strike. Conductive nano-particles were coated directly on the fibers, from which CFRP coupons were made. The coupon were subjected to the strikes with a high voltage/current impulse of 10-40 kA within a few . The effects of nano-particle coating and the degree of damage induced by the simulated lightning strikes on AE activities were examined, and the relationship between the compressive residual strength and AE behavior has been evaluated in terms of AE event counts and the onset of AE activity with the compressive loading. The degree of impact damage was also measured in terms of damage area by using ultrasonic C-scan images. The assessment during the CAI tests of damaged CFRP showed that AE monitoring appeared to be useful to differentiate the degree of damage hence the mechanical integrity of composite structures damaged by lightning strikes.

  6. A novel technique for acoustic emission monitoring in civil structures with global fiber optic sensors

    The application of acoustic emission (AE)-based damage detection is gaining interest in the field of civil structural health monitoring. Damage progress can be detected and located in real time and the recorded AEs hold information on the fracture process which produced them. One of the drawbacks for on-site application in large-scale concrete and masonry structures is the relatively high attenuation of the ultrasonic signal, which limits the detection range of the AE sensors. Consequently, a large number of point sensors are required to cover a certain area. To tackle this issue, a global damage detection system, based on AE detection with a polarization-modulated, single mode fiber optic sensor (FOS), has been developed. The sensing principle, data acquisition and analysis in time and frequency domain are presented. During experimental investigations, this AE-FOS is applied for the first time as a global sensor for the detection of crack-induced AEs in a full-scale concrete beam. Damage progress is monitored during a cyclic four-point bending test and the AE activity, detected with the FOS, is related to the subsequent stages of damage progress in the concrete element. The results obtained with the AE-FOS are successfully linked to the mechanical behavior of the concrete beam and a qualitative correspondence is found with AE data obtained by a commercial system. (papers)

  7. Acoustic monitoring in the Ross Sea, Antarctica, using hydrophone of the Ocean Bottom Seismometer

    Yun, Sukyoung; Lee, Won Sang; Kuk Hong, Jong; Yoo, Hyun Jae; Park, Yongcheol; Schmidt-Aursch, Mechita; Geissler, Wolfram H.

    2016-04-01

    Although a number of active source seismic experiments have been conducted over the last few decades to investigate the crustal structure in the Ross Sea, Antarctica, long-term observation to monitor underwater tectonic activities and changes in the cryospheric environment still remains challenging due to existence of sea ice in the study region. Korea Polar Research Institute has accomplished successful deployment of ocean bottom seismometers (OBS) in the Ross Sea collaborating with Alfred Wegener Institute during the period of 2011-2012 and 2014 by Korean icebreaker RV Araon. The OBS system manufactured by K.U.M. contains a hydrophone sensor that allow us to monitor underwater acoustics generated by tectonic and ice-related events. We present spectrograms of the continuous hydroacoustic data and various types of signals, e.g. seismic T-waves, iceequakes, and tremors. There are periodic and harmonic tremors that might be related with tidal modulation, and the seasonal variation of the background noise seems to be related with sea ice concentration.

  8. Challenge of Using Passive Acoustic Monitoring in High-Energy Environments: UK Tidal Environments and Other Case Studies.

    Booth, Cormac G

    2016-01-01

    The use of passive acoustic monitoring (PAM) around marine developments is commonplace. A buffer-based PAM system (e.g., C-POD) is a cost-effective method for assessing cetacean acoustic presence. Devices have been deployed by Sea Mammal Research Unit (SMRU) Marine around the United Kingdom, allowing an examination of the performance of C-PODs with respect to background noise, tilt angle, and environmental factors. C-PODs were found to often only monitor for a few seconds of each minute, resulting in significant loss of monitoring time. Issues were likely driven by environmental and deployment factors. The practical limitations of buffer-based PAM systems in high-energy/noisy environments are indicated here. PMID:26610949

  9. Acoustic monitoring of sodium boiling in a liquid metal fast breeder reactor from autoregressive models

    Geraldo, Issa Cherif [Laboratoire d’Automatique, Génie Informatique et Signal (LAGIS UMR CNRS 8219), Université Lille 1, Sciences et technologies, Avenue Paul Langevin, BP 48, 59651 Villeneuve d’Ascq CEDEX (France); Bose, Tanmoy [Indian Institute of Technology Kharagpur, Kharagpur 721302, West Bengal (India); Pekpe, Komi Midzodzi, E-mail: midzodzi.pekpe@univ-lille1.fr [Laboratoire d’Automatique, Génie Informatique et Signal (LAGIS UMR CNRS 8219), Université Lille 1, Sciences et technologies, Avenue Paul Langevin, BP 48, 59651 Villeneuve d’Ascq CEDEX (France); Cassar, Jean-Philippe [Laboratoire d’Automatique, Génie Informatique et Signal (LAGIS UMR CNRS 8219), Université Lille 1, Sciences et technologies, Avenue Paul Langevin, BP 48, 59651 Villeneuve d’Ascq CEDEX (France); Mohanty, A.R. [Indian Institute of Technology Kharagpur, Kharagpur 721302, West Bengal (India); Paumel, Kévin [CEA, DEN, Nuclear Technology Department, F-13108 Saint-Paul-lez-Durance (France)

    2014-10-15

    Highlights: • The work deals with sodium boiling detection in a liquid metal fast breeder reactor. • The authors choose to use acoustic data instead of thermal data. • The method is designed to not to be disturbed by the environment noises. • A real time boiling detection methods are proposed in the paper. - Abstract: This paper deals with acoustic monitoring of sodium boiling in a liquid metal fast breeder reactor (LMFBR) based on auto regressive (AR) models which have low computational complexities. Some authors have used AR models for sodium boiling or sodium–water reaction detection. These works are based on the characterization of the difference between fault free condition and current functioning of the system. However, even in absence of faults, it is possible to observe a change in the AR models due to the change of operating mode of the LMFBR. This sets up the delicate problem of how to distinguish a change in operating mode in absence of faults and a change due to presence of faults. In this paper we propose a new approach for boiling detection based on the estimation of AR models on sliding windows. Afterwards, classification of the models into boiling or non-boiling models is made by comparing their coefficients by two statistical methods, multiple linear regression (LR) and support vectors machines (SVM). The proposed approach takes into account operating mode information in order to avoid false alarms. Experimental data include non-boiling background noise data collected from Phenix power plant (France) and provided by the CEA (Commissariat à l’Energie Atomique et aux énergies alternatives, France) and boiling condition data generated in laboratory. High boiling detection rates as well as low false alarms rates obtained on these experimental data show that the proposed method is efficient for boiling detection. Most importantly, it shows that the boiling phenomenon introduces a disturbance into the AR models that can be clearly detected.

  10. Complex monitoring and alert network for electromagnetic, infrasound, acoustic seismotectonic phenomena

    -Emilian Toader, Victorin; Moldovan, Iren-Adelina; Constantin, Ionescu

    2014-05-01

    The Romanian seismicity recorded in 2013 three important events: the largest seismic "silence", the shortest sequence of two earthquakes greater than 4.8R in less than 14 days after the "Romanian National Institute for Earth Physics" (NIEP) developed a digital network, and a very high crustal activity in Galati area. We analyze the variations of the telluric currents and local magnetic field, variations of the atmospheric electrostatic field, infrasound, temperature, humidity, wind speed and direction, atmospheric pressure, variations in the earth crust with inclinometers and animal behavior. The general effect is the first high seismic energy discontinuity that could be a precursor factor. Since 1977 Romania did not register any important earthquake that would generate a sense of fear among the population. In parallel with the seismic network NIEP developed a magneto-telluric, bioseismic, VLF and acoustic network. A large frequency spectrum is covered for mechanical vibration, magnetic and electric field with ground and air sensors. Special software was designed for acquisition, analysis and real time alert using internet direct connection, web page, email and SMS. Many examples show the sensitivity of telluric current, infrasound, acoustic records (from air-ground), and the effect of tectonic stress on the magnetic field or ground deformation. The next update of the multidisciplinary monitoring network will include measurement of ionization, radon emission, sky color, solar radiation and extension of infrasound and VL/LF equipment. NOAA Space Weather satellites transmit solar activity magnetic field data, X ray flux, electron, and proton flux information useful for complex analysis.

  11. Acoustic monitoring of sodium boiling in a liquid metal fast breeder reactor from autoregressive models

    Highlights: • The work deals with sodium boiling detection in a liquid metal fast breeder reactor. • The authors choose to use acoustic data instead of thermal data. • The method is designed to not to be disturbed by the environment noises. • A real time boiling detection methods are proposed in the paper. - Abstract: This paper deals with acoustic monitoring of sodium boiling in a liquid metal fast breeder reactor (LMFBR) based on auto regressive (AR) models which have low computational complexities. Some authors have used AR models for sodium boiling or sodium–water reaction detection. These works are based on the characterization of the difference between fault free condition and current functioning of the system. However, even in absence of faults, it is possible to observe a change in the AR models due to the change of operating mode of the LMFBR. This sets up the delicate problem of how to distinguish a change in operating mode in absence of faults and a change due to presence of faults. In this paper we propose a new approach for boiling detection based on the estimation of AR models on sliding windows. Afterwards, classification of the models into boiling or non-boiling models is made by comparing their coefficients by two statistical methods, multiple linear regression (LR) and support vectors machines (SVM). The proposed approach takes into account operating mode information in order to avoid false alarms. Experimental data include non-boiling background noise data collected from Phenix power plant (France) and provided by the CEA (Commissariat à l’Energie Atomique et aux énergies alternatives, France) and boiling condition data generated in laboratory. High boiling detection rates as well as low false alarms rates obtained on these experimental data show that the proposed method is efficient for boiling detection. Most importantly, it shows that the boiling phenomenon introduces a disturbance into the AR models that can be clearly detected

  12. Analysis of acoustic emission signals of fatigue crack growth and corrosion processes. Investigation of the possibilities for continuous condition monitoring of transport containers by acoustic emission testing

    Fatigue crack growth and active corrosion processes are the main causes of structural failures of transport products like road tankers, railway tank cars and ships. To prevent those failures, preventive, time-based maintenance is performed. However, preventive inspections are costly and include the risk of not detecting a defect, which could lead to a failure within the next service period. An alternative is the idea of continuous monitoring of the whole structure by means of acoustic emission testing (AT). With AT, defects within the material shall be detected and repaired directly after their appearance. Acoustic emission testing is an online non-destructive testing method. Acoustic emission (AE) arises from changes within the material and is transported by elastic waves through the material. If the AE event generates enough energy, the elastic wave propagates to the boundaries of the component, produces a displacement in the picometre scale and can be detected by a piezoelectric sensor. The sensor produces an electrical signal. From this AE signal, AE features such as the maximum amplitude or the frequency can be extracted. Methods of signal analysis are used to investigate the time and frequency dependency of signal groups. The purpose of the signal analysis is to connect the AE signal with the originating AE source. If predefined damage mechanisms are identified, referencing the damage condition of the structure is possible. Acoustic emission from events of the actual crack propagation process can for example lead to the crack growth rate or the stress intensity factor, both specific values from fracture mechanics. A new development in the domain of acoustic emission testing is the pattern recognition of AE signals. Specific features are extracted from the AE signals to assign them to their damage mechanisms. In this thesis the AE signals from the damage mechanisms corrosion and fatigue crack growth are compared and analysed. The damage mechanisms were

  13. Size Distribution of Sperm Whales Acoustically Identified during Long Term Deep-Sea Monitoring in the Ionian Sea.

    Caruso, Francesco; Sciacca, Virginia; Bellia, Giorgio; De Domenico, Emilio; Larosa, Giuseppina; Papale, Elena; Pellegrino, Carmelo; Pulvirenti, Sara; Riccobene, Giorgio; Simeone, Francesco; Speziale, Fabrizio; Viola, Salvatore; Pavan, Gianni

    2015-01-01

    The sperm whale (Physeter macrocephalus) emits a typical short acoustic signal, defined as a "click", almost continuously while diving. It is produced in different time patterns to acoustically explore the environment and communicate with conspecifics. Each emitted click has a multi-pulse structure, resulting from the production of the sound within the sperm whale's head. A Stable Inter Pulse Interval (Stable IPI) can be identified among the pulses that compose a single click. Applying specific algorithms, the measurement of this interval provides useful information to assess the total length of the animal recorded. In January 2005, a cabled hydrophone array was deployed at a depth of 2,100 m in the Central Mediterranean Sea, 25 km offshore Catania (Ionian Sea). The acoustic antenna, named OνDE (Ocean noise Detection Experiment), was in operation until November 2006. OνDE provided real time acoustic data used to perform Passive Acoustic Monitoring (PAM) of cetacean sound emissions. In this work, an innovative approach was applied to automatically measure the Stable IPI of the clicks, performing a cepstrum analysis to the energy (square amplitude) of the signals. About 2,100 five-minute recordings were processed to study the size distribution of the sperm whales detected during the OνDE long term deep-sea acoustic monitoring. Stable IPIs were measured in the range between 2.1 ms and 6.4 ms. The equations of Gordon (1991) and of Growcott (2011) were used to convert the IPIs into measures of size. The results revealed that the sperm whales recorded were distributed in length from about 7.5 m to 14 m. The size category most represented was from 9 m to 12 m (adult females or juvenile males) and specimens longer than 14 m (old males) seemed to be absent. PMID:26675588

  14. Acoustic habitat and shellfish mapping and monitoring in shallow coastal water - Sidescan sonar experiences in The Netherlands

    van Overmeeren, Ronnie; Craeymeersch, Johan; van Dalfsen, Jan; Fey, Frouke; van Heteren, Sytze; Meesters, Erik

    2009-11-01

    Sidescan sonar has been applied in a number of shallow water environments along the Dutch coast to map and monitor shellfish and seabed habitats. The littoral setting of these surveys may hamper data acquisition flying the towfish in zones of turbulence and waves, but also offers valuable opportunities for understanding, interpreting and validating sidescan sonar images because of the ability to ground-truth during low water periods, enabling easy identification and validation. Acoustical images of some of the mussel banks on the tidal flats of the Wadden Sea, recorded at high tide, show a marked resemblance with optical Google Earth images of the same banks. These sonar images may thus serve as ' acoustic type signatures' for the interpretation of sonar patterns recorded in deeper water where ground-truthing is more difficult and more expensive. Similarly, acoustic type signatures of (Japanese) oyster banks were obtained in the estuaries in the southwest of the Netherlands. Automated acoustic pattern recognition of different habitats and acoustical estimation of faunal cover and density are possible applications of sidescan sonar. Both require that the backscattering observed on the sidescan sonar images is directly caused by the biological component of the seafloor. Filtering offers a simple and effective pre-processing technique to separate the faunal signals from linear trends such as emanating from wave ripples or the central tracks of the towfish. Acoustically estimating the faunal density is approached by in-situ counting peaks in backscattering in unit squares. These counts must be calibrated by ground-truthing. Ground-truthing on littoral mussel banks in the Wadden Sea has been carried out by measuring their cover along lines during low tide. Due to its capacity of yielding full-cover, high resolution images of large surfaces, sidescan sonar proves to be an excellent, cost-effective tool for quantitative time-lapse monitoring of habitats.

  15. A custom acoustic emission monitoring system for harsh environments: application to freezing-induced damage in alpine rock walls

    L. Girard

    2012-11-01

    Full Text Available We present a custom acoustic emission (AE monitoring system designed to perform long-term measurements on high-alpine rock walls. AE monitoring is a common technique for characterizing damage evolution in solid materials. The system is based on a two-channel AE sensor node (AE-node integrated into a wireless sensor network (WSN customized for operation in harsh environments. This wireless architecture offers flexibility in the deployment of AE-nodes at any position of the rock wall that needs to be monitored, within a range of a few hundred meters from a core station connected to the internet. The system achieves near real-time data delivery and allows the user to remotely control the AE detection threshold. In order to protect AE sensors and capture acoustic signals from specific depths of the rock wall, a special casing was developed. The monitoring system is completed by two probes that measure rock temperature and liquid water content, both probes being also integrated into the WSN. We report a first deployment of the monitoring system on a rock wall at Jungfraujoch, 3500 m a.s.l., Switzerland. While this first deployment of the monitoring system aims to support fundamental research on processes that damage rock under cold climate, the system could serve a number of other applications, including rock fall hazard surveillance or structural monitoring of concrete structures.

  16. A custom acoustic emission monitoring system for harsh environments: application to freezing-induced damage in alpine rock-walls

    L. Girard

    2012-06-01

    Full Text Available We present a custom acoustic emission (AE monitoring system designed to perform long-term measurements on high-alpine rock-walls. AE monitoring is a common technique for characterizing damage evolution in solid materials. The system is based on a two-channel AE sensor node (AE-node integrated into a Wireless Sensor Network (WSN customized for operation in harsh environments. This wireless architecture offers flexibility in the deployment of AE-nodes at any position of the rock-wall that needs to be monitored, within a range of a few hundred meters from a core station connected to the internet. The system achieves near real-time data delivery and allows the user to remotely control the AE detection threshold. In order to protect AE sensors and capture acoustic signals from specific depths of the rock-wall, a special casing was developed. The monitoring system is completed by two probes that measure rock temperature and liquid water content, both probes being also integrated into the WSN. We report a first deployment of the monitoring system on a rock-wall at Jungfraujoch, 3500 m a.s.l., Switzerland. While this first deployment of the monitoring system aims to support fundamental research on processes that damage rock under cold climate, the system could serve a number of other applications, including rock-fall hazard surveillance or structural monitoring of concrete structures.

  17. Autonomous hydrophone array for long-term acoustic monitoring in the open ocean

    D'Eu, J.-F.; Brachet, C.; Goslin, J.; Royer, J.-Y.; Ammann, J.

    2009-04-01

    We are developing an array of new autonomous hydrophones, benefiting from a long-lasting collaboration with the Pacific Marine Environmental Laboratory (NOAA and Oregon state University). The hydrophones are deployed on a mooring line anchored to the seafloor by an expendable anchor weight. The length of the line is adjusted so that the sensor (and buoy) lies in the middle of the SOFAR channel at about 1000m depth for mid-latitudes (depending on the speed-of-sound profile). The buoy at depth keeps the line under tension and prevents wave-motion noise from the sensor. The instrument continuously samples and records the acoustic signals at 240Hz for seismic studies, or 480Hz (or more) for marine mammal studies. The SOFAR channel acts as an acoustic wave-guide in the ocean so that acoustic waves can propagate with little attenuation over long distances. Autonomous hydrophones allow the detection and localization of the low-magnitude (Mw>2.5) seismic activity along oceanic ridges and in deformed intraplate areas, which remains generally undetected or poorly localized by land-based seismic networks. An array of hydrophones can monitor a much wider area (more than 1000 km across) than ocean-bottom seismometers, which suffer from the rapid attenuation of seismic waves in the crust and upper mantle. Arrays of autonomous hydrophones thus succeed in detecting and locating 30 to 50 times more earthquakes than those listed in the catalogs from land-based seismograph stations. Data are buffered on flash cards and then regularly stored on hard disks or on solid-state drives (e.g. 20Gb of data per year at 240Hz sampling rate). We use 24-bit sigma-delta converters with programmable gain amplifiers. As timing is a key issue for an accurate localisation of the seismic events, instruments are synchronized with GPS time and have a low-power, highly stable calibrated clock (10-8 drift). All electronics and batteries (Li or alcaline) are placed in titanium pressure cases for long

  18. Soundscapes of the Southern Ocean: Passive Acoustic Monitoring in the Weddell Sea

    Menze, Sebastian; Kindermann, Lars; van Opzeeland, Ilse; Rettig, Stefanie; Bombosch, Annette; Zitterbart, Daniel; Boebel, Olaf

    2013-01-01

    The Southern Ocean provides an important habitat for marine mammals, both residential and migratory, yet long term studies of their habitat usage are hampered by the region’s seasonal inaccessibility. To overcome this problem, two autonomous underwater passive acoustic recorders were deployed in the Weddell Sea in 2008 to collect multiyear passive acoustic data. The recorders were retrieved in 2010 and the acoustic recordings were analyzed in terms of broad- and narrow-band noise. Noise in th...

  19. Wireless Acoustic Signal Monitoring Using MEMS sensor and ATmega on LabVIEW Platform

    Swathy L; Lizy Abraham

    2014-01-01

    Acoustics and vibrations caused on machine structures can result in faulty or collapse of the whole mechanical system. These acoustics produced by machinery are vital indicators of machine health. Acoustic signals analysis can be used as a tool for locating the problem and thus taking necessary actions. MEMS sensors provide high accurate low size and low cost microphones which can be even used in low cost space applications such as sounding rockets, nano-satellites etc. This paper...

  20. Software conception of acoustic emission system for monitoring failure formation and propagation in material of primary circuit component

    The subsystem for monitoring the formation and propagation of material defects of the primary circuit using the method of acoustic emission will be a relatively independent part of the system of in-service diagnostics at the Temelin nuclear power plant. The subsystem will, like the other subsystems, be able to communicate with the central computer. The individual conceptual problems are outlined of the software of the subsystem. The concept proceeds on the one hand from the possibilities of the testing instruments and on the other from the concept of the content and form of output data for the diagnostic system. A detailed list is given of demands on software with regard to the operation of the acoustic emission subsystem in the pressure test mode and in the mode of monitoring the condition of the material of the primary circuit, which differ substantially. (Z.M.)

  1. Acoustic emission monitoring of concrete columns and beams strengthened with fiber reinforced polymer sheets

    Ma, Gao; Li, Hui; Zhou, Wensong; Xian, Guijun

    2012-04-01

    Acoustic emission (AE) technique is an effective method in the nondestructive testing (NDT) field of civil engineering. During the last two decades, Fiber reinforced polymer (FRP) has been widely used in repairing and strengthening concrete structures. The damage state of FRP strengthened concrete structures has become an important issue during the service period of the structure and it is a meaningful work to use AE technique as a nondestructive method to assess its damage state. The present study reports AE monitoring results of axial compression tests carried on basalt fiber reinforced polymer (BFRP) confined concrete columns and three-point-bending tests carried on BFRP reinforced concrete beams. AE parameters analysis was firstly utilized to give preliminary results of the concrete fracture process of these specimens. It was found that cumulative AE events can reflect the fracture development trend of both BFRP confined concrete columns and BFRP strengthened concrete beams and AE events had an abrupt increase at the point of BFRP breakage. Then the fracture process of BFRP confined concrete columns and BFRP strengthened concrete beams was studied through RA value-average frequency analysis. The RA value-average frequency tendencies of BFRP confined concrete were found different from that of BFRP strengthened concrete beams. The variation tendency of concrete crack patterns during the loading process was revealed.

  2. Acoustic emission monitoring of cement-based structures immobilising radioactive waste

    The long term performance of cementitious structures immobilising radioactive waste can be affected by physical and chemical processes within the encapsulating materials such as formation of new phases (e.g., vaterite, brucite), degradation of cement phases (e.g., CSH gel, portlandite), degradation of some waste components (e.g., organics), corrosion of metallic constituents (aluminium, magnesium), gas emission, further hydration etc. The corrosion of metals in the high pH cementitious environment is of especial concern as it can potentially cause wasteform cracking. One of the perspective non-destructive methods used to monitor and assess the mechanical properties of materials and structures is based on an acoustic emission (AE) technique. In this study an AE non-destructive technique was used to evaluate the mechanical performance of cementitious structures with encapsulated metallic waste such as aluminium. AE signals generated as a result of aluminium corrosion in a small-size blast furnace slag (BFS)/ordinary Portland cement (OPC) sample were detected, recorded and analysed. A procedure for AE data analysis including conventional parameter-based AE approach and signal-based analysis was applied and demonstrated to provide information on the aluminium corrosion process and its impact on the mechanical performance of the encapsulating cement matrix. (authors)

  3. Acoustic emission monitoring of the fatigue crack activity in steel bridge members

    Acoustic emission technique was employed for the monitoring of crack activity in steel bridge members. Laboratory experiment was carried out to identify active fatigue crack for the several test condition such as a different specimen type, a varying of cyclic load ratio. The results of this test indicated that the crack propagation characteristics for fatigue cycles did not change significantly with different type of beam. Through all of tests, load ratio of specimen affected significantly to the results such as the crack growth rate and the amount of generating AE signals. From fracture mechanics point of view, the straight curve obtained from theoretical calculation by Paris equation was well correlated to the experimental results. AE location events were not early detected although several AE hits from each sensor were generated in the early of the test. However the features of three parameters, that is, crack growth length, AE location events and cumulative AE events, showed almost same trend in their increase with the number of cycles. Although there were somewhat scattered location in the vicinity of upper flange, which were considered as environmental noises, good locations near the actual crack tip were obtained. Post filtering work was carried out to eliminate these unwanted location, good results were obtained from filtering work using AE parameters.

  4. Condition monitoring of a check valve for nuclear power plants by means of acoustic emission technique

    The primary object of this work is to investigate advanced condition monitoring systems based on acoustic emission (AE) detection that can provide timely detection of check valve degradation and service aging so that maintenance/replacement could be performed prior to loss of safety function. The research is focused on the capability of AE technique to provide diagnostic information useful in determining check valve aging and degradation, check valve failures and undesirable operating modes. The systematic approach to classify the dynamic responses of AE signatures associated with typical failure modes of check valve for nuclear power plants is performed in this study. The characteristics of AE signature responses of internal parts of check valves due to local aging and degradation is analyzed by extracting effective AE parameters. This work also includes the investigation and adaptation of several advanced sensor technologies such as accelerometer and advanced ultrasonic technique. In addition, this work will develop advanced sophisticated signal processing, noise reduction, and pattern recognition techniques and algorithms from check valve degradation. (author)

  5. Frequency Analysis of Acoustic Emission Signal to Monitor Damage Evolution in Masonry Structures

    A crucial aspect in damage evaluation of masonry structures is the analysis of long-term behaviour and for this reason fatigue analysis has a great influence on safety assessment of this structures. Acoustic Emission (AE) are very effective non-destructive techniques applied to identify micro and macro-defects and their temporal evolution in several materials. This technique permits to estimate the velocity of ultrasound waves propagation and the amount of energy released during fracture propagation to obtain information on the criticality of the ongoing process. By means of AE monitoring, an experimental analysis on a set of reinforced and unreinforced masonry walls under variable amplitude and static loading has been carried out. During these tests, the AE signals were recorded. The AE signals were analysed using Fast Fourier Transform (FFT) to examine the frequency distribution of the micro and macro cracking. It possible to evaluate the evolution of the wavelength of the AE signal through the two characteristic peak in the AE spectrum signals and the wave speed of the P or S waves. This wavelength evolution can be represent the microcrak and macrocrack evolution in masonry walls. This procedure permits to estimate the fracture dimension characteristic in several loading condition and for several masonry reinforced condition.

  6. Detection of bond failure in the anchorage zone of reinforced concrete beams via acoustic emission monitoring

    Abouhussien, Ahmed A.; Hassan, Assem A. A.

    2016-07-01

    In this study, acoustic emission (AE) monitoring was utilised to identify the onset of bond failure in reinforced concrete beams. Beam anchorage specimens were designed and tested to fail in bond in the anchorage zone. The specimens included four 250 × 250 × 1500 mm beams with four variable bonded lengths (100, 200, 300, and 400 mm). Meanwhile, an additional 250 × 250 × 2440 mm beam, with 200 mm bonded length, was tested to investigate the influence of sensor location on the identification of bond damage. All beams were tested under four-point loading setup and continuously monitored using three distributed AE sensors. These attached sensors were exploited to record AE signals resulting from both cracking and bond deterioration until failure. The variations in the number of AE hits and cumulative signal strength (CSS) versus test time were evaluated to achieve early detection of crack growth and bar slippage. In addition, AE intensity analysis was performed on signal strength of collected AE signals to develop two additional parameters: historic index (H (t)) and severity (S r). The analysis of these AE parameters enabled an early detection of both first cracks (at almost the mid-span of the beam) and bar slip in either of the anchorage zones at the beams’ end before their visual observation, regardless of sensor location. The results also demonstrated a clear correlation between the damage level in terms of crack development/measured free end bar slip and AE parameters (number of hits, CSS, H(t), and S r).

  7. Fatigue crack growth monitoring of idealized gearbox spline component using acoustic emission

    Zhang, Lu; Ozevin, Didem; Hardman, William; Kessler, Seth; Timmons, Alan

    2016-04-01

    The spline component of gearbox structure is a non-redundant element that requires early detection of flaws for preventing catastrophic failures. The acoustic emission (AE) method is a direct way of detecting active flaws; however, the method suffers from the influence of background noise and location/sensor based pattern recognition method. It is important to identify the source mechanism and adapt it to different test conditions and sensors. In this paper, the fatigue crack growth of a notched and flattened gearbox spline component is monitored using the AE method in a laboratory environment. The test sample has the major details of the spline component on a flattened geometry. The AE data is continuously collected together with strain gauges strategically positions on the structure. The fatigue test characteristics are 4 Hz frequency and 0.1 as the ratio of minimum to maximum loading in tensile regime. It is observed that there are significant amount of continuous emissions released from the notch tip due to the formation of plastic deformation and slow crack growth. The frequency spectra of continuous emissions and burst emissions are compared to understand the difference of sudden crack growth and gradual crack growth. The predicted crack growth rate is compared with the AE data using the cumulative AE events at the notch tip. The source mechanism of sudden crack growth is obtained solving the inverse mathematical problem from output signal to input signal. The spline component of gearbox structure is a non-redundant element that requires early detection of flaws for preventing catastrophic failures. In this paper, the fatigue crack growth of a notched and flattened gearbox spline component is monitored using the AE method The AE data is continuously collected together with strain gauges. There are significant amount of continuous emissions released from the notch tip due to the formation of plastic deformation and slow crack growth. The source mechanism of

  8. Wear monitoring of single point cutting tool using acoustic emission techniques

    P Kulandaivelu; P Senthil Kumar; S Sundaram

    2013-04-01

    This paper examines the flank and crater wear characteristics of coated carbide tool inserts during dry turning of steel workpieces. A brief review of tool wear mechanisms is presented together with new evidence showing that wear of the TiC layer on both flank and rake faces is dominated by discrete plastic deformation, which causes the coating to be worn through to the underlying carbide substrate when machining at high cutting speeds and feed rates. Wear also occurs as a result of abrasion, as well as cracking and attrition, with the latter leading to the wearing through the coating on the rake face under low speed conditions. When moderate speeds and feeds are used, the coating remains intact throughout the duration of testing. Wear mechanism maps linking the observed wear mechanisms to machining conditions are presented for the first time. These maps demonstrate clearly that transitions from one dominant wear mechanism to another may be related to variations in measured tool wear rates. Comparisons of the present wear maps with similar maps for uncoated carbide tools show that TiC coatings dramatically expand the range of machining conditions under which acceptable rates of tool wear might be experienced. However, the extent of improvement brought about by the coatings depends strongly on the cutting conditions, with the greatest benefits being seen at higher cutting speeds and feed rates. Among these methods, tool condition monitoring using Acoustic Techniques (AET) is an emerging one. Hence, the present work was carried out to study the stability, applicability and relative sensitivity of AET in tool condition monitoring in turning.

  9. Chemometrics in Fingerprinting by Means of Thin Layer Chromatography

    Łukasz Komsta

    2012-01-01

    Full Text Available The paper is written as an introductory review, presenting summary of current knowledge about chemometric fingerprinting in the context of TLC, due to a rather small interest in the literature about joining TLC and chemometrics. The paper shortly covers the most important aspects of the chemometric fingerprinting in general, creating the TLC fingerprints, denoising, baseline removal, warping/registering, and chemometric processing itself. References being good candidates as a starting point are given for each topic and processing step.

  10. Development of Generic Methodology for Designing a Structural Health Monitoring Installation Based on the Acoustic Emission Technique

    Gagar, D.; Martinez, M.J.; Foote, P.

    2014-01-01

    The Acoustic Emission (AE) technique can be used to perform damage detection and localisation for structural health monitoring purposes. Implementation in aircraft structures however poses a significant challenge as its performance in terms of damage detection and localisation is not well understood when used with complex structural geometries and variable operational service environments. This paper presents initial developments towards a generic methodology for optimal design of a structura...

  11. Real-time temperature estimation and monitoring of HIFU ablation through a combined modeling and passive acoustic mapping approach

    Jensen, C. R.; Cleveland, R. O.; Coussios, C. C.

    2013-09-01

    Passive acoustic mapping (PAM) has been recently demonstrated as a method of monitoring focused ultrasound therapy by reconstructing the emissions created by inertially cavitating bubbles (Jensen et al 2012 Radiology 262 252-61). The published method sums energy emitted by cavitation from the focal region within the tissue and uses a threshold to determine when sufficient energy has been delivered for ablation. The present work builds on this approach to provide a high-intensity focused ultrasound (HIFU) treatment monitoring software that displays both real-time temperature maps and a prediction of the ablated tissue region. This is achieved by determining heat deposition from two sources: (i) acoustic absorption of the primary HIFU beam which is calculated via a nonlinear model, and (ii) absorption of energy from bubble acoustic emissions which is estimated from measurements. The two sources of heat are used as inputs to the bioheat equation that gives an estimate of the temperature of the tissue as well as estimates of tissue ablation. The method has been applied to ex vivo ox liver samples and the estimated temperature is compared to the measured temperature and shows good agreement, capturing the effect of cavitation-enhanced heating on temperature evolution. In conclusion, it is demonstrated that by using PAM and predictions of heating it is possible to produce an evolving estimate of cell death during exposure in order to guide treatment for monitoring ablative HIFU therapy. Portions presented at the 13th International Symposium on Therapeutic Ultrasound, Heidelberg, Germany (2012).

  12. Real-time temperature estimation and monitoring of HIFU ablation through a combined modeling and passive acoustic mapping approach

    Passive acoustic mapping (PAM) has been recently demonstrated as a method of monitoring focused ultrasound therapy by reconstructing the emissions created by inertially cavitating bubbles (Jensen et al 2012 Radiology 262 252–61). The published method sums energy emitted by cavitation from the focal region within the tissue and uses a threshold to determine when sufficient energy has been delivered for ablation. The present work builds on this approach to provide a high-intensity focused ultrasound (HIFU) treatment monitoring software that displays both real-time temperature maps and a prediction of the ablated tissue region. This is achieved by determining heat deposition from two sources: (i) acoustic absorption of the primary HIFU beam which is calculated via a nonlinear model, and (ii) absorption of energy from bubble acoustic emissions which is estimated from measurements. The two sources of heat are used as inputs to the bioheat equation that gives an estimate of the temperature of the tissue as well as estimates of tissue ablation. The method has been applied to ex vivo ox liver samples and the estimated temperature is compared to the measured temperature and shows good agreement, capturing the effect of cavitation-enhanced heating on temperature evolution. In conclusion, it is demonstrated that by using PAM and predictions of heating it is possible to produce an evolving estimate of cell death during exposure in order to guide treatment for monitoring ablative HIFU therapy. (paper)

  13. Does chemometrics enhance the performance of electroanalysis?

    Ni Yongnian [State Key Laboratory of Food Science and Technology, Nanchang University, Nanchang, Jiangxi 330047 (China); Department of Chemistry, Nanchang University, Nanchang, Jiangxi 330047 (China)], E-mail: ynni@ncu.edu.cn; Kokot, Serge [Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, Brisbane, Queensland 4001 (Australia)

    2008-09-26

    This review explores the question whether chemometrics methods enhance the performance of electroanalytical methods. Electroanalysis has long benefited from the well-established techniques such as potentiometric titrations, polarography and voltammetry, and the more novel ones such as electronic tongues and noses, which have enlarged the scope of applications. The electroanalytical methods have been improved with the application of chemometrics for simultaneous quantitative prediction of analytes or qualitative resolution of complex overlapping responses. Typical methods include partial least squares (PLS), artificial neural networks (ANNs), and multiple curve resolution methods (MCR-ALS, N-PLS and PARAFAC). This review aims to provide the practising analyst with a broad guide to electroanalytical applications supported by chemometrics. In this context, after a general consideration of the use of a number of electroanalytical techniques with the aid of chemometrics methods, several overviews follow with each one focusing on an important field of application such as food, pharmaceuticals, pesticides and the environment. The growth of chemometrics in conjunction with electronic tongue and nose sensors is highlighted, and this is followed by an overview of the use of chemometrics for the resolution of complicated profiles for qualitative identification of analytes, especially with the use of the MCR-ALS methodology. Finally, the performance of electroanalytical methods is compared with that of some spectrophotometric procedures on the basis of figures-of-merit. This showed that electroanalytical methods can perform as well as the spectrophotometric ones. PLS-1 appears to be the method of practical choice if the %relative prediction error of {approx}{+-}10% is acceptable.

  14. Does chemometrics enhance the performance of electroanalysis?

    This review explores the question whether chemometrics methods enhance the performance of electroanalytical methods. Electroanalysis has long benefited from the well-established techniques such as potentiometric titrations, polarography and voltammetry, and the more novel ones such as electronic tongues and noses, which have enlarged the scope of applications. The electroanalytical methods have been improved with the application of chemometrics for simultaneous quantitative prediction of analytes or qualitative resolution of complex overlapping responses. Typical methods include partial least squares (PLS), artificial neural networks (ANNs), and multiple curve resolution methods (MCR-ALS, N-PLS and PARAFAC). This review aims to provide the practising analyst with a broad guide to electroanalytical applications supported by chemometrics. In this context, after a general consideration of the use of a number of electroanalytical techniques with the aid of chemometrics methods, several overviews follow with each one focusing on an important field of application such as food, pharmaceuticals, pesticides and the environment. The growth of chemometrics in conjunction with electronic tongue and nose sensors is highlighted, and this is followed by an overview of the use of chemometrics for the resolution of complicated profiles for qualitative identification of analytes, especially with the use of the MCR-ALS methodology. Finally, the performance of electroanalytical methods is compared with that of some spectrophotometric procedures on the basis of figures-of-merit. This showed that electroanalytical methods can perform as well as the spectrophotometric ones. PLS-1 appears to be the method of practical choice if the %relative prediction error of ∼±10% is acceptable

  15. A study of the characteristics of the acoustic emission signals for condition monitoring of check valves in nuclear power plants

    The objective of this study is to demonstrate that a condition-monitoring system based on acoustic emission (AE) detection can provide timely detection of check valve degradation and service aging so that maintenance or replacement can be preformed prior to the loss of safety function. This research is focused on the investigation and understanding of the capability of the acoustic emission technique to provide diagnostic information on check valve failures. AE testing for a check valve under controlled flow loop conditions was performed to detect and valve degradation such as wear and leakage due to foreign object interference. It is clearly demonstrated that the distinction of different types of failure were successful by systematically analyzing the characteristics of various AE parameters

  16. A study of the characteristics of the acoustic emission signals for condition monitoring of check valves in nuclear power plants

    Lee, Joon-Hyun [School of Mechanical Engineering, Pusan National University, San 30 Jangjeon-dong, Kumjeong-gu, Pusan 609-735 (Korea, Republic of)]. E-mail: johlee@pusan.ac.kr; Lee, Min-Rae [Department of Mechanical Design Engineering, Pusan National University (Korea, Republic of); Kim, Jung-Teak [Man-Machine Interface System Team, Korea Atomic Energy Research Institute Yuseong, Daejeon 305-600 (Korea, Republic of); Luk, Vincent [Sandia National Laboratories, Risk and Reliability Analysis Department, Albuquerque, NM (United States); Jung, Yoong-Ho [School of Mechanical Engineering, Pusan National University, San 30 Jangjeon-dong, Kumjeong-gu, Pusan 609-735 (Korea, Republic of)

    2006-07-15

    The objective of this study is to demonstrate that a condition-monitoring system based on acoustic emission (AE) detection can provide timely detection of check valve degradation and service aging so that maintenance or replacement can be preformed prior to the loss of safety function. This research is focused on the investigation and understanding of the capability of the acoustic emission technique to provide diagnostic information on check valve failures. AE testing for a check valve under controlled flow loop conditions was performed to detect and valve degradation such as wear and leakage due to foreign object interference. It is clearly demonstrated that the distinction of different types of failure were successful by systematically analyzing the characteristics of various AE parameters.

  17. Near-Real-Time Acoustic Monitoring of Beaked Whales and Other Cetaceans Using a Seaglider™

    Klinck, Holger; Mellinger, David K.; Klinck, Karolin; Bogue, Neil M.; Luby, James C.; Jump, William A.; Shilling, Geoffrey B.; Litchendorf, Trina; Wood, Angela S.; Schorr, Gregory S.; Baird, Robin W.

    2012-01-01

    In most areas, estimating the presence and distribution of cryptic marine mammal species, such as beaked whales, is extremely difficult using traditional observational techniques such as ship-based visual line transect surveys. Because acoustic methods permit detection of animals underwater, at night, and in poor weather conditions, passive acoustic observation has been used increasingly often over the last decade to study marine mammal distribution, abundance, and movements, as well as for m...

  18. Wireless Acoustic Signal Monitoring Using MEMS sensor and ATmega on LabVIEW Platform

    Swathy L

    2014-08-01

    Full Text Available Acoustics and vibrations caused on machine structures can result in faulty or collapse of the whole mechanical system. These acoustics produced by machinery are vital indicators of machine health. Acoustic signals analysis can be used as a tool for locating the problem and thus taking necessary actions. MEMS sensors provide high accurate low size and low cost microphones which can be even used in low cost space applications such as sounding rockets, nano-satellites etc. This paper explains the algorithm to extract acoustic signals from ADMP401, which is a high quality, high performance, low power, analog output, bottom-ported omnidirectional MEMS microphone. The sensor output will give the error free data even in noisy conditions. ATmega microcontroller is used to read the data from the sensor and send to LabVIEW software running on the computer which will extract and display the data from the serial port in real time. As rotating structures are those machine parts which may experience high vibration and acoustic noises, the same is implemented in wireless also which helps in extracting acoustic signals from rotating as well as inaccessible parts of the machinery.

  19. Acoustic Monitoring of Beluga Whale Interactions with Cook Inlet Tidal Energy Project

    Worthington, Monty [Project Director - AK

    2014-02-05

    Cook Inlet, Alaska is home to some of the greatest tidal energy resources in the U.S., as well as an endangered population of beluga whales (Delphinapterus leucas). Successfully permitting and operating a tidal power project in Cook Inlet requires a biological assessment of the potential and realized effects of the physical presence and sound footprint of tidal turbines on the distribution, relative abundance, and behavior of Cook Inlet beluga whales. ORPC Alaska, working with the Project Team—LGL Alaska Research Associates, University of Alaska Anchorage, TerraSond, and Greeneridge Science—undertook the following U.S. Department of Energy (DOE) study to characterize beluga whales in Cook Inlet – Acoustic Monitoring of Beluga Whale Interactions with the Cook Inlet Tidal Energy Project (Project). ORPC Alaska, LLC, is a wholly-owned subsidiary of Ocean Renewable Power Company, LLC, (collectively, ORPC). ORPC is a global leader in the development of hydrokinetic power systems and eco-conscious projects that harness the power of ocean and river currents to create clean, predictable renewable energy. ORPC is developing a tidal energy demonstration project in Cook Inlet at East Foreland where ORPC has a Federal Energy Regulatory Commission (FERC) preliminary permit (P-13821). The Project collected baseline data to characterize pre-deployment patterns of marine mammal distribution, relative abundance, and behavior in ORPC’s proposed deployment area at East Foreland. ORPC also completed work near Fire Island where ORPC held a FERC preliminary permit (P-12679) until March 6, 2013. Passive hydroacoustic devices (previously utilized with bowhead whales in the Beaufort Sea) were adapted for study of beluga whales to determine the relative abundance of beluga whale vocalizations within the proposed deployment areas. Hydroacoustic data collected during the Project were used to characterize the ambient acoustic environment of the project site pre-deployment to inform the

  20. A new setup for studying thermal microcracking through acoustic emission monitoring

    Griffiths, Luke; Heap, Michael; Baud, Patrick; Schmittbuhl, Jean

    2016-04-01

    Thermal stressing is common in geothermal environments and has been shown in the laboratory to induce changes in the physical and mechanical properties of rocks. These changes are generally considered to be a consequence of the generation of thermal microcracks and debilitating chemical reactions. Thermal microcracks form as a result of the build-up of internal stresses due to: (1) the thermal expansion mismatch between the different phases present in the material, (2) thermal expansion anisotropy within individual minerals, and (3) thermal gradients. The generation of cracks during thermal stressing has been monitored in previous studies using the output of acoustic emissions (AE), a common proxy for microcrack damage, and through microstructural observations. Here we present a new experimental setup which is optimised to record AE from a rock sample at high temperatures and under a servo-controlled uniaxial stress. The design is such that the AE transducer is embedded in the top of the piston, which acts as a continuous wave guide to the sample. In this way, we simplify the ray path geometry whilst minimising the number of interfaces between the microcrack and the transducer, maximising the quality of the signal. This allows for an in-depth study of waveform attributes such as energy, amplitude, counts and duration. Furthermore, the capability of this device to apply a servo-controlled load on the sample, whilst measuring strain in real time, leads to a spectrum of possible tests combining mechanical and thermal stress. It is also an essential feature to eliminate the build-up of stresses through thermal expansion of the pistons and the sample. We plan a systematic experimental study of the AE of thermally stressed rock during heating and cooling cycles. We present results from pilot tests performed on Darley Dale sandstone and Westerly granite. Understanding the effects of thermal stressing in rock is of particular interest at a geothermal site, where

  1. Passive Acoustic Monitoring of the Environmental Impact of Oil Exploration on Marine Mammals in the Gulf of Mexico.

    Sidorovskaia, Natalia A; Ackleh, Azmy S; Tiemann, Christopher O; Ma, Baoling; Ioup, Juliette W; Ioup, George E

    2016-01-01

    The Gulf of Mexico is a region densely populated by marine mammals that must adapt to living in a highly active industrial environment. This paper presents a new approach to quantifying the anthropogenic impact on the marine mammal population. The results for sperm and beaked whales of a case study of regional population dynamics trends after the Deepwater Horizon oil spill, derived from passive acoustic-monitoring data gathered before and after the spill in the vicinity of the accident, are presented. PMID:26611062

  2. Assessment of the application of acoustic emission technology for monitoring the presence of sand under multiphase flow condition

    The monitoring of multiphase flow is an established process that has spanned several decades. This paper demonstrates the use of acoustic emission (AE) technology to investigate sand transport characteristic in three-phase (air-water-sand) flow in a horizontal pipe where the superficial gas velocity (VSG) had a range of between 0.2 ms−1 to 2.0 ms−1 and superficial liquid velocity (VSL) had a range of between 0.2 ms−1 to 1.0 ms−1. The experimental findings clearly show a correlation exists between AE energy levels, sand concentration, superficial gas velocity (VSG) and superficial liquid velocity (VSL)

  3. Acoustic emission analysis for structural health monitoring of hot metal components; Schallemissionsanalyse zur Zustandsueberwachung von heissen Metallkomponenten

    Schulze, Eberhard [Fraunhofer-Institut fuer Keramische Technologien und Systeme, Dresden (Germany). Institutsteil Materialdiagnostik

    2015-07-01

    For the application of acoustic emission analysis on hot components such as pipes special application techniques are necessary to protect the sensor from the heat. The Fraunhofer IKTS-MD has developed a waveguide solution that meets these requirements. Major challenges in the application of acoustic emission analysis in an industrial environment is the strong ambient noise. This requirement meets the developed acoustic measurement system at the Fraunhofer Institute by a high measurement dynamics, storage and assessment of the complete waveforms and by special algorithms. The attractiveness of the method lies in the relatively low number of sensors with which the integrity of large plant areas (e.g. several meters under high alternating load standing superheated steam pipe) can be permanently monitored. [German] Fuer die Anwendung der Schallemissionsanalyse an heissen Komponenten wie Rohrleitungen sind besondere Applikationstechniken notwendig, um den Sensor vor der Hitze zu schuetzen. Das Fraunhofer IKTS-MD hat dafuer eine Wellenleiterloesung entwickelt, die diese Anforderungen erfuellt. Wesentliche Herausforderung bei der Anwendung der Schallemissionsanalyse in industrieller Umgebung ist das starke Umgebungsrauschen. Dieser Anforderung begegnet das am Fraunhofer-Institut entwickelte akustische Messsystem durch eine hohe Messwertdynamik, Speicherung und Bewertung der vollstaendigen Wellenformen sowie durch spezielle Auswertealgorithmen. Die Attraktivitaet des Verfahrens liegt in der vergleichsweise geringen Anzahl von Sensoren, mit denen die Integritaet grosser Anlagenbereiche (z.B. mehrere Meter unter hoher Wechsellast stehender Heissdampfleitung) dauerhaft ueberwacht werden kann.

  4. A Permanent Automated Real-Time Passive Acoustic Monitoring System for Bottlenose Dolphin Conservation in the Mediterranean Sea

    Brunoldi, Marco; Bozzini, Giorgio; Casale, Alessandra; Corvisiero, Pietro; Grosso, Daniele; Magnoli, Nicodemo; Alessi, Jessica; Bianchi, Carlo Nike; Mandich, Alberta; Morri, Carla; Povero, Paolo; Wurtz, Maurizio; Melchiorre, Christian; Viano, Gianni; Cappanera, Valentina; Fanciulli, Giorgio; Bei, Massimiliano; Stasi, Nicola; Taiuti, Mauro

    2016-01-01

    Within the framework of the EU Life+ project named LIFE09 NAT/IT/000190 ARION, a permanent automated real-time passive acoustic monitoring system for the improvement of the conservation status of the transient and resident population of bottlenose dolphin (Tursiops truncatus) has been implemented and installed in the Portofino Marine Protected Area (MPA), Ligurian Sea. The system is able to detect the simultaneous presence of dolphins and boats in the area and to give their position in real time. This information is used to prevent collisions by diffusing warning messages to all the categories involved (tourists, professional fishermen and so on). The system consists of two gps-synchronized acoustic units, based on a particular type of marine buoy (elastic beacon), deployed about 1 km off the Portofino headland. Each one is equipped with a four-hydrophone array and an onboard acquisition system which can record the typical social communication whistles emitted by the dolphins and the sound emitted by boat engines. Signals are pre-filtered, digitized and then broadcast to the ground station via wi-fi. The raw data are elaborated to get the direction of the acoustic target to each unit, and hence the position of dolphins and boats in real time by triangulation. PMID:26789265

  5. A Permanent Automated Real-Time Passive Acoustic Monitoring System for Bottlenose Dolphin Conservation in the Mediterranean Sea.

    Brunoldi, Marco; Bozzini, Giorgio; Casale, Alessandra; Corvisiero, Pietro; Grosso, Daniele; Magnoli, Nicodemo; Alessi, Jessica; Bianchi, Carlo Nike; Mandich, Alberta; Morri, Carla; Povero, Paolo; Wurtz, Maurizio; Melchiorre, Christian; Viano, Gianni; Cappanera, Valentina; Fanciulli, Giorgio; Bei, Massimiliano; Stasi, Nicola; Taiuti, Mauro

    2016-01-01

    Within the framework of the EU Life+ project named LIFE09 NAT/IT/000190 ARION, a permanent automated real-time passive acoustic monitoring system for the improvement of the conservation status of the transient and resident population of bottlenose dolphin (Tursiops truncatus) has been implemented and installed in the Portofino Marine Protected Area (MPA), Ligurian Sea. The system is able to detect the simultaneous presence of dolphins and boats in the area and to give their position in real time. This information is used to prevent collisions by diffusing warning messages to all the categories involved (tourists, professional fishermen and so on). The system consists of two gps-synchronized acoustic units, based on a particular type of marine buoy (elastic beacon), deployed about 1 km off the Portofino headland. Each one is equipped with a four-hydrophone array and an onboard acquisition system which can record the typical social communication whistles emitted by the dolphins and the sound emitted by boat engines. Signals are pre-filtered, digitized and then broadcast to the ground station via wi-fi. The raw data are elaborated to get the direction of the acoustic target to each unit, and hence the position of dolphins and boats in real time by triangulation. PMID:26789265

  6. Artificial Neural Network Model for Monitoring Oil Film Regime in Spur Gear Based on Acoustic Emission Data

    Yasir Hassan Ali

    2015-01-01

    Full Text Available The thickness of an oil film lubricant can contribute to less gear tooth wear and surface failure. The purpose of this research is to use artificial neural network (ANN computational modelling to correlate spur gear data from acoustic emissions, lubricant temperature, and specific film thickness (λ. The approach is using an algorithm to monitor the oil film thickness and to detect which lubrication regime the gearbox is running either hydrodynamic, elastohydrodynamic, or boundary. This monitoring can aid identification of fault development. Feed-forward and recurrent Elman neural network algorithms were used to develop ANN models, which are subjected to training, testing, and validation process. The Levenberg-Marquardt back-propagation algorithm was applied to reduce errors. Log-sigmoid and Purelin were identified as suitable transfer functions for hidden and output nodes. The methods used in this paper shows accurate predictions from ANN and the feed-forward network performance is superior to the Elman neural network.

  7. Passive acoustic monitoring to detect spawning in large-bodied catostomids

    Straight, Carrie A.; Freeman, Byron J.; Freeman, Mary C.

    2014-01-01

    Documenting timing, locations, and intensity of spawning can provide valuable information for conservation and management of imperiled fishes. However, deep, turbid or turbulent water, or occurrence of spawning at night, can severely limit direct observations. We have developed and tested the use of passive acoustics to detect distinctive acoustic signatures associated with spawning events of two large-bodied catostomid species (River Redhorse Moxostoma carinatum and Robust Redhorse Moxostoma robustum) in river systems in north Georgia. We deployed a hydrophone with a recording unit at four different locations on four different dates when we could both record and observe spawning activity. Recordings captured 494 spawning events that we acoustically characterized using dominant frequency, 95% frequency, relative power, and duration. We similarly characterized 46 randomly selected ambient river noises. Dominant frequency did not differ between redhorse species and ranged from 172.3 to 14,987.1 Hz. Duration of spawning events ranged from 0.65 to 11.07 s, River Redhorse having longer durations than Robust Redhorse. Observed spawning events had significantly higher dominant and 95% frequencies than ambient river noises. We additionally tested software designed to automate acoustic detection. The automated detection configurations correctly identified 80–82% of known spawning events, and falsely indentified spawns 6–7% of the time when none occurred. These rates were combined over all recordings; rates were more variable among individual recordings. Longer spawning events were more likely to be detected. Combined with sufficient visual observations to ascertain species identities and to estimate detection error rates, passive acoustic recording provides a useful tool to study spawning frequency of large-bodied fishes that displace gravel during egg deposition, including several species of imperiled catostomids.

  8. Continuous wavelet transform analysis and modal location analysis acoustic emission source location for nuclear piping crack growth monitoring

    Full-text: Source location is an important feature of acoustic emission (AE) damage monitoring in nuclear piping. The ability to accurately locate sources can assist in source characterisation and early warning of failure. This paper describe the development of a novelAE source location technique termed Wavelet Transform analysis and Modal Location (WTML) based on Lamb wave theory and time-frequency analysis that can be used for global monitoring of plate like steel structures. Source location was performed on a steel pipe of 1500 mm long and 220 mm outer diameter with nominal thickness of 5 mm under a planar location test setup using H-N sources. The accuracy of the new technique was compared with other AE source location methods such as the time of arrival (TOA) technique and DeltaTlocation. The results of the study show that the WTML method produces more accurate location results compared with TOA and triple point filtering location methods. The accuracy of the WTML approach is comparable with the deltaT location method but requires no initial acoustic calibration of the structure. (author)

  9. Non-contact acoustic emission measurement for condition monitoring of bearings in rotating machines using laser interferometry

    For advanced maintenance and safety in nuclear power plants, it is necessary to combine various technologies that are used to monitor the status of different equipment. Non-contact measurement methods offer technical advantages over contact measurement methods, such as the ability to perform spot measurements, adapt to high-temperature environments, and inspect dynamic parts. The acoustic emission (AE) method can detect earlier abnormal signs in bearings than vibration analysis, which is commonly used in power plants. The AE method is also able to detect various other events such as wear and leakage of materials. However, currently, non-contact AE measurement is not used for condition monitoring in power plants. To verify the feasibility of a non-contact AE measurement method using laser interferometry for condition monitoring technology, laboratory tests were conducted using a rotating machine fitted with bearings that had deliberately been made defective. The AE signals propagating from these defects were measured using a Michelson interferometer on the rotating polished shaft, and a piezoelectric sensor positioned on the bearing housing. This paper demonstrates that the non-contact AE method can detect various stages of deterioration in bearings, and therefore, the method can be considered as a useful future tool for condition monitoring of bearings in rotating machines. (author)

  10. Detection of explosive events by monitoring acoustically-induced geomagnetic perturbations

    Lewis, J P; Rock, D R; Shaeffer, D L; Warshaw, S I

    1999-10-07

    The Black Thunder Coal Mine (BTCM) near Gillette, Wyoming was used as a test bed to determine the feasibility of detecting explosion-induced geomagnetic disturbances with ground-based induction magnetometers. Two magnetic observatories were fielded at distances of 50 km and 64 km geomagnetically north from the northernmost edge of BTCM. Each observatory consisted of three separate but mutually orthogonal magnetometers, Global Positioning System (GPS) timing, battery and solar power, a data acquisition and storage system, and a three-axis seismometer. Explosions with yields of 1 to 3 kT of TNT equivalent occur approximately every three weeks at BTCM. We hypothesize that explosion-induced acoustic waves propagate upward and interact collisionally with the ionosphere to produce ionospheric electron density (and concomitant current density) perturbations which act as sources for geomagnetic disturbances. These disturbances propagate through an ionospheric Alfven waveguide that we postulate to be leaky (due to the imperfectly conducting lower ionospheric boundary). Consequently, wave energy may be observed on the ground. We observed transient pulses, known as Q-bursts, with pulse widths about 0.5 s and with spectral energy dominated by the Schumann resonances. These resonances appear to be excited in the earth-ionosphere cavity by Alfven solitons that may have been generated by the explosion-induced acoustic waves reaching the ionospheric E and F regions and that subsequently propagate down through the ionosphere to the atmosphere. In addition, we observe late time (> 800 s) ultra low frequency (ULF) geomagnetic perturbations that appear to originate in the upper F region ({approximately}300 km) and appear to be caused by the explosion-induced acoustic wave interacting with that part of the ionosphere. We suggest that explosion-induced Q-bursts may be discriminated from naturally occurring Q-bursts by association of the former with the late time explosion-induced ULF

  11. Chemometrics and modernization of traditional Chinese medicine

    2008-01-01

    Development of chromatographic fingerprinting and its related chemometric methods in the research of quality control of traditional Chinese medicines(TCMs) are discussed. The quality control methods for guarantying the authentication and stability of products and semi-products of TCMs are firstly assessed. The technique based on chromatographic fingerprinting is essentially a kind of high-through put and integral tools to explore the complexity of herbal medicines. In order to further control the comprehensive quality of TCMs,confirmation and identification of their important chemical components are necessary. Some new strategies are proposed to trace the chemical changes of chromatographic fingerprints both in product processing and/or after their administration by modern chromatographic techniques and chemometrics. Combined with systems biology and bioinformatics,it seems possible for one to reveal the working mechanism of TCMs and to further control their intrinsic quality comprehensively.

  12. Acoustic emission for on-line reactor monitoring: results of intermediate vessel test monitoring and reactor hot functional testing

    This article discusses a program designed to develop the use of acoustic emission (AE) methods for continuous surveillance to detect and evaluate flaw growth in reactor pressure boundaries. Technology developed in the laboratory for identifying AE from crack growth and for using AE information to estimate flaw severity is now being evaluated on an intermediate vessel test and on a reactor facility. A vessel, designated ZB-1, has been tested under fatigue loadings with simulated reactor conditions at Mannheim, West Germany, in collaboration with the German Materialpruefungsanstalt (MPA), Stuttgart. Fatigue cracking from machined flaws and in a fabrication weld were both detected clearly by AE. AE data were measured on a US nuclear reactor (Watts Bar, Unit 1) during hot functional preservice testing. This demonstrated that coolant flow noise is a manageable problem and that AE can be detected under operational coolant flow and temperature conditions. (author)

  13. Contribution of acoustic emission to monitor the effect of phosphate based inhibitor on the corrosion behavior of steel reinforcement

    Nahali, Haifa [Laboratoire MATEIS CNRS UMR5511 (Equipe CorrIS), INSA-Lyon, Villeurbanne (France); Univ. de Tunis El Manar, Belvedere (Tunisia). Unite de Recherche ' ' Mecanique-Energetique' ' ; Dhouibi, Leila [Univ. de Tunis El Manar, Belvedere (Tunisia). Unite de Recherche ' ' Mecanique-Energetique' ' ; Idrissi, Hassane [Laboratoire MATEIS CNRS UMR5511 (Equipe CorrIS), INSA-Lyon, Villeurbanne (France)

    2014-11-01

    One of the most important causes of reinforced concrete structures deterioration is the corrosion of the reinforcement steel. This corrosion depends on the presence of aggressive agents such as chlorides in the surrounding medium. Numerous protection techniques have been employed to mitigate this corrosion. Among them, the use of corrosion inhibitors has been considered as one of the most effective solutions. In the present work, the influence of phosphate based inhibitor on the corrosion of reinforcing steels embedded in mortar, and immersed in sodium chloride solution, was investigated by acoustic emission technique. The monitoring of specimens shows that the phosphate based inhibitor addition in the mortar increase the threshold of chloride concentrations, causing the breakdown of steel passivation layer. Thus, the acoustic signatures of concrete fracture and of structure degradation during the corrosion of these specimens have been highlighted. Similarly, the mechanism of phosphate action in terms of preventing steel from corrosion in mortar specimens was analysed by characterization methods (SEM, XRD) of the steel-mortar interface.

  14. In situ monitoring the pulse CO2 laser interaction with 316-L stainless steel using acoustical signals and plasma analysis

    In most laser material processing, material removal by different mechanisms is involved. Here, application of acoustic signals with thermoelastic (below threshold) and breakdown origin (above threshold) together with plasma plume analysis as a simple monitoring system of interaction process is suggested. In this research the interaction of pulse CO2 laser with 200 ns duration and maximum energy of 1.3 J operating at 1 Hz with austenitic stainless steel (316-L) is reported. The results showed that the non-linear point of the curve can serve as a useful indicator of melting fluence threshold (in this case ∼830 J cm-2) with corresponding temperature calculated using plasma plume analysis. Higher acoustic amplitudes and larger plasma plume volume indicates more intense interaction. Also, analysis showed that a phase explosion process with material removal (ejecta) in the form of non-adiabatic (i.e., dt >> α-1) is at play after laser pulse is ended. Also, SEM photographs show different surface quality medication at different laser intensities, which indicates the importance of recoil momentum pressure and possibly electrons and ions densities in heat transfer. Finally, electrochemical test indicate an improved corrosion resistance for laser treated samples compared to untreated ones.

  15. In situ monitoring the pulse CO 2 laser interaction with 316-L stainless steel using acoustical signals and plasma analysis

    Khosroshahi, M. E.; pour, F. Anoosheh; Hadavi, M.; Mahmoodi, M.

    2010-10-01

    In most laser material processing, material removal by different mechanisms is involved. Here, application of acoustic signals with thermoelastic (below threshold) and breakdown origin (above threshold) together with plasma plume analysis as a simple monitoring system of interaction process is suggested. In this research the interaction of pulse CO 2 laser with 200 ns duration and maximum energy of 1.3 J operating at 1 Hz with austenitic stainless steel (316-L) is reported. The results showed that the non-linear point of the curve can serve as a useful indicator of melting fluence threshold (in this case ≈830 J cm -2) with corresponding temperature calculated using plasma plume analysis. Higher acoustic amplitudes and larger plasma plume volume indicates more intense interaction. Also, analysis showed that a phase explosion process with material removal (ejecta) in the form of non-adiabatic (i.e., dt ≫ α-1) is at play after laser pulse is ended. Also, SEM photographs show different surface quality medication at different laser intensities, which indicates the importance of recoil momentum pressure and possibly electrons and ions densities in heat transfer. Finally, electrochemical test indicate an improved corrosion resistance for laser treated samples compared to untreated ones.

  16. Contribution of acoustic emission to monitor the effect of phosphate based inhibitor on the corrosion behavior of steel reinforcement

    One of the most important causes of reinforced concrete structures deterioration is the corrosion of the reinforcement steel. This corrosion depends on the presence of aggressive agents such as chlorides in the surrounding medium. Numerous protection techniques have been employed to mitigate this corrosion. Among them, the use of corrosion inhibitors has been considered as one of the most effective solutions. In the present work, the influence of phosphate based inhibitor on the corrosion of reinforcing steels embedded in mortar, and immersed in sodium chloride solution, was investigated by acoustic emission technique. The monitoring of specimens shows that the phosphate based inhibitor addition in the mortar increase the threshold of chloride concentrations, causing the breakdown of steel passivation layer. Thus, the acoustic signatures of concrete fracture and of structure degradation during the corrosion of these specimens have been highlighted. Similarly, the mechanism of phosphate action in terms of preventing steel from corrosion in mortar specimens was analysed by characterization methods (SEM, XRD) of the steel-mortar interface.

  17. Assessment of the application of acoustic emission technology for monitoring the presence of sand under multiphase flow condition

    El-Alej, M., E-mail: m.elalej@cranfield.ac.uk; Mba, D., E-mail: m.elalej@cranfield.ac.uk; Yeung, H., E-mail: m.elalej@cranfield.ac.uk [School of Engineering, Cranfield University, Cranfield, Bedfordshire, MK43 OAL (United Kingdom)

    2014-04-11

    The monitoring of multiphase flow is an established process that has spanned several decades. This paper demonstrates the use of acoustic emission (AE) technology to investigate sand transport characteristic in three-phase (air-water-sand) flow in a horizontal pipe where the superficial gas velocity (VSG) had a range of between 0.2 ms{sup −1} to 2.0 ms{sup −1} and superficial liquid velocity (VSL) had a range of between 0.2 ms{sup −1} to 1.0 ms{sup −1}. The experimental findings clearly show a correlation exists between AE energy levels, sand concentration, superficial gas velocity (VSG) and superficial liquid velocity (VSL)

  18. Acoustic cavitation-based monitoring of the reversibility and permeability of ultrasound-induced blood-brain barrier opening

    Sun, Tao; Samiotaki, Gesthimani; Wang, Shutao; Acosta, Camilo; Chen, Cherry C.; Konofagou, Elisa E.

    2015-12-01

    Cavitation events seeded by microbubbles have been previously reported to be associated with MR- or fluorescent-contrast enhancement after focused ultrasound (FUS)-induced blood-brain barrier (BBB) opening. However, it is still unknown whether bubble activity can be correlated with the reversibility (the duration of opening and the likelihood of safe reinstatement) and the permeability of opened BBB, which is critical for the clinical translation of using passive cavitation detection to monitor, predict and control the opening. In this study, the dependence of acoustic cavitation on the BBB opening duration, permeability coefficient and histological damage occurrence were thus investigated. Transcranial pulsed FUS at 1.5 MHz in the presence of systemically circulating microbubbles was applied in the mouse hippocampi (n  =  60). The stable and inertial cavitation activities were monitored during sonication. Contrast-enhanced MRI was performed immediately after sonication and every 24 h up to 6 d thereafter, to assess BBB opening, brain tissue permeability and potential edema. Histological evaluations were used to assess the occurrence of neurovascular damages. It was found that stable cavitation was well correlated with: (1) the duration of the BBB opening (r2  =  0.77) (2) the permeability of the opened BBB (r2  =  0.82) (3) the likelihood of safe opening (P  brain and assessing the pharmacokinetics of the compounds delivered can also be achieved by monitoring and controlling the stable cavitation emissions.

  19. Comparison of optical and acoustical monitoring during a crack propagation, implication for slow earthquake dynamics

    Lengliné, Olivier; Schmittbuhl, Jean; Elkhoury, Jean; Toussaint, Renaud; Daniel, Guillaume; Maloy, Knut Jurgen

    2010-05-01

    Observations of aseismic transients in several tectonic context suggest that they might be linked to seismicity. However a clear observation and description of these phenomena and their interaction is lacking. This owes to the difficulty of characterizing with a sufficient resolution processes taking place at depth. Here we aim to study these interactions between aseismic and seismic slip taking advantage of an unique experimental setup. We conducted a series of mode I crack propagation experiments on transparent materials (PMMA). The crack advance is trapped in a weakness plane which is the interface between two previously sandblasted and annealed plexiglass plates. A fast video camera taking up to 500 frames per second ensures the tracking of the front rupture. The acoustic system is composed of a maximum of 44 channels continuously recording at 5 MHz for a few tens of seconds. Piezo-electric sensors are composed of a 32 elements linear array and individual sensors surrounding the crack front. An automatic detection and localization procedure allows us to obtain the position of acoustic emission (A.E.) that occurred during the crack advance. Crack front image processing reveals an intermittent opening which might be linked to the time and space clustering of the AE. An analogy between the mode I (opening) and the mode III (antiplane slip) allows us to interpret our results in term of slip on faults. Our experiment thus helps to reveal the interplay between seismic and aseismic slip on faults.

  20. Neural Network Analysis of Acoustic Emission Signals for Drill Wear Monitoring

    The objective of the proposed study is to produce a tool-condition monitoring (TCM) strategy that will lead to a more efficient and economical drilling tool usage. Drill-wear monitoring is an important attribute in the automatic cutting processes as it can help preventing damages of the tools and workpieces and optimizing the tool usage. This study presents the architectures of a multi-layer feed-forward neural network with back-propagation training algorithm for the monitoring of drill wear. The input features to the neural networks were extracted from the AE signals using the wavelet transform analysis. Training and testing were performed under a moderate range of cutting conditions in the dry drilling of steel plates. The results indicated that the extracted input features from AE signals to the supervised neural networks were effective for drill wear monitoring and the output of the neural networks could be utilized for the tool life management planning.

  1. Failure monitoring of E-glass/vinylester composites using fiber grating acoustic sensor

    Azmi, A. I.; Raju; Peng, G. D.

    2013-06-01

    This paper reports an application of an optical fiber sensor in a continuous and in situ failure testing of an E-glass/vinylester top hat stiffener (THS). The sensor head was constructed from a compact phase-shifted fiber Bragg grating (PS-FBG). The narrow transmission channel of the PS-FBG is highly sensitive to small perturbation, hence suitable to be used in acoustic emission (AE) assessment technique. The progressive failure of THS was tested under transverse loading to experimentally simulate the actual loading in practice. Our experimental tests have demonstrated, in good agreement with the commercial piezoelectric sensors, that the important failures information of the THS was successfully recorded by the simple intensity-type PS-FBG sensor.

  2. Acoustic-seismic monitoring of an underground final repository - a measurement project

    When spent fuel from nuclear power plants is deposited without reprocessing, the produced plutonium - which could be used for nuclear weapons - is still contained in it. Thus, safeguards of the International Atomic Energy Agency (IAEA) are needed for final repositories to detect potential access, during and after the emplacement phase. To find out if acoustic and seismic methods can be used to detect undeclared activities in an underground repository in salt, the German Support Programme for the IAEA has tasked us to do measurements in the exploratory mine in Gorleben, a potential site. To gain the source properties we record sound and vibration at several positions underground and at the surface while various mining activities are carried out singly and in parallel. The evaluations will investigate source detection, localisation and recognition.

  3. Integrated acoustic phase separator and multiphase fluid composition monitoring apparatus and method

    Sinha, Dipen N.

    2016-01-12

    An apparatus and method for down hole gas separation from the multiphase fluid flowing in a wellbore or a pipe, for determining the quantities of the individual components of the liquid and the flow rate of the liquid, and for remixing the component parts of the fluid after which the gas volume may be measured, without affecting the flow stream, are described. Acoustic radiation force is employed to separate gas from the liquid, thereby permitting measurements to be separately made for these two components; the liquid (oil/water) composition is determined from ultrasonic resonances; and the gas volume is determined from capacitance measurements. Since the fluid flows around and through the component parts of the apparatus, there is little pressure difference, and no protection is required from high pressure differentials.

  4. Project of a Near-Real-Time Sismo-acoustic Submarine Station for offshore monitoring (NRTSSS)

    D'Anna, Giuseppe; Istituto Nazionale di Geofisica e Vulcanologia, Sezione CNT, Roma, Italia; Calore, Daniele; Envirtech S.p.A.; Mangano, Giorgio; Istituto Nazionale di Geofisica e Vulcanologia, Sezione CNT, Roma, Italia; D'Alessandro, Antonino; Istituto Nazionale di Geofisica e Vulcanologia, Sezione CNT, Roma, Italia; Favali, Paolo; Istituto Nazionale di Geofisica e Vulcanologia, Sezione Roma2, Roma, Italia

    2011-01-01

    The INGV seismic network ensures reliable and continuous monitoring of the Italian territory. However, the peculiarity of the Italian peninsula, characterised by an intense offshore geodynamic and seismic activity, requires the extension of the seismic monitoring to the sea. The aim of this project is: - to identify bottleneck is related to the construction, installation and use of underwater seismic station; - to define the most appropriate and low-cost architecture to guarantee the...

  5. Efficacy assessment of local doxycycline treatment in periodontal patients using multivariate chemometric approach.

    Bogdanovska, Liljana; Poceva Panovska, Ana; Nakov, Natalija; Zafirova, Marija; Popovska, Mirjana; Dimitrovska, Aneta; Petkovska, Rumenka

    2016-08-25

    The aim of our study was application of chemometric algorithms for multivariate data analysis in efficacy assessment of the local periodontal treatment with doxycycline (DOX). Treatment efficacy was evaluated by monitoring inflammatory biomarkers in gingival crevicular fluid (GCF) samples and clinical indices before and after the local treatment as well as by determination of DOX concentration in GCF after the local treatment. The experimental values from these determinations were submitted to several chemometric algorithms: principal component analysis (PCA), partial least square discriminant analysis (PLS-DA) and orthogonal projection to latent structures-discriminant analysis (OPLS-DA). The data structure and the mutual relations of the selected variables were thoroughly investigated by PCA. The PLS-DA model identified variables responsible for discrimination of classes of data, before and after DOX treatment. The OPLS-DA model compared the efficacy of the two commonly used medications in periodontal treatment, chlorhexidine (CHX) and DOX, at the same time providing insight in their mechanism of action. The obtained results indicate that application of multivariate chemometric algorithms can be used as a valuable approach for assessment of treatment efficacy. PMID:27283484

  6. Chemometric applications to assess quality and critical parameters of virgin and extra-virgin olive oil. A review.

    Gómez-Caravaca, Ana M; Maggio, Rubén M; Cerretani, Lorenzo

    2016-03-24

    Today virgin and extra-virgin olive oil (VOO and EVOO) are food with a large number of analytical tests planned to ensure its quality and genuineness. Almost all official methods demand high use of reagents and manpower. Because of that, analytical development in this area is continuously evolving. Therefore, this review focuses on analytical methods for EVOO/VOO which use fast and smart approaches based on chemometric techniques in order to reduce time of analysis, reagent consumption, high cost equipment and manpower. Experimental approaches of chemometrics coupled with fast analytical techniques such as UV-Vis spectroscopy, fluorescence, vibrational spectroscopies (NIR, MIR and Raman fluorescence), NMR spectroscopy, and other more complex techniques like chromatography, calorimetry and electrochemical techniques applied to EVOO/VOO production and analysis have been discussed throughout this work. The advantages and drawbacks of this association have also been highlighted. Chemometrics has been evidenced as a powerful tool for the oil industry. In fact, it has been shown how chemometrics can be implemented all along the different steps of EVOO/VOO production: raw material input control, monitoring during process and quality control of final product. PMID:26944986

  7. Acoustic Emission Monitoring of Compression-after-Impact Test of Nano-Particles-Coated CFRP Damaged by Simulated Lightning Strikes

    Nanoparticles-coated and impact-damaged carbon-fiber reinforced plastics(CFRP) laminates were tested under compression-after-impact(CAI) mode and the propagation of damage due to compressive loading has been monitored by acoustic emission(AE). The impact damage was induced not by mechanical loading but by a simulated lightning strike. CFRP laminates were made of carbon prepregs prepared by coating of conductive nano-particles directly on the fibers and the coupons were subjected to simulated lightning strikes with a high voltage/current impulse of 10∼40 kA within a few microseconds. The effects of nano-particles coating and the degree of damage induced by the simulated lightning strikes on the AE activities were examined, and the relationship between the compressive residual strength and AE behavior has been evaluated in terms of AE event counts and the onset of AE activity with the compressive loading. The degree of impact damage was also measured in terns of damage area by using ultrasonic C-scan images. From the results assessed during the CAI tests of damaged CFRP showed that AE monitoring appeared to be very useful to differentiate the degree of damage hence the mechanical integrity of composite structures damaged by lightning strikes

  8. On-line acoustic monitoring of EDF nuclear plants in operation and loose-part diagnosis

    In order to detect incipient failures in nuclear power plant components, EDF has now put into operation more than 50 loose-part monitoring systems, on its 900 MW and 1 300 MW units. This paper first reviews the experience gained on the 900 MW reactors in recent years. It then focuses on the 1 300 MW loose part monitoring system (IDEAL) and to the tools developed for the diagnosis off site within a specific Expertise Laboratory at the Research and Development Division. New studies have been undertaken within the Monitoring and Aid to Diagnosis Station (PSAD) in order to extend the capabilities of loose part diagnosis on site. The new tools here presented integrate the recent progress in acquisition technology (SMART system) and in artificial intelligence (MIGRE expert system)

  9. Monitoring the habitat use of common Bottlenose Dolphins (Tursiops truncatus using passive acoustics in a Mediterranean marine protected area

    G. LA MANNA

    2014-07-01

    Full Text Available The Mediterranean Tursiops truncatus subpopulation has been classified as Vulnerable on the IUCN Red List because of its decline. This species in coastal areas is exposed to a wide variety of threats: directed kills, bycatch, reduced prey availability caused by environmental degradation and overfishing, habitat degradation including disturbances from boat traffic and noise. Despite the increase in boat traffic in the Mediterranean Sea, the effect on T. truncatus’ habitat use has been studied in little detail and few data have been published. This study represents the first attempt to characterise spatial and temporal habitat use by T. truncatus and its relation to boat traffic in the Isole Pelagie Marine Protected Area (Italy on the basis of an originally developed passive acoustic monitoring system (PAM. The devices were deployed in 2 areas in the southern waters of Lampedusa, during 2 separate years (2006 and 2009, each time for 3 months (from July to September and in 6 time slots (3 diurnal and 3 nocturnal. Acoustic analysis showed that T. truncatus used the Southern coastal area of Lampedusa independently of the year, primarily during the early summer, a period coinciding with the peak of calving season. Dolphin occurrences appeared independent of boat traffic, with the exception of the smallest temporal scale (time slots: dolphin occurrences were more prevalent during the night when the level of boat traffic was lower. This study provides evidence on T. truncatus habitat use in the Mediterranean Sea and reveals that boat traffic could be one of the factors influencing it, thus stressing the need for further detailed investigation regarding this topic.

  10. Functional Data Analysis Applied in Chemometrics

    Muller, Martha

    nutritional status and metabolic phenotype. We want to understand how metabolomic spectra can be analysed using functional data analysis to detect the in uence of dierent factors on specic metabolites. These factors can include, for example, gender, diet culture or dietary intervention. In Paper I we apply...... novelty of heart plots for spectral data. The important aspect of registration, also called warping or alignment, emerges from both the chemometric and statistical perspectives. In Paper III we apply functional registration in the context of biomechanics, specically to data from a juggling experiment. The...

  11. Acoustic emission monitoring of a fatigue test of an F/A-18 bulkhead

    Scala, C. M.; McCardle, J. F.; Bowles, S. J.

    This paper describes the application of acoustic emission (AE) to identify cracking in several fatigue-critical regions on the port and starboard sides of an l/A-18 aircraft bulkhead undergoing fatigue testing. AE data acquisition was carried out using an array of three sensors on each side of the bulkhead. AE features stored by each array included relative arrival times of AE events at the three sensors, event rise time at the first-hit sensor, and the load level and the position on the load cycle of event occurrence. AE data processing involved a comparison between the features of those AE events stored during the fatigue testing and predicted features for cracking in the complex-shaped bulkhead. Feature prediction was based on wave propagation characteristics obtained by Pentel-lead calibration, and the known load cycle dependence of crack-related AE events. The AE processing was completed following failure of the bulkhead, and gave the correct locations of all cracks, greater than about 1 mm in depth, present in the bulkhead during the fatigue testing. The study shows that AE associated with cracking can be distinguished, even when many extraneous sources are present, and demonstrates that AE is a promising technique for nondestructive evaluation of a complex structure such as the F/A-18 bulkhead.

  12. Application of acoustic emission as a monitoring system during hydrostatic tests of nuclear reactor components

    The paper presents the state of art for the surveillance of nuclear reactor components by acoustic emission during hydrostatic tests as obtained during several inspections made by KWU and Battelle-Frankfurt/Main. The following four points are relevant: a) Measures designed to suppress background noise, b) adapted pressure increase rate, c) extensive and practically oriented calibration measurements, d) suitable measuring technique. These necessary preconditions are discussed and results on the wave propagation, location accuracy, attenuation of AE-signals due to geometrical configurations (nozzles) and on the correlation between AE-sources and defects as detected by other NDE-methods presented. Two selected examples of AE-tests on reactor components will demonstrate the results which can be obtained at the present time. These investigations have shown till now that: 1) AE is a sensitive NDE-method, able to detect even very small flaws. The AE-sources lie for the most part in areas of seam welds, welded-on attachments, nozzles, closure studs, or other prominent areas (see rolling track). 2) Indications which were found by AE need not necessarily be detectable by other NDE-methods, e.g. ultrasound. 3) Small leaks can be identified in a short time and can be located within certain limits. An essential point however is that leaks with higher noise level must be sealed off. (orig.)

  13. Monitoring acoustic emission (AE) energy in slurry impingement using a new model for particle impact

    Droubi, M. G.; Reuben, R. L.; White, G.

    2015-10-01

    A series of systematic impact tests have been carried out to investigate the influence of particle size, free stream velocity, particle impact angle, and nominal particle concentration on the amount of energy dissipated in a carbon steel target using a slurry impingement erosion test rig, as indicated by the acoustic emission (AE) recorded by a sensor mounted on the back of the target. Silica sand particles of mean particle size 152.5, 231, and 362.5 μm were used for impingement on the target at angles varying between 30° and 90° while the free stream velocity was changed between 4.2 and 12.7 m/s. In previous work by the authors, it was demonstrated that the AE time series associated with particle-laden air striking a carbon steel target could be described as the cumulation of individual particle arrival events each drawn from a statistical distribution model. The high arrival rate involved in a slurry jet poses challenges in resolving individual particle impact signatures in the AE record, and so the model has been extended in this paper to account for different particle carrier-fluids and to situations where arrivals cannot necessarily be resolved.

  14. Active monitoring of formaldehyde diffusion into histological tissues with digital acoustic interferometry.

    Bauer, Daniel R; Stevens, Benjamin; Chafin, David; Theiss, Abbey P; Otter, Michael

    2016-01-01

    The preservation of certain labile cancer biomarkers with formaldehyde-based fixatives can be considerably affected by preanalytical factors such as quality of fixation. Currently, there are no technologies capable of quantifying a fixative's concentration or the formation of cross-links in tissue specimens. This work examined the ability to detect formalin diffusion into a histological specimen in real time. As formaldehyde passively diffused into tissue, an ultrasound time-of-flight (TOF) shift of several nanoseconds was generated due to the distinct sound velocities of formalin and exchangeable fluid within the tissue. This signal was resolved with a developed digital acoustic interferometry algorithm, which compared the phase differential between signals and computed the absolute TOF with subnanosecond precision. The TOF was measured repeatedly across the tissue sample for several hours until diffusive equilibrium was realized. The change in TOF from 6-mm thick ex vivo human tonsil fit a single-exponential decay ([Formula: see text]) with rate constants that varied drastically spatially between 2 and 10 h ([Formula: see text]) due to substantial heterogeneity. This technology may prove essential to personalized cancer diagnostics by documenting and tracking biospecimen preanalytical fixation, guaranteeing their suitability for diagnostic assays, and speeding the workflow in clinical histopathology laboratories. PMID:26866049

  15. Aquatic Acoustic Metrics Interface Utility for Underwater Sound Monitoring and Analysis

    Thomas J. Carlson

    2012-05-01

    Full Text Available Fishes and marine mammals may suffer a range of potential effects from exposure to intense underwater sound generated by anthropogenic activities such as pile driving, shipping, sonars, and underwater blasting. Several underwater sound recording (USR devices have been built to acquire samples of the underwater sound generated by anthropogenic activities. Software becomes indispensable for processing and analyzing the audio files recorded by these USRs. In this paper, we provide a detailed description of a new software package, the Aquatic Acoustic Metrics Interface (AAMI, specifically designed for analysis of underwater sound recordings to provide data in metrics that facilitate evaluation of the potential impacts of the sound on aquatic animals. In addition to the basic functions, such as loading and editing audio files recorded by USRs and batch processing of sound files, the software utilizes recording system calibration data to compute important parameters in physical units. The software also facilitates comparison of the noise sound sample metrics with biological measures such as audiograms of the sensitivity of aquatic animals to the sound, integrating various components into a single analytical frame. The features of the AAMI software are discussed, and several case studies are presented to illustrate its functionality.

  16. Using Complementary Acoustic and Optical Techniques for Quantitative Monitoring of Biomolecular Adsorption at Interfaces

    Rupert Konradi

    2012-09-01

    Full Text Available The great wealth of different surface sensitive techniques used in biosensing, most of which claim to measure adsorbed mass, can at first glance look unnecessary. However, with each technique relying on a different transducer principle there is something to be gained from a comparison. In this tutorial review, different optical and acoustic evanescent techniques are used to illustrate how an understanding of the transducer principle of each technique can be exploited for further interpretation of hydrated and extended polymer and biological films. Some of the most commonly used surface sensitive biosensor techniques (quartz crystal microbalance, optical waveguide spectroscopy and surface plasmon resonance are briefly described and five case studies are presented to illustrate how different biosensing techniques can and often should be combined. The case studies deal with representative examples of adsorption of protein films, polymer brushes and lipid membranes, and describe e.g., how to deal with strongly vs. weakly hydrated films, large conformational changes and ordered layers of biomolecules. The presented systems and methods are compared to other representative examples from the increasing literature on the subject.

  17. A case study of real-time monitoring of solid-state phase transformations in acoustically levitated particles using near infrared and Raman spectroscopy

    Rehder, Sönke; Wu, Jian-Xiong; Laackmann, Julian;

    2013-01-01

    The objective of this study was to monitor the amorphous-to-crystalline solid-state phase transformation kinetics of the model drug ibuprofen with spectroscopic methods during acoustic levitation. Chemical and physical information was obtained by real-time near infrared (NIRS) and Raman...... spectroscopy measurements. The recrystallisation kinetic parameters (overall recrystallisation rate constant ß and the time needed to reach 50% of the equilibrated level t(50)), were determined using a multivariate curve resolution approach. The acoustic levitation device coupled with non-invasive spectroscopy....... This observation was explained by the high energy density of the Raman laser beam, which might have led to local heating effects of the sample and thus reduced the recrystallisation onset time. It was concluded that acoustic levitation with NIR and Raman spectroscopy combined with multivariate curve resolution...

  18. Monitoring Gas Void Fraction In Two-Phase Flow With Acoustic Emission

    Addali, Abdulmajid

    2010-01-01

    The two-phase gas/liquid flow phenomenon can be encountered over a range of gas and liquid flow rates in the chemical engineering industry, particularly in oil and gas production transportation pipelines. Monitoring and measurement of their characteristics, such as the gas void fraction, are necessary to minimise the disruption of downstream process facilities. Thus, over the last decade, the investigation, development and use of multiphase flow metering system have been a major focus for the...

  19. A Methodological Review of Piezoelectric Based Acoustic Wave Generation and Detection Techniques for Structural Health Monitoring

    Zhigang Sun; Bruno Rocha; Kuo-Ting Wu; Nezih Mrad

    2013-01-01

    Piezoelectric transducers have a long history of applications in nondestructive evaluation of material and structure integrity owing to their ability of transforming mechanical energy to electrical energy and vice versa. As condition based maintenance has emerged as a valuable approach to enhancing continued aircraft airworthiness while reducing the life cycle cost, its enabling structural health monitoring (SHM) technologies capable of providing on-demand diagnosis of the structure without i...

  20. Acoustic monitoring (RFM of total hip arthroplasty results of a cadaver study

    Unger AC

    2009-06-01

    Full Text Available Abstract Introduction At present there are no reliable non-traumatic and non-invasive methods to analyse the healing process and loosening status after total hip replacement. Therefore early as well as late loosening of prosthesis and interface component problems are difficult to be found or diagnosed at any time. Methods In a cadaver study the potential application of Resonance Frequency Monitoring (RFM will be evaluated as a non-invasive and non-traumatic method to monitor loosening and interface problems in hip replacement. In a 65 year old female cadaver different stability scenarios for a total hip replacement (shaft, head/modular head and cup, ESKA, Luebeck, Germany are simulated in cemented and cement less prosthesis and then analysed with RFM. The types of stability vary from secure/press-fit to interface-shaft disruption. Results The RFM shows in cemented as well as cement less prosthesis significant intra-individual differences in the spectral measurements with a high dynamic (20 dB difference corresponding to the factor 100 (10000%, regarding the simulated status of stability in the prosthesis system. Conclusion The results of the study demonstrate RFM as a highly sensitive non-invasive and non-traumatic method to support the application of RFM as a hip prosthesis monitoring procedure. The data obtained shows the possibility to use RFM for osteointegration surveillance and early detection of interface problems, but will require further evaluation in clinical and experimental studies.

  1. Monitoring fin whale (Balaenoptera physalus) acoustic presence by means of a low frequency seismic hydrophone in Western Ionian Sea, EMSO site.

    Sciacca, Virginia; Caruso, Francesco; Chierici, Francesco; De Domenico, Emilio; Embriaco, Davide; Favali, Paolo; Giovanetti, Gabriele; Larosa, Giuseppina; Pavan, Gianni; Pellegrino, Carmelo; Pulvirenti, Sara; Riccobene, Giorgio; Simeone, Francesco; Viola, Salvatore; Beranzoli, Laura; Marinaro, Giuditta

    2015-04-01

    In 2012, the NEMO-SN1 multidisciplinary seafloor platform was deployed in the Gulf of Catania at a depth of 2100 m. By using the low bandwidth seismic hydrophone SMID DT405D (1Hz whales (Balaenoptera physalus) acoustic activity in the area. The presence of a genetically isolated population of fin whales has been confirmed in recent years in highly productive areas of the Mediterranean Sea. The species acoustic activity has also been monitored in the past within the Western Mediterranean. Despite this, still very little is known about the routes the population follows seasonally throughout the whole basin and, particularly, in the Ionian area. The most common vocalizations attributed to this population are known as "20Hz pulses" and they are grouped in two main types of calls: type "A", downsweep (17Hz whale acoustic signals, recorded for the first time in the area. Furthermore, our results show a previous unknown acoustic presence of fin whales offshore Eastern Sicily throughout all seasons of the investigated year. The new long-term multidisciplinary projects connected to "KM3NeT" and "EMSO" will give us the chance to better understand the animals' occurrence in the area and to investigate their acoustic behavior and population dynamics.

  2. Chemometrics: From classical to genetic algorithms

    Leardi, Riccardo

    2002-03-01

    Full Text Available In this paper the fundamentals of Chemometrics are presented, by means of a quick overview of the most relevant techniques for data display, classification, modeling and calibration. Two emerging techniques such as Genetic Algorithms and Artificial Neural Networks will also be presented. Goal of the paper is to make people aware of the great superiority of multivariate analysis over the commonly used univariate approach. Mathematical and algorithmical details are not presented, since the paper is mainly focused on the general problems to which Chemometrics can be successfully applied in the field of Food Chemistry.En este artículo se muestran los aspectos fundamentales de la Quimiometria por medio de una revisión rápida de las técnicas más relevantes para mostrar los datos, modelar y calibrar. Se describen dos técnicas emergentes como los algoritmos genéticos y las redes neuronales. El objetivo del articulo es que la comunidad científica tome conciencia de la gran superioridad del análisis multivariante sobre el análisis univariante. No se describen los detalles matemáticos y algorítmicos porque el articulo está dirigido a problemas genéricos en los que la Quimiometría puede ser aplicada con éxito dentro del campo de la Química Analítica.

  3. Near-Real-Time Sismo-acoustic Submarine Station for offshore monitoring

    D'Anna, Giuseppe; D'Alessandro, Antonino; Fertitta, Gioacchino; Fraticelli, Nicola; Calore, Daniele

    2016-04-01

    From the early 1980's, Italian seismicity is monitored by the National Seismic Network (NSN). The network has been considerably enhanced by INGV since 2005 by 24-bit digital stations equipped with broad-band sensors. The NSN is nowadays constituted by about 300 on-land seismic station able to detect and locate also small magnitude earthquake in the whole Italian peninsula. However, the lack of offshore seismic stations does not allow the accurate estimation of hypocentral and focal parameters of small magnitude earthquakes occurring in offshore areas. As in the Mediterranean area there is an intense offshore seismic activity, an extension of the seismic monitoring to the sea would be beneficial. There are two types of stations that could be used to extend the network towards the sea: the first type is connected to the coast though a cable, the second type is isolated (or stand alone) and works autonomously. Both solutions have serious limitations: the first one, for several technical and economic problems, linked to the indispensable transmission/alimentation cable, cannot be installed far from the coast; the second one, allows access to the recorded data, only after they are recovered from the seabed. It is clear that these technical solutions are not suitable for the real time monitoring of the offshore seismicity or for the realization of a tsunami warning system. For this reason, in early 2010, the OBSLab of Gibilmanna begins the design of a submarine station able to overcome the limitations of the two systems above. The station isbuilt under the project EMSO-MedIT. The two stations built have already been tested in dock and ready for installation. One of this station will be installed, in few time, in the southern Tyrrhenian Sea, near the epicentre of the Palermo 2002 main shock. The sea bottom station will be equipped with 2 very broadband 3C seismometers, a broad band hydrophone, a differential and an absolute pressure gauge. The station includes a submarine

  4. Supervised and unsupervised condition monitoring of non-stationary acoustic emission signals

    Sigurdsson, Sigurdur; Pontoppidan, Niels Henrik; Larsen, Jan

    2005-01-01

    We are pursuing a system that monitors the engine condition under multiple load settings, i.e. under non-stationary operating conditions. The running speed when data acquired under simulated marine conditions (different load settings on the propeller curve) was in the range from approximately 70 to...... 125 rotations per minute; furthermore the running speed was stable within periods of fixed load. Electronically controlled engines can change the angular timing of certain events, such as fuel injection in order to optimize its performance. However, this behaviour makes it difficult to detect...

  5. A study on the condition monitoring of check valve at nuclear power plants using the acoustic emission and a neural network technique

    Lee, Min Rae; Lee, Joon Hyun [Busan National Univ., Busan (Korea, Republic of); Kim, Jung Teak [KAERI, Daejeon (Korea, Republic of)

    2005-07-01

    The analysis of Acoustic Emission (AE) signals produced during object leakage is promising for condition monitoring of the components. In this study, an advanced condition monitoring technique based on acoustic emission detection and artificial neural networks was applied to a check valve, one of the components being used extensively in a safety system of a nuclear power plant. AE testing for a check valve under controlled flow loop conditions was performed to detect and evaluate disk movement for valve degradation such as wear and leakage due to foreign object interference in a check valve. It is clearly demonstrated that the evaluation of different types of failure modes such as disk wear and check valve leakage were successful by systematically analyzing the characteristics of various AE parameters. It is also shown that the leak size can be determined with an artificial neural network.

  6. A study on the condition monitoring of check valve at nuclear power plants using the acoustic emission and a neural network technique

    The analysis of Acoustic Emission (AE) signals produced during object leakage is promising for condition monitoring of the components. In this study, an advanced condition monitoring technique based on acoustic emission detection and artificial neural networks was applied to a check valve, one of the components being used extensively in a safety system of a nuclear power plant. AE testing for a check valve under controlled flow loop conditions was performed to detect and evaluate disk movement for valve degradation such as wear and leakage due to foreign object interference in a check valve. It is clearly demonstrated that the evaluation of different types of failure modes such as disk wear and check valve leakage were successful by systematically analyzing the characteristics of various AE parameters. It is also shown that the leak size can be determined with an artificial neural network

  7. A novel closure based approach for fatigue crack length estimation using the acoustic emission technique in structural health monitoring applications

    Use of Acoustic Emission (AE) for detecting and locating fatigue cracks in metallic structures is widely reported but studies investigating its potential for fatigue crack length estimation are scarce. Crack growth information enables prediction of the remaining useful life of a component using well established fracture mechanics principles. Hence, the prospects of AE for use in structural health monitoring applications would be significantly improved if it could be demonstrated not only as a means of detecting crack growth but also for estimation of crack lengths. A new method for deducing crack length has been developed based on correlations between AE signals generated during fatigue crack growth and corresponding cyclic loads. A model for crack length calculation was derived empirically using AE data generated during fatigue crack growth tests in 2 mm thick SEN aluminium 2014 T6 specimens subject to a tensile stress range of 52 MPa and an R ratio of 0.1. The model was validated using AE data generated independently in separate tests performed with a stress range of 27 MPa. The results showed that predictions of crack lengths over a range of 10 mm to 80 mm can be obtained with the mean of the normalised absolute errors ranging between 0.28 and 0.4. Predictions were also made using existing AE feature-based methods and the results compared to those obtained with the novel approach developed. (paper)

  8. Identification of a Critical Time with Acoustic Emission Monitoring during Static Fatigue Tests on Ceramic Matrix Composites: Towards Lifetime Prediction

    Nathalie Godin

    2016-02-01

    Full Text Available Non-oxide fiber-reinforced ceramic-matrix composites are promising candidates for some aeronautic applications that require good thermomechanical behavior over long periods of time. This study focuses on the behavior of a SiCf/[Si-B-C] composite with a self-healing matrix at intermediate temperature under air. Static fatigue experiments were performed below 600 °C and a lifetime diagram is presented. Damage is monitored both by strain measurement and acoustic emission during the static fatigue experiments. Two methods of real-time analysis of associated energy release have been developed. They allow for the identification of a characteristic time that was found to be close to 55% of the measured rupture time. This critical time reflects a critical local energy release assessed by the applicability of the Benioff law. This critical aspect is linked to a damage phase where slow crack growth in fibers is prevailing leading to ultimate fracture of the composite.

  9. Inspection of copper canisters for spent nuclear fuel by means of ultrasound. Ultrasonic imaging, FSW monitoring with acoustic emission

    Stepinski, Tadeusz (ed.); Olofsson, Tomas; Wennerstroem, Erik [Uppsala Univ., Dept. of Technical Sciences (Sweden). Signals and Systems

    2006-12-15

    This report contains the research results concerning advanced ultrasound for the inspection of copper canisters for spent nuclear fuel obtained at Signals and Systems, Uppsala University in years 2005/2006. In the first part of the report we propose a concept of monitoring of the friction stir welding (FSW) process by means of acoustic emission (AE) technique. First, we introduce the AE technique and then we present the principle of the system for monitoring the FSW process in cylindrical symmetry specific for the SKB canisters. We propose an omnidirectional circular array of ultrasonic transducers for receiving the AE signals generated by the FSW tool and the releases of the residual stress at canister's circumference. Finally, we review the theory of uniform circular arrays. The second part of the report is concerned with synthetic aperture focusing technique (SAFT) characterized by enhanced spatial resolution. We evaluate three different approaches to perform imaging with less computational cost than that of the extended SAFT (ESAFT) method proposed in our previous reports. First, a sparse version of ESAFT is presented, which solves the reconstruction problem only for a small set of the most probable scatterers in the image. A frequency domain the {omega}-k SAFT algorithm, which relies on the far-field approximation is presented in the second part. Finally, a detailed analysis of the most computationally intense step in the ESAFT and the sparse 2D deconvolution is presented. In the final part of the report we introduce basics of the 3D ultrasonic imaging that has a great potential in the inspection of the FSW welds. We discuss in some detail the three interrelated steps involved in the 3D ultrasonic imaging: data acquisition, 3D reconstruction, and 3D visualization.

  10. Inspection of copper canisters for spent nuclear fuel by means of ultrasound. Ultrasonic imaging, FSW monitoring with acoustic emission

    This report contains the research results concerning advanced ultrasound for the inspection of copper canisters for spent nuclear fuel obtained at Signals and Systems, Uppsala University in years 2005/2006. In the first part of the report we propose a concept of monitoring of the friction stir welding (FSW) process by means of acoustic emission (AE) technique. First, we introduce the AE technique and then we present the principle of the system for monitoring the FSW process in cylindrical symmetry specific for the SKB canisters. We propose an omnidirectional circular array of ultrasonic transducers for receiving the AE signals generated by the FSW tool and the releases of the residual stress at canister's circumference. Finally, we review the theory of uniform circular arrays. The second part of the report is concerned with synthetic aperture focusing technique (SAFT) characterized by enhanced spatial resolution. We evaluate three different approaches to perform imaging with less computational cost than that of the extended SAFT (ESAFT) method proposed in our previous reports. First, a sparse version of ESAFT is presented, which solves the reconstruction problem only for a small set of the most probable scatterers in the image. A frequency domain the ω-k SAFT algorithm, which relies on the far-field approximation is presented in the second part. Finally, a detailed analysis of the most computationally intense step in the ESAFT and the sparse 2D deconvolution is presented. In the final part of the report we introduce basics of the 3D ultrasonic imaging that has a great potential in the inspection of the FSW welds. We discuss in some detail the three interrelated steps involved in the 3D ultrasonic imaging: data acquisition, 3D reconstruction, and 3D visualization

  11. Guidelines for validation of chemometric models for food authentication

    Veer, van der, P.; Ruth, van, A.; Akkermans, W.

    2011-01-01

    The aim of this report is to describe a set of generic guidelines for in-house validation of a method for authenticity testing that are based on a combination of chemical fingerprinting techniques and chemometric classification models.

  12. GC fingerprints coupled to pattern-recognition multivariate SIMCA chemometric analysis for Brazilian gasoline quality studies

    Rodrigues Hatanaka, Rafael; Flumignan, Danilo Luiz; Oliveira, Jose Eduardo de [Sao Paulo State Univ., Araraquara, SP (Brazil). Center for Monitoring and Research of the Quality of Fuels, Biofuels, Crude Oil and Derivatives

    2009-10-15

    ASTM D6729 gas chromatographic fingerprinting coupled to pattern-recognition multivariate soft independent modeling of class analogy (SIMCA) chemometric analysis provides an original and alternative approach to screening Brazilian commercial gasoline quality. SIMCA, was performed on gas chromatographic fingerprints to classify the quality of representative commercial gasoline samples selected by hierarchical cluster analysis and collected over a 5 month period from gas stations in Sao Paulo State, Brazil. Following an optimized ASTM D6729 gas chromatographic-SIMCA algorithm, it was possible to correctly classify the majority of commercial gasoline samples. The method could be employed for rapid monitoring to discourage adulteration. (orig.)

  13. Project of a Near-Real-Time Sismo-acoustic Submarine Station for offshore monitoring (NRTSSS)

    D'Anna, G.; Calore, D.; Mangano, G.; D'Alessandro, A.; Favali, P.

    2011-12-01

    The INGV seismic network ensures reliable and continuous monitoring of the Italian territory. However, the peculiarity of the Italian peninsula, characterised by an intense offshore geodynamic and seismic activity, requires the extension of the seismic monitoring to the sea. The aim of this project is: - to identify bottleneck is related to the construction, installation and use of underwater seismic station; - to define the most appropriate and low-cost architecture to guarantee the minimum functionality required for a seismic station. In order to obtain reliable seafloor seismic signals integrated to land-based network, the requirements to be fulfill are: - an acceptable coupling with the seabed; - the orientation of the components with respect to the magnetic North and to the verticality; - the correct time stamp of the data; - the data transfer to the land for the integration. Currently, the optimal solution for offshore seismic station is a cable connection to power and real-time data transfer, like the case of Western Ionian Sea cabled observatory, one of the operative node of the EMSO research infrastructure (European Multidisciplinary Seafloor and water column Observatory, http://emso-eu.org). But in the Mediterranean many seismic areas are located a few tens-hundreds of miles from the coast and cabled solutions are not feasible essentially for economic reasons. For this kind of installations EMSO research infrastructure foresees no-cabled solution, that requires a surface buoy deployed in the vicinity seafloor modules.This project plans to develop a surface buoy equipped with autonomous power supply system to power also the seafloor platforms and two-way communication system enabling the data transfer through latest generation of broadband radio communication or satellite link (Fig. 1). All the components of the prototype system are described.

  14. Acoustics short-term passive monitoring using sonobuoys in the Bering, Chukchi, and Western Beaufort Seas conducted by Alaska Fisheries Scientific Center, National Marine Mammal Laboratory from 2007-08-01 to 2015-09-28 (NCEI Accession 0138863)

    National Oceanic and Atmospheric Administration, Department of Commerce — The National Marine Mammal Laboratory (NMML) has conducted passive acoustic monitoring in the Bering, Chukchi, and Western Beaufort Seas to determine...

  15. A case study of real-time monitoring of solid-state phase transformations in acoustically levitated particles using near infrared and Raman spectroscopy.

    Rehder, Sönke; Wu, Jian X; Laackmann, Julian; Moritz, Hans-Ulrich; Rantanen, Jukka; Rades, Thomas; Leopold, Claudia S

    2013-01-23

    The objective of this study was to monitor the amorphous-to-crystalline solid-state phase transformation kinetics of the model drug ibuprofen with spectroscopic methods during acoustic levitation. Chemical and physical information was obtained by real-time near infrared (NIRS) and Raman spectroscopy measurements. The recrystallisation kinetic parameters (overall recrystallisation rate constant β and the time needed to reach 50% of the equilibrated level t(50)), were determined using a multivariate curve resolution approach. The acoustic levitation device coupled with non-invasive spectroscopy enabled monitoring of the recrystallisation process of the difficult-to-handle (adhesive) amorphous sample. The application of multivariate curve resolution enabled isolation of the underlying pure spectra, which corresponded well with the reference spectra of amorphous and crystalline ibuprofen. The recrystallisation kinetic parameters were estimated from the recrystallisation profiles. While the empirical recrystallisation rate constant determined by NIR and Raman spectroscopy were comparable, the lag time for recrystallisation was significantly lower with Raman spectroscopy as compared to NIRS. This observation was explained by the high energy density of the Raman laser beam, which might have led to local heating effects of the sample and thus reduced the recrystallisation onset time. It was concluded that acoustic levitation with NIR and Raman spectroscopy combined with multivariate curve resolution allowed direct determination of the recrystallisation kinetics of amorphous drugs and thus is a promising technique for monitoring solid-state phase transformations of adhesive small-sized samples during the early phase of drug development. PMID:23069619

  16. Design of copper/carbon-coated fiber Bragg grating acoustic sensor net for integrated health monitoring of nuclear power plant

    Research highlights: → We develop a cost-effective fiber Bragg grating (FBG) acoustic sensor net for nuclear power plants using copper/carbon (Cu/C)-coated fiber. → A chemical method is proposed to remove the Cu/C coating. A 5 mm FBG is successfully inscribed in a Ge-doped silica core through a 7 mm-long silica section with the coating removed. → The Cu/C-coated fiber net shows good thermal resistance (oC). → The Cu/C-coated FBG sensor using the metallic adhesive successfully detects the acousto-ultrasonic waves generated by pencil lead breaking and laser beam excitation. - Abstract: A nuclear power plant (NPP) is a harsh environment that gives rise to age-related degradation of the plant structures, and eventually leads to radiation leakage that threatens humans. Integrated structural health monitoring (ISHM) technology is a strong candidate for the prevention of the NPP accidents during operation. Prior studies have shown that fiber Bragg gratings (FBGs) and metal-coated fibers have good radiation and high temperature resistance. In this study, a FBG acoustic sensor using a metallic adhesive for installation and a relatively economical copper/carbon (Cu/C)-coated fiber is developed for ISHM of high temperature NPP structures. A chemical method is proposed to remove the Cu/C coating. A 5 mm FBG was successfully inscribed in a Ge-doped silica core through a 7 mm-long silica section with the coating removed. The Cu/C-coated fiber with the same core/clad structure as the standard SMF allowed no-loss fusion splicing, and showed good adaptability to the economical standard fiber, adaptor, connector, and instruments. It showed also good thermal resistance (oC) with no degradation in optical power during the optical transmission. The metallic adhesive used to install the FBG in a one-end-free configuration showed superior bonding reliability during temperature cycles ranging from 25 oC to 345 oC. The FBG reflectivity was stabilized at a 58% drop from the initial

  17. Chemometrics: A new scenario in herbal drug standardization

    Ankit Bansal

    2014-08-01

    Full Text Available Chromatography and spectroscopy techniques are the most commonly used methods in standardization of herbal medicines but the herbal system is not easy to analyze because of their complexity of chemical composition. Many cutting-edge analytical technologies have been introduced to evaluate the quality of medicinal plants and significant amount of measurement data has been produced. Chemometric techniques provide a good opportunity for mining more useful chemical information from the original data. Then, the application of chemometrics in the field of medicinal plants is spontaneous and necessary. Comprehensive methods and hyphenated techniques associated with chemometrics used for extracting useful information and supplying various methods of data processing are now more and more widely used in medicinal plants, among which chemometrics resolution methods and principal component analysis (PCA are most commonly used techniques. This review focuses on the recent various important analytical techniques, important chemometrics tools and interpretation of results by PCA, and applications of chemometrics in quality evaluation of medicinal plants in the authenticity, efficacy and consistency.

  18. Monitoring radio-frequency thermal ablation with ultrasound by low frequency acoustic emissions--in vitro and in vivo study.

    Winkler, Itai; Adam, Dan

    2011-05-01

    The object of this study was to evaluate the monitoring of thermal ablation therapy by measuring the nonlinear response to ultrasound insonation at the region being treated. Previous reports have shown that during tissue heating, microbubbles are formed. Under the application of ultrasound, these microbubbles may be driven into nonlinear motion that produces acoustic emissions at sub-harmonic frequencies and a general increase of emissions at low frequencies. These low frequency emissions may be used to monitor ablation surgery. In this study, a modified commercial ultrasound system was used for transmitting ultrasound pulses and for recording raw RF-lines from a scan plane in porcine (in vitro) and rabbit (in vivo) livers during radio-frequency ablation (RFA). The transmission pulse was 15 cycles in length at 4 MHz (in vitro) and 3.6 MHz (in vivo). Thermocouples were used for monitoring temperatures during the RFA treatment.In the in vitro experiments, recorded RF signals (A-lines) were segmented, and the total energy was measured at two different frequency bands: at a low frequency band (LFB) of 1-2.5 MHz and at the transmission frequency band (TFB) of 3.5-4.5 MHz. The mean energy at the LFB and at the TFB increased substantially in areas adjacent to the RF needle. These energies also changed abruptly at higher temperatures, thus, producing great variance in the received energy. Mean energies in areas distant from RF needle showed little change and variation during treatment. It was also shown that a 3 dB increase of energy at the low frequency band was typically obtained in regions in which temperature was above 53.3 ± 5° C. Thus, this may help in evaluating regions undergoing hyperthermia. In the in vivo experiments, an imaging algorithm based on measuring the LFB energy was used. The algorithm performs a moving average of the LFB energies measured at segments within the scan plane.Results show that a colored region is formed on the image and that it is

  19. Assessment of systolic and diastolic function in heart failure using ambulatory monitoring with acoustic cardiography.

    Dillier, Roger; Zuber, Michel; Arand, Patricia; Erne, Susanne; Erne, Paul

    2011-08-01

    INTRODUCTION. The circadian variation of heart function and heart sounds in patients with and without heart failure (HF) is poorly understood. We hypothesized HF patients would exhibit less circadian variation with worsened cardiac function and sleep apnea. METHODS. We studied 67 HF patients (age 67.4 ± 8.2 years; 42% acute HF) and 63 asymptomatic control subjects with no history of HF (age 61.6 ± 7.7 years). Subjects wore a heart sound/ECG/respiratory monitor. The data were analyzed for sleep apnea, diastolic heart sounds, and systolic time intervals. RESULTS. The HF group had significantly greater prevalence of the third heart sound and prolongation of electro-mechanical activation time, while the control group had an age-related increase in the prevalence of the fourth heart sound. The control group showed more circadian variation in cardiac function. The HF subjects had more sleep apnea and higher occurrence of heart rate non-dipping. CONCLUSIONS. The control subjects demonstrated an increasing incidence of diastolic dysfunction with age, while systolic function was mostly unchanged with aging. Parameters related to systolic function were significantly worse in the HF group with little diurnal variation, indicating a constant stimulation of sympathetic tone in HF and reduction of diurnal regulation. PMID:21361859

  20. FINAL TECHNICAL REPORT: Underwater Active Acoustic Monitoring Network For Marine And Hydrokinetic Energy Projects

    Stein, Peter J.; Edson, Patrick L.

    2013-12-20

    This project saw the completion of the design and development of a second generation, high frequency (90-120 kHz) Subsurface-Threat Detection Sonar Network (SDSN). The system was deployed, operated, and tested in Cobscook Bay, Maine near the site the Ocean Renewable Power Company TidGen™ power unit. This effort resulted in a very successful demonstration of the SDSN detection, tracking, localization, and classification capabilities in a high current, MHK environment as measured by results from the detection and tracking trials in Cobscook Bay. The new high frequency node, designed to operate outside the hearing range of a subset of marine mammals, was shown to detect and track objects of marine mammal-like target strength to ranges of approximately 500 meters. This performance range results in the SDSN system tracking objects for a significant duration - on the order of minutes - even in a tidal flow of 5-7 knots, potentially allowing time for MHK system or operator decision-making if marine mammals are present. Having demonstrated detection and tracking of synthetic targets with target strengths similar to some marine mammals, the primary hurdle to eventual automated monitoring is a dataset of actual marine mammal kinematic behavior and modifying the tracking algorithms and parameters which are currently tuned to human diver kinematics and classification.

  1. Non-destructive monitoring of rolling element bearing components using audio acoustics signals

    The main objective of this paper is to develop a non-destructive machine-component monitoring system, which is non-intrusive and non-contact in nature. Moreover, the system to be developed must be robust enough for it to be implemented in an industrial environment. The application of a desirable non-intrusive and non-contact in nature of sound pressure measurement method is difficult to carry out if the background noise level is high. This is because sound pressure measurement is dependent on the characteristics of the sound field where a measurement is carried out. For this reason, air-particle acceleration signal is introduced and utilized in this study. Air-particle acceleration is a vector quantity. Measurement of vector property will improve signal-to-noise ratio of the measured signal, even in a noisy environment. A dedicated test rig was constructed to carry out the experiments and to test the hypothesis.. Rolling element bearings were used for the experiment because of the many different types of defect that can develo p in them, such as inner race, rolling element and outer race defects. Moreover, the dynamic behavior of bearings is well understood and can be compared with experimental results obtained from the study. The results from using air-particle acceleration signals were compared with results obtained from utilising sound pressure and vibration signals. These results show that the performance of air-particle acceleration method is superior to the performance of sound pressure method. Results from the analysis of air-particle acceleration signal can clearly indicate the presence of a defective component in the test-bearing. This is so even when the overall background noise was 14dB higher than the overall noise level emitted by the defective bearing. Moreover, the sensitivity of the measurement of air-particle acceleration method to indicate the presence of a defective bearing is similar to the sensitivity when using conventional vibration equipment

  2. The Development of Automated Detection Techniques for Passive Acoustic Monitoring as a Tool for Studying Beaked Whale Distribution and Habitat Preferences in the California Current Ecosystem

    Yack, Tina M.

    The objectives of this research were to test available automated detection methods for passive acoustic monitoring and integrate the best available method into standard marine mammal monitoring protocols for ship based surveys. The goal of the first chapter was to evaluate the performance and utility of PAMGUARD 1.0 Core software for use in automated detection of marine mammal acoustic signals during towed array surveys. Three different detector configurations of PAMGUARD were compared. These automated detection algorithms were evaluated by comparing them to the results of manual detections made by an experienced bio-acoustician (author TMY). This study provides the first detailed comparisons of PAMGUARD automated detection algorithms to manual detection methods. The results of these comparisons clearly illustrate the utility of automated detection methods for odontocete species. Results of this work showed that the majority of whistles and click events can be reliably detected using PAMGUARD software. The second chapter moves beyond automated detection to examine and test automated classification algorithms for beaked whale species. Beaked whales are notoriously elusive and difficult to study, especially using visual survey methods. The purpose of the second chapter was to test, validate, and compare algorithms for detection of beaked whales in acoustic line-transect survey data. Using data collected at sea from the PAMGUARD classifier developed in Chapter 2 it was possible to measure the clicks from visually verified Baird's beaked whale encounters and use this data to develop classifiers that could discriminate Baird's beaked whales from other beaked whale species in future work. Echolocation clicks from Baird's beaked whales, Berardius bairdii, were recorded during combined visual and acoustic shipboard surveys of cetacean populations in the California Current Ecosystem (CCE) and with autonomous, long-term recorders at four different sites in the Southern

  3. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2010 and September 2010

    Haycox, Jon (ASC Applied Seismology Consultants (United Kingdom))

    2011-05-15

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox et al. 2009a, b, 2010). Appendix I contains further information about previous monitoring periods. This report covers the period between 1st April 2010 and 30th September 2010 and is the eleventh 6-monthly processing and interpretation of the results from the experiment

  4. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2009 and March 2010

    Haycox, Jon; Andrews, Jennifer [ASC, Applied Seismology Consultants, Shrewsbury, Shropshire (United Kingdom)

    2010-09-15

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, 2009, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring periods can be found in Appendix 1. This report covers the period between 1st October 2009 and 31st March 2010 and is the tenth 6-monthly processing and interpretation of the results from the experiment.

  5. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2009 and September 2009

    Haycox, Jon; Pettitt, Will [ASC, Applied Seismology Consultants, Shrewsbury, Shropshire (United Kingdom)

    2009-12-15

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st April 2009 and 30th September 2009 and is the ninth 6-monthly processing and interpretation of the results from the experiment.

  6. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2008 and March 2009

    Haycox, Jon; Duckworth, Damion [ASC, Applied Seismology Consultants, Shrewsbury, Shropshire (United Kingdom)

    2009-06-15

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st October 2008 and 31st March 2009 and is the eighth 6-monthly processing and interpretation of the results from the experiment.

  7. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2009 and September 2009

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st April 2009 and 30th September 2009 and is the ninth 6-monthly processing and interpretation of the results from the experiment

  8. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2008 and March 2009

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st October 2008 and 31st March 2009 and is the eighth 6-monthly processing and interpretation of the results from the experiment

  9. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2009 and March 2010

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, 2009, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring periods can be found in Appendix 1. This report covers the period between 1st October 2009 and 31st March 2010 and is the tenth 6-monthly processing and interpretation of the results from the experiment

  10. Acoustic emission monitoring of stress corrosion cracking in type 304 stainless steel pipes under cyclic heating and cooling

    Acoustic emission (AE) monitoring was performed during the SCC process in sensitized Type 304 stainless steel pipes under cyclic heating and cooling. The specimens with 20 mm inner diameter and 22 mm outer diameter were solution-treated at 10500C for 30 min and then sensitized at 6500C for 2 hr in vacuum. Test temperature was varied between 1450C and 2900C in triangular wave form with 8 hr period. Two types of loading conditions were used: (1) test condition 1: σsub(theta) (hoop stress) = 157 (MPa) (16 (kg/mm)), σsub(z) (axial stress) = 275 (MPa) (28 (kg/mm)), (2) test condition 2: σsub(theta) = 157 (MPa) (16 (kg/mm)), σsub(z) that altered between 157 MPa and 275 MPa in phase with the test temperature. Dissolved oxygen concentration was about 8 ppm. Main results were as follows: (1) The SCC process under both test condition 1 and test condition 2 could be divided into the former and the latter stages, according to the differences of AE activities per one temperature cycle, (2) The crack of 60 μm in hoop direction could be detected by AE techniques, (3) The maximum AE signal amplitudes in the latter stage were 1.9 mV and 4.5 mV at sensor output under test condition 1 and test condition 2, respectively, (4) The crack growth rates in radial direction, estimated from the AE measurement results, were about 3.4 x 10-9 m/sec for test condition 1 and about 7.7 x 10-9 m/sec for test condition 2, respectively. (author)

  11. Development of hydroacoustical techniques for the monitoring and classification of benthic habitats in Puck Bay: Modeling of acoustic waves scattering by seagrass

    Raczkowska, A.; Gorska, N.

    2012-12-01

    Puck Bay is an area of high species biodiversity belonging to the Coastal Landscape Park of Baltic Sea Protected Areas (BSPA) and is also included in the list of the World Wide Fund for Nature (WWF) and covered by the protection program "Natura 2000". The underwater meadows of the Puck Bay are important for Europe's natural habitats due to their role in enhancing the productivity of marine ecosystems and providing shelter and optimal feeding conditions for many marine organisms. One of the dominant species comprising the underwater meadows of the Southern Baltic Sea is the seagrass Zostera marina. The spatial extent of underwater seagrass meadows is altered by pollution and eutrophication; therefore, to properly manage the area one must monitor its ecological state. Remote acoustic methods are useful tools for the monitoring of benthic habitats in many marine areas because they are non-invasive and allow researchers to obtain data from a large area in a short period of time. Currently there is a need to apply these methods in the Baltic Sea. Here we present an analysis of the mechanism of scattering of acoustic waves on seagrass in the Southern Baltic Sea based on the numerical modeling of acoustic wave scattering by the biological tissues of plants. The study was conducted by adapting a model developed on the basis of DWBA (Distorted Wave Born Approximation) developed by Stanton and Chu (2005) for fluid-like objects, including the characteristics of the Southern Baltic seagrass. Input data for the model, including the morphometry of seagrass leaves, their angle of inclination and the density plant cover, was obtained through the analysis of biological materials collected in the Puck Bay in the framework of a research project financed by the Polish Government (Development of hydroacoustic methods for studies of underwater meadows of Puck Bay, 6P04E 051 20). On the basis of the developed model, we have analyzed the dependence of the target strength of a single

  12. Activated sludge characterization through microscopy: A review on quantitative image analysis and chemometric techniques

    Mesquita, Daniela P. [IBB-Institute for Biotechnology and Bioengineering, Centre of Biological Engineering, Universidade do Minho, Campus de Gualtar, 4710-057 Braga (Portugal); Amaral, A. Luís [IBB-Institute for Biotechnology and Bioengineering, Centre of Biological Engineering, Universidade do Minho, Campus de Gualtar, 4710-057 Braga (Portugal); Instituto Politécnico de Coimbra, ISEC, DEQB, Rua Pedro Nunes, Quinta da Nora, 3030-199 Coimbra (Portugal); Ferreira, Eugénio C., E-mail: ecferreira@deb.uminho.pt [IBB-Institute for Biotechnology and Bioengineering, Centre of Biological Engineering, Universidade do Minho, Campus de Gualtar, 4710-057 Braga (Portugal)

    2013-11-13

    Graphical abstract: -- Highlights: •Quantitative image analysis shows potential to monitor activated sludge systems. •Staining techniques increase the potential for detection of operational problems. •Chemometrics combined with quantitative image analysis is valuable for process monitoring. -- Abstract: In wastewater treatment processes, and particularly in activated sludge systems, efficiency is quite dependent on the operating conditions, and a number of problems may arise due to sludge structure and proliferation of specific microorganisms. In fact, bacterial communities and protozoa identification by microscopy inspection is already routinely employed in a considerable number of cases. Furthermore, quantitative image analysis techniques have been increasingly used throughout the years for the assessment of aggregates and filamentous bacteria properties. These procedures are able to provide an ever growing amount of data for wastewater treatment processes in which chemometric techniques can be a valuable tool. However, the determination of microbial communities’ properties remains a current challenge in spite of the great diversity of microscopy techniques applied. In this review, activated sludge characterization is discussed highlighting the aggregates structure and filamentous bacteria determination by image analysis on bright-field, phase-contrast, and fluorescence microscopy. An in-depth analysis is performed to summarize the many new findings that have been obtained, and future developments for these biological processes are further discussed.

  13. Activated sludge characterization through microscopy: A review on quantitative image analysis and chemometric techniques

    Graphical abstract: -- Highlights: •Quantitative image analysis shows potential to monitor activated sludge systems. •Staining techniques increase the potential for detection of operational problems. •Chemometrics combined with quantitative image analysis is valuable for process monitoring. -- Abstract: In wastewater treatment processes, and particularly in activated sludge systems, efficiency is quite dependent on the operating conditions, and a number of problems may arise due to sludge structure and proliferation of specific microorganisms. In fact, bacterial communities and protozoa identification by microscopy inspection is already routinely employed in a considerable number of cases. Furthermore, quantitative image analysis techniques have been increasingly used throughout the years for the assessment of aggregates and filamentous bacteria properties. These procedures are able to provide an ever growing amount of data for wastewater treatment processes in which chemometric techniques can be a valuable tool. However, the determination of microbial communities’ properties remains a current challenge in spite of the great diversity of microscopy techniques applied. In this review, activated sludge characterization is discussed highlighting the aggregates structure and filamentous bacteria determination by image analysis on bright-field, phase-contrast, and fluorescence microscopy. An in-depth analysis is performed to summarize the many new findings that have been obtained, and future developments for these biological processes are further discussed

  14. Identification and spatial patterns of coastal water pollution sources based on GIS and chemometric approach.

    Zhou, Feng; Guo, Huai-Cheng; Liu, Yong; Hao, Ze-Jia

    2007-01-01

    Comprehensive and joint applications of GIS and chemometric approach were applied in identification and spatial patterns of coastal water pollution sources with a large data set (5 years (2000-2004), 17 parameters) obtained through coastal water monitoring of Southern Water Control Zone in Hong Kong. According to cluster analysis the pollution degree was significantly different between September-next May (the 1st period) and June-August (the 2nd period). Based on these results, four potential pollution sources, such as organic/eutrophication pollution, natural pollution, mineral/anthropic pollution and fecal pollution were identified by factor analysis/principal component analysis. Then the factor scores of each monitoring site were analyzed using inverse distance weighting method, and the results indicated degree of the influence by various potential pollution sources differed among the monitoring sites. This study indicated that hybrid approach was useful and effective for identification of coastal water pollution source and spatial patterns. PMID:17966867

  15. Identification and spatial patterns of coastal water pollution sources based on GIS and chemometric approach

    ZHOU Feng; GUO Huai-cheng; LIU Yong; HAO Ze-jia

    2007-01-01

    Comprehensive and joint applications of GIS and chemometric approach were applied in identification and spatial patterns of coastal water pollution sources with a large data set (5 years (2000-2004), 17 parameters) obtained through coastal water monitoring of Southern Water Control Zone in Hong Kong. According to cluster analysis the pollution degree was significantly different between September-next May (the 1st period) and June-August (the 2nd period). Based on these results, four potential pollution sources, such as organic/eutrophication pollution, natural pollution, mineral/anthropic pollution and fecal pollution were identified by factor analysis/principal component analysis. Then the factor scores of each monitoring site were analyzed using inverse distance weighting method, and the results indicated degree of the influence by various potential pollution sources differed among the monitoring sites. This study indicated that hybrid approach was useful and effective for identification of coastal water pollution source and spatial pattern.

  16. Arctic ocean long-term acoustic monitoring : ambient noise, environmental correlates, and transients north of Barrow, Alaska

    Roth, Ethan H.

    2008-01-01

    The Arctic Ocean has experienced wide-spread decreases in sea ice concentrations that may impact various marine ecosystems. This study analyzes yearlong ocean acoustic recordings from north of Barrow, Alaska, to provide baseline measurements prior to possible increases in anthropogenic activities. In September 2006, two autonomous High-frequency Acoustic Recording Packages (HARPs) were deployed to the seafloor (250m), where sound was continuously recorded by hydrophones for nine months. Ice c...

  17. Undersea acoustic telemetry across the North Anatolian Fault, Marmara Sea: results from the first 6 months of monitoring of the fault displacement

    Royer, J. Y.; Deschamps, A.; Piete, H.; Sakic, P.; Ballu, V.; Apprioual, R.; Kopp, H.; Lange, D.; Ruffine, L.; Géli, L.

    2015-12-01

    Located in the Marmara Sea, the Istanbul-Silivri segment of the North Anatolian Fault (NAF) is known to be a seismic gap since 1766, although, in the last century, the NAF has caused major devastating earthquakes over most of its extent. This fault segment, void of seismicity, may be either creeping aseismically or blocked and accumulating enough strain to produce an earthquake of magnitude 7 or greater. This section of the NAF may thus represent a major seismic and tsunamigenic hazard for the Istanbul megalopolis, located only 40 km away. The objective of the MARSITE project, funded by the European Union and coordinated by the Observatory of the University of Kandilli (KOERI), is to determine the blocking state of the Istanbul-Silivri fault segment. In this context, an array of 10 acoustic transponders has been deployed on either sides of the fault, in the eastern part of the Kumburgaz Basin, to measure the displacements of the fault over a period of 3 to 5 years. The telemetric beacons (4 from the University of Brest and 6 from the GEOMAR Institute in Kiel) form two arrays fitted in one another. The principle of the experiment is to repeatedly measure the distance (ie two-way-travel time of acoustic pings) between pairs of beacons and thus to monitor the deformation of an array of 9 baselines, 500m to 3000m long, of which 5 cross obliquely the assumed fault trace. The French and German arrays are independent but ensure a redundancy of rangings along common baselines. Each acoustic transponder also monitors the temperature, pressure, sound-velocity and attitude (tiltmeters), every one or two hours. Data are stored in each beacon and can be downloaded from the surface using an acoustic modem. We present here the first 6 months of recording by the French array, from November 1st, 2014 to April 25, 2015. All acoustic transponders worked nominally for 6 months and appear to have remained stable on the seafloor. Recorded sea-bottom temperatures provide evidence for

  18. Program to develop acoustic emission-flow relationship for inservice monitoring of nuclear pressure vessels. Progress report, February 1--July 1, 1977

    The purpose of the program reported is to evaluate experimentally the feasibility of further assuring reactor safety by detecting and analyzing flaw growth in reactor pressure boundaries through continuous monitoring for acoustic emission (AE). Program objectives are: (1) characterize AE from a limited range of defects and material property conditions; (2) characterize AE from innocuous sources (including defects); (3) develop criteria for distinguishing significant flaws from innocuous sources; (4) develop an AE-flaw damage model to serve as a basis for relating inservice AE to pressure vessel integrity. Steel plate required for the program has been procured and test specimens are being fabricated. Specimen test system has been assembled and calibrated. A technique for rating AE monitor system sensitivity has been developed. An HSST pressure vessel test has been successfully monitored for AE, and data analysis is in progress

  19. Green Sturgeon Acoustic Monitoring

    National Oceanic and Atmospheric Administration, Department of Commerce — This database is used to hold tracking data for green sturgeon tagged in Central California. The data collection began in late 2002 and is ongoing.

  20. Assessment of noninvasive acoustic respiration rate monitoring in patients admitted to an Emergency Department for drug or alcoholic poisoning.

    Guechi, Youcef; Pichot, Amélie; Frasca, Denis; Rayeh-Pelardy, Fatima; Lardeur, Jean-Yves; Mimoz, Olivier

    2015-12-01

    To compare respiration rate measurement by an acoustic method and thoracic impedance to capnometry as the reference method, in patients at the Emergency Department after drug or alcoholic poisoning. In this observational study, 30 patients aged 18 or older, hospitalized at the Emergency Department for drug or alcoholic poisoning, without any contraindication to a face mask and/or a cervical acoustic sensor, were included in the study. They benefited from a simultaneous recording of their respiration rate by the acoustic method (RRa(®), Masimo Corp., Irvine, CA, USA), by thoracic impedance (Philips Intellivue(®) MP2, Suresnes, France) and by capnometry (Capnostream(®) 20, Oridion, Jerusalem, Israël) through a face mask (Capnomask(®), Mediplus Ltd, Raleigh, NC, USA) for 40-60 min. Of the 86,578 triplets collected, 77,155 (89.1%) were exploitable. Median (range) respiration rate measured by capnometry was 18 (7-29) bpm. Compared to capnometry, bias and limits of agreement were 0.1 ± 3.8 bpm for the acoustic method and 0.3 ± 5.5 bpm for thoracic impedance. The proportions of RR values collected by acoustic method or by thoracic impedance which differed over 10 or 20% during more than 15 s, compared to capnometry, were 8.3 versus 14.3, and 1.5 versus 3.8%, respectively (p face mask capnometry. PMID:25614223

  1. Chemometrics and the identification of counterfeit medicines-A review.

    Krakowska, B; Custers, D; Deconinck, E; Daszykowski, M

    2016-08-01

    This review article provides readers with a number of actual case studies dealing with verifying the authenticity of selected medicines supported by different chemometric approaches. In particular, a general data processing workflow is discussed with the major emphasis on the most frequently selected instrumental techniques to characterize drug samples and the chemometric methods being used to explore and/or model the analytical data. However, further discussion is limited to a situation in which the collected data describes two groups of drug samples - authentic ones and counterfeits. PMID:27133184

  2. Effect of emodin on Candida albicans growth investigated by microcalorimetry combined with chemometric analysis.

    Kong, W J; Wang, J B; Jin, C; Zhao, Y L; Dai, C M; Xiao, X H; Li, Z L

    2009-07-01

    Using the 3114/3115 thermal activity monitor (TAM) air isothermal microcalorimeter, ampoule mode, the heat output of Candida albicans growth at 37 degrees C was measured, and the effect of emodin on C. albicans growth was evaluated by microcalorimetry coupled with chemometric methods. The similarities between the heat flow power (HFP)-time curves of C. albicans growth affected by different concentrations of emodin were calculated by similarity analysis (SA). In the correspondence analysis (CA) diagram of eight quantitative parameters taken from the HFP-time curves, it could be deduced that emodin had definite dose-effect relationship as the distance between different concentrations of it increased along with the dosage and the effect. From the principal component analysis (PCA) on eight quantitative parameters, the action of emodin on C. albicans growth could be easily evaluated by analyzing the change of values of the main two parameters, growth rate constant k (2) and maximum power output P(2)(m). The coherent results of SA, CA, and PCA showed that emodin at different concentrations had different effects on C. albicans growth metabolism: A low concentration (0-10 microg ml(-1)) poorly inhibited the growth of C. albicans, and a high concentration (15-35 microg ml(-1)) could notably inhibit growth of this fungus. This work provided a useful idea of the combination of microcalorimetry and chemometric analysis for investigating the effect of drug and other compounds on microbes. PMID:19543891

  3. Acoustic engineering and technology '90

    Acoustic monitoring, testing and diagnosis in machines, production processes and products enhance the uptimes and profitability of machinery and plants. 18 papers discuss the current state of the art of acoustic monitoring systems including integrated factory planning as well as industrial health, and noise protection. (DG)

  4. Chemometric methods and near-infrared spectroscopy applied to bioenergy production

    The present work examines bioenergy production from different viewpoints. The three main objectives are: (1) to reveal the relation of technology, sustainability and economy in bioenergy processes; (2) to investigate spectroscopic methods as a tool for analytical monitoring of bioenergy processes; and (3) to develop new chemometric methods for advanced analysis of spectroscopic data. At the first stage, this thesis investigates the technological, ecological, and economic features of renewable-resource-based and de-centralized bioenergy production systems. In different scenarios, small-scale bioethanol production is combined with other technologies that provide renewable energy from residuals of the bioethanol process. The general aim is to substitute fossil energy conventionally used within the bioethanol process. The investigated technologies are biogas production and straw incineration. Agricultural aspects are introduced by sustainable crop rotation concepts that reconcile food, feed, and biofuel production. The sustainability of small-scale bioethanol production in the different scenarios is quantified by an ecological footprint method, the sustainable process index, SPI, and compared to conventional fuels. The main findings are: (i) small-scaled bioethanol production can be operated with 100 % renewable energy supply, (ii) the SPI of bioethanol can be reduced up to 92 % compared to conventional fuels, (iii) a complex trade-off between ecology-of-scale and economy-of-scale is necessary. At the second stage, this thesis approaches bioenergy production processes from an analytical perspective, and presents near-infrared spectroscopy (NIR) as promising method for fast process monitoring of bioethanol production and biomass characterization. In addition, new analytical methods are presented for a fast determination of the heating value of solid biomass fuel, based on IR and NIR spectroscopy. The main findings are that NIR spectroscopy and appropriate chemometric

  5. Chemometrics in multispectral imaging for quality inspection of postharvest products

    Noordam, Jan Corstiaan

    2005-01-01

    This thesis describes different novel chemometric techniques applied to multispectral images for quality inspection on agricultural food products. These images do not only have a huge number of spectral bands which makes training set selection a challenging task, they also contain classes with small

  6. Monitoring microstructural evolution of alloy 617 with non-linear acoustics for remaining useful life prediction; multiaxial creep-fatigue and creep-ratcheting

    Lissenden, Cliff [Pennsylvania State Univ., State College, PA (United States); Hassan, Tasnin [North Carolina State Univ., Raleigh, NC (United States); Rangari, Vijaya [Tuskegee Univ., Tuskegee, AL (United States)

    2014-10-30

    The research built upon a prior investigation to develop a unified constitutive model for design-­by-­analysis of the intermediate heat exchanger (IHX) for a very high temperature reactor (VHTR) design of next generation nuclear plants (NGNPs). Model development requires a set of failure data from complex mechanical experiments to characterize the material behavior. Therefore uniaxial and multiaxial creep-­fatigue and creep-­ratcheting tests were conducted on the nickel-­base Alloy 617 at 850 and 950°C. The time dependence of material behavior, and the interaction of time dependent behavior (e.g., creep) with ratcheting, which is an increase in the cyclic mean strain under load-­controlled cycling, are major concerns for NGNP design. This research project aimed at characterizing the microstructure evolution mechanisms activated in Alloy 617 by mechanical loading and dwell times at elevated temperature. The acoustic harmonic generation method was researched for microstructural characterization. It is a nonlinear acoustics method with excellent potential for nondestructive evaluation, and even online continuous monitoring once high temperature sensors become available. It is unique because it has the ability to quantitatively characterize microstructural features well before macroscale defects (e.g., cracks) form. The nonlinear acoustics beta parameter was shown to correlate with microstructural evolution using a systematic approach to handle the complexity of multiaxial creep-­fatigue and creep-­ratcheting deformation. Mechanical testing was conducted to provide a full spectrum of data for: thermal aging, tensile creep, uniaxial fatigue, uniaxial creep-­fatigue, uniaxial creep-ratcheting, multiaxial creep-fatigue, and multiaxial creep-­ratcheting. Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), and Optical Microscopy were conducted to correlate the beta parameter with individual microstructure mechanisms. We researched

  7. Monitoring microstructural evolution of alloy 617 with non-linear acoustics for remaining useful life prediction; multiaxial creep-fatigue and creep-ratcheting

    The research built upon a prior investigation to develop a unified constitutive model for design-@by-@analysis of the intermediate heat exchanger (IHX) for a very high temperature reactor (VHTR) design of next generation nuclear plants (NGNPs). Model development requires a set of failure data from complex mechanical experiments to characterize the material behavior. Therefore uniaxial and multiaxial creep-@fatigue and creep-@ratcheting tests were conducted on the nickel base Alloy 617 at 850 and 950°C. The time dependence of material behavior, and the interaction of time dependent behavior (e.g., creep) with ratcheting, which is an increase in the cyclic mean strain under load-@controlled cycling, are major concerns for NGNP design. This research project aimed at characterizing the microstructure evolution mechanisms activated in Alloy 617 by mechanical loading and dwell times at elevated temperature. The acoustic harmonic generation method was researched for microstructural characterization. It is a nonlinear acoustics method with excellent potential for nondestructive evaluation, and even online continuous monitoring once high temperature sensors become available. It is unique because it has the ability to quantitatively characterize microstructural features well before macroscale defects (e.g., cracks) form. The nonlinear acoustics beta parameter was shown to correlate with microstructural evolution using a systematic approach to handle the complexity of multiaxial creep-@fatigue and creep-@ratcheting deformation. Mechanical testing was conducted to provide a full spectrum of data for: thermal aging, tensile creep, uniaxial fatigue, uniaxial creep-@fatigue, uniaxial creep-ratcheting, multiaxial creep-fatigue, and multiaxial creep-@ratcheting. Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), and Optical Microscopy were conducted to correlate the beta parameter with individual microstructure mechanisms. We researched application of the

  8. Real-time monitoring of focused ultrasound blood-brain barrier opening via subharmonic acoustic emission detection: implementation of confocal dual-frequency piezoelectric transducers

    Tsai, Chih-Hung; Zhang, Jia-Wei; Liao, Yi-Yi; Liu, Hao-Li

    2016-04-01

    Burst-tone focused ultrasound exposure in the presence of microbubbles has been demonstrated to be effective at inducing temporal and local opening of the blood-brain barrier (BBB), which promises significant clinical potential to deliver therapeutic molecules into the central nervous system (CNS). Traditional contrast-enhanced imaging confirmation after focused ultrasound (FUS) exposure serves as a post-operative indicator of the effectiveness of FUS-BBB opening, however, an indicator that can concurrently report the BBB status and BBB-opening effectiveness is required to provide effective feedback to implement this treatment clinically. In this study, we demonstrate the use of subharmonic acoustic emission detection with implementation on a confocal dual-frequency piezoelectric ceramic structure to perform real-time monitoring of FUS-BBB opening. A confocal dual-frequency (0.55 MHz/1.1 MHz) focused ultrasound transducer was designed. The 1.1 MHz spherically-curved ceramic was employed to deliver FUS exposure to induce BBB-opening, whereas the outer-ring 0.55 MHz ceramic was employed to detect the subharmonic acoustic emissions originating from the target position. In stage-1 experiments, we employed spectral analysis and performed an energy spectrum density (ESD) calculation. An optimized 0.55 MHz ESD level change was shown to effectively discriminate the occurrence of BBB-opening. Wideband acoustic emissions received from 0.55 MHz ceramics were also analyzed to evaluate its correlations with erythrocyte extravasations. In stage-2 real-time monitoring experiments, we applied the predetermined ESD change as a detection threshold in PC-controlled algorithm to predict the FUS exposure intra-operatively. In stage-1 experiment, we showed that subharmonic ESD presents distinguishable dynamics between intact BBB and opened BBB, and therefore a threshold ESD change level (5.5 dB) can be identified for BBB-opening prediction. Using this ESD change threshold detection as a

  9. Use of Modal Acoustic Emission to Monitor Damage Progression in Carbon Fiber/Epoxy and Implications for Composite Structures

    Waller, J. M.; Nichols, C. T.; Wentzel, D. J.; Saulsberry R. L.

    2010-01-01

    Broad-band modal acoustic emission (AE) data was used to characterize micromechanical damage progression in uniaxial IM7 and T1000 carbon fiber-epoxy tows and an IM7 composite overwrapped pressure vessel (COPV) subjected to an intermittent load hold tensile stress profile known to activate the Felicity ratio (FR). Damage progression was followed by inspecting the Fast Fourier Transforms (FFTs) associated with acoustic emission events. FFT analysis revealed the occurrence of cooperative micromechanical damage events in a frequency range between 100 kHz and 1 MHz. Evidence was found for the existence of a universal damage parameter, referred to here as the critical Felicity ratio, or Felicity ratio at rupture (FR*), which had a value close to 0.96 for the tows and the COPV tested. The implications of using FR* to predict failure in carbon/epoxy composite materials and related composite components such as COPVs are discussed. Trends in the FFT data are also discussed; namely, the difference between the low and high energy events, the difference between early and late-life events, comparison of IM7 and T1000 damage progression, and lastly, the similarity of events occurring at the onset of significant acoustic emission used to calculate the FR.

  10. The autonomous acoustic buoy

    Pellicer, Francisco; Reitsma, Robert; Agüera, Joaquín; Marinas, Alexandra

    2013-01-01

    The Acoustic Buoy is a project between the Laboratory of Applied Bioacoustics (LAB) and the Universitat Politècnica de Catalunya (UPC). In areas that the human activities produce high noise levels, such as oil exploration or construction, there is a need to monitor the environment for the presence of cetaceans. Another need is for fishing, to prevent endangered species from being killed. This can be done with an Autonomous Acoustic Buoy (AAB). Mooring or anchoring at to the seaflo...

  11. In situ monitoring the pulse CO{sub 2} laser interaction with 316-L stainless steel using acoustical signals and plasma analysis

    Khosroshahi, M.E., E-mail: khosro@aut.ac.ir [Amirkabir University of Technology, Faculty of Biomedical Eng., Biomaterial Group, Laser and Nanobiophotonics Lab., Tehran (Iran, Islamic Republic of); Anoosheh pour, F. [Amirkabir University of Technology, Faculty of Biomedical Eng., Biomaterial Group, Laser and Nanobiophotonics Lab., Tehran (Iran, Islamic Republic of); Hadavi, M. [Amirkabir University of Technology, Faculty of Mining and Metallurgical Eng., Tehran (Iran, Islamic Republic of); Mahmoodi, M. [Amirkabir University of Technology, Faculty of Biomedical Eng., Biomaterial Group, Laser and Nanobiophotonics Lab., Tehran (Iran, Islamic Republic of)

    2010-10-01

    In most laser material processing, material removal by different mechanisms is involved. Here, application of acoustic signals with thermoelastic (below threshold) and breakdown origin (above threshold) together with plasma plume analysis as a simple monitoring system of interaction process is suggested. In this research the interaction of pulse CO{sub 2} laser with 200 ns duration and maximum energy of 1.3 J operating at 1 Hz with austenitic stainless steel (316-L) is reported. The results showed that the non-linear point of the curve can serve as a useful indicator of melting fluence threshold (in this case {approx}830 J cm{sup -2}) with corresponding temperature calculated using plasma plume analysis. Higher acoustic amplitudes and larger plasma plume volume indicates more intense interaction. Also, analysis showed that a phase explosion process with material removal (ejecta) in the form of non-adiabatic (i.e., d{sub t} >> {alpha}{sup -1}) is at play after laser pulse is ended. Also, SEM photographs show different surface quality medication at different laser intensities, which indicates the importance of recoil momentum pressure and possibly electrons and ions densities in heat transfer. Finally, electrochemical test indicate an improved corrosion resistance for laser treated samples compared to untreated ones.

  12. Intensive sound speed monitoring in ocean and its impact on the GPS/acoustic seafloor geodetic measurement

    Kido, Motoyuki

    2016-04-01

    GPS/acoustic (GPS/A) technique, based on GPS positioning and acoustic ranging, is now getting a popular tool to measure seafloor crustal movement. Several groups in the world have been intensively conducted campaign surveys in the region of scientifically interest. As the technology of measurement has been matured and plenty of data are accumulated, researchers are now aware of the limit of its precision mainly due to unexpected undulation of sound speed in ocean, which significantly degrades acoustic ranging. If sound speed structure keeps its figure during survey period, e.g., more than a couple of hours, it can be estimated by a moving survey to get sufficient paths from various directions to illustrate the structure. However the sound speed structure often varies quickly with in a hour due to internal gravitational wave excited by interaction of tidal current and seafloor topography. In this case one cannot separate temporal and spatial variations. We revisited our numerous sound speed profile data derived from numbers of XBT measurements, which were concurrently carried out with GPS/A survey along the Nankai Trough and Japan Trench. Among the measurements, we found notably short-period variation in sound speed profile through intensive XBT survey repeatedly cast every 6 minutes for one hour, which also appeared in residuals in traveltime of acoustic ranging. The same feature is also found in more moderate rate for semidiurnal undulation, in which vertical oscillation of the middle of the profile can be clearly seen rather than variation of absolute sound speed. This also reflects traveltime residuals in the GPS/A measurement. These typical frequencies represent dominant wavelengths of spatial sound speed variation. In the latter, local horizontal variation can be negligible in the vicinity of a point survey area and the traditional analysis can be applicable that assumes time-varying stratified sound speed structure. In the former case, on the contrary, local

  13. Program to develop acoustic emission: flaw relationship for inservice monitoring of nuclear pressure vessels. Progress report No. 1, July 1, 1976--February 1, 1977

    This is a laboratory research program to characterize acoustic emission (AE) from flaw growth and noise from innocuous sources in A533B Class 1 pressure vessel steel. The objectives are: characterize AE from a limited range of defects and material property conditions of concern to reactor pressure vessel integrity; characterize AE from innocuous sources (including defects); develop criteria for distinguishing significant flaws from innocuous sources; and develop an AE flaw damage model to serve as a basis for relating in-service AE to pressure vessel integrity. The purpose of the program is to build an experimental evaluation of the feasibility of detecting and analyzing flaw growth in reactor pressure boundaries by continuously monitoring for AE. A detailed program plan in the form of an analysis-before-test document has been prepared and approved

  14. Intraoperative facial motor evoked potentials monitoring with transcranial electrical stimulation for preservation of facial nerve function in patients with large acoustic neuroma

    LIU Bai-yun; TIAN Yong-ji; LIU Wen; LIU Shu-ling; QIAO Hui; ZHANG Jun-ting; JIA Gui-jun

    2007-01-01

    Background Although various monitoring techniques have been used routinely in the treatment of the lesions in the skull base, iatrogenic facial paresis or paralysis remains a significant clinical problem. The aim of this study was to investigate the effect of intraoperative facial motor evoked potentials monitoring with transcranial electrical stimulation on preservation of facial nerve function.Method From January to November 2005, 19 patients with large acoustic neuroma were treated using intraoperative facial motor evoked potentials monitoring with transcranial electrical stimulation (TCEMEP) for preservation of facial nerve function. The relationship between the decrease of MEP amplitude after tumor removal and the postoperative function of the facial nerve was analyzed.Results MEP amplitude decreased more than 75% in 11 patients, of which 6 presented significant facial paralysis (H-B grade 3), and 5 had mild facial paralysis (H-B grade 2). In the other 8 patients, whose MEP amplitude decreased less than 75%, 1 experienced significant facial paralysis, 5 had mild facial paralysis, and 2 were normal.Conclusions Intraoperative TCEMEP can be used to predict postoperative function of the facial nerve. The decreased MEP amplitude above 75 % is an alarm point for possible severe facial paralysis.

  15. Communication Acoustics

    Blauert, Jens

    Communication Acoustics deals with the fundamentals of those areas of acoustics which are related to modern communication technologies. Due to the advent of digital signal processing and recording in acoustics, these areas have enjoyed an enormous upswing during the last 4 decades. The book...... the book a source of valuable information for those who want to improve or refresh their knowledge in the field of communication acoustics - and to work their way deeper into it. Due to its interdisciplinary character Communication Acoustics is bound to attract readers from many different areas, such as......: acoustics, cognitive science, speech science, and communication technology....

  16. Determination of Commercials Cooking Oils and Fats Using Chemometrics Methods

    In this study, chemometric method has been used in determining the oil quality. The samples used were olive oil, sunflower oil and butter from two different brands. Two different conditions were applied, either it was fresh or fried. Titratio, a conventional method was used to determine free fatty acids content (FFA), iodine value (IV), and peroxide value (PV). Twelve samples were then used for analysis and their FTIR spectra were measured at 4000-400 cm-1. The computer stimulation was used to process the data based on their pattern recognition which optimized by principal component analysis (PCA) and partial least squares (PLS). PCA model was used to distinguish the properties between fresh and fried oil. The PLS model was used to predict the value for validation test in comparison with conventional results. Results showed the validation value for fresh oil was 0.90. This indicated the chemometric method was in agreement with conventional method. (author)

  17. Acoustic communication for Maya Autonomous Underwater Vehicle - performance evaluation of acoustic modem

    Afzulpurkar, S.; Maurya, P.; Navelkar, G.S.; Desa, E.S.; Mascarenhas, A.A.M.Q.; Dabholkar, N.A.; Madhan, R.; Prabhudesai, S.P.

    traffic. This necessitates monitoring the AUV status and data quality through an acoustic link which needs to perform reliably under such conditions, at long range. To address these situations partially, acoustic communication capability is planned...

  18. LEGACY - EOP Acoustic tagging and monitorings of cultured and wild juvenile crimson jobfish (Pristipomoides filamentosus) in a nursery habitat

    National Oceanic and Atmospheric Administration, Department of Commerce — Raw data from Vemco receivers that monitored the Kaneohe, Oahu nursery grounds while tagged juvenile snapper were released in 2006 (cultured) and 2007 (wild). Also...

  19. Bat Species Occurrence and Long-Term Bat Population Monitoring on Refuges Using Acoustical Detection - 2012-2015 Summary

    US Fish and Wildlife Service, Department of the Interior — Long-term trend monitoring efforts for bats on National Wildlife Refuges have been prompted by a paucity of significant population information and precipitous...

  20. Multivariate analysis and chemometric characterisation of textile wastewater streams:

    Kavšek, Darja; Bednárová, Adriána; Jerič, Tina; Vajnhandl, Simona; Majcen Le Marechal, Alenka; Brodnjak-Vončina, Darinka

    2013-01-01

    The aim of this work was to design a quick and reliable method for the evaluation and classification of wastewater streams into treatable and non-treatable effluents for reuse/recycling. Different chemometric methods were used for this purpose handling the enormous amount of data, and additionally to find any hidden information, which would increase our knowledge and improve the classification. The data obtained from the processes description, together with the analytical results of measured ...

  1. Acoustic Neuroma

    An acoustic neuroma is a benign tumor that develops on the nerve that connects the ear to the brain. The tumor ... press against the brain, becoming life-threatening. Acoustic neuroma can be difficult to diagnose, because the symptoms ...

  2. Acoustic Neuroma

    An acoustic neuroma is a benign tumor that develops on the nerve that connects the ear to the brain. ... can press against the brain, becoming life-threatening. Acoustic neuroma can be difficult to diagnose, because the ...

  3. Screening Brazilian commercial gasoline quality by hydrogen nuclear magnetic resonance spectroscopic fingerprintings and pattern-recognition multivariate chemometric analysis.

    Flumignan, Danilo Luiz; Boralle, Nivaldo; de Oliveira, José Eduardo

    2010-06-30

    The identification of gasoline adulteration by organic solvents is not an easy task, because compounds that constitute the solvents are already in gasoline composition. In this work, the combination of Hydrogen Nuclear Magnetic Resonance ((1)H NMR) spectroscopic fingerprintings with pattern-recognition multivariate Soft Independent Modeling of Class Analogy (SIMCA) chemometric analysis provides an original and alternative approach to screening Brazilian commercial gasoline quality in a Monitoring Program for Quality Control of Automotive Fuels. SIMCA was performed on spectroscopic fingerprints to classify the quality of representative commercial gasoline samples selected by Hierarchical Cluster Analysis (HCA) and collected over a 6-month period from different gas stations in the São Paulo state, Brazil. Following optimized the (1)H NMR-SIMCA algorithm, it was possible to correctly classify 92.0% of commercial gasoline samples, which is considered acceptable. The chemometric method is recommended for routine applications in Quality-Control Monitoring Programs, since its measurements are fast and can be easily automated. Also, police laboratories could employ this method for rapid screening analysis to discourage adulteration practices. PMID:20685442

  4. Application of chemometric methods for assessment and modelling of microbiological quality data concerning coastal bathing water in Greece

    Agelos Papaioannou

    2014-12-01

    Full Text Available Background. Worldwide, the aim of managing water is to safeguard human health whilst maintaining sustainable aquatic and associated terrestrial, ecosystems. Because human enteric viruses are the most likely pathogens responsible for waterborne diseases from recreational water use, but detection methods are complex and costly for routine monitoring, it is of great interest to determine the quality of coastal bathing water with a minimum cost and maximum safety. Design and methods. This study handles the assessment and modelling of the microbiological quality data of 2149 seawater bathing areas in Greece over 10-year period (1997-2006 by chemometric methods. Results. Cluster analysis results indicated that the studied bathing beaches are classified in accordance with the seasonality in three groups. Factor analysis was applied to investigate possible determining factors in the groups resulted from the cluster analysis, and also two new parameters were created in each group; VF1 includes E. coli, faecal coliforms and total coliforms and VF2 includes faecal streptococci/enterococci. By applying the cluster analysis in each seasonal group, three new groups of coasts were generated, group A (ultraclean, group B (clean and group C (contaminated. Conclusions. The above analysis is confirmed by the application of discriminant analysis, and proves that chemometric methods are useful tools for assessment and modeling microbiological quality data of coastal bathing water on a large scale, and thus could attribute to effective and economical monitoring of the quality of coastal bathing water in a country with a big number of bathing coasts, like Greece.

  5. Real-time monitoring of acoustic linear and nonlinear behavior of titanium alloys during low-cycle fatigue and high-cycle fatigue

    Frouin, Jerome; Sathish, Shamachary; Na, Jeong K.

    2000-05-01

    An in-situ technique to measure sound velocity, ultrasonic attenuation and acoustic nonlinear property has been developed for characterization and early detection of fatigue damage in aerospace materials. For this purpose we have developed a computer software and measurement technique including hardware for the automation of the measurement. New transducer holder and special grips are designed. The automation has allowed us to test the long-term stability of the electronics over a period of time and so proof of the linearity of the system. Real-time monitoring of the material nonlinearity has been performed on dog-bone specimens from zero fatigue all the way to the final fracture under low-cycle fatigue test condition (LCF) and high-cycle test condition (HCF). Real-time health monitoring of the material can greatly contribute to the understanding of material behavior under cyclic loading. Interpretation of the results show that correlation exist between the slope of the curve described by the material nonlinearity and the life of the component. This new methodology was developed with an objective to predict the initiation of fatigue microcracks, and to detect, in-situ fatigue crack initiation as well as to quantify early stages of fatigue damage.

  6. Acoustic emission monitoring of the cracking/spallation in the oxide scales developed over microstructurally different regions of a chrome-moly ferritic steel

    Acoustic emission (AE) monitoring has been used to confirm the difference in initiation and intensity of the cracking and spallation of the scales over the regions with different microstructures in 9Cr-1Mo steel. As indicated by in-air thermogravimetric (TG) tests at 973K, the oxide scale on 9Cr-1Mo steel with 0.26%Si and fine grain size (90μm) suffered a pronounced weight-loss after about 60min., where as the scale on the coarse grain (360μm) steel suffered weight-loss only after 240min. AE monitoring under identical conditions suggest sudden and pronounced increase in AE activity after the respective durations in the two cases. Hence, the weight losses in both cases have been ascribed to spallation of the oxide scale. As suggested both by TG and AE tests, onset of pronounced scale spallation is considerably delayed in the case of the steel with a higher (0.75%) Si-content. Hence it is concluded that increase in Si-content and grain size of 9Cr-1Mo steel improves spallation resistance at high temperatures. (author)

  7. Damage assessed by wavelet scale bands and b-value in dynamical tests of a reinforced concrete slab monitored with acoustic emission

    Zitto, Miguel E.; Piotrkowski, Rosa; Gallego, Antolino; Sagasta, Francisco; Benavent-Climent, Amadeo

    2015-08-01

    The complex Morlet Continuous Wavelet Transform (CWT) was applied to acoustic emission (AE) signals from dynamic tests conducted on a reinforced concrete slab with a shaking table. The steel reinforcement bars did not yield during the tests, but a severe loss of bond between reinforcement bars and surrounding concrete was detected. Comparison of the evolution of the scale position of maximum values of CWT coefficients and the histories of response acceleration obtained in different seismic simulations allowed us to identify the (45-64 kHz) frequency band corresponding to the fracture of concrete. The Cumulative Acoustic Emission Energy (CAE) obtained by reconstructing the AE signals in this scale (frequency) band was compared with the Cumulative Dissipated Energy (CDE) of the tested structure. The CDE is accepted as a good parameter for characterizing the mechanical damage in structures. A reasonably good agreement was found between the normalized histories of CAE and CDE. This made it possible to categorize the cracking of concrete as the main source of damage in the reinforced concrete slab. Conversely, the differences between the CAE and CDE curves observed for high levels of peak acceleration applied to the shaking table can be attributed to the deformation of the steel that formed the columns. The AE coming from the plastic deformation of the steel is not detected by CAE due to the threshold amplitude (45 dB) used in the AE monitoring, but the strain energy dissipated by the steel through plastic deformations is included in the CDE. Further, a study of the evolution of the b-value in the successive seismic simulations revealed that the b-value can capture the inception of severe cracking in the concrete, which the tests described in this study attributed mainly to the loss of bond between reinforcing steel and surrounding concrete.

  8. Structural health monitoring of liquid-filled tanks: a Bayesian approach for location of acoustic emission sources

    Acoustic emission (AE) is a well-established nondestructive testing method for assessing the condition of liquid-filled tanks. Often the tank can be tested without the need for accurate location of AE sources. But sometimes, accurate location is required, such as in the case of follow-up inspections after AE has indicated a significant defect. Traditional computed location techniques that considered only the wave traveling through the shell of the tank have not proved reliable when applied to liquid-filled tanks. This because AE sensors are often responding to liquid-borne waves, that are not considered in the traditional algorithms. This paper describes an approach for locating AE sources on the wall of liquid filled tanks that includes two novel aspects: (i) the use of liquid-borne waves, and (ii) the use of a probabilistic algorithm. The proposed algorithm is developed within a Bayesian framework that considers uncertainties in the wave velocities and the time of arrival. A Markov Chain Monte Carlo is used to estimate the distribution of the AE source location. This approach was applied on a 102 inch diameter (29 000 gal) railroad tank car by estimating the source locations from pencil lead break with waveforms recorded. Results show that the proposed Bayesian approach for source location can be used to calculate the most probable region of the tank wall where the AE source is located. (paper)

  9. COMBUSTION ACOUSTICS DIAGNOSTICS

    This is an Exploratory Research Project that was awarded by APPCD for research on developing an acoustic flame condition monitor. It will involve a bench scale experiment of 4-6 weeks duration to record adjacent audible energy of a Bunsen burner. The experiment will require a d...

  10. Latest Trends in Acoustic Sensing

    Cinzia Caliendo

    2014-03-01

    Full Text Available Acoustics-based methods offer a powerful tool for sensing applications. Acoustic sensors can be applied in many fields ranging from materials characterization, structural health monitoring, acoustic imaging, defect characterization, etc., to name just a few. A proper selection of the acoustic wave frequency over a wide spectrum that extends from infrasound (<20 Hz up to ultrasound (in the GHz–band, together with a number of different propagating modes, including bulk longitudinal and shear waves, surface waves, plate modes, etc., allow acoustic tools to be successfully applied to the characterization of gaseous, solid and liquid environments. The purpose of this special issue is to provide an overview of the research trends in acoustic wave sensing through some cases that are representative of specific applications in different sensing fields.

  11. Application of chemometric techniques to classify the quality of surface water in the watershed of the river Bermudez in Heredia, Costa Rica

    The application of selected chemometric techniques have been investigated: cluster analysis, principal component analysis and factor analysis, to classify the quality of rivers water and evaluate pollution data. Fourteen physicochemical parameters were monitored at 10 stations located in the watershed of the river Bermudez, from August 2005 to February 2007. The results have identified the existence of two natural clusters of monitoring sites with similar characteristics of contamination and identify the DQO, DBO, NO3-, SO4-2 and SST, as the main variables that discriminate between sampling sites. (author)

  12. Experimental study on CO2 monitoring and saturation with combined acoustic velocity and electrical resistivity in sandstone reservoirs

    Omolo, Lamech Omondi

    2015-01-01

    CO2 storage is considered as one of the most promising solutions to overcome global increase in temperature. In order to ensure the safety of the sequestrated CO2, several geophysical monitoring methods are required, among them electrical resistivity and seismic velocity which depends on porosity, texture, mineralogy and fluid saturation. However, seismic data seldom allow us to estimate saturation accurately in geological reservoirs. On the other hand, resistivity is very sensitive to porosi...

  13. Acoustic cloaking and transformation acoustics

    Chen Huanyang [School of Physical Science and Technology, Soochow University, Suzhou, Jiangsu 215006 (China); Chan, C T, E-mail: kenyon@ust.h, E-mail: phchan@ust.h [Department of Physics and the William Mong Institute of NanoScience and Technology, The Hong Kong University of Science and Technology, Clear Water Bay (Hong Kong)

    2010-03-24

    In this review, we give a brief introduction to the application of the new technique of transformation acoustics, which draws on a correspondence between coordinate transformation and material properties. The technique is formulated for both acoustic waves and linear liquid surface waves. Some interesting conceptual devices can be designed for manipulating acoustic waves. For example, we can design acoustic cloaks that make an object invisible to acoustic waves, and the cloak can either encompass or lie outside the object to be concealed. Transformation acoustics, as an analog of transformation optics, can go beyond invisibility cloaking. As an illustration for manipulating linear liquid surface waves, we show that a liquid wave rotator can be designed and fabricated to rotate the wave front. The acoustic transformation media require acoustic materials which are anisotropic and inhomogeneous. Such materials are difficult to find in nature. However, composite materials with embedded sub-wavelength resonators can in principle be made and such 'acoustic metamaterials' can exhibit nearly arbitrary values of effective density and modulus tensors to satisfy the demanding material requirements in transformation acoustics. We introduce resonant sonic materials and Helmholtz resonators as examples of acoustic metamaterials that exhibit resonant behaviour in effective density and effective modulus. (topical review)

  14. Acoustic cloaking and transformation acoustics

    In this review, we give a brief introduction to the application of the new technique of transformation acoustics, which draws on a correspondence between coordinate transformation and material properties. The technique is formulated for both acoustic waves and linear liquid surface waves. Some interesting conceptual devices can be designed for manipulating acoustic waves. For example, we can design acoustic cloaks that make an object invisible to acoustic waves, and the cloak can either encompass or lie outside the object to be concealed. Transformation acoustics, as an analog of transformation optics, can go beyond invisibility cloaking. As an illustration for manipulating linear liquid surface waves, we show that a liquid wave rotator can be designed and fabricated to rotate the wave front. The acoustic transformation media require acoustic materials which are anisotropic and inhomogeneous. Such materials are difficult to find in nature. However, composite materials with embedded sub-wavelength resonators can in principle be made and such 'acoustic metamaterials' can exhibit nearly arbitrary values of effective density and modulus tensors to satisfy the demanding material requirements in transformation acoustics. We introduce resonant sonic materials and Helmholtz resonators as examples of acoustic metamaterials that exhibit resonant behaviour in effective density and effective modulus. (topical review)

  15. Acoustical Imaging

    Litniewski, Jerzy; Kujawska, Tamara; 31st International Symposium on Acoustical Imaging

    2012-01-01

    The International Symposium on Acoustical Imaging is a unique forum for advanced research, covering new technologies, developments, methods and theories in all areas of acoustics. This interdisciplinary Symposium has been taking place continuously since 1968. In the course of the years the proceedings volumes in the Acoustical Imaging Series have become a reference for cutting-edge research in the field. In 2011 the 31st International Symposium on Acoustical Imaging was held in Warsaw, Poland, April 10-13. Offering both a broad perspective on the state-of-the-art as well as  in-depth research contributions by the specialists in the field, this Volume 31 in the Series contains an excellent collection of papers in six major categories: Biological and Medical Imaging Physics and Mathematics of Acoustical Imaging Acoustic Microscopy Transducers and Arrays Nondestructive Evaluation and Industrial Applications Underwater Imaging

  16. Application of NIR chemometric methods for quantification of the crystalline fraction of warfarin sodium in drug product.

    Korang-Yeboah, Maxwell; Akhtar, Sohail; Siddiqui, Akhtar; Rahman, Ziyaur; Khan, Mansoor A

    2016-01-01

    Monitoring of the physical state of warfarin sodium (WS) in products is essential for minimizing product quality variability in order to ensure consistent clinical performance. This study reports the development of chemometric models for quantifying the crystalline and amorphous fractions of WS in commercial drug products using NIR spectroscopy. Formulations based on commercially available products with different API to excipient ratio were used for the study. For each content, two formulations containing either lactose monohydrate or lactose anhydrous as the predominant formulation excipient were prepared. Two formulations containing either 100% amorphous WS (AWS) or crystalline WS (CWS) were prepared and mixed in various ratios to obtain sample matrices containing AWS/CWS 0-100%. The uniformity of the samples was confirmed by near infrared chemical imaging. Data were mathematically pretreated by multiplicative signal correction and Savitzky-Golay second derivative. Principal component regression and partial least square regression models were developed from mathematically treated data. All the models showed linear trend for amorphous and crystalline fractions of the WS as indicated by correlation and R(2) > 0.99 and >0.98, respectively. The models demonstrated good performance parameters with a low-root mean squared error, standard error and bias. The model predicted CWS and AWS contents were in very close agreement with the actual values. The study indicated the utility of NIR chemometric methods in quantification of the crystalline and/or amorphous fraction of WS in its products. PMID:26161939

  17. Food intake monitoring: an acoustical approach to automated food intake activity detection and classification of consumed food

    Obesity and nutrition-related diseases are currently growing challenges for medicine. A precise and timesaving method for food intake monitoring is needed. For this purpose, an approach based on the classification of sounds produced during food intake is presented. Sounds are recorded non-invasively by miniature microphones in the outer ear canal. A database of 51 participants eating seven types of food and consuming one drink has been developed for algorithm development and model training. The database is labeled manually using a protocol with introductions for annotation. The annotation procedure is evaluated using Cohen's kappa coefficient. The food intake activity is detected by the comparison of the signal energy of in-ear sounds to environmental sounds recorded by a reference microphone. Hidden Markov models are used for the recognition of single chew or swallowing events. Intake cycles are modeled as event sequences in finite-state grammars. Classification of consumed food is realized by a finite-state grammar decoder based on the Viterbi algorithm. We achieved a detection accuracy of 83% and a food classification accuracy of 79% on a test set of 10% of all records. Our approach faces the need of monitoring the time and occurrence of eating. With differentiation of consumed food, a first step toward the goal of meal weight estimation is taken. (paper)

  18. Prediction of class membership of biodiesels using chemometrics.

    Mustafa, Zylia; Milina, Rumyana; Simeonova, Pavlina A; Tsakovski, Stefan L; Simeonov, Vasil D

    2015-01-01

    Recently, serious scientific and technological attention is paid to creation of alternative energy sources, including biofuels. The assessment of the quality of the biofuels produced and of the raw materials needed for the production technology is an important scientific challenge. One of the major sources for biodiesel production is plant oils material (sunflower, rapeseed, palm, soya etc.). Since plants are complex system from the biota it is not easy to find specific chemical components responsible for their ability to serve as biodiesels. The characterization and classification of plant sources as biofuel material could be reliably estimated only by the use of multivariate statistical approaches (chemometrics). The chemometric expertise makes it possible not only to classify different biofuel sources into similarity classes but also to predict the membership of unknown by origin chemically analyzed samples to already existing classes. The present study deals with the prediction of the class membership of several unknown by origin samples, which are included in a large data set with FAME profiles of biodiesel plant sources. Using a data set from chromatographic analysis of fatty acid methyl esters profiles (FAME) of different plant biodiesel sources and applying the chemometric technique know as partial least squares-discriminant analysis (PLS - DA) a pattern recognition procedure is developed to: I. Model classes of similarity of biodiesel plant sources using their FAME profiles not taking into account the samples with unknown origin; II. Classify correctly the samples with unknown origin to the previously defined classes of biodiesel sources (palm oil, soybean oil, peanut oil, rapeseed oil, sunflower oil and maize oil). The prediction is successfully achieved for all samples with previously unknown origin. This pattern recognition approach is applied for the first time in the field of biodiesel classification and modeling tasks. PMID:25438133

  19. Chemometrics approach to substrate development, case: semisyntetic cheese

    Nielsen, Per Væggemose; Hansen, Birgitte Vedel

    1998-01-01

    from food production facilities.The Chemometrics approach to substrate development is illustrated by the development of a semisyntetic cheese substrate. Growth, colour formation and mycotoxin production of 6 cheese related fungi were studied on 9 types of natural cheeses and 24 synthetic cheese......, the most frequently occurring contaminant on semi-hard cheese. Growth experiments on the substrate were repeatable and reproducible. The substrate was also suitable for the starter P. camemberti. Mineral elements in cheese were shown to have strong effect on growth, mycotoxin production and colour...

  20. Acoustic Emission Health Monitoring of Fill Purge COPV's Used in Aerospace and Automotive Applications and Designed for Long Cycle Life

    Waller, Jess

    2013-01-01

    Cumulative composite damage in composite pressure vessels (CPVs) currently is not monitored on-orbit. Consequently, hazards due to catastrophic burst before leak (BBL) or compromised CPV reliability cannot be ascertained or mitigated, posing a risk to crew and mission assurance. The energy associated with CPV rupture can be significant, especially with high pressure gases are under containment, and the energy releases can be severe enough to cause injury, death, loss of assets or mission. Dual-Use Rationale: CPVs similar to those used by NASA on ISS, for example, are finding increasing use in automotive and transportation industry applications. These CPVs generally have a nonload sharing liner and are repeatedly filled over their service lifetime, typically with hydrogen or compressed natural gas (CNG). The same structural health monitoring equipment and software developed by NASA WSTF for evaluating, in real-time, the health of NASA CPVs on ISS will be used to evaluate the health of automotive CPVs, the only differences being the type and design of the CPV, and the in-service lifetime pressure histories. HSF Need(s)/Performance Characteristic(s) Supported: 1) Enable on-board vehicle systems management for mission critical functions at destinations with > 3 second time delay 2) Enable autonomous nominal operations and FDIR for crewed and un-crewed systems 3) Reduce on-board crew time to sustain and manage vehicle by factor of 2x at destinations with > 6 second time delay (see Crew Autonomy sheet) 4) Reduce earth-based mission ops "back room engineering" requirements for distant mission support delay (see Mission Autonomy sheet)

  1. 大型听神经瘤显微切除术中电生理监测的临床意义%Clinical significance of neurophysiological monitoring in microsurgery for large acoustic neuroma

    戴易; 徐善水; 江晓春; 陶进; 陈建民; 王宣之; 狄广福; 夏大勇

    2012-01-01

    目的:探讨大型听神经瘤显微切除术中电生理监测对面神经功能的保护技巧及意义.方法:以2008年10月~2012年2月术中行电生理监测者为监测组(n=37),2006年1月~2008年7月术中未行电生理监测者为对照组(n=31).统计分析两组肿瘤全切除率、面神经解剖和功能保留率.结果:监测组的肿瘤全切除率、面神经解剖和功能保留率均明显高于对照组(P<0.05).结论:听神经瘤术中行电生理监测可有效保护面神经功能.%Objective: To assess the clinical significance of applying neurophysiological monitoring to preventing the facial nerve from injury during microsurgery of large acoustic neuroma. Methods: Between Oct. 2008 and Feb. 2012, 37 patients with large acoustic neuroma undergone microsurgery assisted with neurophysiological monitoring were recruited as monitored group, while another 31 undergone the similar surgery between Jan. 2006 and Jul. 2008 without monitoring were included in control group. Two groups were statistically compared regarding the total resection rate for the tumor, rates for both facial anatomical retaining and intact facial nerve function. Results: The results were significantly better in the monitored group than the control group concerning the total resection rate for the mass, retained anatomical facial nerve and facial nerve function pre-served( P < 0. 05 ). Conclusion: Applying neurophysiological monitoring to microsurgery for large acoustic neuroma may lead to preservation of facial nerve function.

  2. Acoustic emission monitoring of tensile testing of corroded and un-corroded clad aluminum 2024-T3 and characterization of effects of corrosion on AE source events and material tensile properties

    Okafor, A. Chukwujekwu; Natarajan, Shridhar

    2014-02-01

    Corrosion damage affects structural integrity and deteriorates material properties of aluminum alloys in aircraft structures. Acoustic Emission (AE) is an effective nondestructive evaluation (NDE) technique for monitoring such damages and predicting failure in large structures of an aircraft. For successful interpretation of data from AE monitoring, sources of AE and factors affecting it need to be identified. This paper presents results of AE monitoring of tensile testing of corroded and un-corroded clad Aluminum 2024-T3 test specimens, and characterization of the effects of strain-rate and corrosion damage on material tensile properties and AE source events. Effect of corrosion was studied by inducing corrosion in the test specimens by accelerated corrosion testing in a Q-Fog accelerated corrosion chamber for 12 weeks. Eight (8) masked dog-bone shaped specimens were placed in the accelerated corrosion chamber at the beginning of the test. Two (2) dog-bone shaped specimens were removed from the corrosion chamber after exposure time of 3, 6, 9, and 12 weeks respectively, and subjected to tension testing till specimen failure along with AE monitoring, as well as two (2) reference samples not exposed to corrosion. Material tensile properties (yield strength, ultimate tensile strength, toughness, and elongation) obtained from tension test and AE parameters obtained from AE monitoring were analyzed and characterized. AE parameters increase with increase in exposure period of the specimens in the corrosive environment. Aluminum 2024-T3 is an acoustically silent material during tensile deformation without any damage. Acoustic emission events increase with increase of corrosion damage and with increase in strain rate above a certain value. Thus AE is suitable for structural health monitoring of corrosion damage. Ultimate tensile strength, toughness and elongation values decrease with increase of exposure period in corrosion chamber.

  3. Aespoe Hard Rock Laboratory. Prototype Repository. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2007 and March 2008

    Duckworth, D.; Haycox, J.; Pettitt, W.S. (Applied Seismology Consultants, Shrewsbury (United Kingdom))

    2008-12-15

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The experiment has been designed to simulate a disposal tunnel in a real deep repository environment for storage of high-level radioactive waste. The test consists of a 90 m long, 5 m diameter subhorizontal tunnel excavated in dioritic granite. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and pore pressures induced from tunnel sealing.

  4. 声发射技术在抽杆疲劳实验中的应用%Application of acoustic emission (AE) technique in crack monitor during fatigue test of pump rods

    夏永发; 李海玲

    2007-01-01

    The acoustic emission(AE)real time monitoring of fatigue damage of pump rods samples during fatigue test was introduced.Under severe environmental noise caused by vibration,the real time monitoring of the fatigue crack initiation and expansion was realized successfully by using the parameters analysis method combined by AE Hits and Amplitude.The characters of the methods are simple and real time,which can provide a more accurate and impersonal basis for judging whether the fatigue test piece has been destroyed,thus can provide a scientific assistant method for accurately determining the life of pump rod.

  5. Practical acoustic emission testing

    2016-01-01

    This book is intended for non-destructive testing (NDT) technicians who want to learn practical acoustic emission testing based on level 1 of ISO 9712 (Non-destructive testing – Qualification and certification of personnel) criteria. The essential aspects of ISO/DIS 18436-6 (Condition monitoring and diagnostics of machines – Requirements for training and certification of personnel, Part 6: Acoustic Emission) are explained, and readers can deepen their understanding with the help of practice exercises. This work presents the guiding principles of acoustic emission measurement, signal processing, algorithms for source location, measurement devices, applicability of testing methods, and measurement cases to support not only researchers in this field but also and especially NDT technicians.

  6. Radiation acoustics

    Lyamshev, Leonid M

    2004-01-01

    Radiation acoustics is a developing field lying at the intersection of acoustics, high-energy physics, nuclear physics, and condensed matter physics. Radiation Acoustics is among the first books to address this promising field of study, and the first to collect all of the most significant results achieved since research in this area began in earnest in the 1970s.The book begins by reviewing the data on elementary particles, absorption of penetrating radiation in a substance, and the mechanisms of acoustic radiation excitation. The next seven chapters present a theoretical treatment of thermoradiation sound generation in condensed media under the action of modulated penetrating radiation and radiation pulses. The author explores particular features of the acoustic fields of moving thermoradiation sound sources, sound excitation by single high-energy particles, and the efficiency and optimal conditions of thermoradiation sound generation. Experimental results follow the theoretical discussions, and these clearl...

  7. Feature optimization in chemometric algorithms for explosives detection

    Pinkham, Daniel W.; Bonick, James R.; Woodka, Marc D.

    2012-06-01

    This paper details the use of a genetic algorithm (GA) as a method to preselect spectral feature variables for chemometric algorithms, using spectroscopic data gathered on explosive threat targets. The GA was applied to laserinduced breakdown spectroscopy (LIBS) and ultraviolet Raman spectroscopy (UVRS) data, in which the spectra consisted of approximately 10000 and 1000 distinct spectral values, respectively. The GA-selected variables were examined using two chemometric techniques: multi-class linear discriminant analysis (LDA) and support vector machines (SVM), and the performance from LDA and SVM was fed back to the GA through a fitness function evaluation. In each case, an optimal selection of features was achieved within 20 generations of the GA, with few improvements thereafter. The GA selected chemically significant signatures, such as oxygen and hydron peaks from LIBS spectra and characteristic Raman shifts for AN, TNT, and PETN. Successes documented herein suggest that this GA approach could be useful in analyzing spectroscopic data in complex environments, where the discriminating features of desired targets are not yet fully understood.

  8. Aespoe Hard Rock Laboratory. Prototype Repository. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2008 and September 2008

    Duckworth, D.; Haycox, J.; Pettitt, W.S. (Applied Seismology Consultants, Shrewsbury (United Kingdom))

    2009-03-15

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation [Pettitt et al., 1999], and during stages of canister heating and tunnel pressurisation [Haycox et al., 2005a and 2005b; Haycox et al., 2006a and 2006b; Zolezzi et al., 2007 and Duckworth et al., 2008]. Further information on this monitoring can be found in Appendix I. This report covers the period between 1st April 2008 and 30th September 2008 and is the seventh instalment of the 6-monthly processing and interpretation of the results from the experiment.

  9. Aespoe Hard Rock Laboratory. Prototype Repository. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2008 and September 2008

    This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation [Pettitt et al., 1999], and during stages of canister heating and tunnel pressurisation [Haycox et al., 2005a and 2005b; Haycox et al., 2006a and 2006b; Zolezzi et al., 2007 and Duckworth et al., 2008]. Further information on this monitoring can be found in Appendix I. This report covers the period between 1st April 2008 and 30th September 2008 and is the seventh instalment of the 6-monthly processing and interpretation of the results from the experiment

  10. Outcomes of facial nerve reservation during acoustic neuroma surgery under neural electrophysiological monitoring%神经电生理监测在听神经瘤切除术中保留面神经的效果

    张旸; 徐海涛; 许媛; 陆小明; 刘宁; 鲁艾林

    2015-01-01

    Objective To summarize the outcomes of facial nerve reservation during acoustic neuroma surgery under neural electrophysiological monitoring .Methods Acoustic neuroma resection under microscope was performed via suboccipital retrosigmoid approach in 161 patients .Intraoperative continuous monitoring of evoked potential of the facial nerve was carried out during operation .The facial nerve function was valuated during and after surgery .Results The results of facial nerve function after surgery in 101 cases were consistent with those monitored during operation with an accordance rate of 62.7% .Conclusion The anatomy and facial nerve reservation during acoustic neuroma resection can be improved by intraoperative continuous monitoring of evoked potential of the facial nerve .Some interference factors need to be eliminated in order to improve the accuracy of intraoperative neurophysiological monitoring .%目的:总结电生理监测对听神经瘤术中保留面神经的效果。方法听神经瘤患者161例,采用经枕下乙状窦后入路,显微镜下实施听神经瘤切除术。术中采用神经电生理技术监测面神经诱发电位;术中和术后评估面神经功能。结果术后面神经功能评估结果与术中神经电生理监测结果一致率为62.7%(101/161)。结论神经电生理监测技术应用于听神经瘤显微外科手术可提高面神经解剖和神经功能保留效果;但同时应排除干扰因素,提高电生理监测的准确性。

  11. Monitoring microbe-induced physical property changes using high-frequency acoustic waveform data: Toward the development of a microbial megascope

    Williams, Kenneth Hurst

    2002-05-20

    A laboratory investigation was undertaken to determine the effect of microbe generated gas bubbles in controlled, saturated sediment columns utilizing a novel technique involving acoustic wave propagation. Specifically, the effect of denitrifying bacteria on saturated flow conditions was evaluated in light of the stimulated production of N{sub 2} gas and the resulting plugging of the pore throats. The propagation of high frequency acoustic waves through the sediment columns was used to locate those regions in the column where gas accumulation occurred. Over a period of six weeks, regions of gas accumulation resulted in the attenuation of acoustic wave energies with the decreases in amplitude typically greater than one order of magnitude.

  12. Assessing the performance of the photo-acoustic infrared gas monitor for measuring CO(2), N(2)O, and CH(4) fluxes in two major cereal rotations.

    Tirol-Padre, Agnes; Rai, Munmun; Gathala, Mahesh; Sharma, Sheetal; Kumar, Virender; Sharma, Parbodh C; Sharma, Dinesh K; Wassmann, Reiner; Ladha, Jagdish

    2014-01-01

    Rapid, precise, and globally comparable methods for monitoring greenhouse gas (GHG) fluxes are required for accurate GHG inventories from different cropping systems and management practices. Manual gas sampling followed by gas chromatography (GC) is widely used for measuring GHG fluxes in agricultural fields, but is laborious and time-consuming. The photo-acoustic infrared gas monitoring system (PAS) with on-line gas sampling is an attractive option, although it has not been evaluated for measuring GHG fluxes in cereals in general and rice in particular. We compared N2 O, CO2 , and CH4 fluxes measured by GC and PAS from agricultural fields under the rice-wheat and maize-wheat systems during the wheat (winter), and maize/rice (monsoon) seasons in Haryana, India. All the PAS readings were corrected for baseline drifts over time and PAS-CH4 (PCH4 ) readings in flooded rice were corrected for water vapor interferences. The PCH4 readings in ambient air increased by 2.3 ppm for every 1000 mg cm(-3) increase in water vapor. The daily CO2 , N2 O, and CH4 fluxes measured by GC and PAS from the same chamber were not different in 93-98% of all the measurements made but the PAS exhibited greater precision for estimates of CO2 and N2 O fluxes in wheat and maize, and lower precision for CH4 flux in rice, than GC. The seasonal GC- and PAS-N2 O (PN2 O) fluxes in wheat and maize were not different but the PAS-CO2 (PCO2 ) flux in wheat was 14-39% higher than that of GC. In flooded rice, the seasonal PCH4 and PN2 O fluxes across N levels were higher than those of GC-CH4 and GC-N2 O fluxes by about 2- and 4fold, respectively. The PAS (i) proved to be a suitable alternative to GC for N2 O and CO2 flux measurements in wheat, and (ii) showed potential for obtaining accurate measurements of CH4 fluxes in flooded rice after making correction for changes in humidity. PMID:23929733

  13. 小型矿山声发射监测与强地压活动预测%Acoustic Emission Monitoring and Predict of Strong Ground Pressure Activities in Small Mines

    欧阳治华; 江露

    2012-01-01

    鄂东地区许多小型矿山经多年空场法开采,已形成大量采空区。资金缺乏使得小型矿山只能选用简易的单通道YSSC型岩体声发射监测仪,人工定时定点读数,监测重点区域。以垴窖铁矿为例,通过有限元数值分析,将声发射监测点布置在声发射源可能发生的区域(即应力集中区),解决该仪器无法对声发射源定位的问题。信号去噪则是通过非生产时段的声发射监测,直接避免噪音干扰监测数据,提高预测强地压活动的准确性,以保证矿山安全生产。%There is a large number of mined-out areas in small-scale mines,eastern Hubei,because of mining with open stoping method for several years.For lack of funds,the small-scale mines can only select YSSC single-channel acoustic emission instrument to monitor ground pressure activations in some major areas,with artificial record of data at a fixed time.Taking Naojiao iron mine as an example,acoustic emission monitoring points was arranged at the area(stress concentration area) in which acoustic emission source might occur based on the finite element analysis,so as to solve the problem that this instrument can not located acoustic emission source.Single de-noising was achieved by acoustic emission monitoring in non-production periods to avoid the noise disturbing the monitoring data directly,then the accuracy of forecasting in strong ground pressure activities could be enhanced,in order to ensure mine safety.

  14. Characterization and Classification of Crude Oils Using a Combination of Spectroscopy and Chemometrics

    Peinder, Peter de

    2009-01-01

    Research has been carried out to the utility of chemometric models to predict long residue (LR) and short residue (SR) properties of a crude oil directly from its absorption or magnetic resonance spectrum. Such a combined spectroscopic-chemometric approach might offer a fast alternative for the elaborate crude oil assays that are currently used in petrochemical industries. Six different spectroscopic techniques have been explored: infrared (IR), near IR (NIR), Raman, UV-Vis, 1H-NMR and 13C-NM...

  15. Pyrolysis-Gas Chromatography-Mass Spectometry and Chemometric Analysis for the Characterization of Complex Matrices

    Montalbani, Simona

    2012-01-01

    The present PhD thesis was focused on the development and application of chemical methodology (Py-GC-MS) and data-processing method by multivariate data analysis (chemometrics). The chromatographic and mass spectrometric data obtained with this technique are particularly suitable to be interpreted by chemometric methods such as PCA (Principal Component Analysis) as regards data exploration and SIMCA (Soft Independent Models of Class Analogy) for the classification. As a first approach, som...

  16. Battlefield acoustics

    Damarla, Thyagaraju

    2015-01-01

    This book presents all aspects of situational awareness in a battlefield using acoustic signals. It starts by presenting the science behind understanding and interpretation of sound signals. The book then goes on to provide various signal processing techniques used in acoustics to find the direction of sound source, localize gunfire, track vehicles, and detect people. The necessary mathematical background and various classification and fusion techniques are presented. The book contains majority of the things one would need to process acoustic signals for all aspects of situational awareness in one location. The book also presents array theory, which is pivotal in finding the direction of arrival of acoustic signals. In addition, the book presents techniques to fuse the information from multiple homogeneous/heterogeneous sensors for better detection. MATLAB code is provided for majority of the real application, which is a valuable resource in not only understanding the theory but readers, can also use the code...

  17. Acoustical Imaging

    Akiyama, Iwaki

    2009-01-01

    The 29th International Symposium on Acoustical Imaging was held in Shonan Village, Kanagawa, Japan, April 15-18, 2007. This interdisciplinary Symposium has been taking place every two years since 1968 and forms a unique forum for advanced research, covering new technologies, developments, methods and theories in all areas of acoustics. In the course of the years the volumes in the Acoustical Imaging Series have developed and become well-known and appreciated reference works. Offering both a broad perspective on the state-of-the-art in the field as well as an in-depth look at its leading edge research, this Volume 29 in the Series contains again an excellent collection of seventy papers presented in nine major categories: Strain Imaging Biological and Medical Applications Acoustic Microscopy Non-Destructive Evaluation and Industrial Applications Components and Systems Geophysics and Underwater Imaging Physics and Mathematics Medical Image Analysis FDTD method and Other Numerical Simulations Audience Researcher...

  18. Acoustic telemetry

    National Oceanic and Atmospheric Administration, Department of Commerce — To determine movements of green turtles in the nearshore foraging areas, we deployed acoustic tags and determined their movements through active and passive...

  19. Acoustics Research

    National Oceanic and Atmospheric Administration, Department of Commerce — Fisheries acoustics data are collected from more than 200 sea-days each year aboard the FRV DELAWARE II and FRV ALBATROSS IV (decommissioned) and the FSV Henry B....

  20. AFSC/NMML: Acoustics long-term passive monitoring using moored autonomous recorders in the Bering, Chukchi, and Western Beaufort Seas, 2007-2012

    National Oceanic and Atmospheric Administration, Department of Commerce — The National Marine Mammal Laboratory (NMML) has deployed long-term passive acoustic recorders in various locations in Alaskan waters and in the High Arctic to...

  1. [Prediction of Encapsulation Temperatures of Copolymer Films in Photovoltaic Cells Using Hyperspectral Imaging Techniques and Chemometrics].

    Lin, Ping; Chen, Yong-ming; Yao, Zhi-lei

    2015-11-01

    A novel method of combination of the chemometrics and the hyperspectral imaging techniques was presented to detect the temperatures of Ethylene-Vinyl Acetate copolymer (EVA) films in photovoltaic cells during the thermal encapsulation process. Four varieties of the EVA films which had been heated at the temperatures of 128, 132, 142 and 148 °C during the photovoltaic cells production process were used for investigation in this paper. These copolymer encapsulation films were firstly scanned by the hyperspectral imaging equipment (Spectral Imaging Ltd. Oulu, Finland). The scanning band range of hyperspectral equipemnt was set between 904.58 and 1700.01 nm. The hyperspectral dataset of copolymer films was randomly divided into two parts for the training and test purpose. Each type of the training set and test set contained 90 and 10 instances, respectively. The obtained hyperspectral images of EVA films were dealt with by using the ENVI (Exelis Visual Information Solutions, USA) software. The size of region of interest (ROI) of each obtained hyperspectral image of EVA film was set as 150 x 150 pixels. The average of reflectance hyper spectra of all the pixels in the ROI was used as the characteristic curve to represent the instance. There kinds of chemometrics methods including partial least squares regression (PLSR), multi-class support vector machine (SVM) and large margin nearest neighbor (LMNN) were used to correlate the characteristic hyper spectra with the encapsulation temperatures of of copolymer films. The plot of weighted regression coefficients illustrated that both bands of short- and long-wave near infrared hyperspectral data contributed to enhancing the prediction accuracy of the forecast model. Because the attained reflectance hyperspectral data of EVA materials displayed the strong nonlinearity, the prediction performance of linear modeling method of PLSR declined and the prediction precision only reached to 95%. The kernel-based forecast models were

  2. Quality control of the paracetamol drug by chemometrics and imaging spectroscopy in the near infrared region

    Baptistao, Mariana; Rocha, Werickson Fortunato de Carvalho; Poppi, Ronei Jesus

    2011-09-01

    In this work, it was used imaging spectroscopy and chemometric tools for the development and analysis of paracetamol and excipients in pharmaceutical formulations. It was also built concentration maps to study the distribution of the drug in the tablets surface. Multivariate models based on PLS regression were developed for paracetamol and excipients concentrations prediction. For the construction of the models it was used 31 samples in the tablet form containing the active principle in a concentration range of 30.0-90.0% (w/w) and errors below to 5% were obtained for validation samples. Finally, the study of the distribution in the drug was performed through the distribution maps of concentration of active principle and excipients. The analysis of maps showed the complementarity between the active principle and excipients in the tablets. The region with a high concentration of a constituent must have, necessarily, absence or low concentration of the other one. Thus, an alternative method for the paracetamol drug quality monitoring is presented.

  3. A chemometric approach to the characterisation of historical mortars

    The compositional knowledge of historical mortars is of great concern in case of provenance and dating investigations and of conservation works since the nature of the raw materials suggests the most compatible conservation products. The classic characterisation usually goes through various analytical determinations, while conservation laboratories call for simple and quick analyses able to enlighten the nature of mortars, usually in terms of the binder fraction. A chemometric approach to the matter is here undertaken. Specimens of mortars were prepared with calcitic and dolomitic binders and analysed by Atomic Spectroscopy. Principal Components Analysis (PCA) was used to investigate the features of specimens and samples. A Partial Least Square (PLS1) regression was done in order to predict the binder/aggregate ratio. The model was applied to historical mortars from the churches of St. Lorenzo (Milan) and St. Abbondio (Como). The accordance between the predictive model and the real samples is discussed

  4. Eliminate indeterminacies of independent component analysis for chemometrics

    2008-01-01

    An improved method has been proposed to eliminate the indeterminacies of independent component analysis (ICA) for chemomet- rics. Following the arrangement of principal components analysis (PCA), the ICA mixing matrix is selected as signal content indexes, and ICA output are sorted and directed. After many times reputations, independent components (Ics) are paired according to the maximum correlation coefficient, and then the mean values of each IC substitutes the original Ics. This indicates that the ICA inde- terminacies are eliminated. A simulation example is tested to validate this improvement. Finally, a set of experimental LC-MS data is processed without any prior knowledge or specific limitation and the results show that the improved ICA can directly separate the mixed signals in chemometrics, and it is simpler and more reasonable than the simple to use interactive self-modeling mixture analysis (SIMPLISMA).

  5. IMMAN: free software for information theory-based chemometric analysis.

    Urias, Ricardo W Pino; Barigye, Stephen J; Marrero-Ponce, Yovani; García-Jacas, César R; Valdes-Martiní, José R; Perez-Gimenez, Facundo

    2015-05-01

    The features and theoretical background of a new and free computational program for chemometric analysis denominated IMMAN (acronym for Information theory-based CheMoMetrics ANalysis) are presented. This is multi-platform software developed in the Java programming language, designed with a remarkably user-friendly graphical interface for the computation of a collection of information-theoretic functions adapted for rank-based unsupervised and supervised feature selection tasks. A total of 20 feature selection parameters are presented, with the unsupervised and supervised frameworks represented by 10 approaches in each case. Several information-theoretic parameters traditionally used as molecular descriptors (MDs) are adapted for use as unsupervised rank-based feature selection methods. On the other hand, a generalization scheme for the previously defined differential Shannon's entropy is discussed, as well as the introduction of Jeffreys information measure for supervised feature selection. Moreover, well-known information-theoretic feature selection parameters, such as information gain, gain ratio, and symmetrical uncertainty are incorporated to the IMMAN software ( http://mobiosd-hub.com/imman-soft/ ), following an equal-interval discretization approach. IMMAN offers data pre-processing functionalities, such as missing values processing, dataset partitioning, and browsing. Moreover, single parameter or ensemble (multi-criteria) ranking options are provided. Consequently, this software is suitable for tasks like dimensionality reduction, feature ranking, as well as comparative diversity analysis of data matrices. Simple examples of applications performed with this program are presented. A comparative study between IMMAN and WEKA feature selection tools using the Arcene dataset was performed, demonstrating similar behavior. In addition, it is revealed that the use of IMMAN unsupervised feature selection methods improves the performance of both IMMAN and WEKA

  6. Acoustic Bat Inventory and Monitoring

    US Fish and Wildlife Service, Department of the Interior — The Sheldon-Hart Mountain National Wildlife Refuge Complex (Complex) occupies close to 1 million acres in the Great Basin. In 2009 and 2010, the Complex initiated...

  7. Using an autonomous passive acoustic observational system to monitor the environmental impact of the Gulf of Mexico oil spill on deep-diving marine mammals

    Sidorovskaia, N.; Ackleh, A.; Ma, B.; Tiemann, C.; Ioup, J. W.; Ioup, G. E.

    2012-12-01

    The Littoral Acoustic Demonstration Center (LADC) is a consortium of scientists from four universities and the U.S. Navy, which performs acoustic measurements and analysis in littoral waters. For the present work, six passive autonomous broadband acoustic sensors were deployed by LADC in the vicinity of the Deep Water Horizon oil spill site in the Northern Gulf of Mexico in fall 2010. The objective of the project is to assess long-term impact of the spill on the deep-diving residential population of marine mammals, particularly, sperm and beaked whales. Collected data were processed to detect, extract, and count acoustic signals produced by different types of marine mammals. As a next step, a statistical model which uses acoustic inputs was developed to estimate residential populations of different types of marine mammals at different distances from the spill site. The estimates were compared to population estimates from years prior to the spill, using pre-spill collected data in the area by LADC from 2001, 2002, and 2007. The results indicate different responses from sperm and beaked whales in the first months following the spill. A recently published article by our research group (Ackleh et al., J. Acoust. Soc. Am. 131, 2306-2314) provides a comparison of 2007 and 2010 estimates showing a decrease in acoustic activity and abundance of sperm whales at the 9-mile distant site, whereas acoustic activity and abundance at the 25-mile distant site has clearly increased. This may indicate that some sperm whales have relocated farther away from the spill subject to food source availability. The beaked whale population appears to return to 2007 numbers after the spill even at the closest 9-mile distant site. Several acoustically observed changes in the animals' habitat associated with the spill, such as anthropogenic noise level, prey presence, etc., can be connected with the observed population trends. Preliminary results for interpreting observed population trends will

  8. Monitor

    US Agency for International Development — A custom-built, dual-language (English and Spanish) system (http://www.monitor.net.co/) developed by DevTech that debuted in January 2011. It features a central PMP...

  9. Development and Validation of Chemometric Assisted Spectrophotometric Technique for Simultaneous Estimation of Cinitapride and Pantoprazole from Bulk and Combined Dosage Form

    Jasmine Karanjia

    2015-01-01

    This paper describes two sensitive, accurate and precise chemometric spectrophotometric methods for the simultaneous determination of Cinitapride hydrogen tartarate (CNT) and Pantoprazole sodium (PANTO) in bulk powder and capsules without prior separation. Multivariate calibration chemometric methods are proposed for simultaneous determination of CNT and PANTO. The chemometric methods applied are Principal Component Regression (PCR) and Partial Least Squares (PLS). These approaches are succes...

  10. Analysis of acoustic emission signals of fatigue crack growth and corrosion processes. Investigation of the possibilities for continuous condition monitoring of transport containers by acoustic emission testing; Analyse der Schallemissionssignale aus Ermuedungsrisswachstum und Korrosionsprozessen. Untersuchung der Moeglichkeiten fuer die kontinuierliche Zustandsueberwachung von Transportbehaeltern mittels Schallemissionspruefung

    Wachsmuth, Janne

    2016-05-01

    Fatigue crack growth and active corrosion processes are the main causes of structural failures of transport products like road tankers, railway tank cars and ships. To prevent those failures, preventive, time-based maintenance is performed. However, preventive inspections are costly and include the risk of not detecting a defect, which could lead to a failure within the next service period. An alternative is the idea of continuous monitoring of the whole structure by means of acoustic emission testing (AT). With AT, defects within the material shall be detected and repaired directly after their appearance. Acoustic emission testing is an online non-destructive testing method. Acoustic emission (AE) arises from changes within the material and is transported by elastic waves through the material. If the AE event generates enough energy, the elastic wave propagates to the boundaries of the component, produces a displacement in the picometre scale and can be detected by a piezoelectric sensor. The sensor produces an electrical signal. From this AE signal, AE features such as the maximum amplitude or the frequency can be extracted. Methods of signal analysis are used to investigate the time and frequency dependency of signal groups. The purpose of the signal analysis is to connect the AE signal with the originating AE source. If predefined damage mechanisms are identified, referencing the damage condition of the structure is possible. Acoustic emission from events of the actual crack propagation process can for example lead to the crack growth rate or the stress intensity factor, both specific values from fracture mechanics. A new development in the domain of acoustic emission testing is the pattern recognition of AE signals. Specific features are extracted from the AE signals to assign them to their damage mechanisms. In this thesis the AE signals from the damage mechanisms corrosion and fatigue crack growth are compared and analysed. The damage mechanisms were

  11. Acoustic emission in uranium under thermal stimulus

    Acoustic emission (AE) monitoring was carried out during heating and cooling of uranium through alpha-to-beta phase transformation temperature. Intense AE activity was observed during heating as well as cooling of uranium in the alpha phase. During alpha ↔ beta phase transformation also, distinct AE activity was observed. The mechanisms of acoustic emission from uranium during thermal stimulus are explained. (author)

  12. Applications of acoustics in insect pest management

    Acoustic technology has been applied for many years in studies of insect communication and in the monitoring of calling-insect population levels, geographic distributions, and diversity, as well as in the detection of cryptic insects in soil, wood, container crops, and stored products. Acoustic devi...

  13. Acoustic emission

    This paper is related to our activities on acoustic emission (A.E.). The work is made with different materials: metals and fibre reinforced plastics. At present, acoustic emission transducers are being developed for low and high temperature. A test to detect electrical discharges in electrical transformers was performed. Our experience in industrial tests to detect cracks or failures in tanks or tubes is also described. The use of A.E. for leak detection is considered. Works on pattern recognition of A.E. signals are also being performed. (Author)

  14. 面神经电生理监测在大型听神经瘤术中的应用%Intraoperative electrophysiologic monitoring of the facial nerve in operation of large acoustic neuromas

    赵学明; 药天乐; 万大海; 王永红; 范益民; 郝解贺

    2011-01-01

    Objective To explore intraoperative protection of facial nerve and evaluate its function after operation in large acoustic neuromas surgery by electrophysiologic monitoring. Method A total of 42 patients'clinical data with large acoustic neuromas between Jun, 2007 and Mar, 2010 were analyzed retrospectively,who were treated microsurgically with intraoperative electrophysiological monitoring in our department. Results The facial nerve was preserved anatomically in 37 patients (88%). The function of facial nerve was kept well in 30 cases (71%). Stimulative intensity of 1 ~ 3 V at the end of operation is related to the good function of facial nerve. The proximal - to - distal amplitude ratio of facial nerve after surgery less than 0. 3 presented with a bad facial function. ConclusionsIntraoperative monitoring has significantly decreased facial nerve morbidity in large acoustic neuromas surgery. Stimulative intensity at the exit of facial nerve from brainstem is related to the facial nerve function negatively. The proximal - to - distal amplitude ratio can predict the facial nerve function positively following acoustic neuromas resection.%目的 探讨大型听神经瘤术中面神经监测对面神经保护及评估术后面神经功能的临床意义。方法回顾性分析我科2007年6月至2010年3月术中行面神经监测的42例大型听神经瘤的临床资料。结果 面神经解剖保留37例(88%),面神经功能保留30例(71%)。术末刺激强度1~3V即引起肌电反应者预后良好;而术末面神经近端与远端波幅之比<0.3者预后差。结论 大型听神经瘤术中面神经监测可显著降低术后面神经瘫痪的发生率,术末面神经脑干端的刺激强度与面神经功能呈负相关,而面神经近端与远端波幅之比与面神经功能呈正相关。

  15. Acoustic fault injection tool (AFIT)

    Schoess, Jeffrey N.

    1999-05-01

    On September 18, 1997, Honeywell Technology Center (HTC) successfully completed a three-week flight test of its rotor acoustic monitoring system (RAMS) at Patuxent River Flight Test Center. This flight test was the culmination of an ambitious 38-month proof-of-concept effort directed at demonstrating the feasibility of detecting crack propagation in helicopter rotor components. The program was funded as part of the U.S. Navy's Air Vehicle Diagnostic Systems (AVDS) program. Reductions in Navy maintenance budgets and available personnel have dictated the need to transition from time-based to 'condition-based' maintenance. Achieving this will require new enabling diagnostic technologies. The application of acoustic emission for the early detection of helicopter rotor head dynamic component faults has proven the feasibility of the technology. The flight-test results demonstrated that stress-wave acoustic emission technology can detect signals equivalent to small fatigue cracks in rotor head components and can do so across the rotating articulated rotor head joints and in the presence of other background acoustic noise generated during flight operation. During the RAMS flight test, 12 test flights were flown from which 25 Gbyte of digital acoustic data and about 15 hours of analog flight data recorder (FDR) data were collected from the eight on-rotor acoustic sensors. The focus of this paper is to describe the CH-46 flight-test configuration and present design details about a new innovative machinery diagnostic technology called acoustic fault injection. This technology involves the injection of acoustic sound into machinery to assess health and characterize operational status. The paper will also address the development of the Acoustic Fault Injection Tool (AFIT), which was successfully demonstrated during the CH-46 flight tests.

  16. Monitoring

    Ložek, Vojen; Němec, J.

    Praha : Consult, 2003 - (Němec, J.), s. 111-115 ISBN 80-902132-4-3 Grant ostatní: Magistrát hlavního města Prahy(CZ) DAG/67/04/000176/2001 Institutional research plan: CEZ:AV0Z3013912 Keywords : monitoring * environmental quality * Prague Subject RIV: DB - Geology ; Mineralogy

  17. Monitoring

    ... its main source of fuel. To keep your blood sugar level on target and avoid problems with your eyes, kidneys, heart and feet, you should eat right ... better. And monitoring doesn’t stop at measuring blood sugar levels. Because ... blood testing) Eye health (eye exams) Foot health (foot exams and ...

  18. Effects of subsampling of passive acoustic recordings on acoustic metrics.

    Thomisch, Karolin; Boebel, Olaf; Zitterbart, Daniel P; Samaran, Flore; Van Parijs, Sofie; Van Opzeeland, Ilse

    2015-07-01

    Passive acoustic monitoring is an important tool in marine mammal studies. However, logistics and finances frequently constrain the number and servicing schedules of acoustic recorders, requiring a trade-off between deployment periods and sampling continuity, i.e., the implementation of a subsampling scheme. Optimizing such schemes to each project's specific research questions is desirable. This study investigates the impact of subsampling on the accuracy of two common metrics, acoustic presence and call rate, for different vocalization patterns (regimes) of baleen whales: (1) variable vocal activity, (2) vocalizations organized in song bouts, and (3) vocal activity with diel patterns. To this end, above metrics are compared for continuous and subsampled data subject to different sampling strategies, covering duty cycles between 50% and 2%. The results show that a reduction of the duty cycle impacts negatively on the accuracy of both acoustic presence and call rate estimates. For a given duty cycle, frequent short listening periods improve accuracy of daily acoustic presence estimates over few long listening periods. Overall, subsampling effects are most pronounced for low and/or temporally clustered vocal activity. These findings illustrate the importance of informed decisions when applying subsampling strategies to passive acoustic recordings or analyses for a given target species. PMID:26233026

  19. Acoustic Transmitters for Underwater Neutrino Telescopes

    Ardid, Miguel; Bou-Cabo, Manuel; Larosa, Giuseppina; Adrián-Martínez, Silvia; Llorens, Carlos D

    2012-01-01

    In this paper acoustic transmitters that were developed for use in underwater neutrino telescopes are presented. Firstly, an acoustic transceiver has been developed as part of the acoustic positioning system of neutrino telescopes. These infrastructures are not completely rigid and require a positioning system in order to monitor the position of the optical sensors which move due to sea currents. To guarantee a reliable and versatile system, the transceiver has the requirements of reduced cost, low power consumption, high pressure withstanding (up to 500 bars), high intensity for emission, low intrinsic noise, arbitrary signals for emission and the capacity of acquiring and processing received signals. Secondly, a compact acoustic transmitter array has been developed for the calibration of acoustic neutrino detection systems. The array is able to mimic the signature of ultra-high-energy neutrino interaction in emission directivity and signal shape. The technique of parametric acoustic sources has been used to...

  20. Discrimination of sugarcane according to cultivar by 1H NMR and chemometric analyses

    Alves Filho, Elenilson G.; Silva, Lorena M.A.; Choze, Rafael; Liao, Luciano M. [Laboratorio de Ressonancia Magnetica Nuclear, Instituto de Quimica, Universidade Federal de Goias (UFG), Goiania, GO (Brazil); Honda, Neli K.; Alcantara, Glaucia B. [Departamento de Quimica, Universidade Federal de Mato Grosso do Sul (UFMS), Campo Grande, MS (Brazil)

    2012-07-01

    Several technologies for the development of new sugarcane cultivars have mainly focused on the increase in productivity and greater disease resistance. Sugarcane cultivars are usually identified by the organography of the leaves and stems, the analysis of peroxidase and esterase isoenzyme activities and the total soluble protein as well as soluble solid content. Nuclear magnetic resonance (NMR) associated with chemometric analysis has proven to be a valuable tool for cultivar assessment. Thus, this article describes the potential of chemometric analysis applied to 1H high resolution magic angle spinning (HRMAS) and NMR in solution for the investigation of sugarcane cultivars. For this purpose, leaves from eight different cultivars of sugarcane were investigated by {sup 1}H NMR spectroscopy in combination with chemometric analysis. The approach shows to be a useful tool for the distinction and classification of different sugarcane cultivars as well as to access the differences on its chemical composition. (author)

  1. Chemometric evaluation of trace elements in Brazilian medicinal plants

    Silva, Paulo S.C. da; Francisconi, Lucilaine S.; Goncalves, Rodolfo D.M.R., E-mail: pscsilva@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil). Centro do Reator de Pesquisas

    2013-07-01

    The growing interest in herbal medicines has required standardization in order to ensure their safe use, therapeutic efficacy and quality of the products. Despite the vast flora and the extensive use of medicinal plants by the Brazilian population, scientific studies on the subject are still insufficiency In this study, 59 medicinal plans were analyzed for the determination of As, Ba, Br, Ca, Cl, Cs, Co, Cr, Fe, Hf, K, Mg, Mn, Na, Rb, Sb, Sc, Se, Ta, Th, U, Zn and Zr by neutron activation analysis and Cu, Ni, Pb, Cd and Hg by atomic absorption. The results were analyzed by chemometric methods: correlation analysis, principal component analysis and cluster analysis, in order to verify whether or not there is similarity with respect to their mineral and trace metal contents. Results obtained permitted to classify distinct groups among the analyzed plants and extracts so that these data can be useful in future studies, concerning the therapeutic action the elements here determined may exert. (author)

  2. Application of Chemometrics in the Determination of Spirits Authenticity

    Estrella Patricia Zayas Ruiz

    2013-02-01

    Full Text Available The authenticity of food and food ingredients is a major problem today for the industry and manytechnologies have been applied to detect adulteration and contamination of food. This paper presentsresults of a study conducted at University College Dublin, Ireland, about vodka and whiskey andmixtures thereof, and another study in Cuba, at the Faculty of Chemical Engineering of the HigherPolytechnic Institute «Jose Antonio Echeverria», in collaboration with the Cuban Research Institute ofSugarcane Derivatives (ICIDCA, with historical data of Cuban rums. In the first study three techniqueswere used to determine whether pure drinks could be separated from mixtures: mid-infrared spectroscopywith a Fourier transform and Attenuated Total Reflectance cell, near infrared spectroscopy and ultravioletvisiblespectroscopy. In the second historical determinations of acidity, acetaldehyde, ethyl acetate,methanol, isoamyl alcohol, isobutanol, propanol and ethanol content of different types of Cuban agedrums to establish the possibility to differentiate the aged rum Vigía from the rest of Cuban aged onesby means of that analytic information. Unscramble software was used to apply Chemometrics. PrincipalComponent Analysis and various pretreatments were applied to data acquired experimentally toreduce the dispersion thereof. Near spectroscopy, Ultraviolet visible and Mid-infrared spectroscopyhave potential for the separation of pure whiskey and vodka from mixtures thereof The Cuban agedrums differ from Vigía aged rum successfully with the use of Principal Component Analysis applied tochemical data.

  3. Chemometrics of differentially expressed proteins from colorectal cancer patients

    Lay-Chin Yeoh; Saravanan Dharmaraj; Boon-Hui Gooi; Manjit Singh; Lay-Harn Gam

    2011-01-01

    AIM: To evaluate the usefulness of differentially expressed proteins from colorectal cancer (CRC) tissues for differentiating cancer and normal tissues. METHODS: A Proteomic approach was used to identify the differentially expressed proteins between CRC and normal tissues. The proteins were extracted using Tris buffer and thiourea lysis buffer (TLB) for extraction of aqueous soluble and membrane-associated proteins, respectively. Chemometrics, namely principal component analysis (PCA) and linear discriminant analysis (LDA), were used to assess the usefulness of these proteins for identifying the cancerous state of tissues. RESULTS: Differentially expressed proteins identified were 37 aqueous soluble proteins in Tris extracts and 24 membrane-associated proteins in TLB extracts. Based on the protein spots intensity on 2D-gel images, PCA by applying an eigenvalue > 1 was successfully used to reduce the number of principal components (PCs) into 12 and seven PCs for Tris and TLB extracts, respectively, and subsequently six PCs, respectively from both the extracts were used for LDA. The LDA classification for Tris extract showed 82.7% of original samples were correctly classified, whereas 82.7% were correctly classified for the cross-validated samples. The LDA for TLB extract showed that 78.8% of original samples and 71.2% of the cross-validated samples were correctly classified. CONCLUSION: The classification of CRC tissues by PCA and LDA provided a promising distinction between normal and cancer types. These methods can possibly be used for identification of potential biomarkers among the differentially expressed proteins identified.

  4. Chemometric assessment of enhanced bioremediation of oil contaminated soils.

    Soleimani, Mohsen; Farhoudi, Majid; Christensen, Jan H

    2013-06-15

    Bioremediation is a promising technique for reclamation of oil polluted soils. In this study, six methods for enhancing bioremediation were tested on oil contaminated soils from three refinery areas in Iran (Isfahan, Arak, and Tehran). The methods included bacterial enrichment, planting, and addition of nitrogen and phosphorous, molasses, hydrogen peroxide, and a surfactant (Tween 80). Total petroleum hydrocarbon (TPH) concentrations and CHEMometric analysis of Selected Ion Chromatograms (SIC) termed CHEMSIC method of petroleum biomarkers including terpanes, regular, diaromatic and triaromatic steranes were used for determining the level and type of hydrocarbon contamination. The same methods were used to study oil weathering of 2 to 6 ring polycyclic aromatic compounds (PACs). Results demonstrated that bacterial enrichment and addition of nutrients were most efficient with 50% to 62% removal of TPH. Furthermore, the CHEMSIC results demonstrated that the bacterial enrichment was more efficient in degradation of n-alkanes and low molecular weight PACs as well as alkylated PACs (e.g. C₃-C₄ naphthalenes, C₂ phenanthrenes and C₂-C₃ dibenzothiophenes), while nutrient addition led to a larger relative removal of isoprenoids (e.g. norpristane, pristane and phytane). It is concluded that the CHEMSIC method is a valuable tool for assessing bioremediation efficiency. PMID:23644688

  5. [Studies on Cancer Diagnosis by Using Spectroscopy Combined with Chemometrics].

    Zhang, Zhuo-yong

    2015-09-01

    Studies on cancer diagnosis using various spectroscopic methods combined with chemometrics are briefly reviewed. Elemental contents in serum samples were determined by inductively coupled plasma atomic emission spectroscopy (ICP-AES), bidirectional associative memory (BAM) networks were used to establish diagnosis models for the relationships between elemental contents and lung cancer, liver cancer, and stomach cancer, respectively. Near infrared spectroscopy (NIRS) is a non-destructive detection technology. Near infrared spectra of endometrial carcinoma samples were determined and spectral features were extracted by chemoometric methods, a fuzzy rule-based expert system (FuRES) was used for establishing diagnosis model, satisfactory results were obtained. We also proposed a novel variable selection method based on particle swarm optimization (PSO) for near infrared spectra of endometrial carcinoma samples. Spectra with optimized variable were then modeled by support victor machine (SVM). Terahertz technology is an emerging technology for non-destructive detection, which has some unique characteristics. Terahertz time domain spectroscopy (THz-TDS) was used for cervical carcinoma measurement. Absorption coefficients were calculated from the measured time domain spectra and then processed with derivative, orthogonal signal correction (PC-OSC) to reduce interference components, and then fuzzy rule-based expert system (FuRES), fuzzy optimal associative memory (FOAM), support victor machine (SVM), and partial least squares discriminant analysis (PLS-DA) were used for diagnosis model establishment. The above results provide useful information for cancer occurring and development, and provide novel approaches for early stage diagnosis of various cancers. PMID:26669135

  6. Chemometric approach for prediction of uranium pathways in the soil

    Understanding the effect of soil parameters (pH, Eh and organic and inorganic ligands availability) on uranium mobility under different geochemical conditions is fundamental for reliable prediction of its behaviour and fate in the environment. In this study, the impact of total and available phosphorus content, humus and acidity of Serbian agricultural soils on the content of total and available uranium were evaluated by Response Surface Methodology (RSM), second order polynomial regression models (SOPs) and artificial neural networks (ANNs). The performance of ANNs was compared with the performance of SOPs and experimental results. SOPs showed high coefficients of determination (0.785-0.956), while ANN model performed high prediction accuracy: 0.8893-0.904. According to the results, total and available uranium content in the soil were mostly affected by pH, statistically significant at p < 0.05 level. For the same responses the total phosphorus was found to be also very influential, statistically significant at p < 0.05 and p < 0.10 levels. The impact of available phosphorus and humus was much more influential on total and available uranium content, compared to total phosphorus content. Proposed chemometric approach will be very helpful in preserving the natural resources and practical application for risk assessment modeling of uranium environmental pathways.

  7. Chemometric approach for prediction of uranium pathways in the soil

    Stojanovic, Mirjana; Nihajlovic, Marija; Petrovic, Jelena; Petrovic, Marija; Sostaric, Tanja; Milojkovic, Jelena [Inst. for Technology of Nuclear and Other Mineral Raw Materials, Belgrad (Serbia); Pezo, Lato [Univ. Belgrad (Serbia). Inst. of General and Physical Chemistry

    2014-10-01

    Understanding the effect of soil parameters (pH, Eh and organic and inorganic ligands availability) on uranium mobility under different geochemical conditions is fundamental for reliable prediction of its behaviour and fate in the environment. In this study, the impact of total and available phosphorus content, humus and acidity of Serbian agricultural soils on the content of total and available uranium were evaluated by Response Surface Methodology (RSM), second order polynomial regression models (SOPs) and artificial neural networks (ANNs). The performance of ANNs was compared with the performance of SOPs and experimental results. SOPs showed high coefficients of determination (0.785-0.956), while ANN model performed high prediction accuracy: 0.8893-0.904. According to the results, total and available uranium content in the soil were mostly affected by pH, statistically significant at p < 0.05 level. For the same responses the total phosphorus was found to be also very influential, statistically significant at p < 0.05 and p < 0.10 levels. The impact of available phosphorus and humus was much more influential on total and available uranium content, compared to total phosphorus content. Proposed chemometric approach will be very helpful in preserving the natural resources and practical application for risk assessment modeling of uranium environmental pathways.

  8. Chemometric evaluation of trace elements in Brazilian medicinal plants

    The growing interest in herbal medicines has required standardization in order to ensure their safe use, therapeutic efficacy and quality of the products. Despite the vast flora and the extensive use of medicinal plants by the Brazilian population, scientific studies on the subject are still insufficiency In this study, 59 medicinal plans were analyzed for the determination of As, Ba, Br, Ca, Cl, Cs, Co, Cr, Fe, Hf, K, Mg, Mn, Na, Rb, Sb, Sc, Se, Ta, Th, U, Zn and Zr by neutron activation analysis and Cu, Ni, Pb, Cd and Hg by atomic absorption. The results were analyzed by chemometric methods: correlation analysis, principal component analysis and cluster analysis, in order to verify whether or not there is similarity with respect to their mineral and trace metal contents. Results obtained permitted to classify distinct groups among the analyzed plants and extracts so that these data can be useful in future studies, concerning the therapeutic action the elements here determined may exert. (author)

  9. Chemometric Evaluation of Urinary Steroid Hormone Levels as Potential Biomarkers of Neuroendocrine Tumors

    Barbara Seroczyńska

    2013-10-01

    Full Text Available Neuroendocrine tumors (NETs are uncommon tumors which can secrete specific hormone products such as peptides, biogenic amines and hormones. So far, the diagnosis of NETs has been difficult because most NET markers are not specific for a given tumor and none of the NET markers can be used to fulfil the criteria of high specificity and high sensitivity for the screening procedure. However, by combining the measurements of different NET markers, they become highly sensitive and specific diagnostic tests. The aim of the work was to identify whether urinary steroid hormones can be identified as potential new biomarkers of NETs, which could be used as prognostic and clinical course monitoring factors. Thus, a rapid and sensitive reversed-phase high-performance liquid chromatographic method (RP-HPLC with UV detection has been developed for the determination of cortisol, cortisone, corticosterone, testosterone, epitestosterone and progesterone in human urine. The method has been validated for accuracy, precision, selectivity, linearity, recovery and stability. The limits of detection and quantification were 0.5 and 1 ng mL−1 for each steroid hormone, respectively. Linearity was confirmed within a range of 1–300 ng mL−1 with a correlation coefficient greater than 0.9995 for all analytes. The described method was successfully applied for the quantification of six endogenous steroid levels in human urine. Studies were performed on 20 healthy volunteers and 19 patients with NETs. Next, for better understanding of tumor biology in NETs and for checking whether steroid hormones can be used as potential biomarkers of NETs, a chemometric analysis of urinary steroid hormone levels in both data sets was performed.

  10. Chemometric evaluation of urinary steroid hormone levels as potential biomarkers of neuroendocrine tumors.

    Plenis, Alina; Miękus, Natalia; Olędzka, Ilona; Bączek, Tomasz; Lewczuk, Anna; Woźniak, Zofia; Koszałka, Patrycja; Seroczyńska, Barbara; Skokowski, Jarosław

    2013-01-01

    Neuroendocrine tumors (NETs) are uncommon tumors which can secrete specific hormone products such as peptides, biogenic amines and hormones. So far, the diagnosis of NETs has been difficult because most NET markers are not specific for a given tumor and none of the NET markers can be used to fulfil the criteria of high specificity and high sensitivity for the screening procedure. However, by combining the measurements of different NET markers, they become highly sensitive and specific diagnostic tests. The aim of the work was to identify whether urinary steroid hormones can be identified as potential new biomarkers of NETs, which could be used as prognostic and clinical course monitoring factors. Thus, a rapid and sensitive reversed-phase high-performance liquid chromatographic method (RP-HPLC) with UV detection has been developed for the determination of cortisol, cortisone, corticosterone, testosterone, epitestosterone and progesterone in human urine. The method has been validated for accuracy, precision, selectivity, linearity, recovery and stability. The limits of detection and quantification were 0.5 and 1 ng mL-1 for each steroid hormone, respectively. Linearity was confirmed within a range of 1-300 ng mL-1 with a correlation coefficient greater than 0.9995 for all analytes. The described method was successfully applied for the quantification of six endogenous steroid levels in human urine. Studies were performed on 20 healthy volunteers and 19 patients with NETs. Next, for better understanding of tumor biology in NETs and for checking whether steroid hormones can be used as potential biomarkers of NETs, a chemometric analysis of urinary steroid hormone levels in both data sets was performed. PMID:24135941

  11. Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

    Santos, Maiara S.; Pereira-Filho, Edenir R.; Ferreira, Antonio G. [Universidade Federal de Sao Carlos (UFSCAR), SP (Brazil). Dept. de Quimica; Boffo, Elisangela F. [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Inst. de Quimica; Figueira, Glyn M., E-mail: maiarassantos@yahoo.com.br [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Centro Pluridisciplinar de Pesquisas Quimicas, Biologicas e Agricolas

    2012-07-01

    The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, {sup 1}H HR-MAS NMR and {sup 1}H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

  12. Air-quality assessment of Pico-mountain environment (Azores) by using chemometric and trajectory analyses

    This article illustrates the use of chemometrics in the interpretation of aerosol data collected by a seven wavelength aethalometer at the PICO-NARE observatory, in Pico island, Azores, Portugal. Samples were assessed through k0-standardized, instrumental neutron activation analysis (k0-INAA), and concentrations of up to 20 airborne elements were determined. The chemometric analysis by self-organizing maps (SOM) tried to identify groups of similarity for sampling events and chemical tracers, discriminating in this way each group of similarity thus obtained. Additionally, synoptic back trajectories for each of the sampling days distributed into four clusters were calculated, in order to associate the classified groups with possible pollution sources. (author)

  13. Grape juice quality control by means of ¹H nmr spectroscopy and chemometric analyses

    Caroline Werner Pereira da Silva Grandizoli

    2014-01-01

    Full Text Available This work shows the application of ¹H NMR spectroscopy and chemometrics for quality control of grape juice. A wide range of quality assurance parameters were assessed by single ¹H NMR experiments acquired directly from juice. The investigation revealed that conditions and time of storage should be revised and indicated on all labels. The sterilization process of homemade grape juices was efficient, making it possible to store them for long periods without additives. Furthermore, chemometric analysis classified the best commercial grape juices to be similar to homemade grape juices, indicating that this approach can be used to determine the authenticity after adulteration.

  14. Authenticity study of Phyllanthus species by NMR and FT-IR Techniques coupled with chemometric methods

    Maiara S. Santos

    2012-01-01

    Full Text Available The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as "quebra-pedras" in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, ¹H HR-MAS NMR and ¹H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques.

  15. Attempt to separate the fluorescence spectra of adrenaline and noradrenaline using chemometrics

    Nikolajsen, Rikke P; Hansen, Åse Marie; Bro, R

    2000-01-01

    An investigation was conducted on whether the fluorescence spectra of the very similar catecholamines adrenaline and noradrenaline could be separated using chemometric methods. The fluorescence landscapes (several excitation and emission spectra were measured) of two data sets with respectively 16...... regression (Unfold-PLSR) on the larger data set and parallel factor analysis (PARAFAC) of the six samples of the smaller set showed that there was no difference between the fluorescence landscapes of adrenaline and noradrenaline. It can be concluded that chemometric separation of adrenaline and noradrenaline...

  16. Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

    The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, 1H HR-MAS NMR and 1H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

  17. Acoustic lenses

    Acoustic lenses focus ultrasound to produce pencil-like beams with reduced near fields. When fitted to conventional (flat-faced) transducers, such lenses greatly improve the ability to detect and size defects. This paper describes a program developed to design acoustic lenses for use in immersion or contact inspection, using normal or angle beam mode with flat or curved targets. Lens surfaces are circular in geometry to facilitate machining. For normal beam inspection of flat plate, spherical or cylindrical lenses are used. For angle beam or curved surface inspections, a compound lens is required to correct for the extra induced aberration. Such a lens is aspherical with one radius of curvature in the plane of incidence, and a different radius of curvature in the plane perpendicular to the incident plane. The resultant beam profile (i.e., location of the acoustic focus, beam diameter, 6 dB working range) depends on the degree of focusing and the transducer used. The operating frequency and bandwidth can be affected by the instrumentation used. Theoretical and measured beam profiles are in good agreement. Various applications, from zone focusing used for defect sizing in thick plate, to line focusing for pipe weld inspection, are discussed

  18. Acoustic Emission Health Monitoring of Fill Purge COPV's Used in Aerospace and Automotive Applications and Designed for Long Cycle Life Project

    National Aeronautics and Space Administration — Abstract Problem Description: Cumulative composite damage in composite pressure vessels (CPVs) currently is not monitored on-orbit. Consequently, hazards due to...

  19. Chemometric Analysis of Multicomponent Biodegradable Plastics by Fourier Transform Infrared Spectrometry: The R-Matrix Method

    A new chemometric method based on absorbance ratios from Fourier transform infrared spectra was devised to analyze multicomponent biodegradable plastics. The method uses the BeerLambert law to directly compute individual component concentrations and weight losses before and after biodegradation of c...

  20. Simultaneous spectrophotometric determination of paracetamol, ibuprofen and caffeine in pharmaceuticals by chemometric methods

    Khoshayand, M. R.; Abdollahi, H.; Shariatpanahi, M.; Saadatfard, A.; Mohammadi, A.

    2008-08-01

    In this study, the simultaneous determination of paracetamol, ibuprofen and caffeine in pharmaceuticals by chemometric approaches using UV spectrophotometry has been reported as a simple alternative to using separate models for each component. Spectra of paracetamol, ibuprofen and caffeine were recorded at several concentrations within their linear ranges and were used to compute the calibration mixture between wavelengths 200 and 400 nm at an interval of 1 nm in methanol:0.1 HCl (3:1). Partial least squares regression (PLS), genetic algorithm coupled with PLS (GA-PLS), and principal component-artificial neural network (PC-ANN) were used for chemometric analysis of data and the parameters of the chemometric procedures were optimized. The analytical performances of these chemometric methods were characterized by relative prediction errors and recoveries (%) and were compared with each other. The GA-PLS shows superiority over other applied multivariate methods due to the wavelength selection in PLS calibration using a genetic algorithm without loss of prediction capacity. Although the components show an important degree of spectral overlap, they have been determined simultaneously and rapidly requiring no separation step. These three methods were successfully applied to pharmaceutical formulation, capsule, with no interference from excipients as indicated by the recovery study results. The proposed methods are simple and rapid and can be easily used in the quality control of drugs as alternative analysis tools.

  1. The dimerization study of some cationic monomethine cyanine dyes by chemometrics method

    Ahmadi, S.; Deligeorgiev, T.G.; Vasilev, A.; Kubista, Mikael

    2012-01-01

    Roč. 86, č. 13 (2012), s. 1974-1981. ISSN 0036-0244 Institutional research plan: CEZ:AV0Z50520701 Keywords : dimerization * chemometrics * UV-vis spectroscopy * monomethine cyanine dyes Subject RIV: CF - Physical ; Theoretical Chemistry Impact factor: 0.386, year: 2012

  2. Acoustic hemostasis

    Crum, L.; Andrew, M.; Bailey, M.; Beach, K.; Brayman, A.; Curra, F.; Kaczkowski, P.; Kargl, S.; Martin, R.; Vaezy, S.

    2003-04-01

    Over the past several years, the Center for Industrial and Medical Ultrasound (CIMU) at the Applied Physics Laboratory in the University of Washington has undertaken a broad research program in the general area of High Intensity Focused Ultrasound (HIFU). Our principal emphasis has been on the use of HIFU to induce hemostasis; in particular, CIMU has sought to develop a small, lightweight, portable device that would use ultrasound for both imaging and therapy. Such a technology is needed because nearly 50% of combat casualty mortality results from exsanguinations, or uncontrolled bleeding. A similar percentage occurs for civilian death due to trauma. In this general review, a presentation of the general problem will be given, as well as our recent approaches to the development of an image-guided, transcutaneous, acoustic hemostasis device. [Work supported in part by the USAMRMC, ONR and the NIH.

  3. Cyclic Crack Growth Testing of an A.O. Smith Multilayer Pressure Vessel with Modal Acoustic Emission Monitoring and Data Assessment

    Ziola, Steven M.

    2014-01-01

    Digital Wave Corp. (DWC) was retained by Jacobs ATOM at NASA Ames Research Center to perform cyclic pressure crack growth sensitivity testing on a multilayer pressure vessel instrumented with DWC's Modal Acoustic Emission (MAE) system, with captured wave analysis to be performed using DWCs WaveExplorerTM software, which has been used at Ames since 2001. The objectives were to document the ability to detect and characterize a known growing crack in such a vessel using only MAE, to establish the sensitivity of the equipment vs. crack size and / or relevance in a realistic field environment, and to obtain fracture toughness materials properties in follow up testing to enable accurate crack growth analysis. This report contains the results of the testing.

  4. Acoustic telemetry.

    Drumheller, Douglas Schaeffer; Kuszmaul, Scott S.

    2003-08-01

    Broadcasting messages through the earth is a daunting task. Indeed, broadcasting a normal telephone conversion through the earth by wireless means is impossible with todays technology. Most of us don't care, but some do. Industries that drill into the earth need wireless communication to broadcast navigation parameters. This allows them to steer their drill bits. They also need information about the natural formation that they are drilling. Measurements of parameters such as pressure, temperature, and gamma radiation levels can tell them if they have found a valuable resource such as a geothermal reservoir or a stratum bearing natural gas. Wireless communication methods are available to the drilling industry. Information is broadcast via either pressure waves in the drilling fluid or electromagnetic waves in the earth and well tubing. Data transmission can only travel one way at rates around a few baud. Given that normal Internet telephone modems operate near 20,000 baud, these data rates are truly very slow. Moreover, communication is often interrupted or permanently blocked by drilling conditions or natural formation properties. Here we describe a tool that communicates with stress waves traveling through the steel drill pipe and production tubing in the well. It's based on an old idea called Acoustic Telemetry. But what we present here is more than an idea. This tool exists, it's drilled several wells, and it works. Currently, it's the first and only acoustic telemetry tool that can withstand the drilling environment. It broadcasts one way over a limited range at much faster rates than existing methods, but we also know how build a system that can communicate both up and down wells of indefinite length.

  5. Online monitoring of accessories for underground electrical installations through acoustics emissions; Monitoreo en linea de accesorios de instalaciones electricas subterraneas mediante emisiones acusticas

    Casals-Torrens, P. [Universidad Politecnica de Cataluna, Barcelona (Espana)]. E-mail: p.casals@upc.edu; Gonzalez-Parada, A. [Universidad de Guanajuato, Guanajuato (Mexico)]. E-mail: gonzaleza@salamanca.ugto.mx; Bosch-Tous, R. [Universidad Politecnica de Cataluna, Barcelona (Espana)

    2012-04-15

    The acoustic waves caused by Partial Discharges inside the dielectric materials, can be detected by acoustic emission (AE) sensors and analyzed in the time domain. The experimental results presented, show the online detection capability of these sensors in the environment near a cable accessory, such as a splice or terminal. The AE sensors are immune to electromagnetic interference and constitute a detection method non-intrusive and non-destructive, which ensures a galvanic decoupling with respect to electric networks, this technique of partial discharge detection can be applied as a test method for preventive or predictive maintenance (condition-based maintenance) to equipment or facilities of medium and high voltage in service and represents an alternative method to electrical detection systems, conventional or not, that continue to rely on the detection of current pulses. This paper presents characterization tests of the sensors AE through comparative tests of partial discharge on accessories for underground power cables. [Spanish] Las ondas acusticas provocadas por las descargas parciales en el interior de un dielectrico pueden ser detectadas por sensores de Emisiones Acusticas (EA) y analizadas en el dominio del tiempo. Los resultados experimentales que se presentan, evidencian la capacidad de deteccion en linea de estos sensores, en el entorno proximo a un accesorio de cable, empalme o terminal. Los sensores EA son inmunes a las interferencias electromagneticas, son un metodo de deteccion no destructivo y garantizan desacople galvanico respecto a la red electrica; esta tecnica de deteccion de descargas parciales puede ser aplicada como metodo de prueba para mantenimiento preventivo o predictivo (mantenimiento basado en la condicion), en equipos o instalaciones de media y alta tension en servicio, y representa una alternativa a los sistemas electricos de deteccion, convencionales o no, que continuan basandose en la deteccion del impulsos de corriente. En el

  6. Acoustic Neuroma Educational Video

    Full Text Available Educational Video Home What is an AN What is an Acoustic Neuroma? Identifying an AN Symptoms Acoustic Neuroma Keywords Educational Video ... for pre- and post-treatment acoustic neuroma patients. Home What is an AN What is an Acoustic ...

  7. A rapid and non-invasive method for authenticating the origin of pistachio samples by NIR spectroscopy and chemometrics

    Vitale, Raffaele; BEVILACQUA, MARTA; Bucci, R.; Magrì, A.D.; Magri, A.L.; Marini, F.

    2013-01-01

    In this study, near-infrared spectroscopy coupled to chemometrics is used to build an analytical protocol to authenticate the origin of pistachio nuts (Pistacia vera L.), a high value-added food product. In particular, 483 samples from six different origins (Sicily, India, Iran, Syria, Turkey and U.S.A.) were analyzed by NIR spectroscopy. Spectra were recorded on half seeds cut longitudinally in reflectance mode. Spectral data were then processed by chemometrics to build classification mo...

  8. Use of acoustic vortices in acoustic levitation

    Cutanda Henriquez, Vicente; Santillan, Arturo Orozco; Juhl, Peter Møller

    2009-01-01

    Acoustic fields are known to exert forces on the surfaces of objects. These forces are noticeable if the sound pressure is sufficiently high. Two phenomena where acoustic forces are relevant are: i) acoustic levitation, where strong standing waves can hold small objects at certain positions...... of acoustical vortices uses an efficient numerical implementation based on the superposition of two orthogonal sound fields with a delay of 90° between them. It is shown that acoustic levitation and the use of acoustic vortices can be combined to manipulate objects in an efficient and controlled manner without......, counterbalancing their weight, and ii) acoustic vortices, spinning sound fields that can impinge angular momentum and cause rotation of objects. In this contribution, both force-creating sound fields are studied by means of numerical simulations. The Boundary Element Method is employed to this end. The simulation...

  9. Feasibility of Chemometrics Assisted Exploration and Management of Geothermal Resources in the Kenya Rift System Utilizing Stable Isotope and Related Measurements

    The utility of isotopes is more effective if combined with chemical monitoring. Trace radiogenic and element characteristics of geothermal field matrices associated with the high background radiation areas (HBRA) of Kenya were studied and the combined potential of their profiles and multivariate relationships in surficial hydrothermal expressions system matrices of geothermally active HBRA were exploited for resource prospecting and environmental impact modelling. Some results are reported and it is shown how chemometrics and geostatistics assisted measurements could be combined with stable isotope studies. It is outlined how this work, part of the IAEA Project RAF/8/047 (''Introducing Isotope Hydrology for Exploration and Management of Geothermal Resources in the African Rift System''), will build on and enrich Kenya's previous participation in IAEA supported projects on the sustainable development of groundwater resources which aimed to facilitate the integration of isotope techniques with non-nuclear techniques for water resource development. (author)

  10. International Space Station Acoustics - A Status Report

    Allen, Christopher S.

    2015-01-01

    It is important to control acoustic noise aboard the International Space Station (ISS) to provide a satisfactory environment for voice communications, crew productivity, alarm audibility, and restful sleep, and to minimize the risk for temporary and permanent hearing loss. Acoustic monitoring is an important part of the noise control process on ISS, providing critical data for trend analysis, noise exposure analysis, validation of acoustic analyses and predictions, and to provide strong evidence for ensuring crew health and safety, thus allowing Flight Certification. To this purpose, sound level meter (SLM) measurements and acoustic noise dosimetry are routinely performed. And since the primary noise sources on ISS include the environmental control and life support system (fans and airflow) and active thermal control system (pumps and water flow), acoustic monitoring will reveal changes in hardware noise emissions that may indicate system degradation or performance issues. This paper provides the current acoustic levels in the ISS modules and sleep stations and is an update to the status presented in 2011. Since this last status report, many payloads (science experiment hardware) have been added and a significant number of quiet ventilation fans have replaced noisier fans in the Russian Segment. Also, noise mitigation efforts are planned to reduce the noise levels of the T2 treadmill and levels in Node 3, in general. As a result, the acoustic levels on the ISS continue to improve.

  11. Acoustic dispersive prism

    Hussein Esfahlani; Sami Karkar; Herve Lissek; Mosig, Juan R.

    2016-01-01

    The optical dispersive prism is a well-studied element, which allows separating white light into its constituent spectral colors, and stands in nature as water droplets. In analogy to this definition, the acoustic dispersive prism should be an acoustic device with capability of splitting a broadband acoustic wave into its constituent Fourier components. However, due to the acoustical nature of materials as well as the design and fabrication difficulties, there is neither any natural acoustic ...

  12. Acoustic Transmitters for Underwater Neutrino Telescopes

    Carlos D. Llorens

    2012-03-01

    Full Text Available In this paper acoustic transmitters that were developed for use in underwater neutrino telescopes are presented. Firstly, an acoustic transceiver has been developed as part of the acoustic positioning system of neutrino telescopes. These infrastructures are not completely rigid and require a positioning system in order to monitor the position of the optical sensors which move due to sea currents. To guarantee a reliable and versatile system, the transceiver has the requirements of reduced cost, low power consumption, high pressure withstanding (up to 500 bars, high intensity for emission, low intrinsic noise, arbitrary signals for emission and the capacity of acquiring and processing received signals. Secondly, a compact acoustic transmitter array has been developed for the calibration of acoustic neutrino detection systems. The array is able to mimic the signature of ultra-high-energy neutrino interaction in emission directivity and signal shape. The technique of parametric acoustic sources has been used to achieve the proposed aim. The developed compact array has practical features such as easy manageability and operation. The prototype designs and the results of different tests are described. The techniques applied for these two acoustic systems are so powerful and versatile that may be of interest in other marine applications using acoustic transmitters.

  13. Classification of Tempranillo wines according to geographic origin: Combination of mass spectrometry based electronic nose and chemometrics

    Cynkar, Wies, E-mail: wies.cynkar@awri.com.au [Australian Wine Research Institute, PO Box 197, Glen Osmond, SA 5064 (Australia); Dambergs, Robert [Australian Wine Research Institute, Tasmanian Institute of Agricultural Research, University of Tasmania, Private Bag 98, Hobart Tasmania 7001 (Australia); Smith, Paul; Cozzolino, Daniel [Australian Wine Research Institute, PO Box 197, Glen Osmond, SA 5064 (Australia)

    2010-02-15

    Rapid methods employing instruments such as electronic noses (EN) or gas sensors are used in the food and beverage industries to monitor and assess the composition and quality of products. Similar to other food industries, the wine industry has a clear need for simple, rapid and cost effective techniques for objectively evaluating the quality of grapes, wine and spirits. In this study a mass spectrometry based electronic nose (MS-EN) instrument combined with chemometrics was used to predict the geographical origin of Tempranillo wines produced in Australia and Spain. The MS-EN data generated were analyzed using principal components analysis (PCA), partial least squares discriminant analysis (PLS-DA) and stepwise linear discriminant analysis (SLDA) with full cross validation (leave-one-out method). The SLDA classified correctly 86% of the samples while PLS-DA 85% of Tempranillo wines according to their geographical origin. The relative benefits of using MS-EN will provide capability for rapid screening of wines. However, this technique does not provide the identification and quantitative determination of individual compounds responsible for the different aroma notes in the wine.

  14. Chemometric model for simultaneous spectrophotometric estimation of phenobarbitone and phenytoin sodium in tablets using back-propagation neural network

    Satyanarayana D

    2006-01-01

    Full Text Available A chemometric model for the simultaneous estimation of phenobarbitone and phenytoin sodium anticonvulsant tablets using the back-propagation neural network calibration has been presented. The use of calibration datasets constructed from the spectral data of pure components is proposed. The calibration sets were designed such that the concentrations were orthogonal and span the possible mixture space fairly evenly. Spectra of phenobarbitone and phenytoin sodium were recorded at several concentrations within their linear range and used to compute the calibration mixture between wavelengths 220 and 260 nm at an interval of 1 nm. The back-propagation neural network model was optimized using three different sets of calibration and monitoring data for the number of hidden sigmoid neurons. The calibration model was thoroughly evaluated at several concentration levels using spectra obtained for 95 synthetic binary mixtures prepared using orthogonal designs. The optimized model showed sufficient robustness even when the calibration sets were constructed from different sets of pure spectra of components. Although the components showed complete spectral overlap, the model could accurately estimate the drugs, with satisfactory precision and accuracy, in tablet dosage with no interference from excipients, as indicated by the recovery study results.

  15. Laser-induced breakdown spectroscopy-based investigation and classification of pharmaceutical tablets using multivariate chemometric analysis.

    Myakalwar, Ashwin Kumar; Sreedhar, S; Barman, Ishan; Dingari, Narahara Chari; Venugopal Rao, S; Prem Kiran, P; Tewari, Surya P; Manoj Kumar, G

    2011-12-15

    We report the effectiveness of laser-induced breakdown spectroscopy (LIBS) in probing the content of pharmaceutical tablets and also investigate its feasibility for routine classification. This method is particularly beneficial in applications where its exquisite chemical specificity and suitability for remote and on site characterization significantly improves the speed and accuracy of quality control and assurance process. Our experiments reveal that in addition to the presence of carbon, hydrogen, nitrogen and oxygen, which can be primarily attributed to the active pharmaceutical ingredients, specific inorganic atoms were also present in all the tablets. Initial attempts at classification by a ratiometric approach using oxygen (∼777 nm) to nitrogen (742.36 nm, 744.23 nm and 746.83 nm) compositional values yielded an optimal value at 746.83 nm with the least relative standard deviation but nevertheless failed to provide an acceptable classification. To overcome this bottleneck in the detection process, two chemometric algorithms, i.e. principal component analysis (PCA) and soft independent modeling of class analogy (SIMCA), were implemented to exploit the multivariate nature of the LIBS data demonstrating that LIBS has the potential to differentiate and discriminate among pharmaceutical tablets. We report excellent prospective classification accuracy using supervised classification via the SIMCA algorithm, demonstrating its potential for future applications in process analytical technology, especially for fast on-line process control monitoring applications in the pharmaceutical industry. PMID:22099648

  16. Classification of Tempranillo wines according to geographic origin: Combination of mass spectrometry based electronic nose and chemometrics

    Rapid methods employing instruments such as electronic noses (EN) or gas sensors are used in the food and beverage industries to monitor and assess the composition and quality of products. Similar to other food industries, the wine industry has a clear need for simple, rapid and cost effective techniques for objectively evaluating the quality of grapes, wine and spirits. In this study a mass spectrometry based electronic nose (MS-EN) instrument combined with chemometrics was used to predict the geographical origin of Tempranillo wines produced in Australia and Spain. The MS-EN data generated were analyzed using principal components analysis (PCA), partial least squares discriminant analysis (PLS-DA) and stepwise linear discriminant analysis (SLDA) with full cross validation (leave-one-out method). The SLDA classified correctly 86% of the samples while PLS-DA 85% of Tempranillo wines according to their geographical origin. The relative benefits of using MS-EN will provide capability for rapid screening of wines. However, this technique does not provide the identification and quantitative determination of individual compounds responsible for the different aroma notes in the wine.

  17. Sonification of acoustic emission data

    Raith, Manuel; Große, Christian

    2014-05-01

    While loading different specimens, acoustic emissions appear due to micro crack formation or friction of already existing crack edges. These acoustic emissions can be recorded using suitable ultrasonic transducers and transient recorders. The analysis of acoustic emissions can be used to investigate the mechanical behavior of different specimens under load. Our working group has undertaken several experiments, monitored with acoustic emission techniques. Different materials such as natural stone, concrete, wood, steel, carbon composites and bone were investigated. Also the experimental setup has been varied. Fire-spalling experiments on ultrahigh performance concrete and pullout experiments on bonded anchors have been carried out. Furthermore uniaxial compression tests on natural stone and animal bone had been conducted. The analysis tools include not only the counting of events but the analysis of full waveforms. Powerful localization algorithms and automatic onset picking techniques (based on Akaikes Information Criterion) were established to handle the huge amount of data. Up to several thousand events were recorded during experiments of a few minutes. More sophisticated techniques like moment tensor inversion have been established on this relatively small scale as well. Problems are related to the amount of data but also to signal-to-noise quality, boundary conditions (reflections) sensor characteristics and unknown and changing Greens functions of the media. Some of the acoustic emissions recorded during these experiments had been transferred into audio range. The transformation into the audio range was done using Matlab. It is the aim of the sonification to establish a tool that is on one hand able to help controlling the experiment in-situ and probably adjust the load parameters according to the number and intensity of the acoustic emissions. On the other hand sonification can help to improve the understanding of acoustic emission techniques for training

  18. Monitoring and characterization of yeasts behavior under fermentation processes using technometric approaches

    Castro, Cristiana C.

    2013-01-01

    Tese de doutoramento em Chemical and Biological Engineering Technometrics concerns on the development and use of statistical methods in different fields, such as biotechnological processes, in order to understand their multivariate and multidimensional complexity. Chemical changes occurring within these processes can be monitored using chemometric tools that combined with bioinformatic methodologies, can provide an enlarged overview of the process, enabling the unbiased study ...

  19. Experimental Study on Bridge Monitoring Based on Optical Fiber Acoustic Emission Sensing Technology%基于光纤声发射传感技术的桥梁监测实验研究

    单宁

    2011-01-01

    The optical fiber sensor can meet the requirements of the real-time health monitoring of the bridge structure with its features of good wearing, small size and easy to realize the distribution detection. A extrinsic optical fiber F-P sensor structure has been designed in this work and the sensing mechanism of the optical fiber F-P acoustic emission has been analyzed. A detection system based on the optical fiber F-P acoustic emission technolgy has been fabricated for detecting the health state of the concrete bridge on-line in real time. The experimemtal results showed that the sesor has the features of simple structure, small size, cost-effectiveness and easy-to-fabricate. It can be used for the bridge health detection effectively and is easy to produce commercially.%光纤传感器耐久性好,体积小,质量轻,易于实现分布式检测,能满足桥梁等土木结构的实时健康监测.该文设计了一非本征光纤法布里-珀罗(F-P)传感器结构,分析了光纤F-P声发射传感机理,建立了基于光纤F-P声发射传感技术的检测系统,用于混凝土桥梁健康状况的实时在线检测.实验结果表明,该传感器结构简单,体积小,成本低,制作容易,能有效用于桥梁健康监测,易于实现商品化.

  20. Acoustic Neurinomas

    Mohammad Faraji Rad

    2011-01-01

    Full Text Available Acoustic neuromas (AN are schwann cell-derived tumors that commonly arise from the vestibular portion of the eighth cranial nerve also known as vestibular schwannoma(VS causes unilateral hearing loss, tinnitus, vertigo and unsteadiness. In many cases, the tumor size may remain unchanged for many years following diagnosis, which is typically made by MRI. In the majority of cases the tumor is small, leaving the clinician and patient with the options of either serial scanning or active treatment by gamma knife radiosurgery (GKR or microneurosurgery. Despite the vast number of published treatment reports, comparative studies are few. The predominant clinical endpoints of AN treatment include tumor control, facial nerve function and hearing preservation. Less focus has been put on symptom relief and health-related quality of life (QOL. It is uncertain if treating a small tumor leaves the patient with a better chance of obtaining relief from future hearing loss, vertigo or tinnitus than by observing it without treatment.   In this paper we review the literature for the natural course, the treatment alternatives and the results of AN. Finally, we present our experience with a management strategy applied for more than 30 years.

  1. Acoustic Spatiality

    Brandon LaBelle

    2012-06-01

    Full Text Available Experiences of listening can be appreciated as intensely relational, bringing us into contact with surrounding events, bodies and things. Given that sound propagates and expands outwardly, as a set of oscillations from a particular source, listening carries with it a sensual intensity, whereby auditory phenomena deliver intrusive and disruptive as well as soothing and assuring experiences. The physicality characteristic of sound suggests a deeply impressionistic, locational "knowledge structure" – that is, the ways in which listening affords processes of exchange, of being in the world, and from which we extend ourselves. Sound, as physical energy reflecting and absorbing into the materiality around us, and even one's self, provides a rich platform for understanding place and emplacement. Sound is always already a trace of location.Such features of auditory experience give suggestion for what I may call an acoustical paradigm – how sound sets in motion not only the material world but also the flows of the imagination, lending to forces of signification and social structure, and figuring us in relation to each other. The relationality of sound brings us into a steady web of interferences, each of which announces the promise or problematic of being somewhere.

  2. Evaluation of damage accumulation behavior and strength anisotropy of NITE SiC/SiC composites by acoustic emission, digital image correlation and electrical resistivity monitoring

    Nozawa, Takashi; Ozawa, Kazumi; Asakura, Yuuki; Kohyama, Akira; Tanigawa, Hiroyasu

    2014-12-01

    Understanding the cracking process of the composites is essential to establish the design basis for practical applications. This study aims to investigate the damage accumulation process and its anisotropy for nano-infiltration transient eutectic sintered (NITE) SiC/SiC composites by various characterization techniques such as the acoustic emission (AE), digital image correlation (DIC) and electrical resistivity (ER) measurements. Cracking behavior below the proportional limit stress (PLS) was specifically addressed. Similar to the other generic SiC/SiC composites, the 1st AE event was identified below the PLS for NITE SiC/SiC composites with a dependency of fabric orientation. The DIC results support that the primary failure mode depending on fiber orientation affected more than the other minor modes did. Detailed AE waveform analysis by wavelet shows a potential to classify the failure behavior depending on architecture. Cracking below the PLS is a potential concern in component deign but the preliminary ER measurements imply that the impact of cracking below the PLS on composite function was limited.

  3. Love Acoustic Wave-Based Devices and Molecularly-Imprinted Polymers as Versatile Sensors for Electronic Nose or Tongue for Cancer Monitoring.

    Dejous, Corinne; Hallil, Hamida; Raimbault, Vincent; Lachaud, Jean-Luc; Plano, Bernard; Delépée, Raphaël; Favetta, Patrick; Agrofoglio, Luigi; Rebière, Dominique

    2016-01-01

    Cancer is a leading cause of death worldwide and actual analytical techniques are restrictive in detecting it. Thus, there is still a challenge, as well as a need, for the development of quantitative non-invasive tools for the diagnosis of cancers and the follow-up care of patients. We introduce first the overall interest of electronic nose or tongue for such application of microsensors arrays with data processing in complex media, either gas (e.g., Volatile Organic Compounds or VOCs as biomarkers in breath) or liquid (e.g., modified nucleosides as urinary biomarkers). Then this is illustrated with a versatile acoustic wave transducer, functionalized with molecularly-imprinted polymers (MIP) synthesized for adenosine-5'-monophosphate (AMP) as a model for nucleosides. The device including the thin film coating is described, then static measurements with scanning electron microscopy (SEM) and electrical characterization after each step of the sensitive MIP process (deposit, removal of AMP template, capture of AMP target) demonstrate the thin film functionality. Dynamic measurements with a microfluidic setup and four targets are presented afterwards. They show a sensitivity of 5 Hz·ppm(-1) of the non-optimized microsensor for AMP detection, with a specificity of three times compared to PMPA, and almost nil sensitivity to 3'AMP and CMP, in accordance with previously published results on bulk MIP. PMID:27331814

  4. Springer Handbook of Acoustics

    Rossing, Thomas D

    2007-01-01

    Acoustics, the science of sound, has developed into a broad interdisciplinary field encompassing the academic disciplines of physics, engineering, psychology, speech, audiology, music, architecture, physiology, neuroscience, and others. The Springer Handbook of Acoustics is an unparalleled modern handbook reflecting this richly interdisciplinary nature edited by one of the acknowledged masters in the field, Thomas Rossing. Researchers and students benefit from the comprehensive contents spanning: animal acoustics including infrasound and ultrasound, environmental noise control, music and human speech and singing, physiological and psychological acoustics, architectural acoustics, physical and engineering acoustics, signal processing, medical acoustics, and ocean acoustics. This handbook reviews the most important areas of acoustics, with emphasis on current research. The authors of the various chapters are all experts in their fields. Each chapter is richly illustrated with figures and tables. The latest rese...

  5. Responsive acoustic surfaces

    Peters, Brady; Tamke, Martin; Nielsen, Stig Anton;

    2011-01-01

    Acoustic performance is defined by the parameter of reverberation time; however, this does not capture the acoustic experience in some types of open plan spaces. As many working and learning activities now take place in open plan spaces, it is important to be able to understand and design for the...... acoustic conditions of these spaces. This paper describes an experimental research project that studied the design processes necessary to design for sound. A responsive acoustic surface was designed, fabricated and tested. This acoustic surface was designed to create specific sonic effects. The design was...... simulated using custom integrated acoustic software and also using Odeon acoustic analysis software. The research demonstrates a method for designing space- and sound-defining surfaces, defines the concept of acoustic subspace, and suggests some new parameters for defining acoustic subspaces....

  6. Fingerprinting profile of polysaccharides from Lycium barbarum using multiplex approaches and chemometrics.

    Liu, Wei; Xu, Jinnan; Zhu, Rui; Zhu, Yiqing; Zhao, Yang; Chen, Pei; Pan, Chun; Yao, Wenbing; Gao, Xiangdong

    2015-07-01

    Techniques including ultraviolet-visible spectra (UV), high performance size-exclusion chromatography (HPSEC), Fourier-transform infrared spectroscopy (FT-IR) and pre-column derivatization high-performance liquid chromatography (PCD-HPLC) were used in the fingerprinting analysis of Lycium barbarum polysaccharides (LBPs) from different locations and varieties. Multiple fingerprinting profiles were used to evaluate the similarity and classification of different LBPs with the help of chemometrics. The results indicated that sixteen batches of LBPs had good consistency, and fingerprinting techniques were simple and robust for quality control of LBPs as well as related products. In addition, fingerprinting techniques combined with chemometrics could also be used to identify different cultivation locations of LBPs samples. Finally, four monosaccharides (galacturonic acid, glucose, galactose and arabinose) and the absorptions of stretching vibration of ester carbonyl groups as well as NH variable angle vibration of -CONH- could be selected as herbal markers to distinguish different samples. PMID:25847838

  7. (1)H NMR spectroscopy and chemometrics evaluation of non-thermal processing of orange juice.

    Alves Filho, Elenilson G; Almeida, Francisca D L; Cavalcante, Rosane S; de Brito, Edy S; Cullen, Patrick J; Frias, Jesus M; Bourke, Paula; Fernandes, Fabiano A N; Rodrigues, Sueli

    2016-08-01

    This study evaluated the effect of atmospheric cold plasma and ozone treatments on the key compounds (sugars, amino acids and short chain organic acids) in orange juice by NMR and chemometric analysis. The juice was directly and indirectly exposed to atmospheric cold plasma field at 70kV for different treatment time (15, 30, 45 and 60sec). For ozone processing different loads were evaluated. The Principal Component Analysis shown that the groups of compounds are affected differently depending on the processing. The ozone was the processing that more affected the aromatic compounds and atmospheric cold plasma processing affected more the aliphatic compounds. However, these variations did not result in significant changes in orange juice composition as a whole. Thus, NMR data and chemometrics were suitable to follow quality changes in orange juice processing by atmospheric cold plasma and ozone. PMID:26988481

  8. Chemometric simultaneous estimation of clopidogrel bisulphate and aspirin from combined dosage form

    Rajput S

    2008-01-01

    Full Text Available Two chemometric methods, inverse least square and classical least square, were applied to simultaneous assay of clopidogrel bisulphate and aspirin in their combined dosage tablet formulation. Twelve mixed solutions were prepared for the chemometric calibration as training set and 10 mixed solutions were prepared as validation set. The absorbance data matrix was obtained by measuring the absorbance at 16 wavelength points, from 220 to 250 nm with the interval of 2 nm (Dl= 2 nm. The developed calibrations were successfully tested for laboratory mixtures as well as commercial tablet formulation for their clopidogrel bisulphate and aspirin concentration. Mean recoveries for clopidogrel bisulphate and aspirin were found to be in good agreement with the label claim.

  9. Classification of traditional Chinese pork bacon based on physicochemical properties and chemometric techniques.

    Guo, Xin; Huang, Feng; Zhang, Hong; Zhang, Chunjiang; Hu, Honghai; Chen, Wenbo

    2016-07-01

    Sixty-seven pork bacon samples from Hunan, Sichuan Guangdong, Jiangxi, and Yunnan Provinces in China were analyzed to understand their geographical properties. Classification was performed by determining their physicochemical properties through chemometric techniques, including variance analysis, principal component analysis (PCA), and discriminant analysis (DA). Results showed that certain differences existed in terms of nine physicochemical determinations in traditional Chinese pork bacon. PCA revealed the distinction among Hunan, Sichuan, and Guangdong style bacon. Meanwhile, seven key physicochemical determination criteria were identified in line with DA and could be reasonably applied to the classification of traditional Chinese pork bacon. Furthermore, the ratio of overall correct classification was 97.76% and that of cross-validation was 91.76%. These findings indicated that chemometric techniques, together with several physicochemical determination, were effective for the classification of traditional Chinese pork bacon with geographical features. Our study provided a theoretical reference for the classification of traditional Chinese pork bacon. PMID:26994313

  10. NMR spectroscopy and chemometrics to evaluate different processing of coconut water.

    Sucupira, N R; Alves Filho, E G; Silva, L M A; de Brito, E S; Wurlitzer, N J; Sousa, P H M

    2017-02-01

    NMR and chemometrics was applied to understand the variations in chemical composition of coconut water under different processing. Six processing treatments were applied to coconut water and analyzed: two control (with and without sulphite), and four samples thermally processed at 110°C and 136°C (with and without sulphite). Samples processed at lower temperature and without sulphite presented pink color under storage. According to chemometrics, samples processed at higher temperature exhibited lower levels of glucose and malic acid. Samples with sulphite processed at 136°C presented lower amount of sucrose, suggesting the degradation of the carbohydrates after harshest thermal treatment. Samples with sulphite and processed at lower temperature showed higher concentration of ethanol. However, no significant changes were verified in coconut water composition as a whole. Sulphite addition and the temperature processing to 136°C were effective to prevent the pinking and to maintain the levels of main organic compounds. PMID:27596412

  11. Localization of acoustic emission sources in geometrically sparse structures

    Převorovský, Zdeněk; Chlada, Milan

    Berlín : Deutsche Gesellschaft für Zerstörungsfreie Prüfung e.V, 2014. ISBN 978-3-940283-63-4. [Conference of the European Working Group on Acoustic Emission : EWGAE 2014 /31./. Drážďany (DE), 03.09.2014-05.09.2014] Institutional support: RVO:61388998 Keywords : civil structures * structures health monitoring ( SHM) * acoustic emission * source location Subject RIV: BI - Acoustics

  12. Balance Transmission Mechanism in Underwater Acoustic Sensor Networks

    Jiabao Cao; Jinfeng Dou; Shunle Dong

    2015-01-01

    With the rapid development of underwater acoustic modem technology, underwater acoustic sensor networks (UWASNs) have more applications in long-term monitoring of the deployment area. In the underwater environment, the sensors are costly with limited energy. And acoustic communication medium poses new challenges, including high path loss, low bandwidth, and high energy consumption. Therefore, designing transmission mechanism to decrease energy consumption and to optimize the lifetime of UWASN...

  13. Acoustic source for generating an acoustic beam

    Vu, Cung Khac; Sinha, Dipen N.; Pantea, Cristian

    2016-05-31

    An acoustic source for generating an acoustic beam includes a housing; a plurality of spaced apart piezo-electric layers disposed within the housing; and a non-linear medium filling between the plurality of layers. Each of the plurality of piezoelectric layers is configured to generate an acoustic wave. The non-linear medium and the plurality of piezo-electric material layers have a matching impedance so as to enhance a transmission of the acoustic wave generated by each of plurality of layers through the remaining plurality of layers.

  14. Evaluation of Adhesive Bonding Quality by Acoustic Emission

    Prediction of fatigue life and monitoring of fracture process for adhesively bonded CFRP composites joint have been investigated by analysis of acoustic emission signals during the fatigue and tension tests. During fatigue test, generated acoustic emission is related to stored elastic strain energy. By results of monitoring of AE event rate, fatigue process could be divided into two regions, and boundaries of two regions, fatigue cycles of the initiation of fast crack growth, were 70-80% of fatigue life even though the fatigue life were highly scattered from specimen to specimen. The result shows the possibility of predicting catastrophic failure by acoustic emission monitoring

  15. Prototype Repository. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype. Repository between April 2007 and September 2007

    Zolezzi, F.; Haycox, J.R.; Pettitt, W.S. (Applied Seismology Consultants, Shrewsbury (United Kingdom))

    2008-07-01

    This six-month period of ultrasonic monitoring in the Prototype Repository Experiment, has been undertaken with the following objectives; - Produce accurate source locations for AEs so as to delineate the spatial and temporal extent of any brittle microcracking within the rock mass around the deposition hole and locate any movements on pre-existing macroscopic fractures; - Conduct regular ultrasonic surveys to assess the effect of heating and other environmental changes on the velocity and amplitude of transmitted ultrasonic waves; - Investigate changes in dynamic moduli and crack density to show how the properties of the rock volume around the deposition hole change through the experiment; - Relate the AE and ultrasonic measurements to the measured in situ stress regime and other operating parameters such as temperature and fluid pressure; - Outline how the results from this reporting period relate to previous monitoring periods, and into the overall experimental aims and objectives.

  16. Prototype Repository. Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype. Repository between April 2007 and September 2007

    This six-month period of ultrasonic monitoring in the Prototype Repository Experiment, has been undertaken with the following objectives; - Produce accurate source locations for AEs so as to delineate the spatial and temporal extent of any brittle microcracking within the rock mass around the deposition hole and locate any movements on pre-existing macroscopic fractures; - Conduct regular ultrasonic surveys to assess the effect of heating and other environmental changes on the velocity and amplitude of transmitted ultrasonic waves; - Investigate changes in dynamic moduli and crack density to show how the properties of the rock volume around the deposition hole change through the experiment; - Relate the AE and ultrasonic measurements to the measured in situ stress regime and other operating parameters such as temperature and fluid pressure; - Outline how the results from this reporting period relate to previous monitoring periods, and into the overall experimental aims and objectives

  17. Vibro-acoustic monitoring of technical condition of mine fans in main deaeration system; Wibroakustyczne monitorowanie stanu technicznego kopalnianych wentylatorow glownego odpowietrzania

    Zakrzewski, T. [Politechnika Slaska, Gliwice (Poland)

    1994-12-01

    In hard coal mines a variety of stationery machines and equipment indispensable to ensure continuity of operation at performance of a definite process is used. To ensure their reliability and stability of performance, the continuous monitoring of technical equipment by tests of vibration processes going together with operation of every machinery, is necessary. The article presents the estimation method of technical condition of main deaeration fans, based on on-line register of vibration processes generated by main kinematic pairs of driving system during their normal operation. Due to regular measurement of vibration one can predict, by extrapolation, when a machine has to be repaired and plan necessary repairs in advance. The monitoring trend method allows enlogation of inter repair periods and considerable reduction of repair costs. (author) 9 refs., 7 figs., 1 tab.

  18. Exploring the phenotypic expression of a regulatory proteome- altering gene by spectroscopy and chemometrics

    Munck, L.; Nielsen, J.P.; Møller, B.;

    2001-01-01

    effects of the changed proteome, for example, the amide content, or indirect effects due to changes in carbohydrate and fat composition. It is concluded that the redundancy of biological information on the DNA sequence level is also represented at the phenotypic level in the dataset read by the NIR......, analytical chemistry and chemometrics in modeling the genetically based covariance of physical/chemical fingerprints of the intact phenotype in plant breeding and biotechnology is discussed....

  19. Discrimination of Corsican honey by FT-Raman spectroscopy and chemometrics

    Fernández Pierna, JA.; Abbas, O.; Dardenne, P.; V. Baeten

    2011-01-01

    Honey is a complex and challenging product to analyze due mainly to its composition consisting on various botanical sources. The discrimination of the origin of honey is of prime importance in order to reinforce the consumer trust in this typical food product. But this is not an easy task as usually no single chemical or physical parameter is sufficient. The aim of our paper is to investigate whether FT-Raman spectroscopy as spectroscopic fingerprint technique combined with some chemometric t...

  20. Chemometrics and chromatographic fingerprints to discriminate and classify counterfeit medicines containing PDE-5 inhibitors.

    Deconinck, Eric; Sacre, Pierre-Yves; Courselle, Patricia; De Beer, Jacques

    2012-01-01

    Chromatographic fingerprints recorded for a set of genuine and counterfeit samples of Viagra® and Cialis® were evaluated for their use in the detection and classification of counterfeit samples of these groups of medicines. Therefore several exploratory chemometric techniques were applied to reveal structures in the data sets as well as differences among the samples. The focus was on the differentiation between genuine and counterfeit samples and on the differences between the samples of the ...

  1. Chemometric determination of the length distribution of single walled carbon nanotubes through optical spectroscopy

    Highlights: ► Optical spectroscopy is used as a convenient tool to analyze the length distribution of single walled carbon nanotubes. ► Advanced multivariate chemometric methods are compared, and the best methods can satisfactorily predict the length distribution. ► The entire length distribution, not just the mean, is modelled and calibrated. - Abstract: Current synthesis methods for producing single walled carbon nanotubes (SWCNTs) do not ensure uniformity of the structure and properties, in particular the length, which is an important quality indicator of SWCNTs. As a result, sorting SWCNTs by length is an important post-synthesis processing step. For this purpose, convenient analysis methods are needed to characterize the length distribution rapidly and accurately. In this study, density gradient ultracentrifugation was applied to prepare length-sorted SWCNT suspensions containing individualized surfactant-wrapped SWCNTs. The length of sorted SWCNTs was first determined by atomic force microscope (AFM), and their absorbance was measured in ultraviolet–visible near-infrared (UV–vis-NIR) spectroscopy. Chemometric methods are used to calibrate the spectra against the AFM-measured length distribution. The calibration model enables convenient analysis of the length distribution of SWCNTs through UV–vis-NIR spectroscopy. Various chemometric techniques are investigated, including pre-processing methods and non-linear calibration models. Extended inverted signal correction, extended multiplicative signal correction and Gaussian process regression are found to provide good prediction of the length distribution of SWCNTs with satisfactory agreement with the AFM measurements. In summary, spectroscopy in conjunction with advanced chemometric techniques is a powerful analytical tool for carbon nanotube research.

  2. Determination of the predominant minerals in sedimentary rocks by chemometric analysis of infrared spectra

    Ritz, M.; Vaculíková, Lenka; Plevová, Eva; Matýsek, D.; Mališ, J.

    2012-01-01

    Roč. 60, č. 6 (2012), s. 655-665. ISSN 0009-8604 R&D Projects: GA MŠk ED2.1.00/03.0082 Grant ostatní: GA MŠk(CZ) ED0040/01/01 Institutional support: RVO:68145535 Keywords : infrared spectroscopy * chemometrics * minerals Subject RIV: CB - Analytical Chemistry, Separation Impact factor: 1.114, year: 2012 http://ccm.geoscienceworld.org/content/60/6/655.full.pdf+html

  3. Discrimination of Transgenic Rice containing the Cry1Ab Protein using Terahertz Spectroscopy and Chemometrics

    Wendao Xu; Lijuan Xie; Zunzhong Ye; Weilu Gao; Yang Yao; Min Chen; Jianyuan Qin; Yibin Ying

    2015-01-01

    Spectroscopic techniques combined with chemometrics methods have proven to be effective tools for the discrimination of objects with similar properties. In this work, terahertz time-domain spectroscopy (THz-TDS) combined with discriminate analysis (DA) and principal component analysis (PCA) with derivative pretreatments was performed to differentiate transgenic rice (Hua Hui 1, containing the Cry1Ab protein) from its parent (Ming Hui 63). Both rice samples and the Cry1Ab protein were ground a...

  4. Acoustics in the Martian Atmosphere

    Williams, J.-P.

    2000-10-01

    With the advent of the first attempt to deliver an acoustic microphone to the Martian surface aboard the failed Mars Polar Lander, there has been growing interests in the development of acoustic sensors to compliment scientific payloads on future spacecraft. Terrestrial scientist have been very successful in using infrasound (sound at frequencies below human detection, detect and monitor atmospheric phenomena related to weather, tornadoes, mountain waves, microbaroms, ionospheric and auroral disturbances, and meteror/fireballs, as well as anthropogenic sources such as aircraft and nuclear explosions. Sounds on Mars at the audible frequencies (20 Hz to 20 kHz) will be severely attenuated due to viscous relaxation and thermal diffusion (collectively referred to as classical attenuation) which will be much more severe in the colder, less dense Martian atmosphere. Molecular relaxation of carbon dioxide will also contribute to the sound absorption in the lower audible frequencies. Since classical attenuation increases as a function of the frequency squared, at low infrasonic frequencies ( < 10 Hz), classical attenuation becomes less significant and sound absorption in the Martian atmosphere becomes more similar to that of the terrestrial atmosphere for the same frequencies. At these longer wavelengths, geometric spreading will dominate as the source of attenuation as the acoustic energy is spread out over an ever increasing spherical wave front. This implies that infrasound (10 to 0.01 Hz) will be a useful frequency range for future acoustic sensors developed for scientific payloads delivered to the Martian surface.

  5. Analysis of Flavonoid in Medicinal Plant Extract Using Infrared Spectroscopy and Chemometrics.

    Wulandari, Lestyo; Retnaningtyas, Yuni; Nuri; Lukman, Hilmia

    2016-01-01

    Infrared (IR) spectroscopy combined with chemometrics has been developed for simple analysis of flavonoid in the medicinal plant extract. Flavonoid was extracted from medicinal plant leaves by ultrasonication and maceration. IR spectra of selected medicinal plant extract were correlated with flavonoid content using chemometrics. The chemometric method used for calibration analysis was Partial Last Square (PLS) and the methods used for classification analysis were Linear Discriminant Analysis (LDA), Soft Independent Modelling of Class Analogies (SIMCA), and Support Vector Machines (SVM). In this study, the calibration of NIR model that showed best calibration with R (2) and RMSEC value was 0.9916499 and 2.1521897, respectively, while the accuracy of all classification models (LDA, SIMCA, and SVM) was 100%. R (2) and RMSEC of calibration of FTIR model were 0.8653689 and 8.8958149, respectively, while the accuracy of LDA, SIMCA, and SVM was 86.0%, 91.2%, and 77.3%, respectively. PLS and LDA of NIR models were further used to predict unknown flavonoid content in commercial samples. Using these models, the significance of flavonoid content that has been measured by NIR and UV-Vis spectrophotometry was evaluated with paired samples t-test. The flavonoid content that has been measured with both methods gave no significant difference. PMID:27529051

  6. Discrimination of Corsican honey by FT-Raman spectroscopy and chemometrics

    Fernández Pierna, JA.

    2011-01-01

    Full Text Available Honey is a complex and challenging product to analyze due mainly to its composition consisting on various botanical sources. The discrimination of the origin of honey is of prime importance in order to reinforce the consumer trust in this typical food product. But this is not an easy task as usually no single chemical or physical parameter is sufficient. The aim of our paper is to investigate whether FT-Raman spectroscopy as spectroscopic fingerprint technique combined with some chemometric tools can be used as a rapid and reliable method for the discrimination of honey according to their source. In addition to that, different chemometric models are constructed in order to discriminate between Corsican honeys and honey coming from other regions in France, Italy, Austria, Germany and Ireland based on their FT-Raman spectra. These regions show a large variation in their plants. The developed models include the use of exploratory techniques as the Fisher criterion for wavenumber selection and supervised methods as Partial Least Squares-Discriminant Analysis (PLS-DA or Support Vector Machines (SVM. All these models showed a correct classification ratio between 85% and 90% of average showing that Raman spectroscopy combined to chemometric treatments is a promising way for rapid and non-expensive discrimination of honey according to their origin.

  7. Analysis of Flavonoid in Medicinal Plant Extract Using Infrared Spectroscopy and Chemometrics

    Retnaningtyas, Yuni; Nuri; Lukman, Hilmia

    2016-01-01

    Infrared (IR) spectroscopy combined with chemometrics has been developed for simple analysis of flavonoid in the medicinal plant extract. Flavonoid was extracted from medicinal plant leaves by ultrasonication and maceration. IR spectra of selected medicinal plant extract were correlated with flavonoid content using chemometrics. The chemometric method used for calibration analysis was Partial Last Square (PLS) and the methods used for classification analysis were Linear Discriminant Analysis (LDA), Soft Independent Modelling of Class Analogies (SIMCA), and Support Vector Machines (SVM). In this study, the calibration of NIR model that showed best calibration with R2 and RMSEC value was 0.9916499 and 2.1521897, respectively, while the accuracy of all classification models (LDA, SIMCA, and SVM) was 100%. R2 and RMSEC of calibration of FTIR model were 0.8653689 and 8.8958149, respectively, while the accuracy of LDA, SIMCA, and SVM was 86.0%, 91.2%, and 77.3%, respectively. PLS and LDA of NIR models were further used to predict unknown flavonoid content in commercial samples. Using these models, the significance of flavonoid content that has been measured by NIR and UV-Vis spectrophotometry was evaluated with paired samples t-test. The flavonoid content that has been measured with both methods gave no significant difference. PMID:27529051

  8. Chemometrics and vibrational spectroscopy as green tools for mine phytoremediation strategies

    Mokgalaka-Matlala, N. S.; Regnier, T.; Combrinck, S.; Kouekam, C. R.; Weiersbye, I. M.

    This study describes the use of near infrared (NIR) spectroscopy in combination with chemometrics to characterise Combretum erythrophyllum plant material to determine differences in the chemical profiles of samples harvested from mine contaminated areas and those of natural populations. The chemometric computation of near infrared vibrational spectra was used to generate principal component analysis and partial least squares models. These models were used to determine seasonal differences in the chemical matrices of samples harvested from the mine sites with different levels of contamination. Principal component analysis scatter plots illustrated clustering of phenolic profiles of samples depending on whether they originated from contaminated or uncontaminated soils. A partial least squares model was developed to link the variations in the chemical composition and levels of contamination in all samples collected in the same season (autumn). The levels of total soluble phenolic compounds in leaf extracts of C. erythrophyllum were measured using the Folin-Ciocalteau assay. Data analysis of the samples revealed that plants harvested from mine sites, particularly in summer, produced a higher level of phenolic compounds than those of the natural population, thereby displaying a good correlation with the chemometric models.

  9. Analysis of Flavonoid in Medicinal Plant Extract Using Infrared Spectroscopy and Chemometrics

    Lestyo Wulandari

    2016-01-01

    Full Text Available Infrared (IR spectroscopy combined with chemometrics has been developed for simple analysis of flavonoid in the medicinal plant extract. Flavonoid was extracted from medicinal plant leaves by ultrasonication and maceration. IR spectra of selected medicinal plant extract were correlated with flavonoid content using chemometrics. The chemometric method used for calibration analysis was Partial Last Square (PLS and the methods used for classification analysis were Linear Discriminant Analysis (LDA, Soft Independent Modelling of Class Analogies (SIMCA, and Support Vector Machines (SVM. In this study, the calibration of NIR model that showed best calibration with R2 and RMSEC value was 0.9916499 and 2.1521897, respectively, while the accuracy of all classification models (LDA, SIMCA, and SVM was 100%. R2 and RMSEC of calibration of FTIR model were 0.8653689 and 8.8958149, respectively, while the accuracy of LDA, SIMCA, and SVM was 86.0%, 91.2%, and 77.3%, respectively. PLS and LDA of NIR models were further used to predict unknown flavonoid content in commercial samples. Using these models, the significance of flavonoid content that has been measured by NIR and UV-Vis spectrophotometry was evaluated with paired samples t-test. The flavonoid content that has been measured with both methods gave no significant difference.

  10. Application of mass spectrometry based electronic nose and chemometrics for fingerprinting radiation treatment

    Volatile compounds were isolated from apples and grapes employing solid phase micro extraction (SPME) and subsequently analyzed by GC/MS equipped with a transfer line without stationary phase. Single peak obtained was integrated to obtain total mass spectrum of the volatile fraction of samples. A data matrix having relative abundance of all mass-to-charge ratios was subjected to principal component analysis (PCA) and linear discriminant analysis (LDA) to identify radiation treatment. PCA results suggested that there is sufficient variability between control and irradiated samples to build classification models based on supervised techniques. LDA successfully aided in segregating control from irradiated samples at all doses (0.1, 0.25, 0.5, 1.0, 1.5, 2.0 kGy). SPME-MS with chemometrics was successfully demonstrated as simple screening method for radiation treatment. - Highlights: • Total mass spectra obtained from HS-MS for control and irradiated fruits. • Grapes and apples are chosen for present study. • Total mass spectrum was analyzed by two chemometric techniques (PCA and LDA). • Successful segregation of control and irradiated samples achieved using chemometrics

  11. Atlantic Herring Acoustic Surveys

    National Oceanic and Atmospheric Administration, Department of Commerce — The NEFSC Advanced Sampling Technologies Research Group conducts annual fisheries acoustic surveys using state-of-the-art acoustic, midwater trawling, and...

  12. Acoustic Neuroma Educational Video

    Full Text Available ... Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask Yourself ... Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask Yourself ...

  13. Acoustic Neuroma Educational Video

    Full Text Available ... is ANA? Mission Statement Board of Directors ANA Staff Medical Advisory Board News ANA Annual Reports Acoustic ... is ANA? Mission Statement Board of Directors ANA Staff Medical Advisory Board News ANA Annual Reports Acoustic ...

  14. Acoustic Neuroma Educational Video

    Full Text Available ... ANA Annual Reports Acoustic Neuroma Legacy Society Programs & Services Join/Renew Ways to Give ANA Discussion Forum ... ANA Annual Reports Acoustic Neuroma Legacy Society Programs & Services Search ANAUSA.org Connect with us! Educational Video ...

  15. Acoustic Neuroma Educational Video

    Full Text Available ... Resources Patient Surveys Related Links Clinical Trials.gov Health Care Insurance Toolkit Additional Resources ANA Public Webinars © 2016 Acoustic Neuroma Association Acoustic Neuroma Association ® • ...

  16. Acoustic Neuroma Educational Video

    Full Text Available ... Options Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask ... Options Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask ...

  17. Acoustic Neuroma Educational Video

    Full Text Available ... ANA Staff Medical Advisory Board News ANA Annual Reports Acoustic Neuroma Legacy Society Programs & Services Join/Renew ... ANA Staff Medical Advisory Board News ANA Annual Reports Acoustic Neuroma Legacy Society Programs & Services Search ANAUSA. ...

  18. Cystic acoustic neuromas

    Chitkara, Naveen; Chanda, Rakesh; Yadav, S. P. S.; N.K. Sharma

    2002-01-01

    Predominantly cystic acoustic neuromas are rare and they usually present with clinical and radiological features different from their more common solid counterparts. Two cases of cystic acoustic neuromas are reported here.

  19. Nonlinear ultrasonic spectroscopy and acoustic emission in SHM of aircrafts

    Převorovský, Zdeněk; Chlada, Milan; Krofta, Josef

    2012-01-01

    Roč. 2012, SI (2012), s. 36-40. ISSN 1213-3825 R&D Projects: GA MPO(CZ) FR-TI1/274 Institutional support: RVO:61388998 Keywords : NDT * structural health monitoring * acoustic emission * nonlinear elastic wave spectroscopy * time reversal mirrors Subject RIV: BI - Acoustics

  20. Acoustic emission monitoring in Cooke 4 gold mine in South Africa -summary of the main findings of a 5-year SATREPS project-

    Naoi, M.; Nakatani, M.; Moriya, H.; Otsuki, K.; Kgarume, T.; Philipp, J.; Murakami, O.; Masakale, T.; Ribeiro, L.; Yabe, Y.; Kawakata, H.; Ward, A.; Durrheim, R.; Ogasawara, H.

    2015-12-01

    We deployed a network targeting acoustic emissions (AEs) down to Mw~ -5 at 1-km depth in the Cooke 4 mine in South Africa as a part of a 5-year project called "Observational Studies in South African Mines to Mitigate Seismic Risks." This network of 30 sensors spans ~100 m, and collected waveform data for more than 4.5-million triggers in 5 years. We provide an overview of the main findings. 1) Naoi et al. (2015; Pageoph) reported that 90% of observed AEs aggregated along the advancing mining front. Their size distribution obeyed the Gutenberg-Richter law down to Mw -4, and their b-values were invariant with time from blasting, contradicting a previous study. 2) Moriya et al. (under review) showed that this AE aggregation consists of several tabular clusters, which were formed regularly as the mining front advanced. Although large earthquakes (Mw > 1) were not found, the clusters likely represent the preparation process of large shear fracture events because their geometry resembles large shear fractures, known by in-situ wall-rock observation, which formed concurrently with large seismic events. 3) Naoi et al. (2015; Tectonophysics) reported that the remaining 10% of AEs exhibit very sharp, planar distributions, with high b-values. They are likely events located on pre-existing geological faults loaded by mining-induced stresses. Such on-fault events are rare for intraplate faults, where microseismic events generally occur in the surrounding region. 4) Naoi et al. (2015; JGR) found planar clusters that newly emerged ahead of a mining front and gradually expanded to 20 m. They likely represent the evolution of a slow-slip patch on a pre-existing fault. The b-value of those AEs decreased drastically from 2.5 to 1.5, consistent with stress buildup by the approaching mining front. This project is supported by JST/JICA, SATREPS, JSPS KAKENHI Grant Numbers 21224012, 21246134, 26249137, 26887022, and MEXT's Earthquake and Volcano Hazards Observation and Research Program.

  1. Acoustic energy transmission in cast iron pipelines

    Kiziroglou, Michail E.; Boyle, David E.; Wright, Steven W.; Yeatman, Eric M.

    2015-12-01

    In this paper we propose acoustic power transfer as a method for the remote powering of pipeline sensor nodes. A theoretical framework of acoustic power propagation in the ceramic transducers and the metal structures is drawn, based on the Mason equivalent circuit. The effect of mounting on the electrical response of piezoelectric transducers is studied experimentally. Using two identical transducer structures, power transmission of 0.33 mW through a 1 m long, 118 mm diameter cast iron pipe, with 8 mm wall thickness is demonstrated, at 1 V received voltage amplitude. A near-linear relationship between input and output voltage is observed. These results show that it is possible to deliver significant power to sensor nodes through acoustic waves in solid structures. The proposed method may enable the implementation of acoustic - powered wireless sensor nodes for structural and operation monitoring of pipeline infrastructure.

  2. Passive Acoustic Monitoring the Diel, Lunar, Seasonal and Tidal Patterns in the Biosonar Activity of the Indo-Pacific Humpback Dolphins (Sousa chinensis in the Pearl River Estuary, China.

    Zhi-Tao Wang

    Full Text Available A growing demand for sustainable energy has led to an increase in construction of offshore windfarms. Guishan windmill farm will be constructed in the Pearl River Estuary, China, which sustains the world's largest known population of Indo-Pacific humpback dolphins (Sousa chinensis. Dolphin conservation is an urgent issue in this region. By using passive acoustic monitoring, a baseline distribution of data on this species in the Pearl River Estuary during pre-construction period had been collected. Dolphin biosonar detection and its diel, lunar, seasonal and tidal patterns were examined using a Generalized Linear Model. Significant higher echolocation detections at night than during the day, in winter-spring than in summer-autumn, at high tide than at flood tide were recognized. Significant higher echolocation detections during the new moon were recognized at night time. The diel, lunar and seasonal patterns for the echolocation encounter duration also significantly varied. These patterns could be due to the spatial-temporal variability of dolphin prey and illumination conditions. The baseline information will be useful for driving further effective action on the conservation of this species and in facilitating later assessments of the effects of the offshore windfarm on the dolphins by comparing the baseline to post construction and post mitigation efforts.

  3. Passive Acoustic Monitoring the Diel, Lunar, Seasonal and Tidal Patterns in the Biosonar Activity of the Indo-Pacific Humpback Dolphins (Sousa chinensis) in the Pearl River Estuary, China.

    Wang, Zhi-Tao; Nachtigall, Paul E; Akamatsu, Tomonari; Wang, Ke-Xiong; Wu, Yu-Ping; Liu, Jian-Chang; Duan, Guo-Qin; Cao, Han-Jiang; Wang, Ding

    2015-01-01

    A growing demand for sustainable energy has led to an increase in construction of offshore windfarms. Guishan windmill farm will be constructed in the Pearl River Estuary, China, which sustains the world's largest known population of Indo-Pacific humpback dolphins (Sousa chinensis). Dolphin conservation is an urgent issue in this region. By using passive acoustic monitoring, a baseline distribution of data on this species in the Pearl River Estuary during pre-construction period had been collected. Dolphin biosonar detection and its diel, lunar, seasonal and tidal patterns were examined using a Generalized Linear Model. Significant higher echolocation detections at night than during the day, in winter-spring than in summer-autumn, at high tide than at flood tide were recognized. Significant higher echolocation detections during the new moon were recognized at night time. The diel, lunar and seasonal patterns for the echolocation encounter duration also significantly varied. These patterns could be due to the spatial-temporal variability of dolphin prey and illumination conditions. The baseline information will be useful for driving further effective action on the conservation of this species and in facilitating later assessments of the effects of the offshore windfarm on the dolphins by comparing the baseline to post construction and post mitigation efforts. PMID:26580966

  4. Passive Acoustic Studies of North Atlantic Right Whales

    National Oceanic and Atmospheric Administration, Department of Commerce — Passive acoustic monitoring buoys have been deployed in shallow waters between North Carolina and Northern Florida since 2003. These units are bottom mounted...

  5. Potential of acoustic emissions from three point bending tests as rock failure precursors

    Agioutantis Z.; Kaklis K.; Mavrigiannakis S.; Verigakis M.; Vallianatos F.; Saltas V.

    2016-01-01

    Development of failure in brittle materials is associated with microcracks, which release energy in the form of elastic waves called acoustic emissions. This paper presents results from acoustic emission mea-surements obtained during three point bending tests on Nestos marble under laboratory conditions. Acoustic emission activity was monitored using piezoelectric acoustic emission sensors, and the potential for accurate prediction of rock damage based on acoustic emission data was investigated. Damage local-ization was determined based on acoustic emissions generated from the critically stressed region as scat-tered events at stresses below and close to the strength of the material.

  6. Study and monitoring by acoustic emission coupled with electrochemical techniques of steel and rubber steel corrosion in acid medium; Etude et suivi par emission accoustique associe a des techniques electrochimiques de la corrosion d'acier et d'acier revetu d'elastomeres en milieu acide

    Idrissi, H. [Institut National des Sciences Appliquees, INSA, 69 - Villeurbanne (France); Boulif, R.; Maghnouj, J. [CERPHOS, Groupe Office Cherifienne des Phosphates, OCP, Casablanca (Morocco)

    2001-07-01

    During the past ten years the application of the acoustic emission technique in the field of corrosion allowed a detection and a characterization on factory site of the stress corrosion and corrosion-abrasion phenomena. In this spirit, its use can be extended to the monitoring of general corrosion and of corrosion under deposit. This work constitutes the base of a study aiming to a better understanding and a better controlling of corrosion phenomenon of steels covered or not, with a later objective: the development of a simple follow-up technique on industrial site. Within this framework, our objective is not only to study by electrochemical and acoustics techniques the general corrosion of various ordinary steels naked or covered with an elastomer coating, but also to develop a procedure, based on the acoustic emission, allowing the early detection of these steels corrosion when the protective coatings used are damaged. So, series of electrochemical tests coupled with the acoustic emission, such as the layouts of the volt-amperometric curves and measurements of the resistance of polarization, were carried out on two steels XC48 and A60 at ambient temperature and in concentrated phosphoric acid with 30% of P2O5 with the presence of impurities of Cl -, F -, SO42 -. For the covered samples we insisted more particularly on the presence or not of defects in the elastomer coating used. The obtained results made it possible, first to show the principal emissive sources during corrosion, secondly to specify the characteristics of the acoustic signals and finally to correlate these signals with traditional electrochemical measurements and the micrographic observations after tests. The characterization of the acoustic and electrochemical parameters enabled us to specify the sensitivity of the EA to this corrosion phenomenon of steels naked or covered with an elastomer coating. (authors)

  7. ACOUSTICAL STANDARDS NEWS.

    Blaeser, Susan B; Struck, Christopher J

    2016-03-01

    American National Standards (ANSI Standards) developed by Accredited Standards Committees S1, S2, S3, S3/SC 1, and S12 in the areas of acoustics, mechanical vibration and shock, bioacoustics, animal bioacoustics, and noise, respectively, are published by the Acoustical Society of America (ASA). In addition to these standards, ASA publishes a catalog of Acoustical American National Standards. To receive a copy of the latest Standards catalog, please contact Susan B. Blaeser.Comments are welcomed on all material in Acoustical Standards News.This Acoustical Standards News section in JASA, as well as the National Catalog of Acoustical Standards and other information on the Standards Program of the Acoustical Society of America, are available via the ASA home page: http://acousticalsociety.org. PMID:27036268

  8. Sensor combination and chemometric variable selection for online monitoring of Streptomyces coelicolor fed-batch cultivations

    Ödman, Peter; Johansen, C.L.; Olsson, L.;

    2010-01-01

    of biomass and substrate (casamino acids) concentrations, respectively. The effect of combination of fluorescence and gas analyzer data as well as of different variable selection methods was investigated. Improved prediction models were obtained by combination of data from the two sensors and by...... variable selection using a genetic algorithm, interval PLS, and the principal variables method, respectively. A stepwise variable elimination method was applied to the three-way fluorescence data, resulting in simpler and more accurate N-PLS models. The prediction models were validated using leave...

  9. Blue and fin whale acoustics and ecology off Antarctic Peninsula

    Sirovic, Ana

    2006-01-01

    Blue (Balaenoptera musculus) and fin whales (B. physalus) in the Southern Ocean were subjects of extensive whaling industry during the twentieth century. Their current population numbers remain low, making population monitoring using traditional visual surveys difficult. Both blue and fin whales produce low frequency, regularly repeated calls and are suitable for acoustic monitoring. Eight, continuously recording acoustic recorders were deployed off the Western Antarctic Peninsula (WAP) betwe...

  10. Holographic and acoustic emission evaluation of pressure vessels

    Optical holographic interfereometry and acoustic emission monitoring were simultaneously used to evaluate two small, high pressure vessels during pressurization. The techniques provide pressure vessel designers with both quantitative information such as displacement/strain measurements and qualitative information such as flaw detection. The data from the holographic interferograms were analyzed for strain profiles. The acoustic emission signals were monitored for crack growth and vessel quality

  11. Chemometric techniques in distribution, characterisation and source apportionment of polycyclic aromatic hydrocarbons (PAHS) in aquaculture sediments in Malaysia.

    Retnam, Ananthy; Zakaria, Mohamad Pauzi; Juahir, Hafizan; Aris, Ahmad Zaharin; Zali, Munirah Abdul; Kasim, Mohd Fadhil

    2013-04-15

    This study investigated polycyclic aromatic hydrocarbons (PAHs) pollution in surface sediments within aquaculture areas in Peninsular Malaysia using chemometric techniques, forensics and univariate methods. The samples were analysed using soxhlet extraction, silica gel column clean-up and gas chromatography mass spectrometry. The total PAH concentrations ranged from 20 to 1841 ng/g with a mean of 363 ng/g dw. The application of chemometric techniques enabled clustering and discrimination of the aquaculture sediments into four groups according to the contamination levels. A combination of chemometric and molecular indices was used to identify the sources of PAHs, which could be attributed to vehicle emissions, oil combustion and biomass combustion. Source apportionment using absolute principle component scores-multiple linear regression showed that the main sources of PAHs are vehicle emissions 54%, oil 37% and biomass combustion 9%. Land-based pollution from vehicle emissions is the predominant contributor of PAHs in the aquaculture sediments of Peninsular Malaysia. PMID:23452623

  12. Program to develop acoustic emission-flaw relationship for inservice monitoring of nuclear pressure vessels. Annual report, July 1, 1976--October 1, 1977

    Laboratory mechanical tests were conducted to evaluate AE during uniaxial tensile, fracture and fatigue crack growth in A533B pressure vessel steel. The A533B steel included two heats of Class 1, one heat of Class 2 and a weldment made for the Heavy Section Steel Technology (HSST) Program. Specimen types included uniaxial tensile specimens, size 2 compact tension specimens for fatigue crack growth and fracture tests, and a single-edge notch specimen also for fatigue crack growth through material that was uniformly strained 3% prior to fatigue testing. In addition, AE monitoring was conducted on the HSST V-7B 6-inch thick pressure vessel test. AE data were partitioned into four ranges of signal amplitude and rise time. All the AE data were analyzed, with respect to mechanical behavior of A533B steel. Linear elastic fracture mechanics analysis methods were used to relate AE parameters to fracture and fatigue crack growth parameters. AE data from the V-7B vessel test were correlated with stress intensity factor and crack opening displacement. AE data from the fatigue crack growth tests were investigated using models based on fatigue crack growth rate, fatigue crack area and theoretical crack tip plastic zone size

  13. Inspection of copper canister for spent nuclear fuel by means of ultrasound. Copper characterization, FSW monitoring with acoustic emission and ultrasonic imaging

    Stepinski, Tadeusz (ed.); Engholm, Marcus; Olofsson, Tomas (Uppsala Univ., Signals and Systems, Dept. of Technical Sciences, Uppsala (Sweden))

    2009-08-15

    This report contains the research results concerning advanced ultrasound for the inspection of copper canisters for spent nuclear fuel obtained at Signals and Systems, Uppsala University in 2008. The first part of the report is concerned with aspects related to ultrasonic attenuation of copper material used for canisters. We present results of attenuation measurement performed for a number of samples taken from a real canister; two from the lid and four from different parts of canister wall. Ultrasonic attenuation of the material originating from canister lid is relatively low (less that 50 dB/m) and essentially frequency independent in the frequency range up to 5 MHz. However, for the material originating from the extruded canister part considerable variations of the attenuation are observed, which can reach even 200 dB/m at 3.5 MHz. In the second part of the report we present further development of the concept of the friction stir welding process monitoring by means of multiple sensors formed into a uniform circular array (UCA). After a brief introduction into modeling Lamb waves and UCA we focus on array processing techniques that enable estimating direction of arrival of multimodal Lamb waves. We consider two new techniques, the Capon beamformer and the broadband multiple signal classification technique (MUSIC). We present simulation results illustrating their performance. In the final part we present the phase shift migration algorithm for ultrasonic imaging of layered media using synthetic aperture concept. We start from explaining theory of the phase migration concept, which is followed by the results of experiments performed on copper blocks with drilled holes. We show that the proposed algorithm performs well for immersion inspection of metal objects and yields both improved spatial resolution and suppressed grain noise

  14. Inspection of copper canister for spent nuclear fuel by means of ultrasound. Copper characterization, FSW monitoring with acoustic emission and ultrasonic imaging

    This report contains the research results concerning advanced ultrasound for the inspection of copper canisters for spent nuclear fuel obtained at Signals and Systems, Uppsala University in 2008. The first part of the report is concerned with aspects related to ultrasonic attenuation of copper material used for canisters. We present results of attenuation measurement performed for a number of samples taken from a real canister; two from the lid and four from different parts of canister wall. Ultrasonic attenuation of the material originating from canister lid is relatively low (less that 50 dB/m) and essentially frequency independent in the frequency range up to 5 MHz. However, for the material originating from the extruded canister part considerable variations of the attenuation are observed, which can reach even 200 dB/m at 3.5 MHz. In the second part of the report we present further development of the concept of the friction stir welding process monitoring by means of multiple sensors formed into a uniform circular array (UCA). After a brief introduction into modeling Lamb waves and UCA we focus on array processing techniques that enable estimating direction of arrival of multimodal Lamb waves. We consider two new techniques, the Capon beamformer and the broadband multiple signal classification technique (MUSIC). We present simulation results illustrating their performance. In the final part we present the phase shift migration algorithm for ultrasonic imaging of layered media using synthetic aperture concept. We start from explaining theory of the phase migration concept, which is followed by the results of experiments performed on copper blocks with drilled holes. We show that the proposed algorithm performs well for immersion inspection of metal objects and yields both improved spatial resolution and suppressed grain noise

  15. AST Launch Vehicle Acoustics

    Houston, Janice; Counter, D.; Giacomoni, D.

    2015-01-01

    The liftoff phase induces acoustic loading over a broad frequency range for a launch vehicle. These external acoustic environments are then used in the prediction of internal vibration responses of the vehicle and components which result in the qualification levels. Thus, predicting these liftoff acoustic (LOA) environments is critical to the design requirements of any launch vehicle. If there is a significant amount of uncertainty in the predictions or if acoustic mitigation options must be implemented, a subscale acoustic test is a feasible pre-launch test option to verify the LOA environments. The NASA Space Launch System (SLS) program initiated the Scale Model Acoustic Test (SMAT) to verify the predicted SLS LOA environments and to determine the acoustic reduction with an above deck water sound suppression system. The SMAT was conducted at Marshall Space Flight Center and the test article included a 5% scale SLS vehicle model, tower and Mobile Launcher. Acoustic and pressure data were measured by approximately 250 instruments. The SMAT liftoff acoustic results are presented, findings are discussed and a comparison is shown to the Ares I Scale Model Acoustic Test (ASMAT) results.

  16. Acoustic estimation of suspended sediment concentration

    ZHU; Weiqing(

    2001-01-01

    [1]Morse, P. H. , Theoretical Acoustics, New York: McGraw-Hill Book Co. , 1968.[2]Skudrjuk, E., Die Grundlagen der Akustik, Wien: Springer-Verlag, 1954.[3]Olshevskii, V. V., Statistical Characteristics of Sea Reverberation, Moscow: Nauka Publisher, 1966.[4]Thorne, P. D., Hardcastl, P. J., Soulsby, R. L., Analysis of acoustic measurements of suspended sediments, J. Geop.Res. , 1993, 98: 899.[5]Guo Jijie, Ren Laifa, Li Yunwu, ln-situ calibration of acoustic measurement of suspended sedienmt, Acta Oceanologica Sini-ca, 1998, (20): 120-125.[6]Zhang Shuying, Li Yunwu, Development and application of an acoustic suspended sediemnt monitoring system, Acta Oceanologica Sinica, 1998, (20): 114-119.[7]Zhang Shuying, Li Yunwu, A theoretical analysis of acoustic suspended sediment obsvervation, Acta Acoustica, 1999, (24):267-274.[8]Zhu Weiqing, Pan Feng, Zhu Min et al. , IOA-1 Multi-function Acoustic Doppler Current Profiler (MADCP), OCEAN'2000,Rhode Island, USA.

  17. Chemometric resolution of coeluting peaks of eleven antihypertensives from multiple classes in high performance liquid chromatography: a comprehensive research in human serum, health product and Chinese patent medicine samples.

    Zhao, Juan; Wu, Hai-Long; Niu, Jing-Fang; Yu, Yong-Jie; Yu, Li-Li; Kang, Chao; Li, Quan; Zhang, Xiao-Hua; Yu, Ru-Qin

    2012-08-01

    A novel chemometric-assisted high performance liquid chromatography method coupled with diode array detector (HPLC-DAD) was presented for the simultaneous determination of eleven antihypertensives from multiple classes in most concerned matrix systems. With the aid of second-order calibration which enables specific information of analytes to be well extracted, the heavily overlapping profiles between analytes and the coeluting interferences can be successfully separated and thus accurately quantified. A great advantage of the novel strategy lies in the fact that the analysis could be carried out with the same isocratic mobile phase (methanol/KH(2)PO(4): 58:42, v/v, pH 2.60) in a short time regardless of the changes of matrices, such as human serum, health product and Chinese patent medicine. Both qualitative and quantitative results indicate that the hybrid strategy that using HPLC-DAD coupled with second-order chemometric method would be a high performance approach for the purpose of simultaneously quantifying multiple classes of antihypertensives in complex systems. Additionally, the analytical strategy can potentially benefit drug monitoring in both therapeutic research and pharmaceutical quality control. Moreover, the accuracy and reliability of the proposed methodology has been evaluated using several statistical parameters such as root mean squared error of prediction (RMSEP), figures of merit (FOM) and reproducibility of inter-day analysis. PMID:22795572

  18. Acoustical experiment of yogurt fermentation process.

    Ogasawara, H; Mizutani, K; Ohbuchi, T; Nakamura, T

    2006-12-22

    One of the important factors through food manufacturing is hygienic management. Thus, food manufactures prove their hygienic activities by taking certifications like a Hazard Analysis and Critical Control Point (HACCP). This concept also applies to food monitoring. Acoustical measurements have advantage for other measurement in food monitoring because they make it possible to measure with noncontact and nondestructive. We tried to monitor lactic fermentation of yogurt by a probing sensor using a pair of acoustic transducers. Temperature of the solution changes by the reaction heat of fermentation. Consequently the sound velocity propagated through the solution also changes depending on the temperature. At the same time, the solution change its phase from liquid to gel. The transducers usage in the solution indicates the change of the temperature as the change of the phase difference between two transducers. The acoustic method has advantages of nondestructive measurement that reduces contamination of food product by measuring instrument. The sensor was inserted into milk with lactic acid bacterial stain of 19 degrees C and monitored phase retardation of propagated acoustic wave and its temperature with thermocouples in the mild. The monitoring result of fermentation from milk to Caspian Sea yogurt by the acoustic transducers with the frequency of 3.7 MHz started to show gradient change in temperature caused by reaction heat of fermentation but stop the gradient change at the end although the temperature still change. The gradient change stopped its change because of phase change from liquid to gel. The present method will be able to measure indirectly by setting transducers outside of the measuring object. This noncontact sensing method will have great advantage of reduces risk of food contamination from measuring instrument because the measurement probes are set out of fermentation reactor or food containers. Our proposed method will contribute to the

  19. ATR-FTIR spectroscopy and chemometrics: An interesting tool to discriminate and characterize counterfeit medicines.

    Custers, D; Cauwenbergh, T; Bothy, J L; Courselle, P; De Beer, J O; Apers, S; Deconinck, E

    2015-08-10

    Counterfeit medicines pose a huge threat to public health worldwide. High amounts of counterfeit pharmaceuticals enter the European market and therefore detection of these products is essential. Attenuated Total Reflection Fourier-Transform infrared spectroscopy (ATR-FTIR) might be useful for the screening of counterfeit medicines since it is easy to use and little sample preparation is required. Furthermore, this approach might be helpful to customs to obtain a first evaluation of suspected samples. This study proposes a combination of ATR-FTIR and chemometrics to discriminate and classify counterfeit medicines. A sample set, containing 209 samples in total, was analyzed using ATR-FTIR and the obtained spectra were used as fingerprints in the chemometric data-analysis which included Principal Component Analysis (PCA), k-Nearest Neighbours (k-NN), Classification and Regression Trees (CART) and Soft Independent Modelling of Class Analogy (SIMCA). First it was verified whether the mentioned techniques are capable to distinguish samples containing different active pharmaceutical ingredients (APIs). PCA showed a clear tendency of discrimination based on the API present; k-NN, CART and SIMCA were capable to create suitable prediction models based on the presence of different APIs. However k-NN performs the least while SIMCA performs the best. Secondly, it was tested whether these three models could be expanded to discriminate between genuine and counterfeit samples as well. k-NN was not able to make the desired discrimination and therefore it was not useful. CART performed better but also this model was less suited. SIMCA, on the other hand, resulted in a model with a 100% correct discrimination between genuine and counterfeit drugs. This study shows that chemometric analysis of ATR-FTIR fingerprints is a valuable tool to discriminate genuine from counterfeit samples and to classify counterfeit medicines. PMID:25476739

  20. Hybrid approach combining chemometrics and likelihood ratio framework for reporting the evidential value of spectra.

    Martyna, Agnieszka; Zadora, Grzegorz; Neocleous, Tereza; Michalska, Aleksandra; Dean, Nema

    2016-08-10

    Many chemometric tools are invaluable and have proven effective in data mining and substantial dimensionality reduction of highly multivariate data. This becomes vital for interpreting various physicochemical data due to rapid development of advanced analytical techniques, delivering much information in a single measurement run. This concerns especially spectra, which are frequently used as the subject of comparative analysis in e.g. forensic sciences. In the presented study the microtraces collected from the scenarios of hit-and-run accidents were analysed. Plastic containers and automotive plastics (e.g. bumpers, headlamp lenses) were subjected to Fourier transform infrared spectrometry and car paints were analysed using Raman spectroscopy. In the forensic context analytical results must be interpreted and reported according to the standards of the interpretation schemes acknowledged in forensic sciences using the likelihood ratio approach. However, for proper construction of LR models for highly multivariate data, such as spectra, chemometric tools must be employed for substantial data compression. Conversion from classical feature representation to distance representation was proposed for revealing hidden data peculiarities and linear discriminant analysis was further applied for minimising the within-sample variability while maximising the between-sample variability. Both techniques enabled substantial reduction of data dimensionality. Univariate and multivariate likelihood ratio models were proposed for such data. It was shown that the combination of chemometric tools and the likelihood ratio approach is capable of solving the comparison problem of highly multivariate and correlated data after proper extraction of the most relevant features and variance information hidden in the data structure. PMID:27282749

  1. Classification of different tomato seed cultivars by multispectral visible-near infrared spectroscopy and chemometrics

    Shrestha, Santosh; Deleuran, Lise Christina; Gislum, René

    2016-01-01

    nm were extracted from multispectral images of tomato seeds. Principal component analysis (PCA) was used for data exploration, while partial least squares discriminant analysis (PLS-DA) and support vector machine discriminant analysis (SVM-DA) were used to classify the five different tomato cultivars....... The results showed very good classification accuracy for two independent test sets ranging from 94% to 100% for all tomato cultivars irrespective of chemometric methods. The overall classification error rates were 3.2% and 0.4% for the PLS-DA and SVM-DA calibration models, respectively. The results...

  2. Provenance of pottery determined by soil physicochemical and chemometric methods: A case study from Frederiksgave, Ghana

    Rasmussen, Lars Holm; Bredwa-Mensah, Y.; Borggaard, Ole K.;

    2009-01-01

    The suitability of using traditional soil chemical and mineralogical methods combined with chemometrics to trace provenance of archaeological samples was tested on potsherds from Frederiksgave, a former Danish plantation in southern Ghana, in use from 18301850. Soil and six potsherds from...... Frederiksgave, together with potsherds from two likely production sites at Ga and Dangme Shai, were investigated by visual inspection, total element analysis and X-ray diffraction and the results analyzed by principal component analysis (PCA) and cluster analysis. The investigation clearly showed that the...

  3. Acoustic sensor array extracts physiology during movement

    Scanlon, Michael V.

    2001-08-01

    An acoustic sensor attached to a person's neck can extract heart and breath sounds, as well as voice and other physiology related to their health and performance. Soldiers, firefighters, law enforcement, and rescue personnel, as well as people at home or in health care facilities, can benefit form being remotely monitored. ARLs acoustic sensor, when worn around a person's neck, picks up the carotid artery and breath sounds very well by matching the sensor's acoustic impedance to that of the body via a gel pad, while airborne noise is minimized by an impedance mismatch. Although the physiological sounds have high SNR, the acoustic sensor also responds to motion-induced artifacts that obscure the meaningful physiology. To exacerbate signal extraction, these interfering signals are usually covariant with the heart sounds, in that as a person walks faster the heart tends to beat faster, and motion noises tend to contain low frequency component similar to the heart sounds. A noise-canceling configuration developed by ARL uses two acoustic sensor on the front sides of the neck as physiology sensors, and two additional acoustic sensor on the back sides of the neck as noise references. Breath and heart sounds, which occur with near symmetry and simultaneously at the two front sensor, will correlate well. The motion noise present on all four sensor will be used to cancel the noise on the two physiology sensors. This report will compare heart rate variability derived from both the acoustic array and from ECG data taken simultaneously on a treadmill test. Acoustically derived breath rate and volume approximations will be introduced as well. A miniature 3- axis accelerometer on the same neckband provides additional noise references to validate footfall and motion activity.

  4. Acoustic streaming in microchannels

    Tribler, Peter Muller

    , and experimental results for the streaming-induced drag force dominated motion of particles suspended in a water-filled microchannel supporting a transverse half-wavelength resonance. The experimental and theoretical results agree within a mean relative dierence of approximately 20%, a low deviation given state......This thesis presents studies of boundary-driven acoustic streaming in microfluidic channels, which is a steady flow of the fluid initiated by the interactions of an oscillating acoustic standing wave and the rigid walls of the microchannel. The studies present analysis of the acoustic resonance......, the acoustic streaming flow, and the forces on suspended microparticles. The work is motivated by the application of particle focusing by acoustic radiation forces in medical, environmental and food sciences. Here acoustic streaming is most often unwanted, because it limits the focusability of particles...

  5. Vibro-acoustics

    Nilsson, Anders

    2015-01-01

    This three-volume book gives a thorough and comprehensive presentation of vibration and acoustic theories. Different from traditional textbooks which typically deal with some aspects of either acoustic or vibration problems, it is unique of this book to combine those two correlated subjects together. Moreover, it provides fundamental analysis and mathematical descriptions for several crucial phenomena of Vibro-Acoustics which are quite useful in noise reduction, including how structures are excited, energy flows from an excitation point to a sound radiating surface, and finally how a structure radiates noise to a surrounding fluid. Many measurement results included in the text make the reading interesting and informative. Problems/questions are listed at the end of each chapter and the solutions are provided. This will help the readers to understand the topics of Vibro-Acoustics more deeply. The book should be of interest to anyone interested in sound and vibration, vehicle acoustics, ship acoustics and inter...

  6. Springer handbook of acoustics

    2014-01-01

    Acoustics, the science of sound, has developed into a broad interdisciplinary field encompassing the academic disciplines of physics, engineering, psychology, speech, audiology, music, architecture, physiology, neuroscience, and electronics. The Springer Handbook of Acoustics is also in his 2nd edition an unparalleled modern handbook reflecting this richly interdisciplinary nature edited by one of the acknowledged masters in the field, Thomas Rossing. Researchers and students benefit from the comprehensive contents. This new edition of the Handbook features over 11 revised and expanded chapters, new illustrations, and 2 new chapters covering microphone arrays  and acoustic emission.  Updated chapters contain the latest research and applications in, e.g. sound propagation in the atmosphere, nonlinear acoustics in fluids, building and concert hall acoustics, signal processing, psychoacoustics, computer music, animal bioacousics, sound intensity, modal acoustics as well as new chapters on microphone arrays an...

  7. Monitoring of pipeline hydrostatic testing with artificial flaws applying acoustic emission and ultra-sonic techniques; Monitoracao de teste hidrostatico de tubos com descontinuidades artificiais empregando as tecnicas de emissao acustica e ultra-som

    Soares, Sergio Damasceno [PETROBRAS, Rio de Janeiro, RJ (Brazil). Centro de Pesquisas (CENPES)

    2003-07-01

    Charts and parameters used to perform and analyzing the acoustic emission data collected during the hydrostatic test in pipe samples build in API XL 60 with 20 inches of diameter and 14 millimeters of thickness are shown. These pipes had internal and external artificial flaws done by electro-erosion process with aspect ratio 1 x 20. A relationship between acoustic emission results, ultrasound and J-Integral were established using the applied pressurization sequence. Characteristics values of acoustic emission signals were shown as a criteria of field tests. (author)

  8. Localized Acoustic Surface Modes

    Farhat, Mohamed

    2015-08-04

    We introduce the concept of localized acoustic surface modes (ASMs). We demonstrate that they are induced on a two-dimensional cylindrical rigid surface with subwavelength corrugations under excitation by an incident acoustic plane wave. Our results show that the corrugated rigid surface is acoustically equivalent to a cylindrical scatterer with uniform mass density that can be represented using a Drude-like model. This, indeed, suggests that plasmonic-like acoustic materials can be engineered with potential applications in various areas including sensing, imaging, and cloaking.

  9. Shallow Water Acoustic Laboratory

    Federal Laboratory Consortium — FUNCTION: Supports experimental research where high-frequency acoustic scattering and surface vibration measurements of fluid-loaded and non-fluid-loaded structures...

  10. Handbook of Engineering Acoustics

    Möser, Michael

    2013-01-01

    This book examines the physical background of engineering acoustics, focusing on empirically obtained engineering experience as well as on measurement techniques and engineering methods for prognostics. Its goal is not only to describe the state of art of engineering acoustics but also to give practical help to engineers in order to solve acoustic problems. It deals with the origin, the transmission and the methods of the abating different kinds of air-borne and structure-borne sounds caused by various mechanisms – from traffic to machinery and flow-induced sound. In addition the modern aspects of room and building acoustics, as well as psychoacoustics and active noise control, are covered.

  11. Acoustic dispersive prism

    Esfahlani, Hussein; Karkar, Sami; Lissek, Herve; Mosig, Juan R.

    2016-01-01

    The optical dispersive prism is a well-studied element, which allows separating white light into its constituent spectral colors, and stands in nature as water droplets. In analogy to this definition, the acoustic dispersive prism should be an acoustic device with capability of splitting a broadband acoustic wave into its constituent Fourier components. However, due to the acoustical nature of materials as well as the design and fabrication difficulties, there is neither any natural acoustic counterpart of the optical prism, nor any artificial design reported so far exhibiting an equivalent acoustic behaviour. Here, based on exotic properties of the acoustic transmission-line metamaterials and exploiting unique physical behaviour of acoustic leaky-wave radiation, we report the first acoustic dispersive prism, effective within the audible frequency range 800 Hz-1300 Hz. The dispersive nature, and consequently the frequency-dependent refractive index of the metamaterial are exploited to split the sound waves towards different and frequency-dependent directions. Meanwhile, the leaky-wave nature of the structure facilitates the sound wave radiation into the ambient medium.

  12. What Is an Acoustic Neuroma

    ... org Connect with us! What is an Acoustic Neuroma? Each heading slides to reveal information. Important Points ... Neuroma Important Points To Know About an Acoustic Neuroma An acoustic neuroma, also called a vestibular schwannoma, ...

  13. Prediction of cereal feed value using spectroscopy and chemometrics

    Jørgensen, Johannes Ravn; Gislum, René

    2009-01-01

    determination of EDOM, EDOMi, FEso and FEsv. The outcome of a successful NIRS calibration will be a relatively cheap tool to monitor, diversify and evaluate the quality of cereals for animal feed, a possible tool to assess the feed value of new varieties in the variety testing and a useful, cheap and rapid tool...... that there is a significant variation between varieties as well as due to an environmental variation between regions and the harvest year. The chemical analysis is, however, time-consuming and costly, and it is therefore desirable to have a rapid and less expensive method, which makes it possible to...... carry out more analyses in-situ. Near infra-red reflection spectroscopy (NIRS) is appropriate as a standard analysis of dry matter, total N and starch in grains, since it is rapid (approximately 1 minute per measurement of a ground test) and cheap. NIRS is therefore appropriate as a quick method for the...

  14. An Advanced Analytical Chemistry Experiment Using Gas Chromatography-Mass Spectrometry, MATLAB, and Chemometrics to Predict Biodiesel Blend Percent Composition

    Pierce, Karisa M.; Schale, Stephen P.; Le, Trang M.; Larson, Joel C.

    2011-01-01

    We present a laboratory experiment for an advanced analytical chemistry course where we first focus on the chemometric technique partial least-squares (PLS) analysis applied to one-dimensional (1D) total-ion-current gas chromatography-mass spectrometry (GC-TIC) separations of biodiesel blends. Then, we focus on n-way PLS (n-PLS) applied to…

  15. Simultaneous kinetic spectrophotometric determination of norfloxacin and rifampicin in pharmaceutical formulation and human urine samples by use of chemometrics approaches

    KOKOT; Serge

    2008-01-01

    A kinetic spectrophotometric method with aid of chemometrics is proposed for the simultaneous determination of norfloxacin and rifampicin in mixtures. The proposed method was applied for the simultaneous determination of these two compounds in pharmaceutical formulation and human urine samples,and the results obtained are similar to those obtained by high performance liquid chromatography.

  16. Neurophysiological monitoring for preservation of facial nerve function in microsurgery for acoustic neuroma%听神经瘤显微切除术中神经电生理监测保护面神经的效果观察

    苏杰; 严畅; 陈伟强; 杨光

    2011-01-01

    目的:探讨听神经瘤显微切除术中的电生理监测对面神经功能的保护作用.方法:46例听神经瘤患者分别行单纯显微镜下切除肿瘤(非监测组,22例),显微镜下切除肿瘤过程中应用术中神经监测仪对面神经进行监测(监测组,24例),观察术中面神经实时监测情况,随访所有患者术后面神经功能.结果:术后3个月根据House-Brackmann面神经功能分级对病例面瘫情况进行评价,监测组Ⅰ级21例,Ⅱ级2例,Ⅲ级1例;非监测组Ⅰ级13例,Ⅱ级5例,Ⅲ级2例,Ⅴ级2例,差异有统计学意义(P<0.05).结论:听神经瘤手术中行神经电生理监测可有效保护面神经.%Objective:To assess the value of neurophysiological monitoring in preserving the facial nerve in microsurgery for acoustic neuroma. Methods: Forty-six patients with acoustic neuroma were divided into monitoring group and non-monitoring group. The tumor was removed under the microscope without intraoperative facial nerve monitoring in 22 cases and with intraoperative monitoring in 24 cases. All the patients were followed up. Results: House-Brackmann system was used to evaluate the function of the facial nerve 3 months after the operation. Among the 24 cases in monitoring group,grade Ⅰ was observed in 21 cases,grade Ⅱ in 2 cases and grade Ⅲ in 1 case;among the 22 cases in non monitoring group,grade Ⅰ was observed in 13 cases,grade Ⅱ in 5 cases,grade Ⅲ in 2 cases and grade Ⅴ in 2 cases. The difference was significant( P < 0.05 ). Conclusions: Neurophysiological monitoring may effectively preserve the facial nerve function in microsurgery for acoustic neuroma.

  17. Simultaneous quantitative determination of paracetamol and tramadol in tablet formulation using UV spectrophotometry and chemometric methods

    Glavanović, Siniša; Glavanović, Marija; Tomišić, Vladislav

    2016-03-01

    The UV spectrophotometric methods for simultaneous quantitative determination of paracetamol and tramadol in paracetamol-tramadol tablets were developed. The spectrophotometric data obtained were processed by means of partial least squares (PLS) and genetic algorithm coupled with PLS (GA-PLS) methods in order to determine the content of active substances in the tablets. The results gained by chemometric processing of the spectroscopic data were statistically compared with those obtained by means of validated ultra-high performance liquid chromatographic (UHPLC) method. The accuracy and precision of data obtained by the developed chemometric models were verified by analysing the synthetic mixture of drugs, and by calculating recovery as well as relative standard error (RSE). A statistically good agreement was found between the amounts of paracetamol determined using PLS and GA-PLS algorithms, and that obtained by UHPLC analysis, whereas for tramadol GA-PLS results were proven to be more reliable compared to those of PLS. The simplest and the most accurate and precise models were constructed by using the PLS method for paracetamol (mean recovery 99.5%, RSE 0.89%) and the GA-PLS method for tramadol (mean recovery 99.4%, RSE 1.69%).

  18. Chemometric analysis for discrimination of extra virgin olive oils from whole and stoned olive pastes.

    De Luca, Michele; Restuccia, Donatella; Clodoveo, Maria Lisa; Puoci, Francesco; Ragno, Gaetano

    2016-07-01

    Chemometric discrimination of extra virgin olive oils (EVOO) from whole and stoned olive pastes was carried out by using Fourier transform infrared (FTIR) data and partial least squares-discriminant analysis (PLS1-DA) approach. Four Italian commercial EVOO brands, all in both whole and stoned version, were considered in this study. The adopted chemometric methodologies were able to describe the different chemical features in phenolic and volatile compounds contained in the two types of oil by using unspecific IR spectral information. Principal component analysis (PCA) was employed in cluster analysis to capture data patterns and to highlight differences between technological processes and EVOO brands. The PLS1-DA algorithm was used as supervised discriminant analysis to identify the different oil extraction procedures. Discriminant analysis was extended to the evaluation of possible adulteration by addition of aliquots of oil from whole paste to the most valuable oil from stoned olives. The statistical parameters from external validation of all the PLS models were very satisfactory, with low root mean square error of prediction (RMSEP) and relative error (RE%). PMID:26920315

  19. Application of terahertz spectroscopy imaging for discrimination of transgenic rice seeds with chemometrics.

    Liu, Wei; Liu, Changhong; Hu, Xiaohua; Yang, Jianbo; Zheng, Lei

    2016-11-01

    Discrimination of genetically modified organisms is increasingly demanded by legislation and consumers worldwide. The feasibility of a non-destructive discrimination of transgenic rice seeds from its non-transgenic counterparts was examined by terahertz spectroscopy imaging system combined with chemometrics. Principal component analysis (PCA), least squares support vector machines (LS-SVM), PCA-back propagation neural network (PCA-BPNN), and random forest (RF) models with the first and second derivative and standard normal variate transformation (SNV) pre-treatments were applied to classify rice seeds based on genotype. The results demonstrated that differences between non-transgenic and transgenic rice seeds did exist, and an excellent classification (accuracy was 96.67% in the prediction set) could be achieved using the RF model combined with the first derivative pre-treatment. The results indicated that THz spectroscopy imaging together with chemometrics would be a promising technique to identify transgenic rice seeds with high efficiency and without any sample preparation. PMID:27211665

  20. Geographic origins and compositions of virgin olive oils determinated by chemometric analysis of NIR spectra.

    Galtier, O; Dupuy, N; Le Dréau, Y; Ollivier, D; Pinatel, C; Kister, J; Artaud, J

    2007-07-01

    The authentication of virgin olive oil samples requires usually the use of sophisticated and time consuming analytical techniques. There is a need for fast and simple analytical techniques for the objective of a quality control methodology. Virgin olive oils present characteristic NIR spectra. Chemometric treatment of NIR spectra was assessed for the quantification of fatty acids and triacylglycerols in virgin olive oil samples (n=125) and for their classification (PLS1-DA) into five very geographically closed registered designations of origin (RDOs) of French virgin olive oils ("Aix-en-Provence", "Haute-Provence", "Nice", "Nyons" and "Vallée des Baux"). The spectroscopic interpretation of regression vectors showed that each RDO was correlated to one or two specific components of virgin olive oils according to their cultivar compositions. The results were quite satisfactory, in spite of the similarity of cultivar compositions between two denominations of origin ("Aix-en-Provence" and "Vallée des Baux"). Chemometric treatments of NIR spectra allow us to obtain similar results than those obtained by time consuming analytical techniques such as GC and HPLC, and constitute a help fast and robust for authentication of those French virgin olive oils. PMID:17605993