WorldWideScience

Sample records for accurate mass measurements

  1. On uplimit of accurate measurement of tau mass

    Mo, X H

    2016-01-01

    Tau lepton as one of three elementary leptons in nature, the measurement of its mass has ever been performed since its discovery. The present relative accuracy is already at the level of better than 10 to minus 4 and more effects are still made in order to increase the accuracy further. However, the analysis of available techniques for and expectable luminosity from e+e- collider indicates that the precision uplimit of tau mass is almost reached, which means that brand new approaches should be looked for if the great improvement is yearned for.

  2. Accurate on-line mass flow measurements in supercritical fluid chromatography.

    Tarafder, Abhijit; Vajda, Péter; Guiochon, Georges

    2013-12-13

    This work demonstrates the possible advantages and the challenges of accurate on-line measurements of the CO2 mass flow rate during supercritical fluid chromatography (SFC) operations. Only the mass flow rate is constant along the column in SFC. The volume flow rate is not. The critical importance of accurate measurements of mass flow rates for the achievement of reproducible data and the serious difficulties encountered in supercritical fluid chromatography for its assessment were discussed earlier based on the physical properties of carbon dioxide. In this report, we experimentally demonstrate the problems encountered when performing mass flow rate measurements and the gain that can possibly be achieved by acquiring reproducible data using a Coriolis flow meter. The results obtained show how the use of a highly accurate mass flow meter permits, besides the determination of accurate values of the mass flow rate, a systematic, constant diagnosis of the correct operation of the instrument and the monitoring of the condition of the carbon dioxide pump. PMID:24210558

  3. Analysis of plant galactolipids by reversed-phase high-performance liquid chromatography/mass spectrometry with accurate mass measurement

    Zábranská, Marie; Vrkoslav, Vladimír; Sobotníková, J.; Cvačka, Josef

    2012-01-01

    Roč. 165, č. 5 (2012), s. 601-607. ISSN 0009-3084 R&D Projects: GA ČR GA203/09/0139 Grant ostatní: GA UK(CZ) SVV 2012-265201 Institutional research plan: CEZ:AV0Z40550506 Keywords : accurate mass measurement * DGDG * equivalent carbon number * MGDG * RP-HPLC/MS Subject RIV: CB - Analytical Chemistry, Separation Impact factor: 2.147, year: 2012

  4. Induced Dual-Nanospray: A Novel Internal Calibration Method for Convenient and Accurate Mass Measurement

    Li, Yafeng; Zhang, Ning; Zhou, Yueming; Wang, Jianing; Zhang, Yiming; Wang, Jiyun; Xiong, Caiqiao; Chen, Suming; Nie, Zongxiu

    2013-09-01

    Accurate mass information is of great importance in the determination of unknown compounds. An effective and easy-to-control internal mass calibration method will dramatically benefit accurate mass measurement. Here we reported a simple induced dual-nanospray internal calibration device which has the following three advantages: (1) the two sprayers are in the same alternating current field; thus both reference ions and sample ions can be simultaneously generated and recorded. (2) It is very simple and can be easily assembled. Just two metal tubes, two nanosprayers, and an alternating current power supply are included. (3) With the low-flow-rate character and the versatility of nanoESI, this calibration method is capable of calibrating various samples, even untreated complex samples such as urine and other biological samples with small sample volumes. The calibration errors are around 1 ppm in positive ion mode and 3 ppm in negative ion mode with good repeatability. This new internal calibration method opens up new possibilities in the determination of unknown compounds, and it has great potential for the broad applications in biological and chemical analysis.

  5. Accurate mass measurements of short-lived isotopes with the MISTRAL rf spectrometer

    Toader, C F; Borcea, C; Doubre, H; Duma, M; Jacotin, M; Henry, S; Képinski, J F; Lebée, G; Le Scornet, G; Lunney, M D; Monsanglant, C; De Saint-Simon, M; Thibault, C

    1999-01-01

    The MISTRAL experiment has measured its first masses at ISOLDE. Installed in May 1997, this radiofrequency transmission spectrometer is to concentrate on nuclides with particularly short half-lives. MISTRAL received its first stable beam in October and first radioactive beam in November 1997. These first tests, with a plasma ion source, resulted in excellent isobaric separation and reasonable transmission. Further testing and development enabled first data taking in July 1998 on neutron-rich Na isotopes having half-lives as short as 31 ms.

  6. A Facility for Accurate Heat Load and Mass Leak Measurements on Superfluid Helium Valves

    Bézaguet, Alain-Arthur; Ferlin, G; Losserand-Madoux, R; Perin, A; Vandoni, Giovanna; Van Weelderen, R

    1999-01-01

    The superconducting magnets of the Large Hadron Collider (LHC) will be protected by safety relief valves operating at 1.9 K in superfluid helium (HeII). A test facility was developed to precisely determine the heat load and the mass leakage of cryogenic valves with HeII at their inlet. The temperature of the valve inlet can be varied from 1.8 K to 2 K for pressures up to 3.5 bar. The valve outlet pipe temperature can be regulated between 5 K and 20 K. The heat flow is measured with high precision using a Kapitza-resistance heatmeter and is also crosschecked by a vaporization measurement. After calibration, a precision of 10 mW for heat flows up to 1.1 W has been achieved. The helium leak can be measured up to 15 mg/s with an accuracy of 0.2 mg/s. We present a detailed description of the test facility and the measurements showing its performances.

  7. ICP-MS and ESI orbitrap MS/MS for plant elemental speciation. The need for accurate mass measurements

    Complete text of publication follows. Metallomics approaches based on the combined use of elemental and molecular mass spectrometry have been developed to gain a better understanding of the factors involved in the uptake and distribution of selenium (Se) and arsenic (As) in a well-known hyperaccumulator, Arabidopsis thaliana. Plants, individually and simultaneously supplemented with As and Se (1, 3, 5 μg g-1), were grown hydroponically for 7 weeks in a controlled environment. The effect of the presence of Se on the As uptake by the plant leaves was investigated here for the first time; Se in the growing media was found not to affect As concentrations of the leaves in comparison with individual exposure to As. The use of 1% formic acid (1 deg C, 1 h), compared with buffer extraction (2, 5, 12 h) by sonication, was found to be the choice as a compromise between extraction efficiency and preservation of the compound entity. Using size-exclusion HPLC-ICP-MS, the coelution of the main As peak (70% of the total chromatogram area) with sulphur was observed, suggesting the presence of biomolecules containing S and As in the leaves. A deeper insight into the As species distribution in the leaves was achieved using reversed phase HPLC in combination with ICP-MS and ESI Orbitrap MS/MS. The need for accurate mass measurements (using ESI Orbitrap MS/MS) to minimize ambiguity in species identification will be demonstrated.

  8. Critical evaluation of screening techniques for emerging environmental contaminants based on accurate mass measurements with time-of-flight mass spectrometry.

    Nurmi, Joonas; Pellinen, Jukka; Rantalainen, Anna-Lea

    2012-03-01

    Emerging contaminants from wastewater effluent samples were analysed, using posttarget and nontarget analysis techniques. The samples were analysed with an ultra performance liquid chromatograph-time-of-flight mass spectrometer (UPLC-TOF-MS), and the resulting data were processed with commercial deconvolution software. The method works well for posttarget analysis with prior information about the retention times of the compounds of interest. With positive polarity, 63 of 66 compounds and with negative polarity, 18 of 20 compounds were correctly identified in a spiked sample, while two compounds of a total of 88 fell out of the mass range. Furthermore, a four-stage process for identification was developed for the posttarget analysis lacking the retention time data. In the process, the number of candidate compounds was reduced by using the accurate mass of selected compounds in two steps (stages 1 and 2), structure-property relationships (stage 3) and isotope patterns of the analytes (stage 4). The process developed was validated by analysing wastewater samples spiked with 88 compounds. This procedure can be used to gain a preliminary indication of the presence of certain analytes in the samples. Nontarget analysis was tested by applying a theoretical mass spectra library for a wastewater sample spiked with six pharmaceuticals. The results showed a high number of false identifications. In addition, manual processing of the data was considered laborious and ineffective. Finally, the posttarget analysis was applied to a real wastewater sample. The analysis revealed the presence of six compounds that were afterwards confirmed with standard compounds as being correct. Three psycholeptics (nordiazepam, oxazepam and temazepam) could be tentatively identified, using the identification process developed. Posttarget analysis with UPLC-TOF-MS proved to be a promising method for analysing wastewater samples, while we concluded that the software for nontarget analysis will need

  9. Accurate thickness measurement of graphene

    Shearer, Cameron J.; Slattery, Ashley D.; Stapleton, Andrew J.; Shapter, Joseph G.; Gibson, Christopher T.

    2016-03-01

    Graphene has emerged as a material with a vast variety of applications. The electronic, optical and mechanical properties of graphene are strongly influenced by the number of layers present in a sample. As a result, the dimensional characterization of graphene films is crucial, especially with the continued development of new synthesis methods and applications. A number of techniques exist to determine the thickness of graphene films including optical contrast, Raman scattering and scanning probe microscopy techniques. Atomic force microscopy (AFM), in particular, is used extensively since it provides three-dimensional images that enable the measurement of the lateral dimensions of graphene films as well as the thickness, and by extension the number of layers present. However, in the literature AFM has proven to be inaccurate with a wide range of measured values for single layer graphene thickness reported (between 0.4 and 1.7 nm). This discrepancy has been attributed to tip-surface interactions, image feedback settings and surface chemistry. In this work, we use standard and carbon nanotube modified AFM probes and a relatively new AFM imaging mode known as PeakForce tapping mode to establish a protocol that will allow users to accurately determine the thickness of graphene films. In particular, the error in measuring the first layer is reduced from 0.1-1.3 nm to 0.1-0.3 nm. Furthermore, in the process we establish that the graphene-substrate adsorbate layer and imaging force, in particular the pressure the tip exerts on the surface, are crucial components in the accurate measurement of graphene using AFM. These findings can be applied to other 2D materials.

  10. CLASH-VLT: CONSTRAINTS ON THE DARK MATTER EQUATION OF STATE FROM ACCURATE MEASUREMENTS OF GALAXY CLUSTER MASS PROFILES

    Sartoris, Barbara; Borgani, Stefano; Girardi, Marisa [Dipartimento di Fisica, Sezione di Astronomia, Università di Trieste, Via Tiepolo 11, I-34143 Trieste (Italy); Biviano, Andrea; Balestra, Italo; Nonino, Mario [INAF/Osservatorio Astronomico di Trieste, Via Tiepolo 11, I-34143 Trieste (Italy); Rosati, Piero [Dipartimento di Fisica e Scienze della Terra, Universita' di Ferrara, Via Saragat 1, I-44122 Ferrara (Italy); Umetsu, Keiichi; Czakon, Nicole [Institute of Astronomy and Astrophysics, Academia Sinica, P.O. Box 23-141, Taipei 10617, Taiwan (China); Bartelmann, Matthias [Zentrum für Astronomie der Universität Heidelberg, ITA, Albert-Ueberle-Str. 2, D-69120 Heidelberg (Germany); Grillo, Claudio [Dark Cosmology Centre, Niels Bohr Institute, University of Copenhagen, Juliane Maries Vej 30, DK-2100 Copenhagen (Denmark); Lemze, Doron; Medezinski, Elinor [Department of Physics and Astronomy, The Johns Hopkins University, 3400 North Charles Street, Baltimore, MD 21218 (United States); Zitrin, Adi [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, MS 249-17, Pasadena, CA 91125 (United States); Mercurio, Amata [INAF/Osservatorio Astronomico di Capodimonte, Via Moiariello 16, I-80131 Napoli (Italy); Postman, Marc; Bradley, Larry; Coe, Dan [Space Telescope Science Institute, 3700 San Martin Drive, Baltimore, MD 21218 (United States); Broadhurst, Tom [Department of Theoretical Physics, University of the Basque Country, P.O. Box 644, E-48080 Bilbao (Spain); Melchior, Peter, E-mail: sartoris@oats.inaf.it [Department of Physics, The Ohio State University, Columbus, OH 43210 (United States); and others

    2014-03-01

    A pressureless scenario for the dark matter (DM) fluid is a widely adopted hypothesis, despite the absence of direct observational evidence. According to general relativity, the total mass-energy content of a system shapes the gravitational potential well, but different test particles perceive this potential in different ways depending on their properties. Cluster galaxy velocities, being <mass. We exploit this phenomenon to constrain the equation of state (EoS) parameter of the fluid, primarily DM, contained in galaxy clusters. We use complementary information provided by the kinematic and lensing mass profiles of the galaxy cluster MACS 1206.2–0847 at z = 0.44, as obtained in an extensive imaging and spectroscopic campaign within the Cluster Lensing And Supernova survey with Hubble. The unprecedented high quality of our data set and the properties of this cluster are well suited to determine the EoS parameter of the cluster fluid. Since baryons contribute at most 15% to the total mass in clusters and their pressure is negligible, the EoS parameter we derive describes the behavior of the DM fluid. We obtain the most stringent constraint on the DM EoS parameter to date, w = (p{sub r} + 2 p{sub t} )/(3 c {sup 2}ρ) = 0.00 ± 0.15 (stat) ± 0.08 (syst), averaged over the radial range 0.5 Mpc ≤ r ≤ r {sub 200}, where p{sub r} and p{sub t} are the radial and tangential pressure, and ρ is the density. We plan to further improve our constraint by applying the same procedure to all clusters from the ongoing Cluster Lensing And Supernova Survey with Hubble-Very Large Telescope program.

  11. 38 CFR 4.46 - Accurate measurement.

    2010-07-01

    ... 38 Pensions, Bonuses, and Veterans' Relief 1 2010-07-01 2010-07-01 false Accurate measurement. 4... RATING DISABILITIES Disability Ratings The Musculoskeletal System § 4.46 Accurate measurement. Accurate measurement of the length of stumps, excursion of joints, dimensions and location of scars with respect...

  12. Tandem Mass Spectrometry Measurement of the Collision Products of Carbamate Anions Derived from CO2 Capture Sorbents: Paving the Way for Accurate Quantitation

    Jackson, Phil; Fisher, Keith J.; Attalla, Moetaz Ibrahim

    2011-08-01

    The reaction between CO2 and aqueous amines to produce a charged carbamate product plays a crucial role in post-combustion capture chemistry when primary and secondary amines are used. In this paper, we report the low energy negative-ion CID results for several anionic carbamates derived from primary and secondary amines commonly used as post-combustion capture solvents. The study was performed using the modern equivalent of a triple quadrupole instrument equipped with a T-wave collision cell. Deuterium labeling of 2-aminoethanol (1,1,2,2,-d4-2-aminoethanol) and computations at the M06-2X/6-311++G(d,p) level were used to confirm the identity of the fragmentation products for 2-hydroxyethylcarbamate (derived from 2-aminoethanol), in particular the ions CN-, NCO- and facile neutral losses of CO2 and water; there is precedent for the latter in condensed phase isocyanate chemistry. The fragmentations of 2-hydroxyethylcarbamate were generalized for carbamate anions derived from other capture amines, including ethylenediamine, diethanolamine, and piperazine. We also report unequivocal evidence for the existence of carbamate anions derived from sterically hindered amines ( Tris(2-hydroxymethyl)aminomethane and 2-methyl-2-aminopropanol). For the suite of carbamates investigated, diagnostic losses include the decarboxylation product (-CO2, 44 mass units), loss of 46 mass units and the fragments NCO- ( m/z 42) and CN- ( m/z 26). We also report low energy CID results for the dicarbamate dianion (-O2CNHC2H4NHCO{2/-}) commonly encountered in CO2 capture solution utilizing ethylenediamine. Finally, we demonstrate a promising ion chromatography-MS based procedure for the separation and quantitation of aqueous anionic carbamates, which is based on the reported CID findings. The availability of accurate quantitation methods for ionic CO2 capture products could lead to dynamic operational tuning of CO2 capture-plants and, thus, cost-savings via real-time manipulation of solvent

  13. Accurate, reproducible measurement of blood pressure.

    Campbell, N. R.; Chockalingam, A; Fodor, J. G.; McKay, D. W.

    1990-01-01

    The diagnosis of mild hypertension and the treatment of hypertension require accurate measurement of blood pressure. Blood pressure readings are altered by various factors that influence the patient, the techniques used and the accuracy of the sphygmomanometer. The variability of readings can be reduced if informed patients prepare in advance by emptying their bladder and bowel, by avoiding over-the-counter vasoactive drugs the day of measurement and by avoiding exposure to cold, caffeine con...

  14. Accurate shear measurement with faint sources

    Zhang, Jun; Foucaud, Sebastien [Center for Astronomy and Astrophysics, Department of Physics and Astronomy, Shanghai Jiao Tong University, 955 Jianchuan road, Shanghai, 200240 (China); Luo, Wentao, E-mail: betajzhang@sjtu.edu.cn, E-mail: walt@shao.ac.cn, E-mail: foucaud@sjtu.edu.cn [Key Laboratory for Research in Galaxies and Cosmology, Shanghai Astronomical Observatory, Nandan Road 80, Shanghai, 200030 (China)

    2015-01-01

    For cosmic shear to become an accurate cosmological probe, systematic errors in the shear measurement method must be unambiguously identified and corrected for. Previous work of this series has demonstrated that cosmic shears can be measured accurately in Fourier space in the presence of background noise and finite pixel size, without assumptions on the morphologies of galaxy and PSF. The remaining major source of error is source Poisson noise, due to the finiteness of source photon number. This problem is particularly important for faint galaxies in space-based weak lensing measurements, and for ground-based images of short exposure times. In this work, we propose a simple and rigorous way of removing the shear bias from the source Poisson noise. Our noise treatment can be generalized for images made of multiple exposures through MultiDrizzle. This is demonstrated with the SDSS and COSMOS/ACS data. With a large ensemble of mock galaxy images of unrestricted morphologies, we show that our shear measurement method can achieve sub-percent level accuracy even for images of signal-to-noise ratio less than 5 in general, making it the most promising technique for cosmic shear measurement in the ongoing and upcoming large scale galaxy surveys.

  15. Precision mass measurements

    Gläser, M.; Borys, M.

    2009-12-01

    Mass as a physical quantity and its measurement are described. After some historical remarks, a short summary of the concept of mass in classical and modern physics is given. Principles and methods of mass measurements, for example as energy measurement or as measurement of weight forces and forces caused by acceleration, are discussed. Precision mass measurement by comparing mass standards using balances is described in detail. Measurement of atomic masses related to 12C is briefly reviewed as well as experiments and recent discussions for a future new definition of the kilogram, the SI unit of mass.

  16. Accurate mass error correction in liquid chromatography time-of-flight mass spectrometry based metabolomics

    Mihaleva, V.V.; Vorst, O.F.J.; Maliepaard, C.A.; Verhoeven, H.A.; Vos, de C.H.; Hall, R.D.; Ham, van R.C.H.J.

    2008-01-01

    Compound identification and annotation in (untargeted) metabolomics experiments based on accurate mass require the highest possible accuracy of the mass determination. Experimental LC/TOF-MS platforms equipped with a time-to-digital converter (TDC) give the best mass estimate for those mass signals

  17. Mining tandem mass spectral data to develop a more accurate mass error model for peptide identification.

    Fu, Yan; Gao, Wen; He, Simin; Sun, Ruixiang; Zhou, Hu; Zeng, Rong

    2007-01-01

    The assumption on the mass error distribution of fragment ions plays a crucial role in peptide identification by tandem mass spectra. Previous mass error models are the simplistic uniform or normal distribution with empirically set parameter values. In this paper, we propose a more accurate mass error model, namely conditional normal model, and an iterative parameter learning algorithm. The new model is based on two important observations on the mass error distribution, i.e. the linearity between the mean of mass error and the ion mass, and the log-log linearity between the standard deviation of mass error and the peak intensity. To our knowledge, the latter quantitative relationship has never been reported before. Experimental results demonstrate the effectiveness of our approach in accurately quantifying the mass error distribution and the ability of the new model to improve the accuracy of peptide identification. PMID:17990507

  18. Accurate, Empirical Radii and Masses of Planets with Gaia Parallaxes

    Stassun, Keivan G; Gaudi, B Scott

    2016-01-01

    We present new, empirical measurements of the radii of 132 stars that host transiting planets. These stellar radii are determined using only direct observables---the bolometric flux at Earth, the stellar effective temperature, and the parallax newly provided by the Gaia first data release---and thus are virtually model independent, extinction being the only free parameter. We also determine each star's mass using our newly determined radius and the stellar density, itself a virtually model independent quantity from the previously published transit analysis. The newly determined stellar radii and masses are in turn used to re-determine the transiting planet radii and masses, once again using only direct observables. The uncertainties on the stellar radii and masses are typically 7% and 25%, respectively, and the resulting uncertainties on the planet radii and masses are 8% and 20%, respectively. These accuracies are generally larger than the previously published model-dependent precisions of 5% and 6% on the p...

  19. Mass Customization Measurements Metrics

    Nielsen, Kjeld; Brunø, Thomas Ditlev; Jørgensen, Kaj Asbjørn;

    2014-01-01

    A recent survey has indicated that 17 % of companies have ceased mass customizing less than 1 year after initiating the effort. This paper presents measurement for a company’s mass customization performance, utilizing metrics within the three fundamental capabilities: robust process design, choice...... navigation, and solution space development. A mass customizer when assessing performance with these metrics can identify within which areas improvement would increase competitiveness the most and enable more efficient transition to mass customization....

  20. How accurate are your reported emissions measurements?

    Macak J.J. III [Mostardi Platt Environmental (United States)

    2006-09-15

    Complying with permitted emissions limits may be the most significant operations risk for a power plant. As limits are slowly ratcheted downward, understanding the accuracy and variation of measured pollutant levels becomes even more important. To avoid misunderstandings, regulators and plant owners should factor measurement uncertainty into air quality permit numbers both as the permit is formulated and preceding any subsequent modifications. 4 figs., 2 tabs.

  1. Accurate measurement of oxygen consumption in children undergoing cardiac catheterization.

    Li, Jia

    2013-01-01

    Oxygen consumption (VO(2) ) is an important part of hemodynamics using the direct Fick principle in children undergoing cardiac catheterization. Accurate measurement of VO(2) is vital. Obviously, any error in the measurement of VO(2) will translate directly into an equivalent percentage under- or overestimation of blood flows and vascular resistances. It remains common practice to estimate VO(2) values from published predictive equations. Among these, the LaFarge equation is the most commonly used equation and gives the closest estimation with the least bias and limits of agreement. However, considerable errors are introduced by the LaFarge equation, particularly in children younger than 3 years of age. Respiratory mass spectrometry remains the "state-of-the-art" method, allowing highly sensitive, rapid and simultaneous measurement of multiple gas fractions. The AMIS 2000 quadrupole respiratory mass spectrometer system has been adapted to measure VO(2) in children under mechanical ventilation with pediatric ventilators during cardiac catheterization. The small sampling rate, fast response time and long tubes make the equipment a unique and powerful tool for bedside continuous measurement of VO(2) in cardiac catheterization for both clinical and research purposes. PMID:22488802

  2. Absolute neutrino mass measurements

    Wolf, Joachim

    2011-10-01

    The neutrino mass plays an important role in particle physics, astrophysics and cosmology. In recent years the detection of neutrino flavour oscillations proved that neutrinos carry mass. However, oscillation experiments are only sensitive to the mass-squared difference of the mass eigenvalues. In contrast to cosmological observations and neutrino-less double beta decay (0v2β) searches, single β-decay experiments provide a direct, model-independent way to determine the absolute neutrino mass by measuring the energy spectrum of decay electrons at the endpoint region with high accuracy. Currently the best kinematic upper limits on the neutrino mass of 2.2eV have been set by two experiments in Mainz and Troitsk, using tritium as beta emitter. The next generation tritium β-experiment KATRIN is currently under construction in Karlsruhe/Germany by an international collaboration. KATRIN intends to improve the sensitivity by one order of magnitude to 0.2eV. The investigation of a second isotope (137Rh) is being pursued by the international MARE collaboration using micro-calorimeters to measure the beta spectrum. The technology needed to reach 0.2eV sensitivity is still in the R&D phase. This paper reviews the present status of neutrino-mass measurements with cosmological data, 0v2β decay and single β-decay.

  3. Organ mass measurements

    The term, anatomical measurements, in the context of this Co-ordinated Research Programme refers to measurements of masses of internal organs, although the human body is composed of internal organs and tissues such as skeleton, muscle, skin and adipose. The mass of an organ containing a radionuclide (source organ), and the mass of a target organ which absorbs energy of the radiation, are essential parameters in the ICRP dosimetric model derived from the MIRD method. Twelve specific organs of interest were proposed at the Coordinated Research Programme Project Formulation Meeting (PFM) in 1988. A slightly different set of thirteen organs with potential significance for radiation protection were selected for study at the Research Co-ordination Meeting held at the Bhabha Atomic Research Centre in 1991. The dimensions of the organs could also be useful information, but were considered unimportant for internal dose assessment. Due to the strong concern about the unified method for collecting organ mass data at the PFM, a guide-line was established stressing the need for organ data from subjects that were healthy and normal, at least until shortly before death, or from sudden death cases, following the Japanese experience. In this report, masses of nine to thirteen organs are presented from seven participating countries. Three participants have also reported the organ masses as fractions of the total body mass

  4. Accurately bearing measurement in non-cooperative passive location system

    The system of non-cooperative passive location based on array is proposed. In the system, target is detected by beamforming and Doppler matched filtering; and bearing is measured by a long-base-ling interferometer which is composed of long distance sub-arrays. For the interferometer with long-base-line, the bearing is measured accurately but ambiguously. To realize unambiguous accurately bearing measurement, beam width and multiple constraint adoptive beamforming technique is used to resolve azimuth ambiguous. Theory and simulation result shows this method is effective to realize accurately bearing measurement in no-cooperate passive location system. (authors)

  5. Accurate measurement of liquid transport through nanoscale conduits.

    Alibakhshi, Mohammad Amin; Xie, Quan; Li, Yinxiao; Duan, Chuanhua

    2016-01-01

    Nanoscale liquid transport governs the behaviour of a wide range of nanofluidic systems, yet remains poorly characterized and understood due to the enormous hydraulic resistance associated with the nanoconfinement and the resulting minuscule flow rates in such systems. To overcome this problem, here we present a new measurement technique based on capillary flow and a novel hybrid nanochannel design and use it to measure water transport through single 2-D hydrophilic silica nanochannels with heights down to 7 nm. Our results show that silica nanochannels exhibit increased mass flow resistance compared to the classical hydrodynamics prediction. This difference increases with decreasing channel height and reaches 45% in the case of 7 nm nanochannels. This resistance increase is attributed to the formation of a 7-angstrom-thick stagnant hydration layer on the hydrophilic surfaces. By avoiding use of any pressure and flow sensors or any theoretical estimations the hybrid nanochannel scheme enables facile and precise flow measurement through single nanochannels, nanotubes, or nanoporous media and opens the prospect for accurate characterization of both hydrophilic and hydrophobic nanofluidic systems. PMID:27112404

  6. Accurate measurement of liquid transport through nanoscale conduits

    Alibakhshi, Mohammad Amin; Xie, Quan; Li, Yinxiao; Duan, Chuanhua

    2016-04-01

    Nanoscale liquid transport governs the behaviour of a wide range of nanofluidic systems, yet remains poorly characterized and understood due to the enormous hydraulic resistance associated with the nanoconfinement and the resulting minuscule flow rates in such systems. To overcome this problem, here we present a new measurement technique based on capillary flow and a novel hybrid nanochannel design and use it to measure water transport through single 2-D hydrophilic silica nanochannels with heights down to 7 nm. Our results show that silica nanochannels exhibit increased mass flow resistance compared to the classical hydrodynamics prediction. This difference increases with decreasing channel height and reaches 45% in the case of 7 nm nanochannels. This resistance increase is attributed to the formation of a 7-angstrom-thick stagnant hydration layer on the hydrophilic surfaces. By avoiding use of any pressure and flow sensors or any theoretical estimations the hybrid nanochannel scheme enables facile and precise flow measurement through single nanochannels, nanotubes, or nanoporous media and opens the prospect for accurate characterization of both hydrophilic and hydrophobic nanofluidic systems.

  7. Accurate wall thickness measurement using autointerference of circumferential Lamb wave

    In this paper, a method of accurately measuring the pipe wall thickness by using noncontact air-coupled ultrasonic transducer (NAUT) was presented. In this method, accurate measurement of angular wave number (AWN) is a key technique because the AWN is changes minutely with the wall thickness. An autointerference of the circumferential (C-) Lamb wave was used for accurate measurements of the AWN. Principle of the method was first explained. Modified method for measuring the wall thickness near a butt weld line was also proposed and its accuracy was evaluated within 6 μm error. It was also shown in the paper that wall thickness measurement was accurately carried out beyond the difference among the sensors by calibrating the frequency response of the sensors. (author)

  8. The Use of Accurate Mass Tags for High-Throughput Microbial Proteomics

    We describe and demonstrate a global strategy that extends the sensitivity, dynamic range, comprehensiveness, and throughput of proteomic measurements based upon the use of peptide accurate mass tags (AMTs) produced by global protein enzymatic digestion. The two-stage strategy exploits Fourier transform-ion cyclotron resonance (FT-ICR) mass spectrometry to validate peptide AMTs for a specific organism, tissue or cell type from potential mass tags identified using conventional tandem mass spectrometry (MS/MS) methods, providing greater confidence in identifications as well as the basis for subsequent measurements without the need for MS/MS, and thus with greater sensitivity and increased throughput. A single high resolution capillary liquid chromatography separation combined with high sensitivity, high resolution and ac-curate FT-ICR measurements has been shown capable of characterizing peptide mixtures of significantly more than 10 5 components with mass accuracies of -1 ppm, sufficient for broad protein identification using AMTs. Other attractions of the approach include the broad and relatively unbiased proteome coverage, the capability for exploiting stable isotope labeling methods to realize high precision for relative protein abundance measurements, and the projected potential for study of mammalian proteomes when combined with additional sample fractionation. Using this strategy, in our first application we have been able to identify AMTs for 60% of the potentially expressed proteins in the organism Deinococcus radiodurans

  9. Accurate, reliable control of process gases by mass flow controllers

    Hardy, J.; McKnight, T.

    1997-02-01

    The thermal mass flow controller, or MFC, has become an instrument of choice for the monitoring and controlling of process gas flow throughout the materials processing industry. These MFCs are used on CVD processes, etching tools, and furnaces and, within the semiconductor industry, are used on 70% of the processing tools. Reliability and accuracy are major concerns for the users of the MFCs. Calibration and characterization technologies for the development and implementation of mass flow devices are described. A test facility is available to industry and universities to test and develop gas floe sensors and controllers and evaluate their performance related to environmental effects, reliability, reproducibility, and accuracy. Additional work has been conducted in the area of accuracy. A gravimetric calibrator was invented that allows flow sensors to be calibrated in corrosive, reactive gases to an accuracy of 0.3% of reading, at least an order of magnitude better than previously possible. Although MFCs are typically specified with accuracies of 1% of full scale, MFCs may often be implemented with unwarranted confidence due to the conventional use of surrogate gas factors. Surrogate gas factors are corrections applied to process flow indications when an MFC has been calibrated on a laboratory-safe surrogate gas, but is actually used on a toxic, or corrosive process gas. Previous studies have indicated that the use of these factors may cause process flow errors of typically 10%, but possibly as great as 40% of full scale. This paper will present possible sources of error in MFC process gas flow monitoring and control, and will present an overview of corrective measures which may be implemented with MFC use to significantly reduce these sources of error.

  10. Handbook of mass measurement

    Jones, Frank E

    2002-01-01

    "How much does it weigh?" seems a simple question. To scientists and engineers, however, the answer is far from simple, and determining the answer demands consideration of an almost overwhelming number of factors.With an intriguing blend of history, fundamentals, and technical details, the Handbook of Mass Measurement sets forth the details of achieving the highest precision in mass measurements. It covers the whole field, from the development, calibration, and maintenance of mass standards to detailed accounts of weighing designs, balances, and uncertainty. It addresses the entire measurement process and provides in-depth examinations of the various factors that introduce error.Much of the material is the authors'' own work and some of it is published here for the first time. Jones and Schoonover are both highly regarded veterans of the U.S. National Institute of Standards and Technology. With this handbook, they have provided a service and resource vital to anyone involved not only in the determination of m...

  11. Accurate Mass Determinations in Decay Chains with Missing Energy

    Cheng, Hsin-Chia; Engelhardt, Dalit; Gunion, John F.; Han, Zhenyu; McElrath, Bob

    2008-01-01

    Many beyond the Standard Model theories include a stable dark matter candidate that yields missing / invisible energy in collider detectors. If observed at the Large Hadron Collider, we must determine if its mass and other properties (and those of its partners) predict the correct dark matter relic density. We give a new procedure for determining its mass with small error.

  12. Direct Neutrino Mass measurements

    Neutrino oscillation experiments have shown that neutrino are massive particles, but they are not able to determine the absolute neutrino mass scale. The experiments dedicated to effective electron-neutrino mass determination are the ones based on kinematic analyses of electrons emitted in single β-decay as 3H and 187Re. Nowadays the electrostatic spectrometers and microcalorimeters, two complementary techniques, are the most sensitive detection principles. Two experiments, KATRIN and MARE, are currently being prepared to explore neutrino masses down to 0.2 eV. The KATRIN experiment, which combines an ultra-luminous windowless gaseous tritium source with a high resolution electrostatic spectrometer, will provide high precision in β-studies never achieved before. The MARE project aims at the direct and calorimetric measurement of the electron neutrino mass with sub-eV sensitivity. Although the baseline of the MARE project consists in a large array of rhenium based thermal detectors, a different option for the isotope is also being considered. This contribution gives an outlook for both experiments.

  13. History and progress on accurate measurements of the Planck constant.

    Steiner, Richard

    2013-01-01

    The measurement of the Planck constant, h, is entering a new phase. The CODATA 2010 recommended value is 6.626 069 57 × 10(-34) J s, but it has been a long road, and the trip is not over yet. Since its discovery as a fundamental physical constant to explain various effects in quantum theory, h has become especially important in defining standards for electrical measurements and soon, for mass determination. Measuring h in the International System of Units (SI) started as experimental attempts merely to prove its existence. Many decades passed while newer experiments measured physical effects that were the influence of h combined with other physical constants: elementary charge, e, and the Avogadro constant, N(A). As experimental techniques improved, the precision of the value of h expanded. When the Josephson and quantum Hall theories led to new electronic devices, and a hundred year old experiment, the absolute ampere, was altered into a watt balance, h not only became vital in definitions for the volt and ohm units, but suddenly it could be measured directly and even more accurately. Finally, as measurement uncertainties now approach a few parts in 10(8) from the watt balance experiments and Avogadro determinations, its importance has been linked to a proposed redefinition of a kilogram unit of mass. The path to higher accuracy in measuring the value of h was not always an example of continuous progress. Since new measurements periodically led to changes in its accepted value and the corresponding SI units, it is helpful to see why there were bumps in the road and where the different branch lines of research joined in the effort. Recalling the bumps along this road will hopefully avoid their repetition in the upcoming SI redefinition debates. This paper begins with a brief history of the methods to measure a combination of fundamental constants, thus indirectly obtaining the Planck constant. The historical path is followed in the section describing how the

  14. History and progress on accurate measurements of the Planck constant

    Steiner, Richard

    2013-01-01

    The measurement of the Planck constant, h, is entering a new phase. The CODATA 2010 recommended value is 6.626 069 57 × 10-34 J s, but it has been a long road, and the trip is not over yet. Since its discovery as a fundamental physical constant to explain various effects in quantum theory, h has become especially important in defining standards for electrical measurements and soon, for mass determination. Measuring h in the International System of Units (SI) started as experimental attempts merely to prove its existence. Many decades passed while newer experiments measured physical effects that were the influence of h combined with other physical constants: elementary charge, e, and the Avogadro constant, NA. As experimental techniques improved, the precision of the value of h expanded. When the Josephson and quantum Hall theories led to new electronic devices, and a hundred year old experiment, the absolute ampere, was altered into a watt balance, h not only became vital in definitions for the volt and ohm units, but suddenly it could be measured directly and even more accurately. Finally, as measurement uncertainties now approach a few parts in 108 from the watt balance experiments and Avogadro determinations, its importance has been linked to a proposed redefinition of a kilogram unit of mass. The path to higher accuracy in measuring the value of h was not always an example of continuous progress. Since new measurements periodically led to changes in its accepted value and the corresponding SI units, it is helpful to see why there were bumps in the road and where the different branch lines of research joined in the effort. Recalling the bumps along this road will hopefully avoid their repetition in the upcoming SI redefinition debates. This paper begins with a brief history of the methods to measure a combination of fundamental constants, thus indirectly obtaining the Planck constant. The historical path is followed in the section describing how the improved

  15. History and progress on accurate measurements of the Planck constant

    The measurement of the Planck constant, h, is entering a new phase. The CODATA 2010 recommended value is 6.626 069 57 × 10−34 J s, but it has been a long road, and the trip is not over yet. Since its discovery as a fundamental physical constant to explain various effects in quantum theory, h has become especially important in defining standards for electrical measurements and soon, for mass determination. Measuring h in the International System of Units (SI) started as experimental attempts merely to prove its existence. Many decades passed while newer experiments measured physical effects that were the influence of h combined with other physical constants: elementary charge, e, and the Avogadro constant, NA. As experimental techniques improved, the precision of the value of h expanded. When the Josephson and quantum Hall theories led to new electronic devices, and a hundred year old experiment, the absolute ampere, was altered into a watt balance, h not only became vital in definitions for the volt and ohm units, but suddenly it could be measured directly and even more accurately. Finally, as measurement uncertainties now approach a few parts in 108 from the watt balance experiments and Avogadro determinations, its importance has been linked to a proposed redefinition of a kilogram unit of mass. The path to higher accuracy in measuring the value of h was not always an example of continuous progress. Since new measurements periodically led to changes in its accepted value and the corresponding SI units, it is helpful to see why there were bumps in the road and where the different branch lines of research joined in the effort. Recalling the bumps along this road will hopefully avoid their repetition in the upcoming SI redefinition debates. This paper begins with a brief history of the methods to measure a combination of fundamental constants, thus indirectly obtaining the Planck constant. The historical path is followed in the section describing how the

  16. Accurate Peptide Fragment Mass Analysis: Multiplexed Peptide Identification and Quantification

    Weisbrod, Chad R.; Eng, Jimmy K.; Hoopmann, Michael R.; Baker, Tahmina; Bruce, James E.

    2012-01-01

    FT All Reaction Monitoring (FT-ARM) is a novel approach for the identification and quantification of peptides that relies upon the selectivity of high mass accuracy data and the specificity of peptide fragmentation patterns. An FT-ARM experiment involves continuous, data-independent, high mass accuracy MS/MS acquisition spanning a defined m/z range. Custom software was developed to search peptides against the multiplexed fragmentation spectra by comparing theoretical or empirical fragment ion...

  17. Accurate Insertion Loss Measurements of the Juno Patch Array Antennas

    Chamberlain, Neil; Chen, Jacqueline; Hodges, Richard; Demas, John

    2010-01-01

    This paper describes two independent methods for estimating the insertion loss of patch array antennas that were developed for the Juno Microwave Radiometer instrument. One method is based principally on pattern measurements while the other method is based solely on network analyzer measurements. The methods are accurate to within 0.1 dB for the measured antennas and show good agreement (to within 0.1dB) of separate radiometric measurements.

  18. Accurately measuring dynamic coefficient of friction in ultraform finishing

    Briggs, Dennis; Echaves, Samantha; Pidgeon, Brendan; Travis, Nathan; Ellis, Jonathan D.

    2013-09-01

    UltraForm Finishing (UFF) is a deterministic sub-aperture computer numerically controlled grinding and polishing platform designed by OptiPro Systems. UFF is used to grind and polish a variety of optics from simple spherical to fully freeform, and numerous materials from glasses to optical ceramics. The UFF system consists of an abrasive belt around a compliant wheel that rotates and contacts the part to remove material. This work aims to accurately measure the dynamic coefficient of friction (μ), how it changes as a function of belt wear, and how this ultimately affects material removal rates. The coefficient of friction has been examined in terms of contact mechanics and Preston's equation to determine accurate material removal rates. By accurately predicting changes in μ, polishing iterations can be more accurately predicted, reducing the total number of iterations required to meet specifications. We have established an experimental apparatus that can accurately measure μ by measuring triaxial forces during translating loading conditions or while manufacturing the removal spots used to calculate material removal rates. Using this system, we will demonstrate μ measurements for UFF belts during different states of their lifecycle and assess the material removal function from spot diagrams as a function of wear. Ultimately, we will use this system for qualifying belt-wheel-material combinations to develop a spot-morphing model to better predict instantaneous material removal functions.

  19. Accurate mass filtering of ion chromatograms for metabolite identification using a unit mass resolution liquid chromatography/mass spectrometry system.

    Gu, Ming; Wang, Yongdong; Zhao, Xian-Guo; Gu, Zhe-Ming

    2006-01-01

    Acceleration of liquid chromatography/mass spectrometric (LC/MS) analysis for metabolite identification critically relies on effective data processing since the rate of data acquisition is much faster than the rate of data mining. The rapid and accurate identification of metabolite peaks from complex LC/MS data is a key component to speeding up the process. Current approaches routinely use selected ion chromatograms that can suffer severely from matrix effects. This paper describes a new method to automatically extract and filter metabolite-related information from LC/MS data obtained at unit mass resolution in the presence of complex biological matrices. This approach is illustrated by LC/MS analysis of the metabolites of verapamil from a rat microsome incubation spiked with biological matrix (bile). MS data were acquired in profile mode on a unit mass resolution triple-quadrupole instrument, externally calibrated using a unique procedure that corrects for both mass axis and mass spectral peak shape to facilitate metabolite identification with high mass accuracy. Through the double-filtering effects of accurate mass and isotope profile, conventional extracted ion chromatograms corresponding to the parent drug (verapamil at m/z 455), demethylated verapamil (m/z 441), and dealkylated verapamil (m/z 291), that contained substantial false-positive peaks, were simplified into chromatograms that are substantially free from matrix interferences. These filtered chromatograms approach what would have been obtained by using a radioactivity detector to detect radio-labeled metabolites of interest. PMID:16463359

  20. Radio Astronomers Set New Standard for Accurate Cosmic Distance Measurement

    1999-06-01

    A team of radio astronomers has used the National Science Foundation's Very Long Baseline Array (VLBA) to make the most accurate measurement ever made of the distance to a faraway galaxy. Their direct measurement calls into question the precision of distance determinations made by other techniques, including those announced last week by a team using the Hubble Space Telescope. The radio astronomers measured a distance of 23.5 million light-years to a galaxy called NGC 4258 in Ursa Major. "Ours is a direct measurement, using geometry, and is independent of all other methods of determining cosmic distances," said Jim Herrnstein, of the National Radio Astronomy Observatory (NRAO) in Socorro, NM. The team says their measurement is accurate to within less than a million light-years, or four percent. The galaxy is also known as Messier 106 and is visible with amateur telescopes. Herrnstein, along with James Moran and Lincoln Greenhill of the Harvard- Smithsonian Center for Astrophysics; Phillip Diamond, of the Merlin radio telescope facility at Jodrell Bank and the University of Manchester in England; Makato Inoue and Naomasa Nakai of Japan's Nobeyama Radio Observatory; Mikato Miyoshi of Japan's National Astronomical Observatory; Christian Henkel of Germany's Max Planck Institute for Radio Astronomy; and Adam Riess of the University of California at Berkeley, announced their findings at the American Astronomical Society's meeting in Chicago. "This is an incredible achievement to measure the distance to another galaxy with this precision," said Miller Goss, NRAO's Director of VLA/VLBA Operations. "This is the first time such a great distance has been measured this accurately. It took painstaking work on the part of the observing team, and it took a radio telescope the size of the Earth -- the VLBA -- to make it possible," Goss said. "Astronomers have sought to determine the Hubble Constant, the rate of expansion of the universe, for decades. This will in turn lead to an

  1. Accurate measurement of streamwise vortices using dual-plane PIV

    Waldman, Rye M.; Breuer, Kenneth S. [Brown University, School of Engineering, Providence, RI (United States)

    2012-11-15

    Low Reynolds number aerodynamic experiments with flapping animals (such as bats and small birds) are of particular interest due to their application to micro air vehicles which operate in a similar parameter space. Previous PIV wake measurements described the structures left by bats and birds and provided insight into the time history of their aerodynamic force generation; however, these studies have faced difficulty drawing quantitative conclusions based on said measurements. The highly three-dimensional and unsteady nature of the flows associated with flapping flight are major challenges for accurate measurements. The challenge of animal flight measurements is finding small flow features in a large field of view at high speed with limited laser energy and camera resolution. Cross-stream measurement is further complicated by the predominately out-of-plane flow that requires thick laser sheets and short inter-frame times, which increase noise and measurement uncertainty. Choosing appropriate experimental parameters requires compromise between the spatial and temporal resolution and the dynamic range of the measurement. To explore these challenges, we do a case study on the wake of a fixed wing. The fixed model simplifies the experiment and allows direct measurements of the aerodynamic forces via load cell. We present a detailed analysis of the wake measurements, discuss the criteria for making accurate measurements, and present a solution for making quantitative aerodynamic load measurements behind free-flyers. (orig.)

  2. Alignment of capillary electrophoresis-mass spectrometry datasets using accurate mass information.

    Nevedomskaya, Ekaterina; Derks, Rico; Deelder, André M; Mayboroda, Oleg A; Palmblad, Magnus

    2009-12-01

    Capillary electrophoresis-mass spectrometry (CE-MS) is a powerful technique for the analysis of small soluble compounds in biological fluids. A major drawback of CE is the poor migration time reproducibility, which makes it difficult to combine data from different experiments and correctly assign compounds. A number of alignment algorithms have been developed but not all of them can cope with large and irregular time shifts between CE-MS runs. Here we present a genetic algorithm designed for alignment of CE-MS data using accurate mass information. The utility of the algorithm was demonstrated on real data, and the results were compared with one of the existing packages. The new algorithm showed a significant reduction of elution time variation in the aligned datasets. The importance of mass accuracy for the performance of the algorithm was also demonstrated by comparing alignments of datasets from a standard time-of-flight (TOF) instrument with those from the new ultrahigh resolution TOF maXis (Bruker Daltonics). PMID:19826795

  3. Optimized pulse sequences for the accurate measurement of aortic compliance

    Aortic compliance is potentially an important cardiovascular diagnostic parameter by virtue of a proposed correlation with cardiovascular fitness. Measurement requires cross-sectional images of the ascending and descending aorta in systole and diastole for measurement of aortic lumen areas. Diastolic images have poor vessel- wall delineation due to signal from slow-flowing blood. A comparison has been carried out using presaturation (SAT) RF pulses, transparent RF pulses, and flow-compensated gradients in standard pulse sequences to improve vessel-wall delineation in diastole. Properly timed SAT pulses provide the most consistent vessel-wall delineation and the most accurate measurement of aortic compliance

  4. A Statistical Method for Assessing Peptide Identification Confidence in Accurate Mass and Time Tag Proteomics

    Stanley, Jeffrey R.; Adkins, Joshua N.; Slysz, Gordon W.; Monroe, Matthew E.; Purvine, Samuel O.; Karpievitch, Yuliya V.; Anderson, Gordon A.; Smith, Richard D.; Dabney, Alan R.

    2011-07-15

    High-throughput proteomics is rapidly evolving to require high mass measurement accuracy for a variety of different applications. Increased mass measurement accuracy in bottom-up proteomics specifically allows for an improved ability to distinguish and characterize detected MS features, which may in turn be identified by, e.g., matching to entries in a database for both precursor and fragmentation mass identification methods. Many tools exist with which to score the identification of peptides from LC-MS/MS measurements or to assess matches to an accurate mass and time (AMT) tag database, but these two calculations remain distinctly unrelated. Here we present a statistical method, Statistical Tools for AMT tag Confidence (STAC), which extends our previous work incorporating prior probabilities of correct sequence identification from LC-MS/MS, as well as the quality with which LC-MS features match AMT tags, to evaluate peptide identification confidence. Compared to existing tools, we are able to obtain significantly more high-confidence peptide identifications at a given false discovery rate and additionally assign confidence estimates to individual peptide identifications. Freely available software implementations of STAC are available in both command line and as a Windows graphical application.

  5. Calibration Techniques for Accurate Measurements by Underwater Camera Systems

    Mark Shortis

    2015-01-01

    Calibration of a camera system is essential to ensure that image measurements result in accurate estimates of locations and dimensions within the object space. In the underwater environment, the calibration must implicitly or explicitly model and compensate for the refractive effects of waterproof housings and the water medium. This paper reviews the different approaches to the calibration of underwater camera systems in theoretical and practical terms. The accuracy, reliability, validation a...

  6. Measurements of neutrino mass

    Direct experimental information of neutrino mass as derived from the study of nuclear and elementary-particle weak decays is reviewed. Topics include tritium beta decay; the 3He-T mass difference; electron capture decay of 163Ho and 158Tb; and limits on massive neutrinos from cosmology. 38 references

  7. Mass properties measurement system dynamics

    Doty, Keith L.

    1993-01-01

    The MPMS mechanism possess two revolute degrees-of-freedom and allows the user to measure the mass, center of gravity, and the inertia tensor of an unknown mass. The dynamics of the Mass Properties Measurement System (MPMS) from the Lagrangian approach to illustrate the dependency of the motion on the unknown parameters.

  8. Accurate volume measurement system for plutonium nitrate solution

    An accurate volume measurement system for a large amount of plutonium nitrate solution stored in a reprocessing or a conversion plant has been developed at the Plutonium Conversion Development Facility (PCDF) in the Power Reactor and Nuclear Fuel Development Corp. (PNC) Tokai Works. A pair of differential digital quartz pressure transducers is utilized in the volume measurement system. To obtain high accuracy, it is important that the non-linearity of the transducer is minimized within the measurement range, the zero point is stabilized, and the damping property of the pneumatic line is designed to minimize pressure oscillation. The accuracy of the pressure measurement can always be within 2Pa with re-calibration once a year. In the PCDF, the overall uncertainty of the volume measurement has been evaluated to be within 0.2 %. This system has been successfully applied to the Japanese government's and IAEA's routine inspection since 1984. (author)

  9. Calibration Techniques for Accurate Measurements by Underwater Camera Systems.

    Shortis, Mark

    2015-01-01

    Calibration of a camera system is essential to ensure that image measurements result in accurate estimates of locations and dimensions within the object space. In the underwater environment, the calibration must implicitly or explicitly model and compensate for the refractive effects of waterproof housings and the water medium. This paper reviews the different approaches to the calibration of underwater camera systems in theoretical and practical terms. The accuracy, reliability, validation and stability of underwater camera system calibration are also discussed. Samples of results from published reports are provided to demonstrate the range of possible accuracies for the measurements produced by underwater camera systems. PMID:26690172

  10. Direct neutrino mass measurements

    Thümmler, T.

    2011-07-01

    The determination of the neutrino rest mass plays an important role at the intersections of cosmology, particle physics and astroparticle physics. This topic is currently being addressed by two complementary approaches in laboratory experiments. Neutrinoless double beta decay experiments probe whether neutrinos are Majorana particles and determine an effective neutrino mass value. Single beta decay experiments such as KATRIN and MARE investigate the spectral shape of β-decay electrons close to their kinematic endpoint in order to determine the neutrino rest mass with a model-independent method. Owing to neutrino flavour mixing, the neutrino mass parameter appears as an average of all neutrino mass eigenstates contributing to the electron neutrino. The KArlsruhe TRItium Neutrino experiment (KATRIN) is currently the experiment in the most advanced status of commissioning. Applying an ultra-luminous molecular windowless gaseous tritium source and an integrating high-resolution spectrometer of MAC-E filter type, it allows β-spectroscopy close to the T 2 end-point with unprecedented precision and will reach a sensitivity of 200 meV/ c 2 (90% C.L.) on the neutrino rest mass.

  11. Methods for Accurate Free Flight Measurement of Drag Coefficients

    Courtney, Elya; Courtney, Michael

    2015-01-01

    This paper describes experimental methods for free flight measurement of drag coefficients to an accuracy of approximately 1%. There are two main methods of determining free flight drag coefficients, or equivalent ballistic coefficients: 1) measuring near and far velocities over a known distance and 2) measuring a near velocity and time of flight over a known distance. Atmospheric conditions must also be known and nearly constant over the flight path. A number of tradeoffs are important when designing experiments to accurately determine drag coefficients. The flight distance must be large enough so that the projectile's loss of velocity is significant compared with its initial velocity and much larger than the uncertainty in the near and/or far velocity measurements. On the other hand, since drag coefficients and ballistic coefficients both depend on velocity, the change in velocity over the flight path should be small enough that the average drag coefficient over the path (which is what is really determined)...

  12. Atomic spectroscopy and highly accurate measurement: determination of fundamental constants

    This document reviews the theoretical and experimental achievements of the author concerning highly accurate atomic spectroscopy applied for the determination of fundamental constants. A pure optical frequency measurement of the 2S-12D 2-photon transitions in atomic hydrogen and deuterium has been performed. The experimental setting-up is described as well as the data analysis. Optimized values for the Rydberg constant and Lamb shifts have been deduced (R = 109737.31568516 (84) cm-1). An experiment devoted to the determination of the fine structure constant with an aimed relative uncertainty of 10-9 began in 1999. This experiment is based on the fact that Bloch oscillations in a frequency chirped optical lattice are a powerful tool to transfer coherently many photon momenta to the atoms. We have used this method to measure accurately the ratio h/m(Rb). The measured value of the fine structure constant is α-1 = 137.03599884 (91) with a relative uncertainty of 6.7*10-9. The future and perspectives of this experiment are presented. This document presented before an academic board will allow his author to manage research work and particularly to tutor thesis students. (A.C.)

  13. SPECT-OPT multimodal imaging enables accurate evaluation of radiotracers for β-cell mass assessments.

    Eter, Wael A; Parween, Saba; Joosten, Lieke; Frielink, Cathelijne; Eriksson, Maria; Brom, Maarten; Ahlgren, Ulf; Gotthardt, Martin

    2016-01-01

    Single Photon Emission Computed Tomography (SPECT) has become a promising experimental approach to monitor changes in β-cell mass (BCM) during diabetes progression. SPECT imaging of pancreatic islets is most commonly cross-validated by stereological analysis of histological pancreatic sections after insulin staining. Typically, stereological methods do not accurately determine the total β-cell volume, which is inconvenient when correlating total pancreatic tracer uptake with BCM. Alternative methods are therefore warranted to cross-validate β-cell imaging using radiotracers. In this study, we introduce multimodal SPECT - optical projection tomography (OPT) imaging as an accurate approach to cross-validate radionuclide-based imaging of β-cells. Uptake of a promising radiotracer for β-cell imaging by SPECT, (111)In-exendin-3, was measured by ex vivo-SPECT and cross evaluated by 3D quantitative OPT imaging as well as with histology within healthy and alloxan-treated Brown Norway rat pancreata. SPECT signal was in excellent linear correlation with OPT data as compared to histology. While histological determination of islet spatial distribution was challenging, SPECT and OPT revealed similar distribution patterns of (111)In-exendin-3 and insulin positive β-cell volumes between different pancreatic lobes, both visually and quantitatively. We propose ex vivo SPECT-OPT multimodal imaging as a highly accurate strategy for validating the performance of β-cell radiotracers. PMID:27080529

  14. A spectroscopic transfer standard for accurate atmospheric CO measurements

    Nwaboh, Javis A.; Li, Gang; Serdyukov, Anton; Werhahn, Olav; Ebert, Volker

    2016-04-01

    Atmospheric carbon monoxide (CO) is a precursor of essential climate variables and has an indirect effect for enhancing global warming. Accurate and reliable measurements of atmospheric CO concentration are becoming indispensable. WMO-GAW reports states a compatibility goal of ±2 ppb for atmospheric CO concentration measurements. Therefore, the EMRP-HIGHGAS (European metrology research program - high-impact greenhouse gases) project aims at developing spectroscopic transfer standards for CO concentration measurements to meet this goal. A spectroscopic transfer standard would provide results that are directly traceable to the SI, can be very useful for calibration of devices operating in the field, and could complement classical gas standards in the field where calibration gas mixtures in bottles often are not accurate, available or stable enough [1][2]. Here, we present our new direct tunable diode laser absorption spectroscopy (dTDLAS) sensor capable of performing absolute ("calibration free") CO concentration measurements, and being operated as a spectroscopic transfer standard. To achieve the compatibility goal stated by WMO for CO concentration measurements and ensure the traceability of the final concentration results, traceable spectral line data especially line intensities with appropriate uncertainties are needed. Therefore, we utilize our new high-resolution Fourier-transform infrared (FTIR) spectroscopy CO line data for the 2-0 band, with significantly reduced uncertainties, for the dTDLAS data evaluation. Further, we demonstrate the capability of our sensor for atmospheric CO measurements, discuss uncertainty calculation following the guide to the expression of uncertainty in measurement (GUM) principles and show that CO concentrations derived using the sensor, based on the TILSAM (traceable infrared laser spectroscopic amount fraction measurement) method, are in excellent agreement with gravimetric values. Acknowledgement Parts of this work have been

  15. Black-Hole Mass Measurements

    Vestergaard, Marianne

    2004-01-01

    The applicability and apparent uncertainties of the techniques currently available for measuring or estimating black-hole masses in AGNs are briefly summarized.......The applicability and apparent uncertainties of the techniques currently available for measuring or estimating black-hole masses in AGNs are briefly summarized....

  16. Accurate reconstruction of hyperspectral images from compressive sensing measurements

    Greer, John B.; Flake, J. C.

    2013-05-01

    The emerging field of Compressive Sensing (CS) provides a new way to capture data by shifting the heaviest burden of data collection from the sensor to the computer on the user-end. This new means of sensing requires fewer measurements for a given amount of information than traditional sensors. We investigate the efficacy of CS for capturing HyperSpectral Imagery (HSI) remotely. We also introduce a new family of algorithms for constructing HSI from CS measurements with Split Bregman Iteration [Goldstein and Osher,2009]. These algorithms combine spatial Total Variation (TV) with smoothing in the spectral dimension. We examine models for three different CS sensors: the Coded Aperture Snapshot Spectral Imager-Single Disperser (CASSI-SD) [Wagadarikar et al.,2008] and Dual Disperser (CASSI-DD) [Gehm et al.,2007] cameras, and a hypothetical random sensing model closer to CS theory, but not necessarily implementable with existing technology. We simulate the capture of remotely sensed images by applying the sensor forward models to well-known HSI scenes - an AVIRIS image of Cuprite, Nevada and the HYMAP Urban image. To measure accuracy of the CS models, we compare the scenes constructed with our new algorithm to the original AVIRIS and HYMAP cubes. The results demonstrate the possibility of accurately sensing HSI remotely with significantly fewer measurements than standard hyperspectral cameras.

  17. Study of accurate volume measurement system for plutonium nitrate solution

    Hosoma, T. [Power Reactor and Nuclear Fuel Development Corp., Tokai, Ibaraki (Japan). Tokai Works

    1998-12-01

    It is important for effective safeguarding of nuclear materials to establish a technique for accurate volume measurement of plutonium nitrate solution in accountancy tank. The volume of the solution can be estimated by two differential pressures between three dip-tubes, in which the air is purged by an compressor. One of the differential pressure corresponds to the density of the solution, and another corresponds to the surface level of the solution in the tank. The measurement of the differential pressure contains many uncertain errors, such as precision of pressure transducer, fluctuation of back-pressure, generation of bubbles at the front of the dip-tubes, non-uniformity of temperature and density of the solution, pressure drop in the dip-tube, and so on. The various excess pressures at the volume measurement are discussed and corrected by a reasonable method. High precision-differential pressure measurement system is developed with a quartz oscillation type transducer which converts a differential pressure to a digital signal. The developed system is used for inspection by the government and IAEA. (M. Suetake)

  18. Accurate measurement of streamwise vortices in low speed aerodynamic flows

    Waldman, Rye M.; Kudo, Jun; Breuer, Kenneth S.

    2010-11-01

    Low Reynolds number experiments with flapping animals (such as bats and small birds) are of current interest in understanding biological flight mechanics, and due to their application to Micro Air Vehicles (MAVs) which operate in a similar parameter space. Previous PIV wake measurements have described the structures left by bats and birds, and provided insight to the time history of their aerodynamic force generation; however, these studies have faced difficulty drawing quantitative conclusions due to significant experimental challenges associated with the highly three-dimensional and unsteady nature of the flows, and the low wake velocities associated with lifting bodies that only weigh a few grams. This requires the high-speed resolution of small flow features in a large field of view using limited laser energy and finite camera resolution. Cross-stream measurements are further complicated by the high out-of-plane flow which requires thick laser sheets and short interframe times. To quantify and address these challenges we present data from a model study on the wake behind a fixed wing at conditions comparable to those found in biological flight. We present a detailed analysis of the PIV wake measurements, discuss the criteria necessary for accurate measurements, and present a new dual-plane PIV configuration to resolve these issues.

  19. Accurate measurement of RF exposure from emerging wireless communication systems

    Isotropic broadband probes or spectrum analyzers (SAs) may be used for the measurement of rapidly varying electromagnetic fields generated by emerging wireless communication systems. In this paper this problematic is investigated by comparing the responses measured by two different isotropic broadband probes typically used to perform electric field (E-field) evaluations. The broadband probes are submitted to signals with variable duty cycles (DC) and crest factors (CF) either with or without Orthogonal Frequency Division Multiplexing (OFDM) modulation but with the same root-mean-square (RMS) power. The two probes do not provide accurate enough results for deterministic signals such as Worldwide Interoperability for Microwave Access (WIMAX) or Long Term Evolution (LTE) as well as for non-deterministic signals such as Wireless Fidelity (WiFi). The legacy measurement protocols should be adapted to cope for the emerging wireless communication technologies based on the OFDM modulation scheme. This is not easily achieved except when the statistics of the RF emission are well known. In this case the measurement errors are shown to be systematic and a correction factor or calibration can be applied to obtain a good approximation of the total RMS power.

  20. Accurate measurement of RF exposure from emerging wireless communication systems

    Letertre, Thierry; Monebhurrun, Vikass; Toffano, Zeno

    2013-04-01

    Isotropic broadband probes or spectrum analyzers (SAs) may be used for the measurement of rapidly varying electromagnetic fields generated by emerging wireless communication systems. In this paper this problematic is investigated by comparing the responses measured by two different isotropic broadband probes typically used to perform electric field (E-field) evaluations. The broadband probes are submitted to signals with variable duty cycles (DC) and crest factors (CF) either with or without Orthogonal Frequency Division Multiplexing (OFDM) modulation but with the same root-mean-square (RMS) power. The two probes do not provide accurate enough results for deterministic signals such as Worldwide Interoperability for Microwave Access (WIMAX) or Long Term Evolution (LTE) as well as for non-deterministic signals such as Wireless Fidelity (WiFi). The legacy measurement protocols should be adapted to cope for the emerging wireless communication technologies based on the OFDM modulation scheme. This is not easily achieved except when the statistics of the RF emission are well known. In this case the measurement errors are shown to be systematic and a correction factor or calibration can be applied to obtain a good approximation of the total RMS power.

  1. Accurate determination and certification of bromine in plastic by isotope dilution inductively coupled plasma mass spectrometry

    Ohata, Masaki, E-mail: m-oohata@aist.go.jp; Miura, Tsutomu

    2014-07-21

    Highlights: • Accurate analytical method of Br in plastic was studied by isotope dilution ICPMS. • A microwave acid digestion using quartz vessel was suitable for Br analysis. • Sample dilution by NH{sub 3} solution could remove memory effect for ICPMS measurement. • The analytical result of the ID-ICPMS showed consistency with that of INAA. • The ID-ICPMS developed could apply to certification of Br in candidate plastic CRM. - Abstract: The accurate analytical method of bromine (Br) in plastic was developed by an isotope dilution inductively coupled plasma mass spectrometry (ID-ICPMS). The figures of merit of microwave acid digestion procedures using polytetrafluoroethylene (PTFE) or quartz vessels were studied and the latter one was suitable for Br analysis since its material was free from Br contamination. The sample dilution procedures using Milli-Q water or ammonium (NH{sub 3}) solution were also studied to remove memory effect for ICPMS measurement. Although severe memory effect was observed on Milli-Q water dilution, NH{sub 3} solution could remove it successfully. The accuracy of the ID-ICPMS was validated by a certified reference material (CRM) as well as the comparison with the analytical result obtained by an instrumental neutron activation analysis (INAA) as different analytical method. From these results, the ID-ICPMS developed in the present study could be evaluated as accurate analytical method of Br in plastic materials and it could apply to certification of Br in candidate plastic CRM with respect to such regulations related to RoHS (restriction of the use of hazardous substances in electrical and electronics equipment) directive.

  2. Accurate determination and certification of bromine in plastic by isotope dilution inductively coupled plasma mass spectrometry

    Highlights: • Accurate analytical method of Br in plastic was studied by isotope dilution ICPMS. • A microwave acid digestion using quartz vessel was suitable for Br analysis. • Sample dilution by NH3 solution could remove memory effect for ICPMS measurement. • The analytical result of the ID-ICPMS showed consistency with that of INAA. • The ID-ICPMS developed could apply to certification of Br in candidate plastic CRM. - Abstract: The accurate analytical method of bromine (Br) in plastic was developed by an isotope dilution inductively coupled plasma mass spectrometry (ID-ICPMS). The figures of merit of microwave acid digestion procedures using polytetrafluoroethylene (PTFE) or quartz vessels were studied and the latter one was suitable for Br analysis since its material was free from Br contamination. The sample dilution procedures using Milli-Q water or ammonium (NH3) solution were also studied to remove memory effect for ICPMS measurement. Although severe memory effect was observed on Milli-Q water dilution, NH3 solution could remove it successfully. The accuracy of the ID-ICPMS was validated by a certified reference material (CRM) as well as the comparison with the analytical result obtained by an instrumental neutron activation analysis (INAA) as different analytical method. From these results, the ID-ICPMS developed in the present study could be evaluated as accurate analytical method of Br in plastic materials and it could apply to certification of Br in candidate plastic CRM with respect to such regulations related to RoHS (restriction of the use of hazardous substances in electrical and electronics equipment) directive

  3. New simple method for fast and accurate measurement of volumes

    A new simple method is presented, which allows us to measure in just a few minutes but with reasonable accuracy (less than 1%) the volume confined inside a generic enclosure, regardless of the complexity of its shape. The technique proposed also allows us to measure the volume of any portion of a complex manifold, including, for instance, pipes and pipe fittings, valves, gauge heads, and so on, without disassembling the manifold at all. To this purpose an airtight variable volume is used, whose volume adjustment can be precisely measured; it has an overall capacity larger than that of the unknown volume. Such a variable volume is initially filled with a suitable test gas (for instance, air) at a known pressure, as carefully measured by means of a high precision capacitive gauge. By opening a valve, the test gas is allowed to expand into the previously evacuated unknown volume. A feedback control loop reacts to the resulting finite pressure drop, thus contracting the variable volume until the pressure exactly retrieves its initial value. The overall reduction of the variable volume achieved at the end of this process gives a direct measurement of the unknown volume, and definitively gets rid of the problem of dead spaces. The method proposed actually does not require the test gas to be rigorously held at a constant temperature, thus resulting in a huge simplification as compared to complex arrangements commonly used in metrology (gas expansion method), which can grant extremely accurate measurement but requires rather expensive equipments and results in time consuming methods, being therefore impractical in most applications. A simple theoretical analysis of the thermodynamic cycle and the results of experimental tests are described, which demonstrate that, in spite of its simplicity, the method provides a measurement accuracy within 0.5%. The system requires just a few minutes to complete a single measurement, and is ready immediately at the end of the process. The

  4. Downhole temperature tool accurately measures well bore profile

    This paper reports that an inexpensive temperature tool provides accurate temperatures measurements during drilling operations for better design of cement jobs, workovers, well stimulation, and well bore hydraulics. Valid temperature data during specific wellbore operations can improve initial job design, fluid testing, and slurry placement, ultimately enhancing well bore performance. This improvement applies to cement slurries, breaker activation for slurries, breaker activation for stimulation and profile control, and fluid rheological properties for all downhole operations. The temperature tool has been run standalone mounted inside drill pipe, on slick wire line and braided cable, and as a free-falltool. It has also been run piggyback on both directional surveys (slick line and free-fall) and standard logging runs. This temperature measuring system has been used extensively in field well bores to depths of 20,000 ft. The temperature tool is completely reusable in the field, ever similar to the standard directional survey tools used on may drilling rigs. The system includes a small, rugged, programmable temperature sensor, a standard body housing, various adapters for specific applications, and a personal computer (PC) interface

  5. Accurate Measurements of Aircraft Engine Soot Emissions Using a CAPS PMssa Monitor

    Onasch, Timothy; Thompson, Kevin; Renbaum-Wolff, Lindsay; Smallwood, Greg; Make-Lye, Richard; Freedman, Andrew

    2016-04-01

    We present results of aircraft engine soot emissions measurements during the VARIAnT2 campaign using CAPS PMssa monitors. VARIAnT2, an aircraft engine non-volatile particulate matter (nvPM) emissions field campaign, was focused on understanding the variability in nvPM mass measurements using different measurement techniques and accounting for possible nvPM sampling system losses. The CAPS PMssa monitor accurately measures both the optical extinction and scattering (and thus single scattering albedo and absorption) of an extracted sample using the same sample volume for both measurements with a time resolution of 1 second and sensitivity of better than 1 Mm-1. Absorption is obtained by subtracting the scattering signal from the total extinction. Given that the single scattering albedo of the particulates emitted from the aircraft engine measured at both 630 and 660 nm was on the order of 0.1, any inaccuracy in the scattering measurement has little impact on the accuracy of the ddetermined absorption coefficient. The absorption is converted into nvPM mass using a documented Mass Absorption Coefficient (MAC). Results of soot emission indices (mass soot emitted per mass of fuel consumed) for a turbojet engine as a function of engine power will be presented and compared to results obtained using an EC/OC monitor.

  6. Review of neutrino mass measurements

    The current status of the experimental search for neutrino mass is reviewed, with emphasis on direct kinematic methods. New data on the /tau/ neutrino from the Argus collaboration have reduced the upper mass limit a factor of 2. The situation concerning the electron neutrino mass as measured in tritium beta decay is essentially unchanged from a year ago. Simpson and Hime report finding evidence for a 17-keV neutrino in the β decay of 35S. There may be evidence for neutrino mass and mixing in the SN1987a data. 62 refs., 4 figs

  7. Automatic classification and accurate size measurement of blank mask defects

    Bhamidipati, Samir; Paninjath, Sankaranarayanan; Pereira, Mark; Buck, Peter

    2015-07-01

    complexity of defects encountered. The variety arises due to factors such as defect nature, size, shape and composition; and the optical phenomena occurring around the defect. This paper focuses on preliminary characterization results, in terms of classification and size estimation, obtained by Calibre MDPAutoClassify tool on a variety of mask blank defects. It primarily highlights the challenges faced in achieving the results with reference to the variety of defects observed on blank mask substrates and the underlying complexities which make accurate defect size measurement an important and challenging task.

  8. Assessing temporal flux of plant hormones in stored processing potatoes using high definition accurate mass spectrometry

    José Juan Ordaz-Ortiz; Sofia Foukaraki; Leon Alexander Terry

    2015-01-01

    Plant hormones are important molecules which at low concentration can regulate various physiological processes. Mass spectrometry has become a powerful technique for the quantification of multiple classes of plant hormones because of its high sensitivity and selectivity. We developed a new ultrahigh pressure liquid chromatography–full-scan high-definition accurate mass spectrometry method, for simultaneous determination of abscisic acid and four metabolites phaseic acid, dihydrophaseic acid, ...

  9. Accurate Measurements of Aerosol Hygroscopic Growth over a Wide Range in Relative Humidity.

    Rovelli, Grazia; Miles, Rachael E H; Reid, Jonathan P; Clegg, Simon L

    2016-06-30

    Using a comparative evaporation kinetics approach, we describe a new and accurate method for determining the equilibrium hygroscopic growth of aerosol droplets. The time-evolving size of an aqueous droplet, as it evaporates to a steady size and composition that is in equilibrium with the gas phase relative humidity, is used to determine the time-dependent mass flux of water, yielding information on the vapor pressure of water above the droplet surface at every instant in time. Accurate characterization of the gas phase relative humidity is provided from a control measurement of the evaporation profile of a droplet of know equilibrium properties, either a pure water droplet or a sodium chloride droplet. In combination, and by comparison with simulations that account for both the heat and mass transport governing the droplet evaporation kinetics, these measurements allow accurate retrieval of the equilibrium properties of the solution droplet (i.e., the variations with water activity in the mass fraction of solute, diameter growth factor, osmotic coefficient or number of water molecules per solute molecule). Hygroscopicity measurements can be made over a wide range in water activity (from >0.99 to, in principle, volatile solutes. The approach is benchmarked for binary and ternary inorganic solution aerosols with typical uncertainties in water activity of 0.9 and ∼±1% below 80% RH, and maximum uncertainties in diameter growth factor of ±0.7%. For all of the inorganic systems examined, the time-dependent data are consistent with large values of the mass accommodation (or evaporation) coefficient (>0.1). PMID:27285052

  10. Analysis of hydraulic fracturing flowback and produced waters using accurate mass: identification of ethoxylated surfactants.

    Thurman, E Michael; Ferrer, Imma; Blotevogel, Jens; Borch, Thomas

    2014-10-01

    Two series of ethylene oxide (EO) surfactants, polyethylene glycols (PEGs from EO3 to EO33) and linear alkyl ethoxylates (LAEs C-9 to C-15 with EO3-EO28), were identified in hydraulic fracturing flowback and produced water using a new application of the Kendrick mass defect and liquid chromatography/quadrupole-time-of-flight mass spectrometry. The Kendrick mass defect differentiates the proton, ammonium, and sodium adducts in both singly and doubly charged forms. A structural model of adduct formation is presented, and binding constants are calculated, which is based on a spherical cagelike conformation, where the central cation (NH4(+) or Na(+)) is coordinated with ether oxygens. A major purpose of the study was the identification of the ethylene oxide (EO) surfactants and the construction of a database with accurate masses and retention times in order to unravel the mass spectral complexity of surfactant mixtures used in hydraulic fracturing fluids. For example, over 500 accurate mass assignments are made in a few seconds of computer time, which then is used as a fingerprint chromatogram of the water samples. This technique is applied to a series of flowback and produced water samples to illustrate the usefulness of ethoxylate "fingerprinting", in a first application to monitor water quality that results from fluids used in hydraulic fracturing. PMID:25164376

  11. First mass measurements at LHCb

    Bressieux, J

    2011-01-01

    The LHC opens new frontiers in heavy flavour physics through an unprecedented statistical reach for a variety of interesting states produced in pp collisions. The LHCb spectrometer provides a good mass resolution and is suitable for spectroscopy studies. We present first preliminary mass measurements of several $b$ hadrons and of the exotic $X(3872)$ meson, reconstructed in final states containing a $J/\\psi$ using the data collected in 2010 by the LHCb experiment. An important aspect of the analysis is the calibration of the momentum scale using $J/\\psi \\to \\mu^+ \\mu^-$ decays, as well as the control of systematic uncertainties. While the already very competitive mass measurements for the $B^+$, $B^0$ and $B^0_s$ mesons receive similar contributions from systematic and statistical uncertainties, those of the $\\Lambda_b$, $B^+_c$ and $X(3872)$ particles are dominated by statistical uncertainties, and will therefore substantially improve with more data in the future.

  12. Galaxy And Mass Assembly: accurate panchromatic photometry from optical priors using LAMBDAR

    Wright, A. H.; Robotham, A. S. G.; Bourne, N.; Driver, S. P.; Dunne, L.; Maddox, S. J.; Alpaslan, M.; Andrews, S. K.; Bauer, A. E.; Bland-Hawthorn, J.; Brough, S.; Brown, M. J. I.; Clarke, C.; Cluver, M.; Davies, L. J. M.; Grootes, M. W.; Holwerda, B. W.; Hopkins, A. M.; Jarrett, T. H.; Kafle, P. R.; Lange, R.; Liske, J.; Loveday, J.; Moffett, A. J.; Norberg, P.; Popescu, C. C.; Smith, M.; Taylor, E. N.; Tuffs, R. J.; Wang, L.; Wilkins, S. M.

    2016-07-01

    We present the Lambda Adaptive Multi-Band Deblending Algorithm in R (LAMBDAR), a novel code for calculating matched aperture photometry across images that are neither pixel- nor PSF-matched, using prior aperture definitions derived from high-resolution optical imaging. The development of this program is motivated by the desire for consistent photometry and uncertainties across large ranges of photometric imaging, for use in calculating spectral energy distributions. We describe the program, specifically key features required for robust determination of panchromatic photometry: propagation of apertures to images with arbitrary resolution, local background estimation, aperture normalization, uncertainty determination and propagation, and object deblending. Using simulated images, we demonstrate that the program is able to recover accurate photometric measurements in both high-resolution, low-confusion, and low-resolution, high-confusion, regimes. We apply the program to the 21-band photometric data set from the Galaxy And Mass Assembly (GAMA) Panchromatic Data Release (PDR; Driver et al. 2016), which contains imaging spanning the far-UV to the far-IR. We compare photometry derived from LAMBDAR with that presented in Driver et al. (2016), finding broad agreement between the data sets. None the less, we demonstrate that the photometry from LAMBDAR is superior to that from the GAMA PDR, as determined by a reduction in the outlier rate and intrinsic scatter of colours in the LAMBDAR data set. We similarly find a decrease in the outlier rate of stellar masses and star formation rates using LAMBDAR photometry. Finally, we note an exceptional increase in the number of UV and mid-IR sources able to be constrained, which is accompanied by a significant increase in the mid-IR colour-colour parameter-space able to be explored.

  13. Measuring neutrino mass without neutrinos!

    Peach, Kenneth J

    2004-01-01

    Neutrinoless double beta decay offers the most precise (if challenging) way of measuring the absolute mass of the neutrino. Particle Physics met at the Rutherford Appleton Laboratory last autumn to discuss wether the UK should take a lead in setting up such an experiment

  14. Mass measurements near N = Z

    After an outline of the physics motivations, that illustrate why we think it is important to measure masses in the region N = Z, we report on on experiments performed at Ganil. An experiment aimed at measuring the masses of proton-rich nuclei in the mass region A∼60-80 has been performed, using a direct time-of-flight technique in conjunction with SISSI and the SPEG spectrometer at GANIL. The nuclei were produced via the fragmentation of a 78Kr beam (73 MeV/nucleon). A novel technique for the purification of the secondary beams, based on the stripping of the ions and using the α and the SPEG spectrometers, was successfully checked. It allows for good selectivity without altering the beam quality. Secondary ions of 100Ag, 100Cd, 100In and 100Sn were produced via the fusion-evaporation reaction 50Cr+58Ni at an energy of 5.1 MeV/nucleon, and were accelerated simultaneously in the second cyclotron of GANIL (CSS2). About 10 counts were observed from the production and acceleration of 100Sn22+. The masses of 100Cd, 100In and 100Sn were measured with respect to 100Ag using the CSS2 cyclotron, with precisions of 2 x 10-6, 3 x 10-6 and 10-5 respectively. (orig.)

  15. Top Mass from Electroweak Measurements

    Jacobsen, Bob

    1994-01-01

    The electroweak measurements made at LEP using 1989-1993 data are presented in preliminary form. The agreement with the Standard Model is satisfactory, and allows a combined fit to all available data for the masses of the top quark and standard Higgs boson. The fit yields M_t = 177 +11 -11 +18 -19 GeV/c2, where the second error reflects the uncertainty in the Higgs mass. Talk given at the XXIXth Rencontre de Moriond, `QCD and High Energy Hadronic Interactions', March 1994, Meribel France

  16. Fast and accurate mock catalogue generation for low-mass galaxies

    Koda, Jun; Beutler, Florian; Kazin, Eyal; Marin, Felipe

    2015-01-01

    We present an accurate and fast framework for generating mock catalogues including low-mass halos, based on an implementation of the COmoving Lagrangian Acceleration (COLA) technique. Multiple realisations of mock catalogues are crucial for analyses of large-scale structure, but conventional N-body simulations are too computationally expensive for the production of thousands of realisations. We show that COLA simulations can produce accurate mock catalogues with a moderate computation resource for low- to intermediate- mass galaxies in $10^{12} M_\\odot$ haloes, both in real and redshift space. COLA simulations have accurate peculiar velocities, without systematic errors in the velocity power spectra for k < 0.15 h/Mpc, and with only 3-per-cent error for k < 0.2 h/Mpc. We use COLA with 10 time steps and a Halo Occupation Distribution to produce 600 mock galaxy catalogues of the WiggleZ Dark Energy Survey. Our parallelized code for efficient generation of accurate halo catalogues is publicly available at ...

  17. Fast and accurate mock catalogue generation for low-mass galaxies

    Koda, Jun; Blake, Chris; Beutler, Florian; Kazin, Eyal; Marin, Felipe

    2016-06-01

    We present an accurate and fast framework for generating mock catalogues including low-mass haloes, based on an implementation of the COmoving Lagrangian Acceleration (COLA) technique. Multiple realisations of mock catalogues are crucial for analyses of large-scale structure, but conventional N-body simulations are too computationally expensive for the production of thousands of realizations. We show that COLA simulations can produce accurate mock catalogues with a moderate computation resource for low- to intermediate-mass galaxies in 1012 M⊙ haloes, both in real and redshift space. COLA simulations have accurate peculiar velocities, without systematic errors in the velocity power spectra for k ≤ 0.15 h Mpc-1, and with only 3-per cent error for k ≤ 0.2 h Mpc-1. We use COLA with 10 time steps and a Halo Occupation Distribution to produce 600 mock galaxy catalogues of the WiggleZ Dark Energy Survey. Our parallelized code for efficient generation of accurate halo catalogues is publicly available at github.com/junkoda/cola_halo.

  18. SPECT-OPT multimodal imaging enables accurate evaluation of radiotracers for β-cell mass assessments

    Wael A. Eter; Saba Parween; Lieke Joosten; Cathelijne Frielink; Maria Eriksson; Maarten Brom; Ulf Ahlgren; Martin Gotthardt

    2016-01-01

    Single Photon Emission Computed Tomography (SPECT) has become a promising experimental approach to monitor changes in β-cell mass (BCM) during diabetes progression. SPECT imaging of pancreatic islets is most commonly cross-validated by stereological analysis of histological pancreatic sections after insulin staining. Typically, stereological methods do not accurately determine the total β-cell volume, which is inconvenient when correlating total pancreatic tracer uptake with BCM. Alternative ...

  19. SPECT-OPT multimodal imaging enables accurate evaluation of radiotracers for beta-cell mass assessments

    Wael A. Eter; Parween, Saba; Joosten, Lieke; Frielink, Cathelijne; Eriksson, Maria; Brom, Maarten; Ahlgren, Ulf; Gotthardt, Martin

    2016-01-01

    Single Photon Emission Computed Tomography (SPECT) has become a promising experimental approach to monitor changes in beta-cell mass (BCM) during diabetes progression. SPECT imaging of pancreatic islets is most commonly cross-validated by stereological analysis of histological pancreatic sections after insulin staining. Typically, stereological methods do not accurately determine the total beta-cell volume, which is inconvenient when correlating total pancreatic tracer uptake with BCM. Altern...

  20. Accurate Prediction of the Ammonia Probes of a Variable Proton-to-Electron Mass Ratio

    Owens, Alec; Thiel, Walter; Špirko, Vladimir

    2015-01-01

    A comprehensive study of the mass sensitivity of the vibration-rotation-inversion transitions of $^{14}$NH$_3$, $^{15}$NH$_3$, $^{14}$ND$_3$, and $^{15}$ND$_3$ is carried out variationally using the TROVE approach. Variational calculations are robust and accurate, offering a new way to compute sensitivity coefficients. Particular attention is paid to the $\\Delta k=\\pm 3$ transitions between the accidentally coinciding rotation-inversion energy levels of the $\

  1. Accurate and fast fiber transfer delay measurement based on phase discrimination and frequency measurement

    Dong, J W; Gao, C; Wang, L J

    2016-01-01

    An accurate and fast fiber transfer delay measurement method is demonstrated. As a key technique, a simple ambiguity resolving process based on phase discrimination and frequency measurement is used to overcome the contradiction between measurement accuracy and system complexity. The optimized system achieves a high accuracy of 0.3 ps with a 0.1 ps resolution, and a large dynamic range up to 50 km as well as no dead zone.

  2. The Megamaser Cosmology Project. III. Accurate Masses of Seven Supermassive Black Holes in Active Galaxies with Circumnuclear Megamaser Disks

    Kuo, C Y; Condon, J J; Impellizzeri, C M V; Lo, K Y; Zaw, I; Schenker, M; Henkel, C; Reid, M J; Greene, J E

    2010-01-01

    Observations of H$_2$O masers from circumnuclear disks in active galaxies for the Megamaser Cosmology Project allow accurate measurement of the mass of supermassive black holes (BH) in these galaxies. We present the Very Long Baseline Interferometry (VLBI) images and kinematics of water maser emission in six active galaxies: NGC~1194, NGC~2273, NGC~2960 (Mrk~1419), NGC~4388, NGC~6264 and NGC~6323. We use the Keplerian rotation curves of these six megamaser galaxies, plus a seventh previously published, to determine accurate enclosed masses within the central $\\sim0.3$ pc of these galaxies, smaller than the radius of the sphere of influence of the central mass in all cases. We also set lower limits to the central mass densities of between 0.12 and 60 $\\times 10^{10} M_{\\odot}$~pc$^{-3}$. For six of the seven disks, the high central densities rule out clusters of stars or stellar remnants as the central objects, and this result further supports our assumption that the enclosed mass can be attributed predominant...

  3. Accurate phase measurements for thick spherical objects using optical quadrature microscopy

    Warger, William C., II; DiMarzio, Charles A.

    2009-02-01

    In vitro fertilization (IVF) procedures have resulted in the birth of over three million babies since 1978. Yet the live birth rate in the United States was only 34% in 2005, with 32% of the successful pregnancies resulting in multiple births. These multiple pregnancies were directly attributed to the transfer of multiple embryos to increase the probability that a single, healthy embryo was included. Current viability markers used for IVF, such as the cell number, symmetry, size, and fragmentation, are analyzed qualitatively with differential interference contrast (DIC) microscopy. However, this method is not ideal for quantitative measures beyond the 8-cell stage of development because the cells overlap and obstruct the view within and below the cluster of cells. We have developed the phase-subtraction cell-counting method that uses the combination of DIC and optical quadrature microscopy (OQM) to count the number of cells accurately in live mouse embryos beyond the 8-cell stage. We have also created a preliminary analysis to measure the cell symmetry, size, and fragmentation quantitatively by analyzing the relative dry mass from the OQM image in conjunction with the phase-subtraction count. In this paper, we will discuss the characterization of OQM with respect to measuring the phase accurately for spherical samples that are much larger than the depth of field. Once fully characterized and verified with human embryos, this methodology could provide the means for a more accurate method to score embryo viability.

  4. High-resolution accurate mass spectrometry as a technique for characterization of complex lysimeter leachate samples.

    Hand, Laurence H; Marshall, Samantha J; Saeed, Mansoor; Earll, Mark; Hadfield, Stephen T; Richardson, Kevan; Rawlinson, Paul

    2016-06-01

    Lysimeter studies can be used to identify and quantify soil degradates of agrochemicals (metabolites) that have the potential to leach to groundwater. However, the apparent metabolic profile of such lysimeter leachate samples will often be significantly more complex than would be expected in true groundwater samples. This is particularly true for S-metolachlor, which has an extremely complex metabolic pathway. Consequently, it was not practically possible to apply a conventional analytical approach to identify all metabolites in an S-metolachlor lysimeter study, because there was insufficient mass to enable the use of techniques such as nuclear magnetic resonance. Recent advances in high-resolution accurate mass spectrometry, however, allow innovative screening approaches to characterize leachate samples to a greater extent than previously possible. Leachate from the S-metolachlor study was screened for accurate masses (±5 ppm of the nominal mass) corresponding to more than 400 hypothetical metabolite structures. A refined list of plausible metabolites was constructed from these data to provide a comprehensive description of the most likely metabolites present. The properties of these metabolites were then evaluated using a principal component analysis model, based on molecular descriptors, to visualize the entire chemical space and to cluster the metabolites into a number of subclasses. This characterization and principal component analysis evaluation enabled the selection of suitable representative metabolites that were subsequently used as exemplars to assess the toxicological relevance of the leachate as a whole. Environ Toxicol Chem 2016;35:1401-1412. © 2015 SETAC. PMID:26627902

  5. Potential Direct Single-Star Mass Measurement

    Ghosh, H

    2004-01-01

    We analyze the lightcurve of the microlensing event OGLE-2003-BLG-175/MOA-2003-BLG-45 and show that it has two properties that, when combined with future high resolution astrometry, could lead to a direct, accurate measurement of the lens mass. First, the lightcurve shows clear signs of distortion due to the Earth's accelerated motion, which yields a measurement of the projected Einstein radius \\tilde r_E. Second, from precise astrometric measurements, we show that the blended light in the event is coincident with the microlensed source to within about 15 mas. This argues strongly that this blended light is the lens and hence opens the possibility of directly measuring the lens-source relative proper motion \\vec\\mu_\\rel and so the mass M=(c^2/4G)\\mu_\\rel t_E \\tilde r_E, where t_E is the measured Einstein timescale. While the lightcurve-based measurement of \\tilde r_E is, by itself, severely degenerate, we show that this degeneracy can be completely resolved by measuring the direction of proper motion \\vec\\mu_...

  6. Direct measurements of neutrino masses

    Holzschuh, E. [Zurich Univ. (Switzerland). Inst. fuer Physik

    1996-11-01

    The direct measurements have so far given no indication for a nonzero (positive) mass of any of the three known neutrinos. The experiments measuring the tau and the muon neutrino are good shape. The tritium experiments are in an unfortunate situation. It is unclear to me whether the problems are experimental or theoretical or a combination of both. The electronic final states distribution have been calculated, but the results have never been tested experimentally. The most important question to be answered is about the validity of the sudden approximation. (author) 9 figs., 2 tabs., 16 refs.

  7. Accurate micro Hall effect measurements on scribe line pads

    Østerberg, Frederik Westergaard; Petersen, Dirch Hjorth; Wang, Fei;

    2009-01-01

    Hall mobility and sheet carrier density are important parameters to monitor in advanced semiconductor production. If micro Hall effect measurements are done on small pads in scribe lines, these parameters may be measured without using valuable test wafers. We report how Hall mobility can be extra......Hall mobility and sheet carrier density are important parameters to monitor in advanced semiconductor production. If micro Hall effect measurements are done on small pads in scribe lines, these parameters may be measured without using valuable test wafers. We report how Hall mobility can...... be extracted from micro four-point measurements performed on a rectangular pad. The dimension of the investigated pad is 400 × 430 ¿m2, and the probe pitches range from 20 ¿m to 50 ¿m. The Monte Carlo method is used to find the optimal way to perform the Hall measurement and extract Hall mobility most...

  8. Problems with Accurate Atomic Lfetime Measurements of Multiply Charged Ions

    Trabert, E

    2009-02-19

    A number of recent atomic lifetime measurements on multiply charged ions have reported uncertainties lower than 1%. Such a level of accuracy challenges theory, which is a good thing. However, a few lessons learned from earlier precision lifetime measurements on atoms and singly charged ions suggest to remain cautious about the systematic errors of experimental techniques.

  9. Accurate Measurements of Spectral Reflectance in Picasso's Guernica Painting.

    de Luna, Javier Muñoz; Fernandez-Balbuena, Antonio Alvarez; Vázquez, Daniel; Melgosa, Manuel; Durán, Humberto; García, Jorge; Muro, Carmen

    2016-01-01

    The use of non-invasive spectral measurements to control the conservation status is a part of the preventive conservation of artworks which nowadays is becoming increasingly interesting. This paper describes how to use a spectral measuring device and an illumination system specifically designed for such a task in a very large dimension artwork painting (7.8 m wide × 3.5 m high). The system, controlled by a Cartesian robot, allows spectral measurements in a spectral range of 400-780 nm. The measured data array has a total of 2201 circular regions with 5.5 mm spot diameter placed on a square grid. Colorimetric calculations performed from these spectral measurements may be used to characterize color shifts related to reflectance changes in specific areas of the paint. A color shifting from the expected gray has been shown. PMID:26767640

  10. PRESAGE 3D dosimetry accurately measures Gamma Knife output factors

    Klawikowski, Slade J.; Yang, James N.; Adamovics, John; Ibbott, Geoffrey S.

    2014-12-01

    Small-field output factor measurements are traditionally very difficult because of steep dose gradients, loss of lateral electronic equilibrium, and dose volume averaging in finitely sized detectors. Three-dimensional (3D) dosimetry is ideal for measuring small output factors and avoids many of these potential challenges of point and 2D detectors. PRESAGE 3D polymer dosimeters were used to measure the output factors for the 4 mm and 8 mm collimators of the Leksell Perfexion Gamma Knife radiosurgery treatment system. Discrepancies between the planned and measured distance between shot centers were also investigated. A Gamma Knife head frame was mounted onto an anthropomorphic head phantom. Special inserts were machined to hold 60 mm diameter, 70 mm tall cylindrical PRESAGE dosimeters. The phantom was irradiated with one 16 mm shot and either one 4 mm or one 8 mm shot, to a prescribed dose of either 3 Gy or 4 Gy to the 50% isodose line. The two shots were spaced between 30 mm and 60 mm apart and aligned along the central axis of the cylinder. The Presage dosimeters were measured using the DMOS-RPC optical CT scanning system. Five independent 4 mm output factor measurements fell within 2% of the manufacturer’s Monte Carlo simulation-derived nominal value, as did two independent 8 mm output factor measurements. The measured distances between shot centers varied by ±0.8 mm with respect to the planned shot displacements. On the basis of these results, we conclude that PRESAGE dosimetry is excellently suited to quantify the difficult-to-measure Gamma Knife output factors.

  11. Visual texture accurate material appearance measurement, representation and modeling

    Haindl, Michal

    2013-01-01

    This book surveys the state of the art in multidimensional, physically-correct visual texture modeling. Features: reviews the entire process of texture synthesis, including material appearance representation, measurement, analysis, compression, modeling, editing, visualization, and perceptual evaluation; explains the derivation of the most common representations of visual texture, discussing their properties, advantages, and limitations; describes a range of techniques for the measurement of visual texture, including BRDF, SVBRDF, BTF and BSSRDF; investigates the visualization of textural info

  12. How to perform the most accurate possible phase measurements

    Berry, D. W.; Higgins, B. L.; Bartlett, S. D.; Mitchell, M. W.; Pryde, G. J.; Wiseman, H. M.

    2009-01-01

    We present the theory of how to achieve phase measurements with the minimum possible variance in ways that are readily implementable with current experimental techniques. Measurements whose statistics have high-frequency fringes, such as those obtained from NOON states, have commensurately high information yield. However this information is also highly ambiguous because it does not distinguish between phases at the same point on different fringes. We provide schemes to eliminate this phase am...

  13. ACCUWIND - Accurate wind speed measurements in wind energy - Summary report

    Friis Pedersen, Troels; Dahlberg, J.-Å.; Cuerva, A.; Mouzakis, F.; Busche, P.; Eecen, P.; Sanz-Andres, A.; Franchini, S.; Markkilde Petersen, Søren

    2006-01-01

    verification purposes, and for purposes of optimisation in research and development. The revised IEC standard on power performance measurements has now included requirements for classification of cup anemometers. Thebasis for setting up such requirements of cup anemometers is two EU projects SITEPARIDEN and......The cup anemometer is at present the standard instrument used for mean wind speed measurement in wind energy. It is being applied in high numbers around the world for wind energy assessments. It is also applied exclusively for accredited power performancemeasurements for certification and...... analysis of characteristics of cup and sonic anemometers. The methods and procedures provide a platform, hopefully for use in meeting the requirements of the IEC standard on power performance measurements, as well as for development of improvedinstruments....

  14. How to perform the most accurate possible phase measurements

    Berry, D W; Bartlett, S D; Mitchell, M W; Pryde, G J; Wiseman, H M

    2009-01-01

    We present the theory of how to achieve phase measurements with the minimum possible variance in ways that are readily implementable with current experimental techniques. Measurements whose statistics have high-frequency fringes, such as those obtained from NOON states, have commensurately high information yield. However this information is also highly ambiguous because it does not distinguish between phases at the same point on different fringes. We provide schemes to eliminate this phase ambiguity in a highly efficient way, providing phase estimates with uncertainty that is within a small constant factor of the Heisenberg limit, the minimum allowed by the laws of quantum mechanics. These techniques apply to NOON state and multi-pass interferometry, as well as phase measurements in quantum computing. We have reported the experimental implementation of some of these schemes with multi-pass interferometry elsewhere. Here we present the theoretical foundation, and also present some new experimental results. The...

  15. SPARC: Mass Models for 175 Disk Galaxies with Spitzer Photometry and Accurate Rotation Curves

    Lelli, Federico; Schombert, James M

    2016-01-01

    We introduce SPARC (Spitzer Photometry & Accurate Rotation Curves): a sample of 175 nearby galaxies with new surface photometry at 3.6 um and high-quality rotation curves from previous HI/Halpha studies. SPARC spans a broad range of morphologies (S0 to Irr), luminosities (~5 dex), and surface brightnesses (~4 dex). We derive [3.6] surface photometry and study structural relations of stellar and gas disks. We find that both the stellar mass-HI mass relation and the stellar radius-HI radius relation have significant intrinsic scatter, while the HI mass-radius relation is extremely tight. We build detailed mass models and quantify the ratio of baryonic-to-observed velocity (Vbar/Vobs) for different characteristic radii and values of the stellar mass-to-light ratio (M/L) at [3.6]. Assuming M/L=0.5 Msun/Lsun (as suggested by stellar population models) we find that (i) the gas fraction linearly correlates with total luminosity, (ii) the transition from star-dominated to gas-dominated galaxies roughly correspond...

  16. A capacitance servo control plunger for accurate lifetime measurement

    The recoil distance Doppler shift method has been widely used in the study of nuclear structure to determine the level lifetime and absolute transition probabilities. A capacitance servo control plunger based on this method has been successfully developed by the Nuclear Structure Group of the China Institute of Atomic Energy. Three microscopes were employed to check the parallelism and can therefore guarantee a delicate measurement of the distance between the target and the stopper. This new plunger made a successful performance in the test experiment and the measured lifetime of the 2+→0+ transition in 78Kr is in agreement with the previous value. (authors)

  17. Measuring the delay time of transmission line accurately by oscilloscope

    In the signal measurements and the diagnoses of transmission line's hitch fields, the transmission line's delay time is usually used. In the paper, a method of using oscilloscope to measure transmission line's delay time is discussed. A method diagnosing transmission line's hitches is also provided. The methods have been used successfully. It will help the power transmission line 's and communication line's hitches to be found and restored fast in many fields, for example, the heavy snow disaster in the southern of China. (authors)

  18. THE ARAUCARIA PROJECT: ACCURATE DETERMINATION OF THE DYNAMICAL MASS OF THE CLASSICAL CEPHEID IN THE ECLIPSING SYSTEM OGLE-LMC-CEP-1812

    We have analyzed the double-lined eclipsing binary system OGLE-LMC-CEP-1812 in the LMC and demonstrate that it contains a classical fundamental mode Cepheid pulsating with a period of 1.31 days. The secondary star is a stable giant. We derive the dynamical masses for both stars with an accuracy of 1.5%, making the Cepheid in this system the second classical Cepheid with a very accurate dynamical mass determination, following the OGLE-LMC-CEP-0227 system studied by Pietrzyński et al. The measured dynamical mass agrees very well with that predicted by pulsation models. We also derive the radii of both components and accurate orbital parameters for the binary system. This new, very accurate dynamical mass for a classical Cepheid will greatly contribute to the solution of the Cepheid mass discrepancy problem, and to our understanding of the structure and evolution of classical Cepheids.

  19. Miniature bioelectric device accurately measures and telemeters temperature

    Fryer, T. B.

    1966-01-01

    Miniature micropower solid-state circuit measures and telemeters the body temperature of laboratory animals over periods up to two years. The circuit employs a thermistor as a temperature sensing element and an fm transmitter. It is constructed from conventional discrete components or integrated circuits.

  20. Accurate antenna reflector loss measurements for radiometer calibration budget

    Skou, Niels

    Antenna reflector losses may play an important role in the calibration budget for a microwave radiometer. If the losses are small they are difficult to measure by traditional means. However, they can be assessed directly by radiometric means using the sky brightness temperature as incident...

  1. Accurate physical laws can permit new standard units: The two laws F→=ma→ and the proportionality of weight to mass

    Saslow, Wayne M.

    2014-04-01

    Three common approaches to F→=ma→ are: (1) as an exactly true definition of force F→ in terms of measured inertial mass m and measured acceleration a→; (2) as an exactly true axiom relating measured values of a→, F→ and m; and (3) as an imperfect but accurately true physical law relating measured a→ to measured F→, with m an experimentally determined, matter-dependent constant, in the spirit of the resistance R in Ohm's law. In the third case, the natural units are those of a→ and F→, where a→ is normally specified using distance and time as standard units, and F→ from a spring scale as a standard unit; thus mass units are derived from force, distance, and time units such as newtons, meters, and seconds. The present work develops the third approach when one includes a second physical law (again, imperfect but accurate)—that balance-scale weight W is proportional to m—and the fact that balance-scale measurements of relative weight are more accurate than those of absolute force. When distance and time also are more accurately measurable than absolute force, this second physical law permits a shift to standards of mass, distance, and time units, such as kilograms, meters, and seconds, with the unit of force—the newton—a derived unit. However, were force and distance more accurately measurable than time (e.g., time measured with an hourglass), this second physical law would permit a shift to standards of force, mass, and distance units such as newtons, kilograms, and meters, with the unit of time—the second—a derived unit. Therefore, the choice of the most accurate standard units depends both on what is most accurately measurable and on the accuracy of physical law.

  2. Accurate Measurement of Heat Capacity by Differential Scanning Calorimetry

    1984-01-01

    Experience with high quality heat capacity measurement by differential scanning calorimetry is summarized and illustrated, pointing out three major causes of error: (1) incompatible thermal histories of the sample, reference and blank runs; (2) unstable initial and final isotherms; (3) incompatible differences between initial and final isotherm amplitudes for sample, reference and blank runs. Considering these problems, it is shown for the case of polyoxymethylene that accuracies in heat capacity of 0.1 percent may be possible.

  3. Importance of Accurate Measurements in Nutrition Research: Dietary Flavonoids as a Case Study.

    Harnly, James

    2016-03-01

    Accurate measurements of the secondary metabolites in natural products and plant foods are critical for establishing relations between diet and health. There are as many as 50,000 secondary metabolites that may influence human health. Their structural and chemical diversity presents a challenge to analytical chemistry. With respect to flavonoids, putative identification is accessible, but positive identification and quantification are limited by the lack of standards. Quantification has been tested with use of both nonspecific and specific methods. Nonspecific methods, which include antioxidant capacity methods, fail to provide information on the measured components, suffer from numerous interferences, are not equatable, and are unsuitable for health research. Specific methods, such as LC with diode array and mass spectrometric detection, require the use of internal standards and relative molar response factors. These methods are relatively expensive and require a high level of expertise and experimental verification; however, they represent the only suitable means of relating health outcomes to specific dietary components. PMID:26980821

  4. Blood-Pressure Measuring System Gives Accurate Graphic Output

    1965-01-01

    The problem: To develop an instrument that will provide an external (indirect) measurement of arterial blood pressure in the form of an easily interpreted graphic trace that can be correlated with standard clinical blood-pressure measurements. From sphygmograms produced by conventional sphygmographs, it is very difficult to differentiate the systolic and diastolic blood-pressure pulses and to correlate these indices with the standard clinical values. It is nearly impossible to determine these indices when the subject is under physical or emotional stress. The solution: An electronic blood-pressure system, basically similar to conventional ausculatory sphygmomanometers, employing a standard occluding cuff, a gas-pressure source, and a gas-pressure regulator and valve. An electrical output transducer senses cuff pressure, and a microphone positioned on the brachial artery under the occluding cuff monitors the Korotkoff sounds from this artery. The output signals present the conventional systolic and diastolic indices in a clear, graphical display. The complete system also includes an electronic timer and cycle-control circuit.

  5. Accurate measurement of intestinal transit in the rat

    A new method for quantifying intestinal transit was evaluated by comparison with two other popular techniques. The distribution of radiochromium (51Cr) throughout the small intestine of rats previously treated with saline (1.0 ml/kg s.c.), capsaicin (10 mg/kg s.c.), hexamethonium (20 mg/kg i.p.), D-ala2-met-enkephalinamide (1.0 microgram i.c.v.), or neostigmine (0.1 mg/kg i.p.) was quantified by (1) measuring the most distal intestinal segment reached by chromium, (2) calculating the slope produced by linear regression analysis on cumulative percent chromium that had passed through each segment, and (3) determining the geometric center of the distribution of chromium throughout the small intestine. It was concluded that the geometric center methods for quantifying intestinal transit provides the most sensitive and reliable measure of intestinal transit. Less sensitive techniques often fail to detect important effects of drugs on intestinal transit

  6. Accurate measurement of intestinal transit in the rat

    Miller, M.S.; Galligan, J.J.; Burks, T.F.

    1981-11-01

    A new method for quantifying intestinal transit was evaluated by comparison with two other popular techniques. The distribution of radiochromium (51Cr) throughout the small intestine of rats previously treated with saline (1.0 ml/kg s.c.), capsaicin (10 mg/kg s.c.), hexamethonium (20 mg/kg i.p.), D-ala2-met-enkephalinamide (1.0 microgram i.c.v.), or neostigmine (0.1 mg/kg i.p.) was quantified by (1) measuring the most distal intestinal segment reached by chromium, (2) calculating the slope produced by linear regression analysis on cumulative percent chromium that had passed through each segment, and (3) determining the geometric center of the distribution of chromium throughout the small intestine. It was concluded that the geometric center methods for quantifying intestinal transit provides the most sensitive and reliable measure of intestinal transit. Less sensitive techniques often fail to detect important effects of drugs on intestinal transit.

  7. On accurate differential measurements with electrochemical impedance spectroscopy

    Kernbach, S; Kernbach, O

    2016-01-01

    This paper describes the impedance spectroscopy adapted for analysis of small electrochemical changes in fluids. To increase accuracy of measurements the differential approach with temperature stabilization of fluid samples and electronics is used. The impedance analysis is performed by the single point DFT, signal correlation, calculation of RMS amplitudes and interference phase shift. For test purposes the samples of liquids and colloids are treated by fully shielded electromagnetic generators and passive cone-shaped structures. Fluidic samples collected from different geological locations are also analysed. In all tested cases we obtained different results for impacted and non-impacted samples, moreover, a degradation of electrochemical stability after treatment is observed. This method is used in laboratory analysis of weak emissions and ensures a high repeatability of results.

  8. ACCURATE UNIVERSAL MODELS FOR THE MASS ACCRETION HISTORIES AND CONCENTRATIONS OF DARK MATTER HALOS

    A large amount of observations have constrained cosmological parameters and the initial density fluctuation spectrum to a very high accuracy. However, cosmological parameters change with time and the power index of the power spectrum dramatically varies with mass scale in the so-called concordance ΛCDM cosmology. Thus, any successful model for its structural evolution should work well simultaneously for various cosmological models and different power spectra. We use a large set of high-resolution N-body simulations of a variety of structure formation models (scale-free, standard CDM, open CDM, and ΛCDM) to study the mass accretion histories, the mass and redshift dependence of concentrations, and the concentration evolution histories of dark matter halos. We find that there is significant disagreement between the much-used empirical models in the literature and our simulations. Based on our simulation results, we find that the mass accretion rate of a halo is tightly correlated with a simple function of its mass, the redshift, parameters of the cosmology, and of the initial density fluctuation spectrum, which correctly disentangles the effects of all these factors and halo environments. We also find that the concentration of a halo is strongly correlated with the universe age when its progenitor on the mass accretion history first reaches 4% of its current mass. According to these correlations, we develop new empirical models for both the mass accretion histories and the concentration evolution histories of dark matter halos, and the latter can also be used to predict the mass and redshift dependence of halo concentrations. These models are accurate and universal: the same set of model parameters works well for different cosmological models and for halos of different masses at different redshifts, and in the ΛCDM case the model predictions match the simulation results very well even though halo mass is traced to about 0.0005 times the final mass, when

  9. Identification of Microorganisms by High Resolution Tandem Mass Spectrometry with Accurate Statistical Significance

    Alves, Gelio; Wang, Guanghui; Ogurtsov, Aleksey Y.; Drake, Steven K.; Gucek, Marjan; Suffredini, Anthony F.; Sacks, David B.; Yu, Yi-Kuo

    2016-02-01

    Correct and rapid identification of microorganisms is the key to the success of many important applications in health and safety, including, but not limited to, infection treatment, food safety, and biodefense. With the advance of mass spectrometry (MS) technology, the speed of identification can be greatly improved. However, the increasing number of microbes sequenced is challenging correct microbial identification because of the large number of choices present. To properly disentangle candidate microbes, one needs to go beyond apparent morphology or simple `fingerprinting'; to correctly prioritize the candidate microbes, one needs to have accurate statistical significance in microbial identification. We meet these challenges by using peptidome profiles of microbes to better separate them and by designing an analysis method that yields accurate statistical significance. Here, we present an analysis pipeline that uses tandem MS (MS/MS) spectra for microbial identification or classification. We have demonstrated, using MS/MS data of 81 samples, each composed of a single known microorganism, that the proposed pipeline can correctly identify microorganisms at least at the genus and species levels. We have also shown that the proposed pipeline computes accurate statistical significances, i.e., E-values for identified peptides and unified E-values for identified microorganisms. The proposed analysis pipeline has been implemented in MiCId, a freely available software for Microorganism Classification and Identification. MiCId is available for download at http://www.ncbi.nlm.nih.gov/CBBresearch/Yu/downloads.html.

  10. Accurate lattice parameter measurements of stoichiometric uranium dioxide

    Highlights: • The lattice parameter of stoichiometric uranium dioxide has been re-evaluated. • The new value is substantially higher than the generally accepted value. • The new value has an improved precision. • Earlier published values on the lattice parameter of UO2 are carefully re-assessed. • High accuracy was obtained on both stoichiometry and lattice parameter measurements. - Abstract: The paper presents and discusses lattice parameter analyses of pure, stoichiometric UO2. Attention was paid to prepare stoichiometric samples and to maintain stoichiometry throughout the analyses. The lattice parameter of UO2.000±0.001 was evaluated as being 547.127 ± 0.008 pm at 20 °C, which is substantially higher than many published values for the UO2 lattice constant and has an improved precision by about one order of magnitude. The higher value of the lattice constant is mainly attributed to the avoidance of hyperstoichiometry in the present study and to a minor extent to the use of the currently accepted Cu Kα1 X-ray wavelength value. Many of the early studies used Cu Kα1 wavelength values that differ from the currently accepted value, which also contributed to an underestimation of the true lattice parameter

  11. Accurate measurement of microscopic forces and torques using optical tweezers

    Andrew Forbes

    2011-09-01

    Full Text Available It is now well known that matter may be trapped by optical fields with high intensity gradients. Once trapped, it is then possible to manipulate microscopic particles using such optical fields, in so-called optical tweezers. Such optical trapping and tweezing systems have found widespread application across diverse fields in science, from applied biology to fundamental physics. In this article we outline the design and construction of an optical trapping and tweezing system, and show how the resulting interaction of the laser light with microscopic particles may be understood in terms of the transfer of linear and angular momentum of light. We demonstrate experimentally the use of our optical tweezing configuration for the measurement of microscopic forces and torques. In particular, we make use of digital holography to create so-called vortex laser beams, capable of transferring orbital angular momentum to particles. The use of such novel laser beams in an optical trapping and tweezing set-up allows for the control of biological species at the single-cell level.

  12. Accurate Measurement of Magnetic Resonance Imaging Gradient Characteristics

    Hui Liu

    2013-12-01

    Full Text Available Recently, gradient performance and fidelity has become of increasing interest, as the fidelity of the magnetic resonance (MR image is somewhat dependent on the fidelity of the gradient system. In particular, for high fidelity non-Cartesian imaging, due to non-fidelity of the gradient system, it becomes necessary to know the actual k-space trajectory as opposed to the requested trajectory. In this work we show that, by considering the gradient system as a linear time-invariant system, the gradient impulse response function (GIRF can be reliably measured to a relatively high degree of accuracy with a simple setup, using a small phantom and a series of simple experiments. It is shown experimentally that the resulting GIRF is able to predict actual gradient performance with a high degree of accuracy. The method captures not only the frequency response but also gradient timing errors and artifacts due to mechanical vibrations of the gradient system. Some discussion is provided comparing the method presented here with other analogous methods, along with limitations of these methods.

  13. Accurate lattice parameter measurements of stoichiometric uranium dioxide

    Leinders, Gregory, E-mail: gregory.leinders@sckcen.be [KU Leuven, Department of Chemistry, Celestijnenlaan 200F, P.O. Box 2404, B-3001 Heverlee (Belgium); Belgian Nuclear Research Centre (SCK-CEN), Institute for Nuclear Materials Science, Boeretang 200, B-2400 Mol (Belgium); Cardinaels, Thomas [Belgian Nuclear Research Centre (SCK-CEN), Institute for Nuclear Materials Science, Boeretang 200, B-2400 Mol (Belgium); Binnemans, Koen [KU Leuven, Department of Chemistry, Celestijnenlaan 200F, P.O. Box 2404, B-3001 Heverlee (Belgium); Verwerft, Marc [Belgian Nuclear Research Centre (SCK-CEN), Institute for Nuclear Materials Science, Boeretang 200, B-2400 Mol (Belgium)

    2015-04-15

    Highlights: • The lattice parameter of stoichiometric uranium dioxide has been re-evaluated. • The new value is substantially higher than the generally accepted value. • The new value has an improved precision. • Earlier published values on the lattice parameter of UO{sub 2} are carefully re-assessed. • High accuracy was obtained on both stoichiometry and lattice parameter measurements. - Abstract: The paper presents and discusses lattice parameter analyses of pure, stoichiometric UO{sub 2}. Attention was paid to prepare stoichiometric samples and to maintain stoichiometry throughout the analyses. The lattice parameter of UO{sub 2.000±0.001} was evaluated as being 547.127 ± 0.008 pm at 20 °C, which is substantially higher than many published values for the UO{sub 2} lattice constant and has an improved precision by about one order of magnitude. The higher value of the lattice constant is mainly attributed to the avoidance of hyperstoichiometry in the present study and to a minor extent to the use of the currently accepted Cu Kα{sub 1} X-ray wavelength value. Many of the early studies used Cu Kα{sub 1} wavelength values that differ from the currently accepted value, which also contributed to an underestimation of the true lattice parameter.

  14. Screening of the polyphenol content of tomato-based products through accurate-mass spectrometry (HPLC-ESI-QTOF).

    Vallverdú-Queralt, Anna; Jáuregui, Olga; Di Lecce, Giuseppe; Andrés-Lacueva, Cristina; Lamuela-Raventós, Rosa M

    2011-12-01

    Tomatoes, the second most important vegetable crop worldwide, are a key component in the so-called "Mediterranean diet" and its consumption has greatly increased worldwide over the past 2 decades, mostly due to a growing demand for tomato-based products such as ketchups, gazpachos and tomato juices. In this work, tomato-based products were analysed after a suitable work-up extraction procedure using liquid chromatography/electrospray ionisation-time of flight-mass spectrometry (HPLC-ESI-QTOF) with negative ion detection using information-dependent acquisition (IDA) to determine their phenolic composition. The compounds were confirmed by accurate mass measurements in MS and MS(2) modes. The elemental composition was selected according to the accurate masses and isotopic pattern. In this way, 47 compounds (simple phenolic and hydroxycinnamoylquinic acids and flavone, flavonol, flavanone and dihydrochalcone derivatives) were identified in tomato-based products, five of them, as far as was known, were previously unreported in tomatoes. The phenolic fingerprint showed that tomato-based products differ in phenolic composition, principally in protocatechuic acid-O-hexoside, apigenin and its glycosylated forms, quercetin-O-dihexoside, kaempferol-C-hexoside and eriodictyol-O-dihexoside. Gazpacho showed the highest number of phenolic compounds due to the vegetables added for its production. PMID:25212313

  15. Mass measurement of depleted uranium components with coincidence neutron count

    The technique of the mass measurement of depleted uranium components was studied with active and passive coincidence neutron count. A well neutron coincidence counter was used to measure the coincidence neutron counts of the depleted uranium components with various mass. Am-Be source was selected as the external neutron source for induced fission in the active measurement, and a shield was optimized to reduce the accidental coincidence counts. In the active measurement, the maximum relative deviation of the linear fit mass from the nominal mass of the depleted uranium components is 11.71%, compared to 4.05% in the passive measurement. It is proved that because of the weakening of the shape influence, the passive method is more accurate and reliable to measure the mass of depleted uranium components than the active method. (authors)

  16. Rapid and accurate biofuel moisture content gauging using magnetic resonance measurement technology

    Jaervinen, T.

    2013-04-15

    Biomass is extensively utilised in energy production and as a raw material, such as for the production of liquid biofuels. All those processes will benefit if the moisture content of bio material is known in advance as accurately as possible under transient circumstances. Biofuel trade is increasingly based on the calorific value of fuels. In the first step, this also increases the need for rapid and accurate moisture content determination. During the last few years, large biofuel standardisation has been implemented, emphasising biofuel quality control at all stages of the utilisation chain. In principle, the moisture instrumental measurement can be utilised by many technologies and procedures. Typical techniques are infrared, radiofrequency, microwave, radiometric, electrical conductivity, capacitance, and impedance. Nuclear magnetic resonance (MR) and thermal neutron absorption are also applied. The MR measurement principle has been known and utilised already since the early 1950s. It has become the basic instrumental analysis tool in chemistry. It is also well-known as a very accurate method for analysing most compounds, especially substances containing hydrogen. The utilisation of MR metering is expanded extensively to medical diagnostics as a form of magnetic resonance imaging (MRI). Because of the precision of the MR principle, there have for a long time been efforts to apply it in new and different areas, and to make more user-friendly, smaller, and even portable devices. Such a device was designed by Vaisala a few years ago. VTT has utilised Vaisala's MR prototype for approximately one year for moisture content measurement of different biofuels. The first step in the use of an MR device for moisture determination was the definition of its measurement accuracy compared to the standard method (EN 14774). Those tests proved that the absolute precision seems to be comparable to the standard moisture content measurement method. It was also found out that

  17. A feasibility study of UHPLC-HRMS accurate-mass screening methods for multiclass testing of organic contaminants in food.

    Pérez-Ortega, Patricia; Lara-Ortega, Felipe J; García-Reyes, Juan F; Gilbert-López, Bienvenida; Trojanowicz, Marek; Molina-Díaz, Antonio

    2016-11-01

    The feasibility of accurate-mass multi-residue screening methods using liquid chromatography high-resolution mass spectrometry (UHPLC-HRMS) using time-of-flight mass spectrometry has been evaluated, including over 625 multiclass food contaminants as case study. Aspects such as the selectivity and confirmation capability provided by HRMS with different acquisition modes (full-scan or full-scan combined with collision induced dissociation (CID) with no precursor ion isolation), and chromatographic separation along with main limitations such as sensitivity or automated data processing have been examined. Compound identification was accomplished with retention time matching and accurate mass measurements of the targeted ions for each analyte (mainly (de)protonated molecules). Compounds with the same nominal mass (isobaric species) were very frequent due to the large number of compounds included. Although 76% of database compounds were involved in isobaric groups, they were resolved in most cases (99% of these isobaric species were distinguished by retention time, resolving power, isotopic profile or fragment ions). Only three pairs could not be resolved with these tools. In-source CID fragmentation was evaluated in depth, although the results obtained in terms of information provided were not as thorough as those obtained using fragmentation experiments without precursor ion isolation (all ion mode). The latter acquisition mode was found to be the best suited for this type of large-scale screening method instead of classic product ion scan, as provided excellent fragmentation information for confirmatory purposes for an unlimited number of compounds. Leaving aside the sample treatment limitations, the main weaknesses noticed are basically the relatively low sensitivity for compounds which does not map well against electrospray ionization and also quantitation issues such as those produced by signal suppression due to either matrix effects from coeluting matrix or from

  18. Accurate Measurement of the in vivo Ammonium Concentration in Saccharomyces cerevisiae.

    Cueto-Rojas, Hugo F; Maleki Seifar, Reza; Ten Pierick, Angela; Heijnen, Sef J; Wahl, Aljoscha

    2016-01-01

    Ammonium (NH₄⁺) is the most common N-source for yeast fermentations, and N-limitation is frequently applied to reduce growth and increase product yields. While there is significant molecular knowledge on NH₄⁺ transport and assimilation, there have been few attempts to measure the in vivo concentration of this metabolite. In this article, we present a sensitive and accurate analytical method to quantify the in vivo intracellular ammonium concentration in Saccharomyces cerevisiae based on standard rapid sampling and metabolomics techniques. The method validation experiments required the development of a proper sample processing protocol to minimize ammonium production/consumption during biomass extraction by assessing the impact of amino acid degradation-an element that is often overlooked. The resulting cold chloroform metabolite extraction method, together with quantification using ultra high performance liquid chromatography-isotope dilution mass spectrometry (UHPLC-IDMS), was not only more sensitive than most of the existing methods but also more accurate than methods that use electrodes, enzymatic reactions, or boiling water or boiling ethanol biomass extraction because it minimized ammonium consumption/production during sampling processing and interference from other metabolites in the quantification of intracellular ammonium. Finally, our validation experiments showed that other metabolites such as pyruvate or 2-oxoglutarate (αKG) need to be extracted with cold chloroform to avoid measurements being biased by the degradation of other metabolites (e.g., amino acids). PMID:27120628

  19. Accurate Measurement of the in vivo Ammonium Concentration in Saccharomyces cerevisiae

    Hugo F. Cueto-Rojas

    2016-04-01

    Full Text Available Ammonium (NH4+ is the most common N-source for yeast fermentations, and N-limitation is frequently applied to reduce growth and increase product yields. While there is significant molecular knowledge on NH4+ transport and assimilation, there have been few attempts to measure the in vivo concentration of this metabolite. In this article, we present a sensitive and accurate analytical method to quantify the in vivo intracellular ammonium concentration in Saccharomyces cerevisiae based on standard rapid sampling and metabolomics techniques. The method validation experiments required the development of a proper sample processing protocol to minimize ammonium production/consumption during biomass extraction by assessing the impact of amino acid degradation—an element that is often overlooked. The resulting cold chloroform metabolite extraction method, together with quantification using ultra high performance liquid chromatography-isotope dilution mass spectrometry (UHPLC-IDMS, was not only more sensitive than most of the existing methods but also more accurate than methods that use electrodes, enzymatic reactions, or boiling water or boiling ethanol biomass extraction because it minimized ammonium consumption/production during sampling processing and interference from other metabolites in the quantification of intracellular ammonium. Finally, our validation experiments showed that other metabolites such as pyruvate or 2-oxoglutarate (αKG need to be extracted with cold chloroform to avoid measurements being biased by the degradation of other metabolites (e.g., amino acids.

  20. Cluster abundance in chameleon $f(R)$ gravity I: toward an accurate halo mass function prediction

    Cataneo, Matteo; Lombriser, Lucas; Li, Baojiu

    2016-01-01

    We refine the mass and environment dependent spherical collapse model of chameleon $f(R)$ gravity by calibrating a phenomenological correction inspired by the parameterized post-Friedmann framework against high-resolution $N$-body simulations. We employ our method to predict the corresponding modified halo mass function, and provide fitting formulas to calculate the fractional enhancement of the $f(R)$ halo abundance with respect to that of General Relativity (GR) within a precision of $\\lesssim 5\\%$ from the results obtained in the simulations. Similar accuracy can be achieved for the full $f(R)$ mass function on the condition that the modeling of the reference GR abundance of halos is accurate at the percent level. We use our fits to forecast constraints on the additional scalar degree of freedom of the theory, finding that upper bounds competitive with current Solar System tests are within reach of cluster number count analyses from ongoing and upcoming surveys at much larger scales. Importantly, the flexi...

  1. Zero G Mass Measurement Device (ZGMMD) Project

    National Aeronautics and Space Administration — The Zero Gravity Mass Measurement Device (ZGMMD) provides the ability to measure the mass of samples in a microgravity environment, like that found on the...

  2. Accurate evolutions of unequal-mass neutron-star binaries: properties of the torus and short GRB engines

    We present new results from accurate and fully general-relativistic simulations of the coalescence of unmagnetized binary neutron stars with various mass ratios. The evolution of the stars is followed through the inspiral phase, the merger, and the prompt collapse to a black hole, up until the appearance of a thick accretion disc, which is studied as it enters and remains in a regime of quasi-steady accretion. Although a simple ideal-fluid equation of state with Γ = 2 is used, this work presents a systematic study within a fully general-relativistic framework of the properties of the resulting black-hole-torus system produced by the merger of unequal-mass binaries. More specifically, we show that (1) the mass of the torus increases considerably with the mass asymmetry, and equal-mass binaries do not produce significant tori if they have a total baryonic mass Mtot ∼> 3.7 Mo-dot; (2) tori with masses Mtor ∼ 0.2 Mo-dot are measured for binaries with Mtot ∼ 3.4 Mo-dot and mass ratios q ∼ 0.75-0.85; (3) the mass of the torus can be estimated by the simple expression Mtor-bar(q,Mtot = [c1 (1-q) + c2](Mmax-Mot), involving the maximum mass for the binaries and coefficients constrained from the simulations, and suggesting that the tori can have masses as large as Mtor-bar ∼ 0.35Modot for Mtot ∼ 2.8 Mo-dot and q ∼ 0.75-0.85; (4) using a novel technique to analyze the evolution of the tori, we find no evidence for the onset of non-axisymmetric instabilities and that very little, if any, of their mass is unbound; (5) finally, for all the binaries considered, we compute the complete gravitational waveforms and the recoils imparted to the black holes, discussing the prospects of the detection of these sources for a number of present and future detectors.

  3. High-Precision Mass Measurements of Exotic Nuclei with the Triple-Trap Mass Spectrometer Isoltrap

    Blaum, K; Zuber, K T; Stanja, J

    2002-01-01

    The masses of close to 200 short-lived nuclides have already been measured with the mass spectrometer ISOLTRAP with a relative precision between 1$\\times$10$^{-7}$ and 1$\\times$10^{-8}$. The installatin of a radio-frequency quadrupole trap increased the overall efficiency by two orders of magnitude which is at present about 1%. In a recent upgrade, we installed a carbon cluster laser ion source, which will allow us to use carbon clusters as mass references for absolute mass measurements. Due to these improvements and the high reliability of ISOLTRAP we are now able to perform accurate high-precision mass measurements all over the nuclear chart. We propose therefore mass measurements on light, medium and heavy nuclides on both sides of the valley of stability in the coming four years. ISOLTRAP is presently the only instrument capable of the high precision required for many of the proposed studies.

  4. In-depth glycoproteomic characterization of γ-conglutin by high-resolution accurate mass spectrometry.

    Silvia Schiarea

    Full Text Available The molecular characterization of bioactive food components is necessary for understanding the mechanisms of their beneficial or detrimental effects on human health. This study focused on γ-conglutin, a well-known lupin seed N-glycoprotein with health-promoting properties and controversial allergenic potential. Given the importance of N-glycosylation for the functional and structural characteristics of proteins, we studied the purified protein by a mass spectrometry-based glycoproteomic approach able to identify the structure, micro-heterogeneity and attachment site of the bound N-glycan(s, and to provide extensive coverage of the protein sequence. The peptide/N-glycopeptide mixtures generated by enzymatic digestion (with or without N-deglycosylation were analyzed by high-resolution accurate mass liquid chromatography-multi-stage mass spectrometry. The four main micro-heterogeneous variants of the single N-glycan bound to γ-conglutin were identified as Man2(Xyl (Fuc GlcNAc2, Man3(Xyl (Fuc GlcNAc2, GlcNAcMan3(Xyl (Fuc GlcNAc2 and GlcNAc 2Man3(Xyl (Fuc GlcNAc2. These carry both core β1,2-xylose and core α1-3-fucose (well known Cross-Reactive Carbohydrate Determinants, but corresponding fucose-free variants were also identified as minor components. The N-glycan was proven to reside on Asn131, one of the two potential N-glycosylation sites. The extensive coverage of the γ-conglutin amino acid sequence suggested three alternative N-termini of the small subunit, that were later confirmed by direct-infusion Orbitrap mass spectrometry analysis of the intact subunit.

  5. Enantiomeric separation in comprehensive two-dimensional gas chromatography with accurate mass analysis.

    Chin, Sung-Tong; Nolvachai, Yada; Marriott, Philip J

    2014-11-01

    Chiral comprehensive two-dimensional gas chromatography (eGC×GC) coupled to quadrupole-accurate mass time-of-flight mass spectrometry (QTOFMS) was evaluated for its capability to report the chiral composition of several monoterpenes, namely, α-pinene, β-pinene, and limonene in cardamom oil. Enantiomers in a standard mixture were fully resolved by direct enantiomeric-GC analysis with a 2,3-di-O-methyl-6-t-butylsilyl derivatized β-cyclodextrin phase; however, the (+)-(R)-limonene enantiomer in cardamom oil was overlapped with other background components including cymene and cineole. Verification of (+)-(R)-limonene components based on characteristic ions at m/z 136, 121, and 107 acquired by chiral single-dimension GC-QTOFMS in the alternate MS/MSMS mode of operation was unsuccessful due to similar parent/daughter ions generated by interfering or co-eluting cymene and cineole. Column phases SUPELCOWAX, SLB-IL111, HP-88, and SLB-IL59, were incorporated as the second dimension column ((2)D) in chiral GC×GC analysis; the SLB-IL59 offered the best resolution for the tested monoterpene enantiomers from the matrix background. Enantiomeric ratios for α-pinene, β-pinene, and limonene were determined to be 1.325, 2.703, and 1.040, respectively, in the cardamom oil sample based on relative peak area data. PMID:24420979

  6. CycloBranch: De Novo Sequencing of Nonribosomal Peptides from Accurate Product Ion Mass Spectra

    Novák, Jiří; Lemr, Karel; Schug, Kevin A.; Havlíček, Vladimír

    2015-07-01

    Nonribosomal peptides have a wide range of biological and medical applications. Their identification by tandem mass spectrometry remains a challenging task. A new open-source de novo peptide identification engine CycloBranch was developed and successfully applied in identification or detailed characterization of 11 linear, cyclic, branched, and branch-cyclic peptides. CycloBranch is based on annotated building block databases the size of which is defined by the user according to ribosomal or nonribosomal peptide origin. The current number of involved nonisobaric and isobaric building blocks is 287 and 521, respectively. Contrary to all other peptide sequencing tools utilizing either peptide libraries or peptide fragment libraries, CycloBranch represents a true de novo sequencing engine developed for accurate mass spectrometric data. It is a stand-alone and cross-platform application with a graphical and user-friendly interface; it supports mzML, mzXML, mgf, txt, and baf file formats and can be run in parallel on multiple threads. It can be downloaded for free from http://ms.biomed.cas.cz/cyclobranch/, where the User's manual and video tutorials can be found.

  7. Fatty acids composition of Caenorhabditis elegans using accurate mass GCMS-QTOF.

    Henry, Parise; Owopetu, Olufunmilayo; Adisa, Demilade; Nguyen, Thao; Anthony, Kevin; Ijoni-Animadu, David; Jamadar, Sakha; Abdel-Rahman, Fawzia; Saleh, Mahmoud A

    2016-08-01

    The free living nematode Caenorhabditis elegans is a proven model organism for lipid metabolism research. Total lipids of C. elegans were extracted using chloroform and methanol in 2:1 ratio (v/v). Fatty acids composition of the extracted total lipids was converted to their corresponding fatty acids methyl esters (FAMEs) and analyzed by gas chromatography/accurate mass quadrupole time of flight mass spectrometry using both electron ionization and chemical ionization techniques. Twenty-eight fatty acids consisting of 12 to 22 carbon atoms were identified, 65% of them were unsaturated. Fatty acids containing 12 to17 carbons were mostly saturated with stearic acid (18:0) as the major constituent. Several branched-chain fatty acids were identified. Methyl-14-methylhexadecanoate (iso- 17:0) was the major identified branched fatty acid. This is the first report to detect the intact molecular parent ions of the identified fatty acids in C. elegans using chemical ionization compared to electron ionization which produced fragmentations of the FAMEs. PMID:27166662

  8. Isotopic Measurement of Uranium by Mass Spectrometry

    The growing application of atomic energy creates a wider need for precise and accurate knowledge of the isotopic composition of uranium. This information is particularly of great importance in the accountability and transfer of enriched uranium for reactor and research applications involving millions of dollars worth of fissionable materials. Reliable isotopic measurements are also necessary to ensure compliance of fuel element compositions with the reactor design specifications and to permit calculation of process and fuel burn-up losses. Mass spectrometry methods, which far surpass the capabilities of other methods, Were developed for very precise isotopic determinations. These methods, ''Single Standard'' and ''Double Standard'', involve the comparison of measurements of an unknown sample to similar measurements on known standards. Use of the ''Double Standard'' method eliminates the effects of instrument bias, thus permitting isotopic determinations with precisions (95% limit of error) of the order of ± 0.02% of the values. Accuracies are limited only by the knowledge of the standard values used, which are referenced to the series of uranium isotopic standards available from the US National Bureau of Standards. The mass spectrometers are also useful for the absolute determination of isotopic composition of uranium, especially in forms other than UF6. Thermal ionization techniques using high-resolution (approximately 12-in. radius) spectrometers permit the absolute isotopic characterization of the minor isotopes (i.e. those less than 10 wt.%) with an accuracy and precision of about 0.5% of the values per analysis. These analyses are particularly useful in calibrating highly enriched and highly depleted uranium for subsequent use as blending materials in an isotopic standards programme. Both relative and absolute isotopic measurement methods are described as well as their application in the accountability and operational analytical programmes. These applications

  9. Integrated Post-Experiment Monoisotopic Mass Refinement: An Integrated Approach to Accurately Assign Monoisotopic Precursor Masses to Tandem Mass Spectrometric Data

    Jung, Hee-Jung; Purvine, Samuel O.; Kim, Hokeun; Petyuk, Vladislav A.; Hyung, Seok-Won; Monroe, Matthew E.; Mun, Dong-Gi; Kim, Kyong-Chul; Park, Jong-Moon; Kim, Su-Jin; Tolic, Nikola; Slysz, Gordon W.; Moore, Ronald J.; Zhao, Rui; Adkins, Joshua N.; Anderson, Gordon A.; Lee, Hookeun; Camp, David G.; Yu, Myeong-Hee; Smith, Richard D.; Lee, Sang-Won

    2010-10-15

    Accurate assignment of monoisotopic precursor masses to tandem mass spectrometric (MS/MS) data is a fundamental and critically important step for successful peptide identifications in mass spectrometry based proteomics. Here we describe an integrated approach that combines three previously reported methods of treating MS/MS data for precursor mass refinement. This combined method, “integrated Post-Experiment Monoisotopic Mass Refinement” (iPE MMR), integrates steps: 1) generation of refined MS/MS data by DeconMSn, 2) additional refinement of the resultant MS/MS data by a modified version of PE-MMR, and 3) elimination of systematic errors of precursor masses using DtaRefinery. iPE-MMR is the first method that utilizes all MS information from multiple MS scans of a precursor ion and multiple charge states of it in an MS scan to determine precursor mass. By combining the synergistic features of each of method, iPE MMR increases sensitivity in peptide identification and provides increased accuracy when applied to complex high-throughput proteomics data. iPE MMR also allows incorporating additional data processing step(s) or skipping step(s), if necessary, to enable new developments or applications of the tools, as each step of iPE MMR produces output data in a common and conventional format used in proteomics data processing.

  10. Disentangling correlated scatter in cluster mass measurements

    Noh, Yookyung

    2012-01-01

    The challenge of obtaining galaxy cluster masses is increasingly being addressed by multiwavelength measurements. As scatters in measured cluster masses are often sourced by properties of or around the clusters themselves, correlations between mass scatters are frequent and can be significant, with consequences for errors on mass estimates both directly and those obtained via stacking. Using a high resolution 250 Mpc/h side N-body simulation, combined with proxies for observational cluster mass measurements, we obtain mass scatter correlations and covariances for 243 individual clusters along ~96 lines of sight each, both separately and together. We use principal component analysis (PCA) to characterize scatter trends and variations between clusters. The dominant mass scatter combination identified by PCA is common to many clusters, and tends to dominate the mass scatters when viewing the cluster along its long axis. We also correlate cluster mass scatter, environmental and intrinsic properties, and use PCA t...

  11. Mass Measurement of Very Short Half-Lived Nuclei

    Duma, M; Iacob, V E; Thibault, C

    2002-01-01

    The MISTRAL (Mass measurements at ISolde with a Transmission RAdiofrequency spectrometer on-Line) experiment exploits a rapid measurement technique to make accurate mass determinations of very short-lived nuclei. The physics goals are to elucidate new nuclear structure effects and constrain nuclear mass models in regions of interest to nuclear astrophysics.\\\\ \\\\The spectrometer, installed in May 97, performed as promised in the proposal with mass resolution exceeding 100,000. In its first experiment in July 1998, neutron-rich Na isotopes having half-lives as short as 31 ms were measured. A second experiment in November 1998 enabled us to improve the measurement precision of the isotopes $^{26-30}$Na to about 20 keV. The measurement program continues as experiment IS 373.

  12. Bone Mass Measurement: What the Numbers Mean

    ... supported by your browser. Home Bone Basics Bone Mass Measurement: What the Numbers Mean Publication available in: ... been one or more osteoporotic fractures. Low Bone Mass Versus Osteoporosis The information provided by a BMD ...

  13. Zero G Mass Measurement Device (ZGMMD) Project

    National Aeronautics and Space Administration — The Zero G Mass Measurement Device (ZGMMD) will provide the ability to quantify the mass of objects up to 2,000 grams, including live animal specimens in a zero G...

  14. Measuring solar reflectance Part I: Defining a metric that accurately predicts solar heat gain

    Levinson, Ronnen; Akbari, Hashem; Berdahl, Paul

    2010-05-14

    Solar reflectance can vary with the spectral and angular distributions of incident sunlight, which in turn depend on surface orientation, solar position and atmospheric conditions. A widely used solar reflectance metric based on the ASTM Standard E891 beam-normal solar spectral irradiance underestimates the solar heat gain of a spectrally selective 'cool colored' surface because this irradiance contains a greater fraction of near-infrared light than typically found in ordinary (unconcentrated) global sunlight. At mainland U.S. latitudes, this metric RE891BN can underestimate the annual peak solar heat gain of a typical roof or pavement (slope {le} 5:12 [23{sup o}]) by as much as 89 W m{sup -2}, and underestimate its peak surface temperature by up to 5 K. Using R{sub E891BN} to characterize roofs in a building energy simulation can exaggerate the economic value N of annual cool-roof net energy savings by as much as 23%. We define clear-sky air mass one global horizontal ('AM1GH') solar reflectance R{sub g,0}, a simple and easily measured property that more accurately predicts solar heat gain. R{sub g,0} predicts the annual peak solar heat gain of a roof or pavement to within 2 W m{sup -2}, and overestimates N by no more than 3%. R{sub g,0} is well suited to rating the solar reflectances of roofs, pavements and walls. We show in Part II that R{sub g,0} can be easily and accurately measured with a pyranometer, a solar spectrophotometer or version 6 of the Solar Spectrum Reflectometer.

  15. Galaxy And Mass Assembly (GAMA): Accurate Panchromatic Photometry from Optical Priors using LAMBDAR

    Wright, A H; Bourne, N; Driver, S P; Dunne, L; Maddox, S J; Alpaslan, M; Andrews, S K; Bauer, A E; Bland-Hawthorn, J; Brough, S; Brown, M J I; Cluver, M; Davies, L J M; Holwerda, B W; Hopkins, A M; Jarrett, T H; Kafle, P R; Lange, R; Liske, J; Loveday, J; Moffett, A J; Norberg, P; Popescu, C C; Smith, M; Taylor, E N; Tuffs, R J; Wang, L; Wilkins, S M

    2016-01-01

    We present the Lambda Adaptive Multi-Band Deblending Algorithm in R (LAMBDAR), a novel code for calculating matched aperture photometry across images that are neither pixel- nor PSF-matched, using prior aperture definitions derived from high resolution optical imaging. The development of this program is motivated by the desire for consistent photometry and uncertainties across large ranges of photometric imaging, for use in calculating spectral energy distributions. We describe the program, specifically key features required for robust determination of panchromatic photometry: propagation of apertures to images with arbitrary resolution, local background estimation, aperture normalisation, uncertainty determination and propagation, and object deblending. Using simulated images, we demonstrate that the program is able to recover accurate photometric measurements in both high-resolution, low-confusion, and low-resolution, high-confusion, regimes. We apply the program to the 21-band photometric dataset from the ...

  16. Body mass index and blood pressure measurement during pregnancy.

    Hogan, Jennifer L

    2012-02-01

    OBJECTIVE: The accurate measurement of blood pressure requires the use of a large cuff in subjects with a high mid-arm circumference (MAC). This prospective study examined the need for a large cuff during pregnancy and its correlation with maternal obesity. METHODS: Maternal body mass index (BMI), fat mass, and MAC were measured. RESULTS: Of 179 women studied, 15.6% were obese. With a BMI of level 1 obesity, 44% needed a large cuff and with a BMI of level 2 obesity 100% needed a large cuff. CONCLUSION: All women booking for antenatal care should have their MAC measured to avoid the overdiagnosis of pregnancy hypertension.

  17. Selected top quark mass measurements at CMS

    Bouvier, Elvire

    2016-01-01

    Selected measurements of the top quark mass are presented, obtained from CMS data collected in proton-proton collisions at the LHC at center-of-mass energies of 7, 8, and 13 TeV. ``Standard'' techniques are employed in each decay channel of top quark pair events and their results are combined. The mass of the top quark is also measured using several ``alternative'' methods, including measurements from shapes of top quark decay distributions in single top quark and top quark pair events as well as pole mass measurements.

  18. Accurate Quantification of Lipid Species by Electrospray Ionization Mass Spectrometry — Meets a Key Challenge in Lipidomics

    Kui Yang

    2011-11-01

    Full Text Available Electrospray ionization mass spectrometry (ESI-MS has become one of the most popular and powerful technologies to identify and quantify individual lipid species in lipidomics. Meanwhile, quantitative analysis of lipid species by ESI-MS has also become a major obstacle to meet the challenges of lipidomics. Herein, we discuss the principles, advantages, and possible limitations of different mass spectrometry-based methodologies for lipid quantification, as well as a few practical issues important for accurate quantification of individual lipid species. Accordingly, accurate quantification of individual lipid species, one of the key challenges in lipidomics, can be practically met.

  19. Dynamical Mass Measurements of Contaminated Galaxy Clusters Using Machine Learning

    Ntampaka, Michelle; Trac, Hy; Sutherland, Dougal; Fromenteau, Sebastien; Poczos, Barnabas; Schneider, Jeff

    2016-01-01

    Galaxy clusters are a rich source of information for examining fundamental astrophysical processes and cosmological parameters, however, employing clusters as cosmological probes requires accurate mass measurements derived from cluster observables. We study dynamical mass measurements of galaxy clusters contaminated by interlopers, and show that a modern machine learning (ML) algorithm can predict masses by better than a factor of two compared to a standard scaling relation approach. We create a mock catalog from Multidark's publicly-available N-body MDPL1 simulation where a simple cylindrical cut around the cluster center allows interlopers to contaminate the clusters. In the standard approach, we use a power law scaling relation to infer cluster mass from galaxy line of sight (LOS) velocity dispersion. The presence of interlopers in the catalog produces a wide, flat fractional mass error distribution, with width = 2.13. We employ the Support Distribution Machine (SDM) class of algorithms to learn from distributions of data to predict single values. Applied to distributions of galaxy observables such as LOS velocity and projected distance from the cluster center, SDM yields better than a factor-of-two improvement (width = 0.67). Remarkably, SDM applied to contaminated clusters is better able to recover masses than even a scaling relation approach applied to uncontaminated clusters. We show that the SDM method more accurately reproduces the cluster mass function, making it a valuable tool for employing cluster observations to evaluate cosmological models.

  20. Measuring Accurate Body Parameters of Dressed Humans with Large-Scale Motion Using a Kinect Sensor

    Sidan Du

    2013-08-01

    Full Text Available Non-contact human body measurement plays an important role in surveillance, physical healthcare, on-line business and virtual fitting. Current methods for measuring the human body without physical contact usually cannot handle humans wearing clothes, which limits their applicability in public environments. In this paper, we propose an effective solution that can measure accurate parameters of the human body with large-scale motion from a Kinect sensor, assuming that the people are wearing clothes. Because motion can drive clothes attached to the human body loosely or tightly, we adopt a space-time analysis to mine the information across the posture variations. Using this information, we recover the human body, regardless of the effect of clothes, and measure the human body parameters accurately. Experimental results show that our system can perform more accurate parameter estimation on the human body than state-of-the-art methods.

  1. Volume and mass measurements of liquids

    The report comprises the 10 lectures given at the 74th PTB seminar, which represent the state of the art in the field of liquid flow measurement. The lectures deal with the overflow-pipette as the primary volume standard of PTB, gas elimination devices (compulsory in measuring assemblies with volume meters), measuring assemblies for the reception of milk, electromagnetic flowmeters, vortex-shedding meters, indirect mass measurement from volume and density, direct mass measurement (coriolis flowmeters), pipeline-measurements, level measurement at storage tanks with conventional and optical methods and a development aid project for the set up of test rigs in India. (orig.)

  2. Precise atomic mass measurements by deflection mass spectrometry

    Barber, R C

    2003-01-01

    Since its inception nearly 90 years ago by J.J. Thomson, the precise determination of atomic masses by the classical technique of deflecting charged particles in electric and magnetic fields has provided a large body of data on naturally occurring nuclides. Currently, such measurements on stable nuclides have frequently achieved a precision of better than two parts in 10 sup 9 of the mass. A review of the technique, together with a brief summary of the important historical developments in the field of precise atomic mass measurements, will be given. The more recent contributions to this field by the deflection mass spectrometer at the University of Manitoba will be provided as illustrations of the culmination of the techniques used and the applications that have been studied. A brief comparison between this and newer techniques using Penning traps will be presented.

  3. Precise atomic mass measurements by deflection mass spectrometry

    Barber, R. C.; Sharma, K. S.

    2003-05-01

    Since its inception nearly 90 years ago by J.J. Thomson, the precise determination of atomic masses by the classical technique of deflecting charged particles in electric and magnetic fields has provided a large body of data on naturally occurring nuclides. Currently, such measurements on stable nuclides have frequently achieved a precision of better than two parts in 10 9 of the mass. A review of the technique, together with a brief summary of the important historical developments in the field of precise atomic mass measurements, will be given. The more recent contributions to this field by the deflection mass spectrometer at the University of Manitoba will be provided as illustrations of the culmination of the techniques used and the applications that have been studied. A brief comparison between this and newer techniques using Penning traps will be presented.

  4. Mass properties measurement system: Dynamics and statics measurements

    Doty, Keith L.

    1993-01-01

    This report presents and interprets experimental data obtained from the Mass Properties Measurement System (MPMS). Statics measurements yield the center-of-gravity of an unknown mass and dynamics measurements yield its inertia matrix. Observations of the MPMS performance has lead us to specific design criteria and an understanding of MPMS limitations.

  5. Top quark mass measurements in ATLAS

    The top quark is a fundamental constituent of the Standard Model (SM). The properties of this quark are accurately predicted by this theory, except for its mass, which remains a fundamental parameter of the SM. With the advent of the Large Hadron Collider (LHC), many million of top-antitop quark pairs are available for study. With such statistics, the physics of the top quark has entered the precision era. In this note, the most recent experimental results by ATLAS concerning the top quark mass are reported

  6. Mass measurement of W with UA2

    This thesis describes the measurement of the W mass with the UA2 detector at the CERN antipp collider. In the first section, the importance of the measurement of the W mass in the framework of the Standard Model at the level of radiative corrections is discussed. In the second part, we describe the experimental apparatus used, which is designed for good electron identification and energy measurement and for good missing transverse momentum measurement. We describe the selection of W and Z events, decaying to electron-neutrino and electron-positron, used for the measurements of the masses of these two intermediate bosons. The method used to extract the W mass is described in detail, with emphasis on the informations given by the study of Z events. The values obtained for the W and Z masses are given after discussion of systematic uncertainties. The main uncertainty, which arises from the energy scale uncertainty, vanishes in the masses ratio. This value, combined with the Z mass from LEP, allows us to obtain a precise determination of the W mass: Mw = 80.49 ± 0.37 GeV/c2. The implications of this measurement on the Standard Model parameters are discussed in the last section

  7. Top quark mass measurement in dilepton channel

    In this work, we measured the top quark mass in tt'-' events produced in pp'-' interactions at the center-of-mass energy 1.96 TeV using CDF detector. We used dilepton in tt'-' events where both W bosons from top quarks are decaying into leptons. The data sample corresponds to 340 pb-1. We found there 33 tt'-' candidates while expecting 10.5 ± 1.9 background events. In the measurement, we reconstruct one, representative mass for each event using the assumption about longitudinal momentum of in tt'-' system, in order to be able to kinematically solve the under-constrained system. The mass distributions (templates) are created for simulated signal and background events. Templates are parametrized in order to obtain smooth probability density functions. Likelihood maximization which includes these parametrized templates is then performed on reconstructed masses obtained from data sample in order to obtain final top quark mass estimate. The result of applying this procedure on data events is top quark mass estimate 169.5+7.7-7.2(stat.) ± 4.0(syst.) GeV/c2 for 30 out of 33 candidates, where the solution for top quark mass was found. This measurement was a part of first top quark mass measurement in dilepton channel at CDF in Run II. The top quark mass measured here is consistent with the CDF measurement in dilepton channel from Run I Mtop = 167.4 ± 10.3(stat.) ± 4.8(syst.) GeV/c2. Moreover, the combined result of four top quark mass measurements in dilepton channel from Run II (one of these four measurements is our measurement) Mtop = 167.9 ± 5.2(stat.) ± 3.7(syst.) GeV/c2 significantly (by ∼ 40%) improved the precision of top quark mass determination from Run I. It should be also noted, that this combined result is consistent with measurement obtained in 'lepton+jets' channel at CDF in Run II (Mtop = 173.5+3.9-3.8 GeV/c2). So, we don't have yet any indication about new physics beyond the Standard Model. My main contribution in this analysis was the optimization

  8. Precision Mass Measurement of Argon Isotopes

    Lunney, D

    2002-01-01

    % IS388\\\\ \\\\ A precision mass measurement of the neutron-deficient isotopes $^{32,33,34}$Ar is proposed. Mass values of these isotopes are of importance for: a) a stringent test of the Isobaric-Multiplet- Mass-Equation, b) a verification of the correctness of calculated charge-dependent corrections as used in super-allowed $\\beta$- decay studies aiming at a test of the CVC hypothesis, and c) the determination of the kinematics in electron-neutrino correlation experiments searching for scalar currents in weak interaction. The measurements will be carried out with the ISOLTRAP Penning trap mass spectrometer.

  9. No galaxy left behind: accurate measurements with the faintest objects in the Dark Energy Survey

    Suchyta, E; Aleksić, J; Melchior, P; Jouvel, S; MacCrann, N; Crocce, M; Gaztanaga, E; Honscheid, K; Leistedt, B; Peiris, H V; Ross, A J; Rykoff, E S; Sheldon, E; Abbott, T; Abdalla, F B; Allam, S; Banerji, M; Benoit-Lévy, A; Bertin, E; Brooks, D; Burke, D L; Rosell, A Carnero; Kind, M Carrasco; Carretero, J; Cunha, C E; D'Andrea, C B; da Costa, L N; DePoy, D L; Desai, S; Diehl, H T; Dietrich, J P; Doel, P; Eifler, T F; Estrada, J; Evrard, A E; Flaugher, B; Fosalba, P; Frieman, J; Gerdes, D W; Gruen, D; Gruendl, R A; James, D J; Jarvis, M; Kuehn, K; Kuropatkin, N; Lahav, O; Lima, M; Maia, M A G; March, M; Marshall, J L; Miller, C J; Miquel, R; Neilsen, E; Nichol, R C; Nord, B; Ogando, R; Percival, W J; Reil, K; Roodman, A; Sako, M; Sanchez, E; Scarpine, V; Sevilla-Noarbe, I; Smith, R C; Soares-Santos, M; Sobreira, F; Swanson, M E C; Tarle, G; Thaler, J; Thomas, D; Vikram, V; Walker, A R; Wechsler, R H; Zhang, Y

    2015-01-01

    Accurate statistical measurement with large imaging surveys has traditionally required throwing away a sizable fraction of the data. This is because most measurements have have relied on selecting nearly complete samples, where variations in the composition of the galaxy population with seeing, depth, or other survey characteristics are small. We introduce a new measurement method that aims to minimize this wastage, allowing precision measurement for any class of stars or galaxies detectable in an imaging survey. We have implemented our proposal in Balrog, a software package which embeds fake objects in real imaging in order to accurately characterize measurement biases. We demonstrate this technique with an angular clustering measurement using Dark Energy Survey (DES) data. We first show that recovery of our injected galaxies depends on a wide variety of survey characteristics in the same way as the real data. We then construct a flux-limited sample of the faintest galaxies in DES, chosen specifically for th...

  10. Top quark mass measurement at the Tevatron

    Guimaraes da Costa, Joao; /Harvard U.

    2004-12-01

    The authors report on the latest experimental measurements of the top quark mass by the CDF and D0 Collaborations at the Fermilab Tevatron. They present a new top mass measurement using the t{bar t} events collected by the D0 Collaboration in Run I between 1994 and 1996. This result is combined with previous measurements to yield a new world top mass average. They also describe several preliminary results using up to 193 pb{sup -1} of t{bar t} events produced in {bar p}p collisions at {radical}s = 1.96 TeV during the Run II of the Tevatron.

  11. Measuring Accurate Body Parameters of Dressed Humans with Large-Scale Motion Using a Kinect Sensor

    Sidan Du; Yang Li; Yao Yu; Yu Zhou; Huanghao Xu

    2013-01-01

    Non-contact human body measurement plays an important role in surveillance, physical healthcare, on-line business and virtual fitting. Current methods for measuring the human body without physical contact usually cannot handle humans wearing clothes, which limits their applicability in public environments. In this paper, we propose an effective solution that can measure accurate parameters of the human body with large-scale motion from a Kinect sensor, assuming that the people are wearing clo...

  12. Top quark mass measurements at CDF

    Maki, Tuula; /Helsinki U. /Helsinki Inst. of Phys.

    2007-10-01

    The top quark mass is interesting both as a fundamental parameter of the standard model as well as an important input to precision electroweak tests. The CDF Collaboration has measured the top quark mass with high precision in all decay channels with complementary methods. A combination of the results from CDF gives a top quark mass of 170.5{+-}1.3(stat.){+-}1.8(syst.) GeV/c{sup 2}.

  13. Reanalysing glacier mass balance measurement series

    Zemp, M.; E. Thibert; Huss, M.; Stumm, D.; Rolstad Denby, C.; Nuth, C.; S. U. Nussbaumer; G. Moholdt; A. Mercer; Mayer, C.; Joerg, P. C.; P. Jansson; B. Hynek; Fischer, A.; Escher-Vetter, H.

    2013-01-01

    Glacier-wide mass balance has been measured for more than sixty years and is widely used as an indicator of climate change and to assess the glacier contribution to runoff and sea level rise. Until recently, comprehensive uncertainty assessments have rarely been carried out and mass balance data have often been applied using rough error estimation or without consideration of errors. In this study, we propose a framework for reanalysing glacier mass balance series that includes conceptual and ...

  14. Top Quark Mass Measurements at the LHC

    AUTHOR|(INSPIRE)INSPIRE-00220136; The ATLAS collaboration

    2016-01-01

    The top quark mass ($m_{top}$) is a fundamental parameter of the Standard Model of Particle Physics (SM). As the heaviest of all SM particles with a mass close to the electroweak symmetry-breaking scale, the top quark plays a pivotal role in the theory of elementary particles. The exact value of the top quark mass has implications on a number of theoretical predictions, which motivates the need for precision measurements of $m_{top}$. This document highlights a number of such measurements carried out by the ATLAS and CMS collaborations based on the combined LHC Run 1 datasets at centre-of-mass energies of $\\sqrt{s}=7$ and $8$ TeV. A wide range of analysis strategies are employed for a number of final-state signatures. Measurements of both the top quark pole mass as well as the value of $m_{top}$ as defined by the Monte Carlo generator in simulated signal samples are discussed.

  15. Measurement of mass and isotopic fission yields for heavy fission products with the LOHENGRIN mass spectrometer

    In spite of the huge amount of fission yield data available in different libraries, more accurate values are still needed for nuclear energy applications and to improve our understanding of the fission process. Thus measurements of fission yields were performed at the mass spectrometer Lohengrin at the Institut Laue-Langevin in Grenoble, France. The mass separator Lohengrin is situated at the research reactor of the institute and permits the placement of an actinide layer in a high thermal neutron flux. It separates fragments according to their atomic mass, kinetic energy and ionic charge state by the action of magnetic and electric fields. Coupled to a high resolution ionization chamber the experiment was used to investigate the mass and isotopic yields of the light mass region. Almost all fission yields of isotopes from Th to Cf have been measured at Lohengrin with this method. To complete and improve the nuclear data libraries, these measurements have been extended in this work to the heavy mass region for the reactions 235U(nth,f), 239Pu(nth,f) and 241Pu(nth,f). For these higher masses an isotopic separation is no longer possible. So, a new method was undertaken with the reaction 239Pu(nth,f) to determine the isotopic yields by spectrometry. These experiments have allowed to reduce considerably the uncertainties. Moreover the ionic charge state and kinetic energy distributions were specifically studied and have shown, among others, nanosecond isomers for some masses. (author)

  16. Physical consequences of the alpha/beta rule which accurately calculates particle masses

    Using the fine structure constant α (=1/137.036), the proton vs. electron mass ratio β (= 1836.2) and the integers m and n, the α/β rule: mparticle = α-n x β m x 27.2 eV/c2 allows almost exact calculation of particle masses. (K.O.Greulich, DPG Spring meeting 2014, Mainz, T99.4) With n=2, m=0 the electron mass becomes 510.79 keV/c2 (experimental 511 keV/c2) With n=2, m=1 the proton mass is 937.9 MeV/c2 (literature 938.3 MeV/c2). For n=3 and m=1 a particle with 128.6 GeV/c2 close to the reported Higgs mass, is expected. For n=14 and m=-1 the Planck mass results. The calculated masses for gauge bosons and for quarks have similar accuracy. All masses fit into the same scheme (the alpha/beta rule), indicating that non of these particle masses play an extraordinary role. Particularly, the Higgs Boson, often termed the *God particle* plays in this sense no extraordinary role. In addition, particle masses are intimately correlated with the fine structure constant α. If particle masses have been constant over all times, α must have been constant over these times. In addition, the ionization energy of the hydrogen atom (13.6 eV) needs to have been constant if particle masses have been unchanged or vice versa. In conclusion, the α/β rule needs to be taken into account when cosmological models are developed.

  17. Mass measurements with the GANIL cyclotrons

    An original method of mass measurements using the GANIL facility cyclotrons as an Accelerator-Mass spectrometer system is presented. The first test runs show that a precision of 3.10-6 can be achieved. Further improvement of this value can be obtained. Although some limitations apply to this technique, a broad spectrum of nuclei can be studied by this method

  18. A theoretical study on accurate measurements of thoron with airflow-through scintillation cell method

    For accurate measurements of 220Rn concentration with airflow-through scintillation cell method, a theoretical study was performed for discussing the influences of sampling flow rate, volumes of sampling tube and scintillation cell on the measurements. It is found that a high flow rate and a large inner volume of scintillation cell as well as a small inner volume of sampling tube are not only preferable for measuring low levels of 220Rn, but also helpful for enhancing the measurement accuracy. In calibration experiments, both the sampling flow rate and the sampling tube volume should be noted. The variations of the flow rate and tube volume should be considered for accurate measurements in the fields. (authors)

  19. Applicability of hydraulic dynamometer for measuring load mass on forwarders

    Pandur Zdravko

    2015-01-01

    Full Text Available In the last few years, with the start of wood biomass production from wood residues, the need for determining the quantity of extracted wood residuals on a landing site has appeared. The beginning of intensive usage of wood residues for wood biomass starts in lowland forest where all wood residues are extracted with forwarders. There are several ways to determine load mass on a forwarder, first and probably most accurate is the use of load cells which are installed between forwarder undercarriage and loading space. In Croatia, as far as it is known, there is no forwarder with such equipment, although manufacturers offer the installation of such equipment when buying a new forwarder. The second option is using a portable measuring platform (axle scale which was already used for research of axle loads of trucks and forwarders. The data obtained with the measuring platform are very accurate, while its deficiency is relatively great mass, large dimensions and high price. The third option is determining mass by using hydraulic dynamometer which is installed on crane between the rotator and the telescopic boom. The production and installation of such a system is very simple, and with the price it can easily compete with previously described measuring systems. The main deficiency of this system is its unsatisfying accuracy. The results of assortment mass measuring with hydraulic dynamometer installed on a hydraulic crane and discussion on factors influencing obtained results will be presented in this paper.

  20. Miniature Sensor for Aerosol Mass Measurements Project

    National Aeronautics and Space Administration — This SBIR project seeks to develop a miniature sensor for mass measurement of size-classified aerosols. A cascade impactor will be used to classify aerosol sample...

  1. Cosmological and astrophysical neutrino mass measurements

    Abazajian, K.N.; Calabrese, E.; Cooray, A.;

    2011-01-01

    Cosmological and astrophysical measurements provide powerful constraints on neutrino masses complementary to those from accelerators and reactors. Here we provide a guide to these different probes, for each explaining its physical basis, underlying assumptions, current and future reach....

  2. Cosmological and Astrophysical Neutrino Mass Measurements

    Abazajian, K N; Cooray, A; De Bernardis, F; Dodelson, S; Friedland, A; Fuller, G M; Hannestad, S; Keating, B G; Linder, E V; Lunardini, C; Melchiorri, A; Miquel, R; Pierpaoli, E; Pritchard, J; Serra, P; Takada, M; Wong, Y Y Y

    2011-01-01

    Cosmological and astrophysical measurements provide powerful constraints on neutrino masses complementary to those from accelerators and reactors. Here we provide a guide to these different probes, for each explaining its physical basis, underlying assumptions, current and future reach.

  3. Simplified fundamental force and mass measurements

    Robinson, I. A.

    2016-08-01

    The watt balance relates force or mass to the Planck constant h, the metre and the second. It enables the forthcoming redefinition of the unit of mass within the SI by measuring the Planck constant in terms of mass, length and time with an uncertainty of better than 2 parts in 108. To achieve this, existing watt balances require complex and time-consuming alignment adjustments limiting their use to a few national metrology laboratories. This paper describes a simplified construction and operating principle for a watt balance which eliminates the need for the majority of these adjustments and is readily scalable using either electromagnetic or electrostatic actuators. It is hoped that this will encourage the more widespread use of the technique for a wide range of measurements of force or mass. For example: thrust measurements for space applications which would require only measurements of electrical quantities and velocity/displacement.

  4. Mass Flow Meter Analysis for Reliable Measuring

    Kupanovac, Tihomir; Špoljarić, Željko; Valter, Zdravko

    2012-01-01

    The aim of this paper is to show how to analyze and correctly chose measuring device specially applied on mass flow meter based on Coriolis principle. In the beginning short description of Coriolis based mass flow meter is given. Furthermore, comparison analysis of two flow meters shows where are the problems of wrongly applied method in slurry fluid measurement in production of powder detergents plant. Analysis is made using RS Logix 500 program. In given diagrams which show causes of wrong ...

  5. An improved technique for accurate heat capacity measurements on powdered samples using a commercial relaxation calorimeter

    Highlights: → We have previously published a method for accurate PPMS eat capacity measurements. → The older method had a significant grease problem above 250 K. → Here we publish new results using copper strips instead of grease to pot the sample. → The new method now requires on two measurements instead of four. - Abstract: We have modified our earlier technique for accurate PPMS heat capacity measurements on powdered samples by means of applying Wakefield grease or small copper strips in the sample preparation instead of using Apiezon N high-vacuum grease. For the Wakefield grease measurements, we put a small amount of Wakefield thermal compound in a copper cup instead of potting with Apiezon N, and the accuracy of measurements on powdered benzoic acid was determined to be ±1% and ±4% in the temperature ranges of 10 K -1 . mol-1, which deviates 0.08% and -0.08% from the measurement results of our low-temperature adiabatic and semi-adiabatic calorimeters, respectively. We recommend that this technique become the standard for accurate heat capacity measurements on insulating powdered samples using a PPMS system and the corresponding thermodynamic calculations.

  6. Rapid and accurate U-Th dating of ancient carbonates using inductively coupled plasma-quadrupole mass spectrometry

    Here, the potential for rapid and accurate U-Th dating technique of marine aragonite skeletons (deep-sea corals, Lophelia pertusa) and secondary calcite deposits (speleothems and stalagmites) has been explored using inductively coupled plasma-quadrupole mass spectrometry (ICP-QMS). The analytical procedure includes a largely simplified chemical separation technique for uranium (U) and thorium (Th) using UTEVA resin. The developed technique permits simultaneous quantification of uranium [238U] and thorium [232Th] concentrations and their respective isotopic composition, required for U-series disequilibrium dating. Up to 50 U-Th dates per day can be achieved through ICP-QMS with δ234U and δ230Th reproducibility (2 σ) of 3-4 parts per thousand and 1%, respectively. The high sensitivity (≥3.0 x 105 cps/ppb) together with low background (≤0.5 cps) on each mass between 228 and 236 amu allowed U-Th dating of ancient deep-water corals (15-260 kyr) and stalagmites (30-85 kyr) at precision levels of less than 2%. Consequently, the combination of simplified chemistry using UTEVA with state-of-the-art ICP-QMS isotopic measurements that do not require a U-Th separation step now provides an extremely rapid and low-cost U-series dating technology. The level of precision is most convenient for numerous geochronological applications, such as the determination of climatic influences on ecosystem development and carbonate precipitation. As a first-example application we present ICP-QMS U-Th dates of North Atlantic deep-water coral fragments retrieved in the southeastern Porcupine Seabight (MD01-2463G. Mound Therese), indicating a purely interglacial growth of deep-water corals on so-called carbonate mounds over several climate cycles. (authors)

  7. Rapid and Accurate U-Th Dating of Ancient Carbonates using Inductively Coupled Plasma-Quadrupole Mass Spectrometry

    Douville, Eric; Sallé, Eline; Frank, Norbert; Eisele, Markus; Pons-Branchu, Edwige; Ayrault, Sophie

    2010-05-01

    Here, the potential for rapid and accurate U-Th dating technique of marine aragonite skeletons (deep-sea corals, Lophelia pertusa) and secondary calcite deposits (speleothems and stalagmites) has been explored using inductively-coupled plasma-quadrupole mass spectrometry (ICP-QMS). The analytical procedure includes a largely simplified chemical separation technique for uranium (U) and thorium (Th) using UTEVA resin. The developed technique permits simultaneous quantification of uranium [238U] and thorium [232Th] concentrations and their respective isotopic composition, required for U-series disequilibrium dating. Up to 50 U-Th dates per day can be achieved through ICP-QMS with 234U and 230Th reproducibility (2sigma) of 3-4 permil and 1 percent, respectively. The high sensitivity (> 300 000 cps/ppb) together with low background (<0.5 cps) on each mass between 228-236 amu allowed U-Th dating of ancient deep water corals (15-260 kyrs) and stalagmites (30-85 kyrs) at precision levels of less than 2%. Consequently, the combination of simplified chemistry using UTEVA with state-of-the-art ICP-QMS isotopic measurements that do not require a U-Th separation step now provides an extremely rapid and low-cost U-series dating technology. The level of precision is most convenient for numerous geochronological applications, such as the determination of climatic influences on ecosystem development and carbonate precipitation. As a first-example application we present ICP-QMS U-Th dates of North Atlantic deep-water coral fragments retrieved in the southeastern Porcupine Seabight (MD01-2463G, Mound Thérèse), indicating a purely interglacial growth of deep-water corals on so-called carbonate mounds over several climate cycles.

  8. Impact of Precision Mass Measurements on Nuclear Physics and Astrophysics

    Kreim, Susanne; Dilling, Jens; Litvinov, Yuri A

    2013-01-01

    Among all nuclear ground-state properties, atomic masses are highly specific for each particular combination of neutron and proton number, N and Z, respectively. The data obtained through mass measurements provide details of the nuclear interaction and thus apply to a variety of physics topics. Some of the most crucial questions to be addressed by mass spectrometry of unstable radionuclides are, on the one hand, nuclear forces and structure, describing phenomena such as the so-called neutron-halos or the evolution of magic numbers when moving towards the borders of nuclear existence. On the other hand, the understanding of the processes of element formation in the Universe poses a challenge and requires an accurate knowledge of nuclear astrophysics. Here, precision atomic mass values of a large number of exotic nuclei participating in nucleosynthesis processes are among the key input data in large-scale reaction network calculations.

  9. Accurate measurement of neodymium isotopic composition using Neptune MC-ICP-MS

    Yueheng YANG; Hongfu ZHANG; Liewen XIE; Fuyuan WU

    2008-01-01

    This paper reports the measurement of the Neodymium isotopic composition by Neptune Multiple Collector Inductively Coupled Plasma Mass Spectrometry (MC-ICP-MS) over the last two years. Although there is concomitant Cerium in the chemical separation process, this has no significant influence on the Neodymium analysis. As for the sample containing small amounts of Samarium (Sm/Nd<0.04), direct calibration for isobaric interference and mass discrimina-tion by the exponential law can be obtained by assuming that Samarium mass discrimination is the same as that of Neodymium. Geological samples after traditional chemi-cal separation were measured by Neptune MC-ICP-MS and Thermal Ionization Mass Spectrometry (TIMS) respectively. The results show that Neptune MC-ICP-MS can measure Neodymium isotopic composition as precisely the TIMS does and is even more effective and less time-consuming than the TIMS Method.

  10. A fast and accurate method to compute the mass return from multiple stellar populations

    Calura, F; Nipoti, C

    2013-01-01

    The mass returned to the ambient medium by aging stellar populations over cosmological times sums up to a significant fraction (20% - 30% or more) of their initial mass. This continuous mass injection plays a fundamental role in phenomena such as galaxy formation and evolution, fueling of supermassive black holes in galaxies and the consequent (negative and positive) feedback phenomena, and the origin of multiple stellar populations in globular clusters. In numerical simulations the calculation of the mass return can be time consuming, since it requires at each time step the evaluation of a convolution integral over the whole star formation history, so the computational time increases quadratically with the number of time-steps. The situation can be especially critical in hydrodynamical simulations, where different grid points are characterized by different star formation histories, and the gas cooling and heating times are shorter by orders of magnitude than the characteristic stellar lifetimes. In this pape...

  11. Evaluation of Modified Pycnometric Method for Accurately Measuring the Density of Molten Nickel

    XIAO Feng; FANG Liang; FU Yuechao; YANG Lingchuan

    2004-01-01

    A modified pycnometric method has been developed to obtain accurate densities of molten nickel.The new method allows continuous measurement of density over a wide temperature range from a single experiment.The measurement error of the method was analyzed, and the total uncertainty of the measurement was estimated to be within ±0.34%. The measured density of molten nickel decreases linearly with increasing temperature over a range from the melting point to 1873K. The density at the melting point and the thermal expansion coefficient of molten nickel are 7.90Mg·m-3 and 1.92×10-4 K-1,respectively.

  12. Development of a high accurate gear measuring machine based on laser interferometry

    Lin, Hu; Xue, Zi; Yang, Guoliang; Huang, Yao; Wang, Heyan

    2015-02-01

    Gear measuring machine is a specialized device for gear profile, helix or pitch measurement. The classic method for gear measurement and the conventional gear measuring machine are introduced. In this gear measuring machine, the Abbe errors arisen from the angle error of guideways hold a great weight in affection of profile measurement error. For minimize of the Abbe error, a laser measuring system is applied to develop a high accurate gear measuring machine. In this laser measuring system, two cube-corner reflectors are placed close to the tip of probe, a laser beam from laser head is splited along two paths, one is arranged tangent to the base circle of gear for the measurement of profile and pitch, another is arranged parallel to the gear axis for the measurement of helix, both laser measurement performed with a resolution of 0.3nm. This approach not only improves the accuracy of length measurement but minimize the Abbe offset directly. The configuration of this improved measuring machine is illustrated in detail. The measurements are performed automatically, and all the measurement signals from guide rails, rotary table, probe and laser measuring system are obtained synchronously. Software collects all the data for further calculation and evaluation. The first measurements for a gear involute artifact and a helix artifact are carried out, the results are shown and analyzed as well.

  13. An Accurate Measurement of Planck's Constant using a Watt Balance Experiment

    Williams, Edwin R.

    1998-04-01

    The experiment described here is performed with colleagues Richard Steiner and David Newell ( R. L. Steiner, A. D. Gillespie, K. Fujii, E. R. Williams, D. B. Newell, A. Picard, G. N. Stenbakken, and P. T. Olsen, "The NIST Watt Balance: Progress Toward Monitoring the Kilogram" IEEE Trans. Instrum. Meas. vol. IM46, pp. 601-604, 1997.). By measuring the Watt in both electrical and SI mechanical units, one can measure Planck's constant, h. Electric power measured in terms of the Josephson effect voltage and quantum Hall effect resistance can be compared to mechanical power measured in terms of the kilogram, meter and second in a two part experiment using a coil in a magnetic field (B. P. Kibble, "A measurement of the gyromagnetic ratio of the proton by the strong field method" Atomic Masses and Fundamental Constants. J. H. Sanders and A. H. Wapstra, Eds. New York : Plenum, 1976.). The primary quantities measured are a =B110 mA current that balances a one kilogram mass in local gravity, and a one volt signal generated by the same coil moving at a velocity of 2 mm/s. The velocity measurement is the most challenging. We are presently measuring h with a standard uncertainty near 1 part in 10 million. This also measures the mass of an electron with similar uncertainty. From this work we plan to monitor the stability of the Kilogram artifact with the goal of someday having a quantum based unit of mass.

  14. A simple and accurate model for Love wave based sensors: Dispersion equation and mass sensitivity

    Jiansheng Liu

    2014-01-01

    Dispersion equation is an important tool for analyzing propagation properties of acoustic waves in layered structures. For Love wave (LW) sensors, the dispersion equation with an isotropic-considered substrate is too rough to get accurate solutions; the full dispersion equation with a piezoelectric-considered substrate is too complicated to get simple and practical expressions for optimizing LW-based sensors. In this work, a dispersion equation is introduced for Love waves in a layered struct...

  15. Ratio method of measuring W boson mass

    Guo, Feng [Stony Brook Univ., NY (United States)

    2010-08-01

    This dissertation describes an alternative method of measuring the W boson mass in DØ experiment. Instead of extracting MW from the fitting of W → ev fast Monte Carlo simulations to W → ev data as in the standard method, we make the direct fit of transverse mass between W → ev data and Z → ee data. One of the two electrons from Z boson is treated as a neutrino in the calculation of transverse mass. In ratio method, the best fitted scale factor corresponds to the ratio of W and Z boson mass (MW/MZ). Given the precisely measured Z boson mass, W mass is directly fitted from W → ev and Z → ee data. This dissertation demonstrates that ratio method is a plausible method of measuring the W boson mass. With the 1 fb-1 DØ Run IIa dataset, ratio method gives MW = 80435 ± 43(stat) ± 26(sys) MeV.

  16. Ratio method of measuring $w$ boson mass

    Guo, Feng; /SUNY, Stony Brook

    2010-08-01

    This dissertation describes an alternative method of measuring the W boson mass in D0 experiment. Instead of extracting M{sub W} from the fitting of W {yields} e{nu} fast Monte Carlo simulations to W {yields} e{nu} data as in the standard method, we make the direct fit of transverse mass between W {yields} e{nu} data and Z {yields} ee data. One of the two electrons from Z boson is treated as a neutrino in the calculation of transverse mass. In ratio method, the best fitted scale factor corresponds to the ratio of W and Z boson mass (M{sub W}/M{sub Z}). Given the precisely measured Z boson mass, W mass is directly fitted from W {yields} e{nu} and Z {yields} ee data. This dissertation demonstrates that ratio method is a plausible method of measuring the W boson mass. With the 1 fb{sup -1} D0 Run IIa dataset, ratio method gives M{sub W} = 80435 {+-} 43(stat) {+-} 26(sys) MeV.

  17. Particle Image Velocimetry Measurements in an Anatomically-Accurate Scaled Model of the Mammalian Nasal Cavity

    Rumple, Christopher; Krane, Michael; Richter, Joseph; Craven, Brent

    2013-11-01

    The mammalian nose is a multi-purpose organ that houses a convoluted airway labyrinth responsible for respiratory air conditioning, filtering of environmental contaminants, and chemical sensing. Because of the complexity of the nasal cavity, the anatomy and function of these upper airways remain poorly understood in most mammals. However, recent advances in high-resolution medical imaging, computational modeling, and experimental flow measurement techniques are now permitting the study of respiratory airflow and olfactory transport phenomena in anatomically-accurate reconstructions of the nasal cavity. Here, we focus on efforts to manufacture an anatomically-accurate transparent model for stereoscopic particle image velocimetry (SPIV) measurements. Challenges in the design and manufacture of an index-matched anatomical model are addressed. PIV measurements are presented, which are used to validate concurrent computational fluid dynamics (CFD) simulations of mammalian nasal airflow. Supported by the National Science Foundation.

  18. Generation increases at Cofrentes Nuclear Power Plant based on accurate feedwater flow measurement

    This paper discusses the application of Caldon LEFM ultrasonic flow and temperature measurement systems at Cofrentes Nuclear Power Plant. Based on plant instrumentation, Cofrentes engineering personnel estimated an 8 to 10 MW electric shortfall in generation due to venturi nozzle fouling. An external LEFM ultrasonic flow measurement system installed in October 2000 showed a shortfall of about 9 MW electric, consistent with expectations. The plant has increased generation by using the more accurate ultrasonic system to correct for the venturi nozzle bias. Following the recovery of generation lost to venturi fouling, Cofrentes plans to upgrade the flow meter to Caldon's LEFM CheckPlus system. This system is sufficiently accurate to warrant re-licensing for a power up-rate of up to 1,7% based on improved thermal power measurement. (author)

  19. Defining allowable physical property variations for high accurate measurements on polymer parts

    Mohammadi, A.; Sonne, M. R.; Madruga, D. G.; De Chiffre, L.; Hattel, J. H.

    2016-06-01

    Measurement conditions and material properties have a significant impact on the dimensions of a part, especially for polymers parts. Temperature variation causes part deformations that increase the uncertainty of the measurement process. Current industrial tolerances of a few micrometres demand high accurate measurements in non-controlled ambient. Most of polymer parts are manufactured by injection moulding and their inspection is carried out after stabilization, around 200 hours. The overall goal of this work is to reach ±5μm in uncertainty measurements a polymer products which is a challenge in today`s production and metrology environments. The residual deformations in polymer products at room temperature after injection molding are important when micrometer accuracy needs to be achieved. Numerical modelling can give a valuable insight to what is happening in the polymer during cooling down after injection molding. In order to obtain accurate simulations, accurate inputs to the model are crucial. In reality however, the material and physical properties will have some variations. Although these variations may be small, they can act as a source of uncertainty for the measurement. In this paper, we investigated how big the variation in material and physical properties are allowed in order to reach the 5 μm target on the uncertainty.

  20. Mass Measurement with Rare-RI Rin

    Ozawa, Akira

    2014-09-01

    Mass measurement with Rare-RI Ring in RIKEN RI Beam Factory (RIBF) will be presented. The main purpose of Rare-RI Ring is to measure the mass for very neutron-rich nuclei, the production rate of which is very small (rare RI) and the life-time of which is predicted to be very short (less than 10 ms). In Rare-RI Ring, mass measurements will be performed based on isochronous mass spectrometry. There are two innovative apparatus in Rare-RI Ring: individual injection, which can realize the injection of 200 A MeV rare RI one-by-one, and a cyclotron-like storage ring, which allows high isochronous magnetic fields with large angular and momentum acceptances (~1%). By these apparatus, we will achieve a 10-6 mass resolution, and will be able to access rare RI, the production rate of which is down to 1 event/day/pnA in RIBF. Construction of Rare-RI Ring has started from the 2012 fiscal year. Construction of the storage ring itself was almost completed. In this fiscal year, we succeeded to store alphas from 241Am source and to check the production of isochronous fields in the storage ring. In this talk, present status of Rare-RI Ring and the possible mass measurement there will be presented.

  1. Improved plant economics through accurate feedwater flow measurement with the crossflow ultrasonic flowmeter

    The crossflow ultrasonic flowmeter (UFM) improves nuclear power plant performance through more accurate and reliable feedwater flow measurement. Reactor power levels are typically monitored via secondary-side calorimetric calculations that depend on the accurate measurement of feedwater flow . The feedwater flow is measured with calibrated venturis in most plants. These are subject to chemical fouling and other mechanical problems. If the loss in accuracy of the feedwater flow measurement overstates the actual flow rate, the result is a direct loss in megawatts generated by the plant. This paper describes a new, innovative ultrasonic technique to improve the accuracy, stability and repeatability of ultrasonic flow measurements. By employing this advanced technology to provide a continuous correction to the venturi-measured feed water flow rate, plants have reported the recovery of between 5 and 25 MWe. This technology has been implemented in a new flowmeter called CROSSFLOW. The CROSSFLOW meter utilizes a mathematical process called cross-correlation to process the ultrasonic signal, which is modulated by the flow eddys to determine the velocity of the feedwater. It replaces the older, less accurate transit-time methodology. Comparisons with weigh tank test, calibrated plant instrumentation, and chemical tracer tests have demonstrated a repeatable accuracy of 0.21% or better with this advanced cross-correlation technology. The paper discusses the history of the cross-correlation technique and its theoretical basis, illustrates how this technique addresses the measurement sensitivities for various parameters, demonstrates the calculation of the accuracy of the meter, and discusses the recently completed NRC review of the CROSSFLOW System and methodology. The paper also discusses recent precision flow measurement applications being performed with CROSSFLOW at nuclear plants worldwide. Among these applications are the measurement of Reactor Coolant System flow and the

  2. Recent progress in precision mass measurements

    During the last years, a new generation of technique for measuring directly masses of short-lived isotopes has evolved. The common features of these modern techniques are a transition from the measurement of kinetic energies or voltage ratios to a determination of time and frequency and in most cases storage of the ions for extended periods of time. (orig.)

  3. KATRIN: Measuring the Mass Scale of Neutrinos

    Oblath, Noah; Katrin Collaboration

    2011-10-01

    Over the past decade, experiments studying neutrinos from atmospheric, solar, and reactor sources have shown conclusively that neutrinos change flavor and, as a consequence, have a small but finite mass. However, the scale of neutrino masses remains an open question that is of great importance for many areas of physics. The most direct method to measure the neutrino mass scale is still via beta decay. The talk will focus primarily on the status of the KArlsruhe TRItium Neutrino experiment (KATRIN), currently under construction. KATRIN combines an ultra-luminous molecular windowless gaseous tritium source with a high-resolution integrating spectrometer to gain sensitivity to the absolute mass scale of neutrinos. The projected sensitivity of the experiment on the neutrino mass is 0.2 eV at 90% C.L. In this talk I will discuss the status of the KATRIN experiment.

  4. Measuring the running top-quark mass

    We present the first direct determination of the running top-quark mass based on the total cross section of top-quark pair-production as measured at the Tevatron. Our theory prediction for the cross section includes various next-to-next-to-leading order QCD contributions, in particular all logarithmically enhanced terms near threshold, the Coulomb corrections at two loops and all explicitly scale dependent terms at NNLO accuracy. The result allows for an exact and independent variation of the renormalization and factorization scales. For Tevatron and LHC we study its dependence on all scales, on the parton luminosity and on the top-quark mass using both the conventional pole mass definition as well as the running mass in the MS scheme. We extract for the top-quark an MS mass of m(μ=m) =160.0+3.3-3.2 GeV. (orig.)

  5. Precision measurement of W mass at LHC

    The W mass allows for a precise cross check of the Standard Model (SM), and its uncertainty is the limiting factor for sensitivity to the SM Higgs mass and what may lie beyond. A precise W mass measurement is feasible at the LHC due to large number of events, not only for W decays, but also corresponding Z decays, which will be the key ingredients for precision calibration and understanding of systematic errors. Using statistics corresponding to 10 fb-1 of data at the LHC, we have investigated strategies for improving the uncertainty on the mass measurement beyond 15 MeV, including both theoretical and experimental effects. No single source of uncertainty necessarily contribute more than 5 MeV to the overall uncertainty

  6. Precision measurement of W mass at LHC

    Petersen, Troels C. [Building 40-3D-002, CERN, Geneva (Switzerland)

    2008-03-15

    The W mass allows for a precise cross check of the Standard Model (SM), and its uncertainty is the limiting factor for sensitivity to the SM Higgs mass and what may lie beyond. A precise W mass measurement is feasible at the LHC due to large number of events, not only for W decays, but also corresponding Z decays, which will be the key ingredients for precision calibration and understanding of systematic errors. Using statistics corresponding to 10 fb{sup -1} of data at the LHC, we have investigated strategies for improving the uncertainty on the mass measurement beyond 15 MeV, including both theoretical and experimental effects. No single source of uncertainty necessarily contribute more than 5 MeV to the overall uncertainty.

  7. Accurate disintegration-rate measurement of 55Fe by liquid scintillation counting

    A method involving liquid scintillation counting is described for the accurate measurement of disintegration rate of 55Fe. The method is based on the use of calculated efficiency functions together with either of the nuclides 54Mn and 51Cr as internal standards for measurement of counting efficiencies by coincidence counting. The method was used by the NAC during a recent international intercomparison of radioactivity measurements, and a summary of the results obtained by nine participating laboratories is presented. A spread in results of several percent is evident

  8. Measurement of the W boson mass

    Abazov, Victor Mukhamedovich; /Dubna, JINR; Abbott, Braden Keim; /Oklahoma U.; Abolins, Maris A.; /Michigan State U.; Acharya, Bannanje Sripath; /Tata Inst.; Adams, Mark Raymond; /Illinois U., Chicago; Adams, Todd; /Florida State U.; Aguilo, Ernest; /Alberta U. /Simon Fraser U. /York U., Canada /McGill U.; Ahsan, Mahsana; /Kansas State U.; Alexeev, Guennadi D.; /Dubna, JINR; Alkhazov, Georgiy D.; /St. Petersburg, INP; Alton, Andrew K.; /Michigan U. /Augustana Coll., Sioux Falls /Northeastern U.

    2009-08-01

    The authors present a measurement of the W boson mass in W {yields} e{nu} decays using 1 fb{sup -1} of data collected with the D0 detector during Run II of the Fermilab Tevatron collider. With a sample of 499830 W {yields} e{nu} candidate events, they measure M{sub W} = 80.401 {+-} 0.043 GeV. This is the most precise measurement from a single experiment.

  9. Mass measurements and evaluation around A=22

    Frequency ratio measurements with different combinations of the singly charged ions from 21,22,23Na, 22,24Mg, and 37,39K were performed at the on-line Penning trap mass spectrometer ISOLTRAP, CERN, Geneva. The masses and mass differences were deduced with a relative uncertainty of about or even below one part in 108 for the ions of interest using a least-squares analysis of all measured relations. The results have direct consequences for weak-interaction study as they give additional input to the test of CVC, and for nuclear astrophysics, because they help to establish the minimum observable signal for a NeNa cycle in a nova burst. We report here about the measurements and the detailed evaluation. (orig.)

  10. Measurement of the W boson mass

    We present a preliminary measurement of the W boson mass using data collected by the D null experiment at the Fermilab Tevatron during the 1994-1995 collider run 1b. We use W → eν decays to extract the W mass from the observed spectrum of transverse mass of the electron (|η| 0 → ee decays to constrain our model of the detector response. We measure mW/mZ = 0.8815 ± 0.0011(stat) ± 0.0014(syst) and mW = 80.38 ± 0.07 (W stat) ± 0.13(syst) GeV. Combining this result with our previous measurement from the 1992-1993 data, we obtain mW = 80.37 ± 0.15 GeV (errors combined in quadrature)

  11. Precise and accurate measurements of strong-field photoionisation and a transferrable laser intensity calibration standard

    Wallace, W C; Khurmi, C; U., Satya Sainadh; Calvert, J E; Laban, D E; Pullen, M G; Bartschat, K; Grum-Grzhimailo, A N; Wells, D; Quiney, H M; Tong, X M; Litvinyuk, I V; Sang, R T; Kielpinski, D

    2016-01-01

    Ionization of atoms and molecules in strong laser fields is a fundamental process in many fields of research, especially in the emerging field of attosecond science. So far, demonstrably accurate data have only been acquired for atomic hydrogen (H), a species that is accessible to few investigators. Here we present measurements of the ionization yield for argon, krypton, and xenon with percentlevel accuracy, calibrated using H, in a laser regime widely used in attosecond science. We derive a transferrable calibration standard for laser peak intensity, accurate to 1.3%, that is based on a simple reference curve. In addition, our measurements provide a much-needed benchmark for testing models of ionisation in noble-gas atoms, such as the widely employed single-active electron approximation.

  12. Rapid and accurate broadband absorption cross-section measurement of human bodies in a reverberation chamber

    A measurement methodology for polarization and angle of incidence averaged electromagnetic absorption cross-section using a reverberation chamber is presented. The method is optimized for simultaneous rapid and accurate determination of average absorption cross-section over the frequency range 1–15 GHz, making it suitable for use in human absorption and exposure studies. The typical measurement time of the subject is about 8 min with a corresponding statistical uncertainty of about 3% in the measured absorption cross-section. The method is validated by comparing measurements on a spherical phantom with Mie series calculations. The efficacy of the method is demonstrated with measurements of the posture dependence of the absorption cross-section of a human subject and an investigation of the effects of clothing on the measured absorption which are important considerations for the practical design of experiments for studies on human subjects. (paper)

  13. Accurate potential drop sheet resistance measurements of laser-doped areas in semiconductors

    Heinrich, Martin, E-mail: mh.seris@gmail.com [Solar Energy Research Institute of Singapore, National University of Singapore, Singapore 117574 (Singapore); NUS Graduate School for Integrative Science and Engineering, National University of Singapore, Singapore 117456 (Singapore); Kluska, Sven; Binder, Sebastian [Fraunhofer Institute for Solar Energy Systems (ISE), Heidenhofstrasse 2, D-79110 Freiburg (Germany); Hameiri, Ziv [The School of Photovoltaic and Renewable Energy Engineering, The University of New South Wales, Sydney NSW 2052 (Australia); Hoex, Bram [Solar Energy Research Institute of Singapore, National University of Singapore, Singapore 117574 (Singapore); Aberle, Armin G. [Solar Energy Research Institute of Singapore, National University of Singapore, Singapore 117574 (Singapore); NUS Graduate School for Integrative Science and Engineering, National University of Singapore, Singapore 117456 (Singapore); Department of Electrical and Computer Engineering, National University of Singapore, Singapore 117456 (Singapore)

    2014-10-07

    It is investigated how potential drop sheet resistance measurements of areas formed by laser-assisted doping in crystalline Si wafers are affected by typically occurring experimental factors like sample size, inhomogeneities, surface roughness, or coatings. Measurements are obtained with a collinear four point probe setup and a modified transfer length measurement setup to measure sheet resistances of laser-doped lines. Inhomogeneities in doping depth are observed from scanning electron microscope images and electron beam induced current measurements. It is observed that influences from sample size, inhomogeneities, surface roughness, and coatings can be neglected if certain preconditions are met. Guidelines are given on how to obtain accurate potential drop sheet resistance measurements on laser-doped regions.

  14. Accurate Measurement of Mitochondrial DNA Deletion Level and Copy Number Differences in Human Skeletal Muscle

    Grady, John P.; Murphy, Julie L; Blakely, Emma L.; Haller, Ronald G.; Taylor, Robert W; Turnbull, Doug M.; Tuppen, Helen A. L.

    2014-01-01

    Accurate and reliable quantification of the abundance of mitochondrial DNA (mtDNA) molecules, both wild-type and those harbouring pathogenic mutations, is important not only for understanding the progression of mtDNA disease but also for evaluating novel therapeutic approaches. A clear understanding of the sensitivity of mtDNA measurement assays under different experimental conditions is therefore critical, however it is routinely lacking for most published mtDNA quantification assays. Here, ...

  15. A Novel Multimode Waveguide Coupler for Accurate Power Measurement of Traveling Wave Tube Harmonic Frequencies

    Wintucky, Edwin G.; Simons, Rainee N.

    2014-01-01

    This paper presents the design, fabrication and test results for a novel waveguide multimode directional coupler (MDC). The coupler fabricated from two dissimilar waveguides is capable of isolating the power at the second harmonic frequency from the fundamental power at the output port of a traveling-wave tube (TWT). In addition to accurate power measurements at harmonic frequencies, a potential application of the MDC is in the design of a beacon source for atmospheric propagation studies at millimeter-wave frequencies.

  16. Accurate FRET Measurements within Single Diffusing Biomolecules Using Alternating-Laser Excitation

    Lee, Nam Ki; Kapanidis, Achillefs N.; Wang, You; Michalet, Xavier; Mukhopadhyay, Jayanta; Ebright, Richard H.; Weiss, Shimon

    2005-01-01

    Fluorescence resonance energy transfer (FRET) between a donor (D) and an acceptor (A) at the single-molecule level currently provides qualitative information about distance, and quantitative information about kinetics of distance changes. Here, we used the sorting ability of confocal microscopy equipped with alternating-laser excitation (ALEX) to measure accurate FRET efficiencies and distances from single molecules, using corrections that account for cross-talk terms that contaminate the FRE...

  17. Interpretation of In Situ and Laboratory Thermal Measurements Resulting in Accurate Thermogeological Characterisation

    Hemmingway, Phil; Long, Michael

    2012-01-01

    Growing worldwide interest in the exploitation of geothermal energy resources has led to a scenario where the technology routinely forms part of building-scale renewable energy feasibility studies. A thorough understanding of site-specific thermogeological parameters is a vital design requirement of such systems and accurate measurement and interpretation of these parameters is necessary in order to inform scientifically rigorous system design. An overview of the theory underlying a number of...

  18. Atom interferometry experiments with lithium. Accurate measurement of the electric polarizability

    Atom interferometers are very sensitive tools to make precise measurements of physical quantities. This study presents a measurement of the static electric polarizability of lithium by atom interferometry. Our result, α = (24.33 ± 0.16)*10-30 m3, improves by a factor 3 the most accurate measurements of this quantity. This work describes the tuning and the operation of a Mach-Zehnder atom interferometer in detail. The two interfering arms are separated by the elastic diffraction of the atomic wave by a laser standing wave, almost resonant with the first resonance transition of lithium atom. A set of experimental techniques, often complicated to implement, is necessary to build the experimental set-up. After a detailed study of the atom source (a supersonic beam of lithium seeded in argon), we present our experimental atom signals which exhibit a very high fringe visibility, up to 84.5 % for first order diffraction. A wide variety of signals has been observed by diffraction of the bosonic isotope at higher diffraction orders and by diffraction of the fermionic less abundant isotope. The quality of these signals is then used to do very accurate phase measurements. A first experiment investigates how the atom interferometer signals are modified by a magnetic field gradient. An absolute measurement of lithium atom electric polarizability is then achieved by applying a static electric field on one of the two interfering arms, separated by only 90 micrometers. The construction of such a capacitor, its alignment in the experimental set-up and its operation are fully detailed.We obtain a very accurate phase measurement of the induced Lo Surdo - Stark phase shift (0.07 % precision). For this first measurement, the final uncertainty on the electric polarizability of lithium is only 0.66 %, and is dominated by the uncertainty on the atom beam mean velocity, so that a further reduction of the uncertainty can be expected. (author)

  19. Oxidized Fatty Acid Analysis by Charge Switch Derivatization, Selected Reaction Monitoring and Accurate Mass Quantification

    Liu, Xinping; Moon, Sung Ho; Mancuso, David J.; Jenkins, Christopher M.; Guan, Shaoping; Sims, Harold F.; Gross, Richard W.

    2013-01-01

    A highly sensitive, specific and robust method for the analysis of oxidized metabolites of linoleic, acid (LA), arachidonic acid (AA) and docosahexaenoic acid (DHA) was developed using charge-switch derivatization, LC-ESI MS/MS with selected reaction monitoring (SRM) and quantitation by high mass accuracy analysis of product ions thereby minimizing interferences from contaminating ions. Charge-switch derivatization of LA, AA and DHA metabolites with N-(4-aminomethylphenyl)-pyridinium resulted...

  20. Measurement of the Top Quark Mass

    We present a measurement of the top quark mass using a sample of t bar t decays into an electron or a muon, a neutrino, and four jets. The data were collected in p bar p collisions at √(s)=1.8 TeV with the Collider Detector at Fermilab and correspond to an integrated luminosity of 109 pb-1 . We measure the top quark mass to be 175.9±4.8(stat)±4.9( syst) GeV /c2 . copyright 1998 The American Physical Society

  1. Intravital spectral imaging as a tool for accurate measurement of vascularization in mice

    Tsatsanis Christos

    2010-10-01

    Full Text Available Abstract Background Quantitative determination of the development of new blood vessels is crucial for our understanding of the progression of several diseases, including cancer. However, in most cases a high throughput technique that is simple, accurate, user-independent and cost-effective for small animal imaging is not available. Methods In this work we present a simple approach based on spectral imaging to increase the contrast between vessels and surrounding tissue, enabling accurate determination of the blood vessel area. This approach is put to test with a 4T1 breast cancer murine in vivo model and validated with histological and microvessel density analysis. Results We found that one can accurately measure the vascularization area by using excitation/emission filter pairs which enhance the surrounding tissue's autofluorescence, significantly increasing the contrast between surrounding tissue and blood vessels. Additionally, we found excellent correlation between this technique and histological and microvessel density analysis. Conclusions Making use of spectral imaging techniques we have shown that it is possible to accurately determine blood vessel volume intra-vitally. We believe that due to the low cost, accuracy, user-independence and simplicity of this technique, it will be of great value in those cases where in vivo quantitative information is necessary.

  2. In Pursuit of Highly Accurate Atomic Lifetime Measurements of Multiply Charged Ions

    Trabert, E

    2009-06-01

    Accurate atomic lifetime data are useful for terrestrial and astrophysical plasma diagnostics. At accuracies higher than those required for these applications, lifetime measurements test atomic structure theory in ways complementary to spectroscopic energy determinations. At the highest level of accuracy, the question arises whether such tests reach the limits of modern theory, a combination of quantum mechanics and QED, adn possibly point to physics beyond the Standard Model. If high-precision atomic lifetime measurements, especially on multiply charged ions, have not quite reached this high accuracy yet, then what is necessary to attain this goal?

  3. Using gas blow methods to realize accurate volume measurement of radioactivity liquid

    For liquid which has radioactivity, Realized the accurate volume measurement uncertainty less than 0.2% (k=2) by means of gas blow methods presented in the 'American National Standard-Nuclear Material Control-Volume Calibration Methods(ANSI N15.19-1989)' and the 'ISO Committee Drafts (ISO/TC/85/SC 5N 282 )' and Explored a set methods of Data Processing. In the article, the major problems is to solve data acquisition and function foundation and measurement uncertainty estimate. (authors)

  4. High-precision mass spectrometric hydrogen isotope ratio measurements

    The analytical capabilities of mass spectrometric ion-current measurement systems are described on both a theoretical and a practical basis. From the theoretical standpoint, a signal-to-noise ratio (S/N) model that evaluated the fundamental sources of noise present in ion-current measurement systems was developed. Use of this model accurately predicted the performance (precision) for ion-current ratio measurements made by two isotope ratio mass spectrometers, one designed for carbon isotopic measurements, and the other designed for hydrogen isotopic measurements. Isotope ratio measurements differ from current-ratio measurements in that the observed ion-current ratio must be corrected to reflect the ratio of the ion currents due to the isotopic species of interest, which, for hydrogen isotope ratio mass spectrometry, are HD+ and H2+. Interfaces to these two ion currents are described in detail. To compensate for H3+ three measurement procedures, the two-standard calibration, the one-standard differential measurement with electronic H3+ compensation, and the two-standard differential measurement, are described. The one- and two-standard differential measurements were successfully used for measurement of isotopic abundances. Results of a collaborative investigation to validate the use of 18O in place of D as an isotopic label for total body water measurements are presented. In this research both 18O and D were administered simultaneously to several subjects. The weight of total body water of these subjects as measured by the dilution of D into the body water was in good agreement with the results of the 18O measurements. A brief description of the laboratory computer system is also given

  5. A fast experimental beam hardening correction method for accurate bone mineral measurements in 3D μCT imaging system.

    Koubar, Khodor; Bekaert, Virgile; Brasse, David; Laquerriere, Patrice

    2015-06-01

    Bone mineral density plays an important role in the determination of bone strength and fracture risks. Consequently, it is very important to obtain accurate bone mineral density measurements. The microcomputerized tomography system provides 3D information about the architectural properties of bone. Quantitative analysis accuracy is decreased by the presence of artefacts in the reconstructed images, mainly due to beam hardening artefacts (such as cupping artefacts). In this paper, we introduced a new beam hardening correction method based on a postreconstruction technique performed with the use of off-line water and bone linearization curves experimentally calculated aiming to take into account the nonhomogeneity in the scanned animal. In order to evaluate the mass correction rate, calibration line has been carried out to convert the reconstructed linear attenuation coefficient into bone masses. The presented correction method was then applied on a multimaterial cylindrical phantom and on mouse skeleton images. Mass correction rate up to 18% between uncorrected and corrected images were obtained as well as a remarkable improvement of a calculated mouse femur mass has been noticed. Results were also compared to those obtained when using the simple water linearization technique which does not take into account the nonhomogeneity in the object. PMID:25818096

  6. Stellar mass-to-light ratios from galaxy spectra: how accurate can they be?

    Gallazzi, Anna

    2009-01-01

    Stellar masses play a crucial role in the exploration of galaxy properties and the evolution of the galaxy population. In this paper, we explore the minimum possible uncertainties in stellar mass-to-light (M/L) ratios from the assumed star formation history (SFH) and metallicity distribution, with the goals of providing a minimum set of requirements for observational studies. We use a large Monte Carlo library of SFHs to study as a function of galaxy spectral type and signal-to-noise ratio (S/N) the statistical uncertainties of M/L values using either absorption-line data or broad band colors. The accuracy of M/L estimates can be significantly improved by using metal-sensitive indices in combination with age-sensitive indices, in particular for galaxies with intermediate-age or young stellar populations. While M/L accuracy clearly depends on the spectral S/N ratio, there is no significant gain in improving the S/N much above 50/pix and limiting uncertainties of 0.03 dex are reached. Assuming that dust is accu...

  7. Dynamic Bayesian Network for Accurate Detection of Peptides from Tandem Mass Spectra.

    Halloran, John T; Bilmes, Jeff A; Noble, William S

    2016-08-01

    A central problem in mass spectrometry analysis involves identifying, for each observed tandem mass spectrum, the corresponding generating peptide. We present a dynamic Bayesian network (DBN) toolkit that addresses this problem by using a machine learning approach. At the heart of this toolkit is a DBN for Rapid Identification (DRIP), which can be trained from collections of high-confidence peptide-spectrum matches (PSMs). DRIP's score function considers fragment ion matches using Gaussians rather than fixed fragment-ion tolerances and also finds the optimal alignment between the theoretical and observed spectrum by considering all possible alignments, up to a threshold that is controlled using a beam-pruning algorithm. This function not only yields state-of-the art database search accuracy but also can be used to generate features that significantly boost the performance of the Percolator postprocessor. The DRIP software is built upon a general purpose DBN toolkit (GMTK), thereby allowing a wide variety of options for user-specific inference tasks as well as facilitating easy modifications to the DRIP model in future work. DRIP is implemented in Python and C++ and is available under Apache license at http://melodi-lab.github.io/dripToolkit . PMID:27397138

  8. Improved dynamic compensation for accurate cutting force measurements in milling applications

    Scippa, A.; Sallese, L.; Grossi, N.; Campatelli, G.

    2015-03-01

    Accurate cutting-force measurements appear to be the key information in most of the machining related studies as they are fundamental in understanding the cutting processes, optimizing the cutting operations and evaluating the presence of instabilities that could affect the effectiveness of cutting processes. A variety of specifically designed transducers are commercially available nowadays and many different approaches in measuring cutting forces are presented in literature. The available transducers, though, express some limitations since they are conditioned by the vibration of the surrounding system and by the transducer's natural frequency. These parameters can drastically affect the measurement accuracy in some cases; hence an effective and accurate tool is required to compensate those dynamically induced errors in cutting force measurements. This work is aimed at developing and testing a compensation technique based on Kalman filter estimator. Two different approaches named "band-fitting" and "parallel elaboration" methods, have been developed to extend applications of this compensation technique, especially for milling purpose. The compensation filter has been designed upon the experimentally identified system's dynamic and its accuracy and effectiveness has been evaluated by numerical and experimental tests. Finally its specific application in cutting force measurements compensation is described.

  9. Measurement of caudate nucleus area - a more accurate measurement for Huntington's disease?

    Caudate nucleus atrophy occurs in Huntington's disease and methods of measuring this have been described using axial CT, but these are indirect and lack sensitivity. We measured caudate nucleus area (blind to the subjects' clinical state) in 30 subjects with or at risk of Huntington's disease, and in 100 normal age matched controls. Fifteen subjects with established symptomatic Huntington's disease, 3 with early symptoms, and 3 presymptomatic subjects (2 showing a high probability for the Huntington's disease gene on genetic testing, and one who has since developed symptoms) were correctly identified. Three normal (gene negative) family members were also correctly identified. Outcome is awaited in 6. CT caudate area measurement is simple and reproducible and we have found it to be a useful confirmatory test for Huntington's disease. (orig.)

  10. No Galaxy Left Behind: Accurate Measurements with the Faintest Objects in the Dark Energy Survey

    Suchyta, E. [The Ohio State Univ., Columbus, OH (United States). et al.

    2015-07-29

    Accurate statistical measurement with large imaging surveys has traditionally required throwing away a sizable fraction of the data. This is because most measurements have have relied on selecting nearly complete samples, where variations in the composition of the galaxy population with seeing, depth, or other survey characteristics are small. We introduce a new measurement method that aims to minimize this wastage, allowing precision measurement for any class of stars or galaxies detectable in an imaging survey. We have implemented our proposal in Balrog, a software package which embeds fake objects in real imaging in order to accurately characterize measurement biases. We also demonstrate this technique with an angular clustering measurement using Dark Energy Survey (DES) data. We first show that recovery of our injected galaxies depends on a wide variety of survey characteristics in the same way as the real data. We then construct a flux-limited sample of the faintest galaxies in DES, chosen specifically for their sensitivity to depth and seeing variations. Using the synthetic galaxies as randoms in the standard LandySzalay correlation function estimator suppresses the effects of variable survey selection by at least two orders of magnitude. Now our measured angular clustering is found to be in excellent agreement with that of a matched sample drawn from much deeper, higherresolution space-based COSMOS imaging; over angular scales of 0.004° < θ < 0.2 ° , we find a best-fit scaling amplitude between the DES and COSMOS measurements of 1.00 ± 0.09. We expect this methodology to be broadly useful for extending the statistical reach of measurements in a wide variety of coming imaging surveys.

  11. Measuring accurately liquid and tissue surface tension with a compression plate tensiometer

    Mgharbel, Abbas; Rieu, Jean-Paul

    2009-01-01

    Apparent tissue surface tension allows the quantification of cell-cell cohesion and was reported to be a powerful indicator for the cellular rearrangements that take place during embryonic development or for cancer progression. The measurement is realized with a parallel compression plate tensiometer using the capillary laws. Although it was introduced more than a decade ago, it is based on various geometrical or physical approximations. Surprisingly, these approximations have never been tested. Using a novel tensiometer, we compare the two currently used methods to measure tissue surface tension and propose a third one, based on a local polynomial fit (LPF) of the profile of compressed droplets or cell aggregates. We show the importance of measuring the contact angle between the plate and the drop/aggregate to obtain real accurate measurement of surface tension when applying existing methods. We can suspect that many reported values of surface tension are greatly affected because of not handling this paramet...

  12. Test of the standard model at low energy: accurate measurements of the branching rates of 62Ga; accurate measurements of the half-life of 38Ca

    Precise measurements of Fermi superallowed 0+ → 0+ β decays provide a powerful tool to study the weak interaction properties in the framework of the Standard Model (SM). Collectively, the comparative half-lives (ft) of these transitions allow a sensitive probe of the CVC (Conserved Vector Current) hypothesis and contribute to the most demanding test of the unitarity of the quarks-mixing CKM matrix top-row, by providing, so far, the most accurate determination of its dominant element (Vud). Until recently, an apparent departure from unity enhanced a doubt on the validity of the minimal SM and thus stimulated a considerable effort in order to extend the study to other Fermi emitters available. The 62Ga and 38Ca are among key nuclei to achieve these precision tests and verify the reliability of the corrections applied to the experimental ft-values. The 62Ga β-decay was investigated at the IGISOL separator, with an experimental setup composed of 3 EUROBALL Clovers for γ-ray detection. Very weak intensity (62Zn. The newly established analog branching-ratio (B.RA equals 99.893(24) %) was used to compute the universal Ft-value (62Ga). The latter turned out to be in good agreement with the 12 well-known cases. Compatibility between the upper limit set here on the term (δIM) and the theoretical prediction suggests that the isospin-symmetry-breaking correction is indeed large for the heavy (A ≥ 62) β-emitters. The study of the 38Ca decay was performed at the CERN-ISOLDE facility. Injection of fluorine into the ion source, in order to chemically select the isotopes of interest, assisted by the REXTRAP Penning trap facility and a time-of-flight analysis, enabled us to eliminate efficiently the troublesome 38mK. For the first time, the 38Ca half-life is measured with a highly purified radioactive sample. The preliminary result obtained, T1/2(38Ca) 445.8(10) ms, improves the precision on the half-life as determined from previous measurements by a factor close to 10

  13. Fast and Accurate Fourier Series Solutions to Gravitational Lensing by A General Family of Two Power-Law Mass Distributions

    Chae, K H

    2002-01-01

    Fourier series solutions to the deflection and magnification by a family of three-dimensional cusped two power-law ellipsoidal mass distributions are presented. The cusped two power-law ellipsoidal mass distributions are characterized by inner and outer power-law radial indices and a break (or, transition) radius. The model family includes mass models mimicking Jaffe, Hernquist, and $\\eta$ models and dark matter halo profiles from numerical simulations. The Fourier series solutions for the cusped two power-law mass distributions are relatively simple, and allow a very fast calculation even for a chosen small fractional calculational error (e.g. $10^{-5}$). These results will be particularly useful for studying lensed systems which provide a number of accurate lensing constraints and for systematic analyses of large numbers of lenses. Subroutines employing these results for the two power-law model and the results by Chae, Khersonsky, & Turnshek for the generalized single power-law mass model are made publi...

  14. Fast and Accurate Fourier Series Solutions to Gravitational Lensing by a General Family of Two-Power-Law Mass Distributions

    Chae, Kyu-Hyun

    2002-04-01

    Fourier series solutions to the deflection and magnification by a family of three-dimensional cusped two-power-law ellipsoidal mass distributions are presented. The cusped two-power-law ellipsoidal mass distributions are characterized by inner and outer power-law radial indices and a break (or transition) radius. The model family includes mass models mimicking Jaffe, Hernquist, and η models and dark matter halo profiles from numerical simulations. The Fourier series solutions for the cusped two-power-law mass distributions are relatively simple and allow a very fast calculation, even for a chosen small fractional calculational error (e.g., 10-5). These results will be particularly useful for studying lensed systems that provide a number of accurate lensing constraints and for systematic analyses of large numbers of lenses. Subroutines employing these results for the two-power-law model and the results by Chae, Khersonsky, & Turnshek for the generalized single-power-law mass model are made publicly available.

  15. Particle Image Velocimetry Measurements in Anatomically-Accurate Models of the Mammalian Nasal Cavity

    Rumple, C.; Richter, J.; Craven, B. A.; Krane, M.

    2012-11-01

    A summary of the research being carried out by our multidisciplinary team to better understand the form and function of the nose in different mammalian species that include humans, carnivores, ungulates, rodents, and marine animals will be presented. The mammalian nose houses a convoluted airway labyrinth, where two hallmark features of mammals occur, endothermy and olfaction. Because of the complexity of the nasal cavity, the anatomy and function of these upper airways remain poorly understood in most mammals. However, recent advances in high-resolution medical imaging, computational modeling, and experimental flow measurement techniques are now permitting the study of airflow and respiratory and olfactory transport phenomena in anatomically-accurate reconstructions of the nasal cavity. Here, we focus on efforts to manufacture transparent, anatomically-accurate models for stereo particle image velocimetry (SPIV) measurements of nasal airflow. Challenges in the design and manufacture of index-matched anatomical models are addressed and preliminary SPIV measurements are presented. Such measurements will constitute a validation database for concurrent computational fluid dynamics (CFD) simulations of mammalian respiration and olfaction. Supported by the National Science Foundation.

  16. A measurement of the tau mass

    Using the ARGUS detector at the DORIS II storage ring, a new measurement of the mass of the τ lepton has been obtained. An analysis of the tan pseudomass spectrum for decays of the type τ- → π-π-π+ντ finds mτ = (1776.3 ± 2.4 ± 1.4) MeV/c2. This result also leads to an improvement of the upper limit on the ντ mass to mντ 2 at the 95% confidence level. (orig.)

  17. A measurement of the tau mass

    Albrecht, H.; Ehrlichmann, H.; Hamacher, T.; Hofmann, R.P.; Kirchhoff, T.; Nau, A.; Nowak, S.; Schroeder, H.; Schulz, H.D.; Walter, M.; Wurth, R. (Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)); Appuhn, R.D.; Hast, C.; Kolanoski, H.; Lange, A.; Lindner, A.; Mankel, R.; Schieber, M.; Siegmund, T.; Spaan, B.; Thurn, H.; Toepfer, D.; Walther, A.; Wegener, D. (Dortmund Univ. (Germany). Inst. fuer Physik); Paul

    1992-06-01

    Using the ARGUS detector at the DORIS II storage ring, a new measurement of the mass of the {tau} lepton has been obtained. An analysis of the tan pseudomass spectrum for decays of the type {tau}{sup -} {yields} {pi}{sup -}{pi}{sup -}{pi}{sup +}{nu}{sub {tau}} finds m{sub {tau}} = (1776.3 {+-} 2.4 {+-} 1.4) MeV/c{sup 2}. This result also leads to an improvement of the upper limit on the {nu}{sub {tau}} mass to m{sub {nu}{tau}} < 31 MeV/c{sup 2} at the 95% confidence level. (orig.).

  18. Experiment for a precision neutrino mass measurement

    We describe an experiment which is designed to determine the electron neutrino mass to better than 2 eV. Key features of the experiment are a high activity frozen tritium source and a high resolution electrostatic spectrometer designed to make a careful measurement of the tritium beta decay end point spectrum. The goal is to determine the neutrino mass to better than 1 eV statistically in a four day run. A series of these runs will allow study of potential systematics. The construction phase is nearly complete and preliminary data will be taken in late spring

  19. Top quark mass measurements at the LHC

    Fuster, Juan; The ATLAS collaboration

    2015-01-01

    The latest measurements of the top quark mass using the ATLAS and CMS experiments at the LHC are presented. The discussion includes the results obtained using the conventional methods (Template/Ideogram) and those derived from the so called alternative methods. Results from the conventional methods using the various top final states (lepton+jets, di-lepton and full hadronic) are reviewed. Determinations using the inclusive ttbar production, the ttbar production with an additional jet and the lepton-b-jet invariant mass distribution are also discussed.

  20. Highly accurate measurements of the spontaneous fission half-life of 240,242Pu

    Salvador-Castiñeira, P.; Bryś, T.; Eykens, R.; Hambsch, F.-J.; Moens, A.; Oberstedt, S.; Sibbens, G.; Vanleeuw, D.; Vidali, M.; Pretel, C.

    2013-12-01

    Fast spectrum neutron-induced fission cross-section data for transuranic isotopes are of special demand from the nuclear data community. In particular highly accurate data are needed for the new generation IV nuclear applications. The aim is to obtain precise neutron-induced fission cross sections for 240Pu and 242Pu. To do so, accurate data on spontaneous fission half-lives must be available. Also, minimizing uncertainties in the detector efficiency is a key point. We studied both isotopes by means of a twin Frisch-grid ionization chamber with the goal of improving the present data on the neutron-induced fission cross section. For the two plutonium isotopes the high α-particle decay rates pose a particular problem to experiments due to piling-up events in the counting gas. Argon methane and methane were employed as counting gases, the latter showed considerable improvement in signal generation due to its higher drift velocity. The detection efficiency for both samples was determined, and improved spontaneous fission half-lives were obtained with very low statistical uncertainty (0.13% for 240Pu and 0.04% for 242Pu): for 240Pu, T1/2,SF=1.165×1011 yr (1.1%), and for 242Pu, T1/2,SF=6.74×1010 yr (1.3%). Systematic uncertainties are due to sample mass (0.4% for 240Pu and 0.9% for 242Pu) and efficiency (1%).

  1. Accurate determination of silver nanoparticles in animal tissues by inductively coupled plasma mass spectrometry

    Veverková, Lenka [Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacky University, 17.listopadu 12, CZ 771 46 Olomouc (Czech Republic); Hradilová, Šárka [Regional Centre of Advanced Technologies and Materials, Department of Physical Chemistry, Faculty of Science, Palacky University, 17.listopadu 12, CZ 771 46 Olomouc (Czech Republic); Milde, David, E-mail: david.mlde@upol.cz [Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacky University, 17.listopadu 12, CZ 771 46 Olomouc (Czech Republic); Panáček, Aleš [Regional Centre of Advanced Technologies and Materials, Department of Physical Chemistry, Faculty of Science, Palacky University, 17.listopadu 12, CZ 771 46 Olomouc (Czech Republic); Skopalová, Jana [Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacky University, 17.listopadu 12, CZ 771 46 Olomouc (Czech Republic); Kvítek, Libor [Regional Centre of Advanced Technologies and Materials, Department of Physical Chemistry, Faculty of Science, Palacky University, 17.listopadu 12, CZ 771 46 Olomouc (Czech Republic); Petrželová, Kamila [Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacky University, 17.listopadu 12, CZ 771 46 Olomouc (Czech Republic); National Reference Laboratory for Chemical Elements, Department of Residues in Kroměříž, State Veterinary Institute Olomouc, Hulínská 2286, CZ 767 60 Kroměříž (Czech Republic); and others

    2014-12-01

    This study examined recoveries of silver determination in animal tissues after wet digestion by inductively coupled plasma mass spectrometry. The composition of the mineralization mixture for microwave assisted digestion was optimized and the best recoveries were obtained for mineralization with HNO{sub 3} and addition of HCl promptly after digestion. The optimization was performed on model samples of chicken meat spiked with silver nanoparticles and a solution of ionic silver. Basic calculations of theoretical distribution of Ag among various silver-containing species were implemented and the results showed that most of the silver is in the form of soluble complexes AgCl{sub 2}{sup −} and AgCl{sub 3}{sup 2−} for the optimized composition of the mineralization mixture. Three animal tissue certified reference materials were then analyzed to verify the trueness and precision of the results. - Highlights: • We performed detailed optimization of microwave assisted digestion procedure of animal tissue used prior to Ag determination by ICP-MS. • We provide basic equilibrium calculations to give theoretical explanation of results from optimization of tested mineralization mixtures. • Results from method validation that was done by analysis of several matrix CRMs are presented.

  2. Accurate determination of silver nanoparticles in animal tissues by inductively coupled plasma mass spectrometry

    This study examined recoveries of silver determination in animal tissues after wet digestion by inductively coupled plasma mass spectrometry. The composition of the mineralization mixture for microwave assisted digestion was optimized and the best recoveries were obtained for mineralization with HNO3 and addition of HCl promptly after digestion. The optimization was performed on model samples of chicken meat spiked with silver nanoparticles and a solution of ionic silver. Basic calculations of theoretical distribution of Ag among various silver-containing species were implemented and the results showed that most of the silver is in the form of soluble complexes AgCl2− and AgCl32− for the optimized composition of the mineralization mixture. Three animal tissue certified reference materials were then analyzed to verify the trueness and precision of the results. - Highlights: • We performed detailed optimization of microwave assisted digestion procedure of animal tissue used prior to Ag determination by ICP-MS. • We provide basic equilibrium calculations to give theoretical explanation of results from optimization of tested mineralization mixtures. • Results from method validation that was done by analysis of several matrix CRMs are presented

  3. Interpreting $W$ mass measurements in the SMEFT

    Bjørn, Mikkel

    2016-01-01

    Measurements of the $W^\\pm$ mass ($m_W$) provide an important consistency check of the Standard Model (SM) and constrain the possibility of physics beyond the SM. Precision measurements of $m_W$ at hadron colliders are inferred from kinematic distributions of transverse variables. We examine how this inference is modified when considering the presence of physics beyond the SM expressed in terms of local contact operators. We show that Tevatron measurements of $m_W$ using transverse variables are transparent and applicable as consistent constraints in the Standard Model Effective Field theory (SMEFT) and find the extra error introduced in these measurements due to SMEFT higher dimensional operators to be subdominant to the current experimental systematic errors. This means that the leading challenge to interpreting these measurements in the SMEFT is the pure theoretical uncertainty in how these measurements are mapped to Lagrangian parameters. We stress the need to avoid using naive combinations of Tevatron an...

  4. CLASH-VLT: Insights on the mass substructures in the Frontier Fields Cluster MACS J0416.1-2403 through accurate strong lens modeling

    Grillo, C; Rosati, P; Mercurio, A; Balestra, I; Munari, E; Nonino, M; Caminha, G B; Lombardi, M; De Lucia, G; Borgani, S; Gobat, R; Biviano, A; Girardi, M; Umetsu, K; Coe, D; Koekemoer, A M; Postman, M; Zitrin, A; Halkola, A; Broadhurst, T; Sartoris, B; Presotto, V; Annunziatella, M; Maier, C; Fritz, A; Vanzella, E; Frye, B

    2014-01-01

    We present a detailed mass reconstruction and a novel study on the substructure properties in the core of the CLASH and Frontier Fields galaxy cluster MACS J0416.1-2403. We show and employ our extensive spectroscopic data set taken with the VIMOS instrument as part of our CLASH-VLT program, to confirm spectroscopically 10 strong lensing systems and to select a sample of 175 plausible cluster members to a limiting stellar mass of log(M_*/M_Sun) ~ 8.6. We reproduce the measured positions of 30 multiple images with a remarkable median offset of only 0.3" by means of a comprehensive strong lensing model comprised of 2 cluster dark-matter halos, represented by cored elliptical pseudo-isothermal mass distributions, and the cluster member components. The latter have total mass-to-light ratios increasing with the galaxy HST/WFC3 near-IR (F160W) luminosities. The measurement of the total enclosed mass within the Einstein radius is accurate to ~5%, including systematic uncertainties. We emphasize that the use of multip...

  5. Accurate Young's modulus measurement based on Rayleigh wave velocity and empirical Poisson's ratio

    Li, Mingxia; Feng, Zhihua

    2016-07-01

    This paper presents a method for Young's modulus measurement based on Rayleigh wave speed. The error in Poisson's ratio has weak influence on the measurement of Young's modulus based on Rayleigh wave speed, and Poisson's ratio minimally varies in a certain material; thus, we can accurately estimate Young's modulus with surface wave speed and a rough Poisson's ratio. We numerically analysed three methods using Rayleigh, longitudinal, and transversal wave speed, respectively, and the error in Poisson's ratio shows the least influence on the result in the method involving Rayleigh wave speed. An experiment was performed and has proved the feasibility of this method. Device for speed measuring could be small, and no sample pretreatment is needed. Hence, developing a portable instrument based on this method is possible. This method makes a good compromise between usability and precision.

  6. Accurate 3D shape measurement of multiple separate objects with stereo vision

    3D shape measurement has emerged as a very useful tool in numerous fields because of its wide and ever-increasing applications. In this paper, we present a passive, fast and accurate 3D shape measurement technique using stereo vision approach. The technique first employs a scale-invariant feature transform algorithm to detect point matches at a number of discrete locations despite the discontinuities in the images. Then an automated image registration algorithm is applied to find full-field point matches with subpixel accuracy. After that, the 3D shapes of the objects can be reconstructed according to the obtained point matching and the camera information. The proposed technique is capable of performing a full-field 3D shape measurement with high accuracy even in the presence of discontinuities and multiple separate regions. The validity is verified by experiments. (paper)

  7. Comparison of thermistor linearization techniques for accurate temperature measurement in phase change materials

    Alternate energy technologies are developing rapidly in the recent years. A significant part of this trend is the development of different phase change materials (PCMs). Proper utilization of PCMs requires accurate thermal characterization. There are several methodologies used in this field. This paper stresses the importance of accurate temperature measurements during the implementation of T-history method. Since the temperature sensor size is also important thermistors have been selected as the sensing modality. Two thermistor linearization techniques, one based on Wheatstone bridge and the other based on simple serial-parallel resistor connection, are compared in terms of achievable temperature accuracy through consideration of both, nonlinearity and self-heating errors. Proper calibration was performed before T-history measurement of RT21 (RUBITHERM (registered) GmbH) PCM. Measurement results suggest that the utilization of serial-parallel resistor connection gives better accuracy (less than ±0.1 deg. C) in comparison with the Wheatstone bridge based configuration (up to ±1.5 deg. C).

  8. A Flexible Fringe Projection Vision System with Extended Mathematical Model for Accurate Three-Dimensional Measurement.

    Xiao, Suzhi; Tao, Wei; Zhao, Hui

    2016-01-01

    In order to acquire an accurate three-dimensional (3D) measurement, the traditional fringe projection technique applies complex and laborious procedures to compensate for the errors that exist in the vision system. However, the error sources in the vision system are very complex, such as lens distortion, lens defocus, and fringe pattern nonsinusoidality. Some errors cannot even be explained or rendered with clear expressions and are difficult to compensate directly as a result. In this paper, an approach is proposed that avoids the complex and laborious compensation procedure for error sources but still promises accurate 3D measurement. It is realized by the mathematical model extension technique. The parameters of the extended mathematical model for the 'phase to 3D coordinates transformation' are derived using the least-squares parameter estimation algorithm. In addition, a phase-coding method based on a frequency analysis is proposed for the absolute phase map retrieval to spatially isolated objects. The results demonstrate the validity and the accuracy of the proposed flexible fringe projection vision system on spatially continuous and discontinuous objects for 3D measurement. PMID:27136553

  9. Phase Measurement for Accurate Mapping of Chemical Bonds in Acentric Space Groups

    Although the electron density is fundamental to the study of chemical bonding and density-functional theory, it cannot be accurately mapped experimentally for the important class of crystals lacking inversion symmetry, since structure factor phase information is normally inaccessible. We report the combination of x-ray and electron diffraction experiments for the determination of the electron density in acentric AlN, using multiple-scattering effects in convergent-beam electron diffraction to obtain sensitivity to structure factor phases, and describe a new error metric and weighting scheme for multipole refinement using combined measurements of structure factor magnitudes and phases

  10. Accurate macromolecular structures using minimal measurements from X-ray free-electron lasers

    Hattne, Johan; Echols, Nathaniel; Tran, Rosalie; Kern, Jan; Gildea, Richard J.; Brewster, Aaron S.; Alonso-Mori, Roberto; Glöckner, Carina; Hellmich, Julia; Laksmono, Hartawan; Sierra, Raymond G.; Lassalle-Kaiser, Benedikt; Lampe, Alyssa; Han, Guangye; Gul, Sheraz; DiFiore, Dörte; Milathianaki, Despina; Fry, Alan R.; Miahnahri, Alan; White, William E.; Schafer, Donald W.; Seibert, M. Marvin; Koglin, Jason E.; Sokaras, Dimosthenis; Weng, Tsu-Chien; Sellberg, Jonas; Latimer, Matthew J.; Glatzel, Pieter; Zwart, Petrus H.; Grosse-Kunstleve, Ralf W.; Bogan, Michael J.; Messerschmidt, Marc; Williams, Garth J.; Boutet, Sébastien; Messinger, Johannes; Zouni, Athina; Yano, Junko; Bergmann, Uwe; Yachandra, Vittal K.; Adams, Paul D.; Sauter, Nicholas K.

    2014-01-01

    X-ray free-electron laser (XFEL) sources enable the use of crystallography to solve three-dimensional macromolecular structures under native conditions and free from radiation damage. Results to date, however, have been limited by the challenge of deriving accurate Bragg intensities from a heterogeneous population of microcrystals, while at the same time modeling the X-ray spectrum and detector geometry. Here we present a computational approach designed to extract statistically significant high-resolution signals from fewer diffraction measurements. PMID:24633409

  11. Designer cantilevers for even more accurate quantitative measurements of biological systems with multifrequency AFM

    Contera, S.

    2016-04-01

    Multifrequency excitation/monitoring of cantilevers has made it possible both to achieve fast, relatively simple, nanometre-resolution quantitative mapping of mechanical of biological systems in solution using atomic force microscopy (AFM), and single molecule resolution detection by nanomechanical biosensors. A recent paper by Penedo et al [2015 Nanotechnology 26 485706] has made a significant contribution by developing simple methods to improve the signal to noise ratio in liquid environments, by selectively enhancing cantilever modes, which will lead to even more accurate quantitative measurements.

  12. A simple and accurate measurement method of current density of an electron accelerator for irradiation

    For simple and accurate measurement of the current distribution in a broad beam from electron accelerators, a method for detecting the charge absorbed in a graphite target exposed to the air has been examined. The present report means to solve several fundamental problems. The effective incidence area of the absorber is strictly defined by the design of the geometrical arrangement of the absorber assembly. Electron backscattering from the absorber is corrected with backscattering coefficients in consideration of oblique incidence on the absorber. The influence of ionic charge produced in air is ascribed to the contact potential between the absorber and the guard, and correction methods are proposed. (orig.)

  13. Accurate measurements of surface emission rate for large-area alpha and beta reference sources

    For alpha emitters and beta emitters with maximum beta energy greater than 0.150 MeV, the characteristics of reference sources for the calibration of surface contamination monitors are specified by the international standard ISO 8769. According to this standard, the surface emission rate of reference sources has to be measured by absolute methods or by using an instrument that has been calibrated by means of sources that has been measured absolutely. Moreover, the surface emission rate has to be measured by the national standards laboratory with an uncertainty which must not exceed 3% (one standard deviation). In this paper, the counting system and the experimental conditions needed for accurate measurements of the surface emission rate are presented. The uncertainty of such measurements is much smaller than 3%. The evaluation of this uncertainty is also described. The counting system used for absolute alpha and beta surface emission rate measurements is composed of a large area, gas-flow, windowless proportional detector, an integral and a spectrometric counting channels. The method of measurement for alpha and beta surface emission rate is very simple but it is necessary to achieve the optimum experimental conditions of counting for obtaining accurate measurement results. Thus, the proportional detector has to work under a continuous and stable gas-flow and its plateau has to be long with a very low slope. To obtain a counting efficiency of 100%, it has to use a tight detector and a very pure counting gas. Additionally, the detector must be flushed and then operated under a steady gas-flow for several hours prior to measurements in order to be cleaned of air impurities. To perform alpha and beta surface emission rate measurements we optimized first the conditions of counting. For beta sources, the discrimination level has been adjusted by means of a 55 Fe source. Using this spectrum, we checked the stability of the counting system because the peak, corresponding

  14. Ocean Lidar Measurements of Beam Attenuation and a Roadmap to Accurate Phytoplankton Biomass Estimates

    Hu, Yongxiang; Behrenfeld, Mike; Hostetler, Chris; Pelon, Jacques; Trepte, Charles; Hair, John; Slade, Wayne; Cetinic, Ivona; Vaughan, Mark; Lu, Xiaomei; Zhai, Pengwang; Weimer, Carl; Winker, David; Verhappen, Carolus C.; Butler, Carolyn; Liu, Zhaoyan; Hunt, Bill; Omar, Ali; Rodier, Sharon; Lifermann, Anne; Josset, Damien; Hou, Weilin; MacDonnell, David; Rhew, Ray

    2016-06-01

    Beam attenuation coefficient, c, provides an important optical index of plankton standing stocks, such as phytoplankton biomass and total particulate carbon concentration. Unfortunately, c has proven difficult to quantify through remote sensing. Here, we introduce an innovative approach for estimating c using lidar depolarization measurements and diffuse attenuation coefficients from ocean color products or lidar measurements of Brillouin scattering. The new approach is based on a theoretical formula established from Monte Carlo simulations that links the depolarization ratio of sea water to the ratio of diffuse attenuation Kd and beam attenuation C (i.e., a multiple scattering factor). On July 17, 2014, the CALIPSO satellite was tilted 30° off-nadir for one nighttime orbit in order to minimize ocean surface backscatter and demonstrate the lidar ocean subsurface measurement concept from space. Depolarization ratios of ocean subsurface backscatter are measured accurately. Beam attenuation coefficients computed from the depolarization ratio measurements compare well with empirical estimates from ocean color measurements. We further verify the beam attenuation coefficient retrievals using aircraft-based high spectral resolution lidar (HSRL) data that are collocated with in-water optical measurements.

  15. Accurate mass fragment library for rapid analysis of pesticides on produce using ambient pressure desorption ionization with high-resolution mass spectrometry.

    Kern, Sara E; Lin, Lora A; Fricke, Frederick L

    2014-08-01

    U.S. food imports have been increasing steadily for decades, intensifying the need for a rapid and sensitive screening technique. A method has been developed that uses foam disks to sample the surface of incoming produce. This work provides complimentary information to the extensive amount of published pesticide fragmentation data collected using LCMS systems (Sack et al. Journal of Agricultural and Food Chemistry, 59, 6383-6411, 2011; Mol et al. Analytical and Bioanalytical Chemistry, 403, 2891-2908, 2012). The disks are directly analyzed using transmission-mode direct analysis in real time (DART) ambient pressure desorption ionization coupled to a high resolution accurate mass-mass spectrometer (HRAM-MS). In order to provide more certainty in the identification of the pesticides detected, a library of accurate mass fragments and isotopes of the protonated parent molecular ion (the [M+H]⁺) has been developed. The HRAM-MS is equipped with a quadrupole mass filter, providing the capability of "data-dependent" fragmentation, as opposed to "all -ion" fragmentation (where all of the ions enter a collision chamber and are fragmented at once). A temperature gradient for the DART helium stream and multiple collision energies were employed to detect and fragment 164 pesticides of varying chemical classes, sizes, and polarities. The accurate mass information of precursor ([M+H]⁺ ion) and fragment ions is essential in correctly identifying chemical contaminants on the surface of imported produce. Additionally, the inclusion of isotopes of the [M+H]⁺ in the database adds another metric to the confirmation process. The fragmentation data were collected using a Q-Exactive mass spectrometer and were added to a database used to process data collected with an Exactive mass spectrometer, an instrument that is more readily available for this screening application. The commodities investigated range from smooth-skinned produce such as apples to rougher surfaces like broccoli

  16. Accurate Mass Fragment Library for Rapid Analysis of Pesticides on Produce Using Ambient Pressure Desorption Ionization with High-Resolution Mass Spectrometry

    Kern, Sara E.; Lin, Lora A.; Fricke, Frederick L.

    2014-08-01

    U.S. food imports have been increasing steadily for decades, intensifying the need for a rapid and sensitive screening technique. A method has been developed that uses foam disks to sample the surface of incoming produce. This work provides complimentary information to the extensive amount of published pesticide fragmentation data collected using LCMS systems (Sack et al. Journal of Agricultural and Food Chemistry, 59, 6383-6411, 2011; Mol et al. Analytical and Bioanalytical Chemistry, 403, 2891-2908, 2012). The disks are directly analyzed using transmission-mode direct analysis in real time (DART) ambient pressure desorption ionization coupled to a high resolution accurate mass-mass spectrometer (HRAM-MS). In order to provide more certainty in the identification of the pesticides detected, a library of accurate mass fragments and isotopes of the protonated parent molecular ion (the [M+H]+) has been developed. The HRAM-MS is equipped with a quadrupole mass filter, providing the capability of "data-dependent" fragmentation, as opposed to "all -ion" fragmentation (where all of the ions enter a collision chamber and are fragmented at once). A temperature gradient for the DART helium stream and multiple collision energies were employed to detect and fragment 164 pesticides of varying chemical classes, sizes, and polarities. The accurate mass information of precursor ([M+H]+ ion) and fragment ions is essential in correctly identifying chemical contaminants on the surface of imported produce. Additionally, the inclusion of isotopes of the [M+H]+ in the database adds another metric to the confirmation process. The fragmentation data were collected using a Q-Exactive mass spectrometer and were added to a database used to process data collected with an Exactive mass spectrometer, an instrument that is more readily available for this screening application. The commodities investigated range from smooth-skinned produce such as apples to rougher surfaces like broccoli. The

  17. Fourier Transform Mass Spectrometry and Nuclear Magnetic Resonance Analysis for the Rapid and Accurate Characterization of Hexacosanoylceramide

    Ross, Charles W.; Simonsick, William J.; Bogusky, Michael J.; Celikay, Recep W.; Guare, James P.; Newton, Randall C.

    2016-01-01

    Ceramides are a central unit of all sphingolipids which have been identified as sites of biological recognition on cellular membranes mediating cell growth and differentiation. Several glycosphingolipids have been isolated, displaying immunomodulatory and anti-tumor activities. These molecules have generated considerable interest as potential vaccine adjuvants in humans. Accurate analyses of these and related sphingosine analogues are important for the characterization of structure, biological function, and metabolism. We report the complementary use of direct laser desorption ionization (DLDI), sheath flow electrospray ionization (ESI) Fourier transform ion cyclotron resonance mass spectrometry (FTICR MS) and high-field nuclear magnetic resonance (NMR) analysis for the rapid, accurate identification of hexacosanoylceramide and starting materials. DLDI does not require stringent sample preparation and yields representative ions. Sheath-flow ESI yields ions of the product and byproducts and was significantly better than monospray ESI due to improved compound solubility. Negative ion sheath flow ESI provided data of starting materials and products all in one acquisition as hexacosanoic acid does not ionize efficiently when ceramides are present. NMR provided characterization of these lipid molecules complementing the results obtained from MS analyses. NMR data was able to differentiate straight chain versus branched chain alkyl groups not easily obtained from mass spectrometry. PMID:27367671

  18. Fourier Transform Mass Spectrometry and Nuclear Magnetic Resonance Analysis for the Rapid and Accurate Characterization of Hexacosanoylceramide

    Charles W. Ross

    2016-06-01

    Full Text Available Ceramides are a central unit of all sphingolipids which have been identified as sites of biological recognition on cellular membranes mediating cell growth and differentiation. Several glycosphingolipids have been isolated, displaying immunomodulatory and anti-tumor activities. These molecules have generated considerable interest as potential vaccine adjuvants in humans. Accurate analyses of these and related sphingosine analogues are important for the characterization of structure, biological function, and metabolism. We report the complementary use of direct laser desorption ionization (DLDI, sheath flow electrospray ionization (ESI Fourier transform ion cyclotron resonance mass spectrometry (FTICR MS and high-field nuclear magnetic resonance (NMR analysis for the rapid, accurate identification of hexacosanoylceramide and starting materials. DLDI does not require stringent sample preparation and yields representative ions. Sheath-flow ESI yields ions of the product and byproducts and was significantly better than monospray ESI due to improved compound solubility. Negative ion sheath flow ESI provided data of starting materials and products all in one acquisition as hexacosanoic acid does not ionize efficiently when ceramides are present. NMR provided characterization of these lipid molecules complementing the results obtained from MS analyses. NMR data was able to differentiate straight chain versus branched chain alkyl groups not easily obtained from mass spectrometry.

  19. Precision mass measurements utilizing beta endpoints

    A technique for precise determination of beta endpoints with an intrinsic germanium detector has been developed. The energy calibration was derived from γ-ray photopeak measurements. This analysis procedure has been checked with a 27Si source produced in a (p,n) reaction on an 27Al target and subsequently applied to mass separated samples of 76Rb, 77Rb and 78Rb. Results indicate errors < 50 keV are obtainable. (orig.)

  20. Accurate heat transfer measurements using thermochromic liquid crystal. Part 1: Calibration and characteristics of crystals

    Kakade, V.U. [Department of Mechanical Engineering, University of Bath, Bath, BA2 7AY (United Kingdom); Lock, G.D. [Department of Mechanical Engineering, University of Bath, Bath, BA2 7AY (United Kingdom)], E-mail: ensgdl@bath.ac.uk; Wilson, M.; Owen, J.M.; Mayhew, J.E. [Department of Mechanical Engineering, University of Bath, Bath, BA2 7AY (United Kingdom)

    2009-10-15

    Encapsulated thermochromic liquid crystal (TLC) can accurately measure surface temperature in a variety of heat transfer and fluid flow experiments. Narrow-band TLC, where the colour changes over a temperature range of {approx}1 deg. C, can be used to determine surface temperature within an uncertainty of 0.1 deg. C. Wide-band TLC, typically active over 5-20 deg. C, allow the possibility of mapping surface temperature distributions. In part 1 of this two-part paper, an extensive set of calibrations for narrow-band and wide-band TLC is reported. This generic study provides insight into the importance and influence of the various factors governing the colour-temperature relationship. These governing effects include the variation in optical path, the spectrum of the illumination source, the lighting and viewing angles, the differences between cooling or heating cycles (hysteresis), the variation with the number of heating or cooling cycles (aging) and how this varies with TLC film thickness. Two narrow-band crystals are also specifically calibrated for application to experiments on a transparent disc rotating at high speed ({approx}5000 rpm). Part 2 of this paper describes how these accurately-calibrated crystals were used to measure the transient surface temperature on, and heat transfer to, a rotating disc.

  1. Accurate heat transfer measurements using thermochromic liquid crystal. Part 1: Calibration and characteristics of crystals

    Encapsulated thermochromic liquid crystal (TLC) can accurately measure surface temperature in a variety of heat transfer and fluid flow experiments. Narrow-band TLC, where the colour changes over a temperature range of ∼1 deg. C, can be used to determine surface temperature within an uncertainty of 0.1 deg. C. Wide-band TLC, typically active over 5-20 deg. C, allow the possibility of mapping surface temperature distributions. In part 1 of this two-part paper, an extensive set of calibrations for narrow-band and wide-band TLC is reported. This generic study provides insight into the importance and influence of the various factors governing the colour-temperature relationship. These governing effects include the variation in optical path, the spectrum of the illumination source, the lighting and viewing angles, the differences between cooling or heating cycles (hysteresis), the variation with the number of heating or cooling cycles (aging) and how this varies with TLC film thickness. Two narrow-band crystals are also specifically calibrated for application to experiments on a transparent disc rotating at high speed (∼5000 rpm). Part 2 of this paper describes how these accurately-calibrated crystals were used to measure the transient surface temperature on, and heat transfer to, a rotating disc.

  2. Comprehensive two-dimensional liquid chromatography tandem diode array detector (DAD) and accurate mass QTOF-MS for the analysis of flavonoids and iridoid glycosides in Hedyotis diffusa.

    Li, Duxin; Schmitz, Oliver J

    2015-01-01

    The analysis of chemical constituents in Chinese herbal medicines (CHMs) is a challenge because of numerous compounds with various polarities and functional groups. Liquid chromatography coupled with quadrupole time-of-flight (QTOF) mass spectrometry (LC/MS) is of particular interest in the analysis of herbal components. One of the main attributes of QTOF that makes it an attractive analytical technique is its accurate mass measurement for both precursor and product ions. For the separation of CHMs, comprehensive two-dimensional chromatography (LCxLC) provides much higher resolving power than traditional one-dimensional separation. Therefore, a LCxLC-QTOF-MS system was developed and applied to the analysis of flavonoids and iridoid glycosides in aqueous extracts of Hedyotis diffusa (Rubiaceae). Shift gradient was applied in the two-dimensional separation in the LCxLC system to increase the orthogonality and effective peak distribution area of the analysis. Tentative identification of compounds was done by accurate mass interpretation and validation by UV spectrum. A clear classification of flavonol glycosides (FGs), acylated FGs, and iridoid glycosides (IGs) was shown in different regions of the LCxLC contour plot. In total, five FGs, four acylated FGs, and three IGs were tentatively identified. In addition, several novel flavonoids were found, which demonstrates that LCxLC-QTOF-MS detection also has great potential in herbal medicine analysis. PMID:25171829

  3. Wide-band mass measurements with a multi-reflection time-of-flight mass spectrograph

    Schury, P.; Ito, Y.; Wada, M; Wollnik, H.

    2013-01-01

    We characterize the mass bandwidth of the a multi-reflection time-of-flight mass spectrograph, showing both the functional and useful mass bandwidth. We then demonstrate the use of a multi-reflection time-of-flight mass spectrograph to perform mass measurements in mass bands much wider than the mass bandwidth.

  4. ACCURATE: Greenhouse Gas Profiles Retrieval from Combined IR-Laser and Microwave Occultation Measurements

    Proschek, Veronika; Kirchengast, Gottfried; Schweitzer, Susanne; Fritzer, Johannes

    2010-05-01

    The new climate satellite concept ACCURATE (Atmospheric Climate and Chemistry in the UTLS Region And climate Trends Explorer) enables simultaneous measurement of profiles of greenhouse gases, isotopes, wind and thermodynamic variables from Low Earth Orbit (LEO) satellites. The measurement principle applied is a combination of the novel LEO-LEO infrared laser occultation (LIO) technique and the already better studied LEO-LEO microwave occultation (LMO) technique. Resulting occultation events are evenly distributed around the world, have high vertical resolution and accuracy and are stable over long time periods. The LIO uses near-monochromatic signals in the short-wave infrared range (~2-2.5 μm for ACCURATE). These signals are absorbed by various trace species in the Earth's atmosphere. Profiles of the concentration of the absorbing species can be derived from signal transmission measurements. Accurately known temperature, pressure and humidity profiles derived from simultaneously measured LMO signals are essential pre-information for the retrieval of the trace species profiles. These LMO signals lie in the microwave band region from 17-23 GHz and, optionally, 178-195 GHz. The current ACCURATE mission design is arranged for the measurement of six greenhouse gases (GHG) (H2O, CO2, CH4, N2O, O3, CO) and four isotopes (13CO2, C18OO, HDO, H218O), with focus on the upper troposphere/lower stratosphere region (UTLS, 5-35 km). Wind speed in line-of-sight can be derived from a line-symmetric transmission difference which is caused by wind-induced Doppler shift. By-products are information on cloud layering, aerosol extinction, and scintillation strength. We introduce the methodology to retrieve GHG profiles from quasi-realistic forward-simulated intensities of LIO signals and thermodynamic profiles retrieved in a preceding step from LMO signals. Key of the retrieval methodology is the differencing of two LIO transmission signals, one being GHG sensitive on a target

  5. An accurate measurement of PMT TTS based on the photoelectron spectrum

    Huang, Wei-Ping; Tang, Ze-Bo; Li, Cheng; Jiang, Kun; Zhao, Xiao-Kun; Wang, Peng-Fei

    2015-06-01

    The water Cherenkov detector array (WCDA) for the Large High Altitude Air Shower Observatory (LHAASO) will employ more than 3600 hemisphere 8-inch photomultiplier tubes (PMTs). Good time performance of the PMT, especially the transit time spread (TTS), is required for the WCDA. In order to meet the demand of the WCDA experiment, an accurate measurement of PMT TTS based on the photoelectron spectrum is studied. The method is appropriate for multi-photoelectrons and makes it possible to measure the TTS of different photoelectrons simultaneously. The TTS of different photoelectrons for a Hamamatsu R5912 PMT is tested with a specially designed divider circuit. The relationship between TTS and number of photoelectrons is also presented in this paper. Supported by Natural Science Foundation of China (11275196) and “Strategic Priority Program” of the Chinese Academy of Sciences (XDA03010100)

  6. Accurate Resolution Measurement for X-Ray Micro-CT Systems

    Sharma, K. Sen; Seshadri, S.; Feser, M.; Wang, G.

    2011-09-01

    Accurate measurement of modulation transfer function (MTF), or alternatively point spread function, of an x-ray micro-CT system is essential for various purposes—to determine scanner resolution, to retrieve further information about a scanned object by image-processing, etc. In this paper, a new method for MTF measurement is proposed that can be used with any resolution pattern and is more adept at studying MTF spatial variation than the traditional method of using bar pattern analysis. A resolution target used to determine micro-CT resolution was scanned in a lab-based nano-CT system—the image from the nano-CT gave the `ground truth'. The ground truth was quantitavely compared with the micro-CT projection of same target to determine the point spread function of the system. Results matched well with bar pattern analysis, but the new method was able to study spatial variations while the bar pattern analysis failed.

  7. Highly accurate thickness measurement of multi-layered automotive paints using terahertz technology

    Krimi, Soufiene; Klier, Jens; Jonuscheit, Joachim; von Freymann, Georg; Urbansky, Ralph; Beigang, René

    2016-07-01

    In this contribution, we present a highly accurate approach for thickness measurements of multi-layered automotive paints using terahertz time domain spectroscopy in reflection geometry. The proposed method combines the benefits of a model-based material parameters extraction method to calibrate the paint coatings, a generalized Rouard's method to simulate the terahertz radiation behavior within arbitrary thin films, and the robustness of a powerful evolutionary optimization algorithm to increase the sensitivity of the minimum thickness measurement limit. Within the framework of this work, a self-calibration model is introduced, which takes into consideration the real industrial challenges such as the effect of wet-on-wet spray in the painting process.

  8. Generalized weighted ratio method for accurate turbidity measurement over a wide range.

    Liu, Hongbo; Yang, Ping; Song, Hong; Guo, Yilu; Zhan, Shuyue; Huang, Hui; Wang, Hangzhou; Tao, Bangyi; Mu, Quanquan; Xu, Jing; Li, Dejun; Chen, Ying

    2015-12-14

    Turbidity measurement is important for water quality assessment, food safety, medicine, ocean monitoring, etc. In this paper, a method that accurately estimates the turbidity over a wide range is proposed, where the turbidity of the sample is represented as a weighted ratio of the scattered light intensities at a series of angles. An improvement in the accuracy is achieved by expanding the structure of the ratio function, thus adding more flexibility to the turbidity-intensity fitting. Experiments have been carried out with an 850 nm laser and a power meter fixed on a turntable to measure the light intensity at different angles. The results show that the relative estimation error of the proposed method is 0.58% on average for a four-angle intensity combination for all test samples with a turbidity ranging from 160 NTU to 4000 NTU. PMID:26699060

  9. Accurate mass screening and identification of emerging contaminants in environmental samples by liquid chromatography-hybrid linear ion trap Orbitrap mass spectrometry.

    Hogenboom, A C; van Leerdam, J A; de Voogt, P

    2009-01-16

    The European Reach legislation will possibly drive producers to develop newly designed chemicals that will be less persistent, bioaccumulative or toxic. If this innovation leads to an increased use of more hydrophilic chemicals it may result in higher mobilities of chemicals in the aqueous environment. As a result, the drinking water companies may face stronger demands on removal processes as the hydrophilic compounds inherently are more difficult to remove. Monitoring efforts will also experience a shift in focus to more water-soluble compounds. Screening source waters on the presence of (emerging) contaminants is an essential step in the control of the water cycle from source to tap water. In this article, some of our experiences are presented with the hybrid linear ion trap (LTQ) FT Orbitrap mass spectrometer, in the area of chemical water analysis. A two-pronged strategy in mass spectrometric research was employed: (i) exploring effluent, surface, ground- and drinking-water samples searching for accurate masses corresponding to target compounds (and their product ions) known from, e.g. priority lists or the scientific literature and (ii) full-scan screening of water samples in search of 'unknown' or unexpected masses, followed by MS(n) experiments to elucidate the structure of the unknowns. Applications of both approaches to emerging water contaminants are presented and discussed. Results are presented for target analysis search for pharmaceuticals, benzotriazoles, illicit drugs and for the identification of unknown compounds in a groundwater sample and in a polar extract of a landfill soil sample (a toxicity identification evaluation bioassay sample). The applications of accurate mass screening and identification described in this article demonstrate that the LC-LTQ FT Orbitrap MS is well equipped to meet the challenges posed by newly emerging polar contaminants. PMID:18771771

  10. Isotopic Ratio Outlier Analysis of the S. cerevisiae Metabolome Using Accurate Mass Gas Chromatography/Time-of-Flight Mass Spectrometry: A New Method for Discovery.

    Qiu, Yunping; Moir, Robyn; Willis, Ian; Beecher, Chris; Tsai, Yu-Hsuan; Garrett, Timothy J; Yost, Richard A; Kurland, Irwin J

    2016-03-01

    Isotopic ratio outlier analysis (IROA) is a (13)C metabolomics profiling method that eliminates sample to sample variance, discriminates against noise and artifacts, and improves identification of compounds, previously done with accurate mass liquid chromatography/mass spectrometry (LC/MS). This is the first report using IROA technology in combination with accurate mass gas chromatography/time-of-flight mass spectrometry (GC/TOF-MS), here used to examine the S. cerevisiae metabolome. S. cerevisiae was grown in YNB media, containing randomized 95% (13)C, or 5%(13)C glucose as the single carbon source, in order that the isotopomer pattern of all metabolites would mirror the labeled glucose. When these IROA experiments are combined, the abundance of the heavy isotopologues in the 5%(13)C extracts, or light isotopologues in the 95%(13)C extracts, follows the binomial distribution, showing mirrored peak pairs for the molecular ion. The mass difference between the (12)C monoisotopic and the (13)C monoisotopic equals the number of carbons in the molecules. The IROA-GC/MS protocol developed, using both chemical and electron ionization, extends the information acquired from the isotopic peak patterns for formulas generation. The process that can be formulated as an algorithm, in which the number of carbons, as well as the number of methoximations and silylations are used as search constraints. In electron impact (EI/IROA) spectra, the artifactual peaks are identified and easily removed, which has the potential to generate "clean" EI libraries. The combination of chemical ionization (CI) IROA and EI/IROA affords a metabolite identification procedure that enables the identification of coeluting metabolites, and allowed us to characterize 126 metabolites in the current study. PMID:26820234

  11. A solution for measuring accurate reaction time to visual stimuli realized with a programmable microcontroller.

    Ohyanagi, Toshio; Sengoku, Yasuhito

    2010-02-01

    This article presents a new solution for measuring accurate reaction time (SMART) to visual stimuli. The SMART is a USB device realized with a Cypress Programmable System-on-Chip (PSoC) mixed-signal array programmable microcontroller. A brief overview of the hardware and firmware of the PSoC is provided, together with the results of three experiments. In Experiment 1, we investigated the timing accuracy of the SMART in measuring reaction time (RT) under different conditions of operating systems (OSs; Windows XP or Vista) and monitor displays (a CRT or an LCD). The results indicated that the timing error in measuring RT by the SMART was less than 2 msec, on average, under all combinations of OS and display and that the SMART was tolerant to jitter and noise. In Experiment 2, we tested the SMART with 8 participants. The results indicated that there was no significant difference among RTs obtained with the SMART under the different conditions of OS and display. In Experiment 3, we used Microsoft (MS) PowerPoint to present visual stimuli on the display. We found no significant difference in RTs obtained using MS DirectX technology versus using the PowerPoint file with the SMART. We are certain that the SMART is a simple and practical solution for measuring RTs accurately. Although there are some restrictions in using the SMART with RT paradigms, the SMART is capable of providing both researchers and health professionals working in clinical settings with new ways of using RT paradigms in their work. PMID:20160303

  12. Limitations on Precision Cosmology using Mass Measurements of Galaxy Clusters

    Hallman, E J; Burns, J O; Norman, M L; Hallman, Eric J.; Motl, Patrick M.; Burns, Jack O.; Norman, Michael L.

    2005-01-01

    We critically analyze the role of clusters of galaxies as probes for precision cosmology. Using synthetic observations of numerically simulated clusters viewed through their X-ray emission and thermal Sunyaev-Zeldovich effect (SZE), we reduce the observations to attain measurements of the cluster gas mass. We utilize both parametric models such as the isothermal cluster model and non-parametric models that involve the geometric deprojection of the cluster emission assuming spherical symmetry. We are thus able to quantify the possible sources of uncertainty and systematic bias associated with the common simplifying assumptions used in reducing real cluster observations including isothermality and hydrostatic equilibrium. We find that intrinsic variations in clusters limit the precision of observational gas mass estimation to ~10% to 80% confidence excluding instrumental effects. For the full cluster sample, methods that use SZE profiles out to roughly the virial radius are the most accurate and precise way to ...

  13. Top mass measurements at the Tevatron run II

    Velev, Gueorgui V.; /Fermilab

    2005-10-01

    The latest top quark mass measurements by the CDF and D0 experiments are presented here. The mass has been determined in the dilepton (t{bar t} {yields} e{mu}, ee, {mu}{mu} + jets + E{sub T}) and lepton plus jets (t{bar t} {yields} e or {mu} + jets + E{sub T}) final states. The most accurate single result from lepton plus jets channel is 173.5{sub -3.6}{sup +3.7}(stat. + Jet Energy Scale Systematic) {+-} 1.3(syst.) GeV/c{sup 2}, which is better than the combined CDF and D0 Run I average. A preliminary and unofficial average of the best experimental Run II results gives M{sub top} = 172.7 {+-} 3.5 GeV/c{sup 2}.

  14. Accurate measurements of 129I concentration by isotope dilution using MC-ICPMS for half-life determination

    Determining the 129I concentration, a long-lived radionuclide present in spent nuclear fuel, is a major issue for nuclear waste disposal purpose. 129I also has to be measured in numerous environmental, nuclear and biological samples. To be able to accurately determine the 129I concentration, an analytical method based on the use of a multicollector-inductively coupled plasma mass spectrometer (MC-ICPMS) combined with an isotope dilution technique using an 127I spike, was developed. First, the influence of different media (HNO3, NaOH and TMAH) on natural 127I signal intensity and stability and on memory effects was studied. Then an analytical procedure was developed by taking into account the correction of blanks and interferences. Tellurium was chosen for instrumental mass bias correction, as no certified standards with suitable 127I/129I ratio are available. Finally, the results, reproducibility and uncertainties obtained for the 129I concentration determined by isotope dilution with a 127I spike are presented and discussed. The final expanded relative uncertainty obtained for the iodine-129 concentration was lower than 0.7% (k = 1). This precise 129I determination in association with further activity measurements of this nuclide on the same sample will render it possible to determine a new value of the 129I half-life with a reduced uncertainty (0.76%, k = 1).

  15. An accurate measurement of the baryonic Tully-Fisher relation with heavily gas-dominated ALFALFA galaxies

    Papastergis, E; van der Hulst, J M

    2016-01-01

    We use a sample of 97 galaxies selected from the ALFALFA 21cm survey to make an accurate measurement of the baryonic Tully-Fisher relation (BTFR). These galaxies are specifically selected to be heavily gas-dominated (Mgas/M* >~ 2.7) and to be oriented edge-on. The former property ensures that the error on the galactic baryonic mass is small, despite the large systematic uncertainty involved in galactic stellar mass estimates. The latter property means that rotational velocities can be derived directly from the width of the 21cm emission line, without any need for inclination corrections. The resulting linewidth-based BTFR has a slope of alpha = 3.58 +- 0.11, a value that is in agreement with previous literature results. The relation is remarkably tight, with almost all galaxies being located within a perpendicular distance of +- 0.1 dex from the best fit line. The low observational error budget for our sample allows us to establish that, despite its tightness, the measured linewidth-based BTFR has some small ...

  16. Accurate measurements of {sup 129}I concentration by isotope dilution using MC-ICPMS for half-life determination

    Isnard, Helene; Nonell, Anthony; Marie, Mylene [Commissariat a l' Energie Atomique et aux Energies alternatives (CEA), Gif Sur Yvette (France). DEN, DPC, SEARS, LANIE; Chartier, Frederic [Commissariat a l' Energie Atomique et aux Energies alternatives (CEA), Gif Sur Yvette (France). DEN, DPC

    2016-05-01

    Determining the {sup 129}I concentration, a long-lived radionuclide present in spent nuclear fuel, is a major issue for nuclear waste disposal purpose. {sup 129}I also has to be measured in numerous environmental, nuclear and biological samples. To be able to accurately determine the {sup 129}I concentration, an analytical method based on the use of a multicollector-inductively coupled plasma mass spectrometer (MC-ICPMS) combined with an isotope dilution technique using an {sup 127}I spike, was developed. First, the influence of different media (HNO{sub 3}, NaOH and TMAH) on natural {sup 127}I signal intensity and stability and on memory effects was studied. Then an analytical procedure was developed by taking into account the correction of blanks and interferences. Tellurium was chosen for instrumental mass bias correction, as no certified standards with suitable {sup 127}I/{sup 129}I ratio are available. Finally, the results, reproducibility and uncertainties obtained for the {sup 129}I concentration determined by isotope dilution with a {sup 127}I spike are presented and discussed. The final expanded relative uncertainty obtained for the iodine-129 concentration was lower than 0.7% (k = 1). This precise {sup 129}I determination in association with further activity measurements of this nuclide on the same sample will render it possible to determine a new value of the {sup 129}I half-life with a reduced uncertainty (0.76%, k = 1).

  17. Accurate and precise 40Ar/39Ar dating by high-resolution, multi-collection, mass spectrometry

    Storey, Michael; Rivera, Tiffany; Flude, Stephanie

    -Instruments multi-collector Noblesse noble gas mass spectrometer configured with a faraday detector and three ion-counting electron multipliers. The instrument has the capability to measure several noble gas isotopes simultaneously and to change measurement configurations instantaneously by the use of QUAD lenses......New generation, high resolution, multi-collector noble gas mass spectrometers equipped with ion-counting electron multipliers provide opportunities for improved accuracy and precision in 40Ar/39Ar dating. Here we report analytical protocols and age cross-calibration studies using a NU...... (zoom optics). The Noblesse offer several advantages over previous generation noble gas mass spectrometers and is particularly suited for single crystal 40Ar/39Ar dating because of: (i) improved source sensitivity (ii) ion-counting electron multipliers, which have much lower signal to noise ratios than...

  18. Smart density: a more accurate method of measuring rural residential density for health-related research

    Gibson Lucinda

    2010-02-01

    Full Text Available Abstract Background Studies involving the built environment have typically relied on US Census data to measure residential density. However, census geographic units are often unsuited to health-related research, especially in rural areas where development is clustered and discontinuous. Objective We evaluated the accuracy of both standard census methods and alternative GIS-based methods to measure rural density. Methods We compared residential density (units/acre in 335 Vermont school neighborhoods using conventional census geographic units (tract, block group and block with two GIS buffer measures: a 1-kilometer (km circle around the school and a 1-km circle intersected with a 100-meter (m road-network buffer. The accuracy of each method was validated against the actual residential density for each neighborhood based on the Vermont e911 database, which provides an exact geo-location for all residential structures in the state. Results Standard census measures underestimate residential density in rural areas. In addition, the degree of error is inconsistent so even the relative rank of neighborhood densities varies across census measures. Census measures explain only 61% to 66% of the variation in actual residential density. In contrast, GIS buffer measures explain approximately 90% of the variation. Combining a 1-km circle with a road-network buffer provides the closest approximation of actual residential density. Conclusion Residential density based on census units can mask clusters of development in rural areas and distort associations between residential density and health-related behaviors and outcomes. GIS-defined buffers, including a 1-km circle and a road-network buffer, can be used in conjunction with census data to obtain a more accurate measure of residential density.

  19. Measuring Intermediate-Mass Black-Hole Binaries with Advanced Gravitational Wave Detectors.

    Veitch, John; Pürrer, Michael; Mandel, Ilya

    2015-10-01

    We perform a systematic study to explore the accuracy with which the parameters of intermediate-mass black-hole binary systems can be measured from their gravitational wave (GW) signatures using second-generation GW detectors. We make use of the most recent reduced-order models containing inspiral, merger, and ringdown signals of aligned-spin effective-one-body waveforms to significantly speed up the calculations. We explore the phenomenology of the measurement accuracies for binaries with total masses between 50M(⊙) and 500M(⊙) and mass ratios between 0.1 and 1. We find that (i) at total masses below ∼200M(⊙), where the signal-to-noise ratio is dominated by the inspiral portion of the signal, the chirp mass parameter can be accurately measured; (ii) at higher masses, the information content is dominated by the ringdown, and total mass is measured more accurately; (iii) the mass of the lower-mass companion is poorly estimated, especially at high total mass and more extreme mass ratios; and (iv) spin cannot be accurately measured for our injection set with nonspinning components. Most importantly, we find that for binaries with nonspinning components at all values of the mass ratio in the considered range and at a network signal-to-noise ratio of 15, analyzed with spin-aligned templates, the presence of an intermediate-mass black hole with mass >100M(⊙) can be confirmed with 95% confidence in any binary that includes a component with a mass of 130M(⊙) or greater. PMID:26551801

  20. Measuring Intermediate-Mass Black-Hole Binaries with Advanced Gravitational Wave Detectors

    Veitch, John; Pürrer, Michael; Mandel, Ilya

    2015-10-01

    We perform a systematic study to explore the accuracy with which the parameters of intermediate-mass black-hole binary systems can be measured from their gravitational wave (GW) signatures using second-generation GW detectors. We make use of the most recent reduced-order models containing inspiral, merger, and ringdown signals of aligned-spin effective-one-body waveforms to significantly speed up the calculations. We explore the phenomenology of the measurement accuracies for binaries with total masses between 50 M⊙ and 500 M⊙ and mass ratios between 0.1 and 1. We find that (i) at total masses below ˜200 M⊙, where the signal-to-noise ratio is dominated by the inspiral portion of the signal, the chirp mass parameter can be accurately measured; (ii) at higher masses, the information content is dominated by the ringdown, and total mass is measured more accurately; (iii) the mass of the lower-mass companion is poorly estimated, especially at high total mass and more extreme mass ratios; and (iv) spin cannot be accurately measured for our injection set with nonspinning components. Most importantly, we find that for binaries with nonspinning components at all values of the mass ratio in the considered range and at a network signal-to-noise ratio of 15, analyzed with spin-aligned templates, the presence of an intermediate-mass black hole with mass >100 M⊙ can be confirmed with 95% confidence in any binary that includes a component with a mass of 130 M⊙ or greater.

  1. CLASH-VLT: INSIGHTS ON THE MASS SUBSTRUCTURES IN THE FRONTIER FIELDS CLUSTER MACS J0416.1–2403 THROUGH ACCURATE STRONG LENS MODELING

    Grillo, C. [Dark Cosmology Centre, Niels Bohr Institute, University of Copenhagen, Juliane Maries Vej 30, DK-2100 Copenhagen (Denmark); Suyu, S. H.; Umetsu, K. [Institute of Astronomy and Astrophysics, Academia Sinica, P.O. Box 23-141, Taipei 10617, Taiwan (China); Rosati, P.; Caminha, G. B. [Dipartimento di Fisica e Scienze della Terra, Università degli Studi di Ferrara, Via Saragat 1, I-44122 Ferrara (Italy); Mercurio, A. [INAF - Osservatorio Astronomico di Capodimonte, Via Moiariello 16, I-80131 Napoli (Italy); Balestra, I.; Munari, E.; Nonino, M.; De Lucia, G.; Borgani, S.; Biviano, A.; Girardi, M. [INAF - Osservatorio Astronomico di Trieste, via G. B. Tiepolo 11, I-34143, Trieste (Italy); Lombardi, M. [Dipartimento di Fisica, Università degli Studi di Milano, via Celoria 16, I-20133 Milano (Italy); Gobat, R. [Laboratoire AIM-Paris-Saclay, CEA/DSM-CNRS-Universitè Paris Diderot, Irfu/Service d' Astrophysique, CEA Saclay, Orme des Merisiers, F-91191 Gif sur Yvette (France); Coe, D.; Koekemoer, A. M.; Postman, M. [Space Telescope Science Institute, 3700 San Martin Drive, Baltimore, MD 21208 (United States); Zitrin, A. [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, MS 249-17, Pasadena, CA 91125 (United States); Halkola, A., E-mail: grillo@dark-cosmology.dk; and others

    2015-02-10

    We present a detailed mass reconstruction and a novel study on the substructure properties in the core of the Cluster Lensing And Supernova survey with Hubble (CLASH) and Frontier Fields galaxy cluster MACS J0416.1–2403. We show and employ our extensive spectroscopic data set taken with the VIsible Multi-Object Spectrograph instrument as part of our CLASH-VLT program, to confirm spectroscopically 10 strong lensing systems and to select a sample of 175 plausible cluster members to a limiting stellar mass of log (M {sub *}/M {sub ☉}) ≅ 8.6. We reproduce the measured positions of a set of 30 multiple images with a remarkable median offset of only 0.''3 by means of a comprehensive strong lensing model comprised of two cluster dark-matter halos, represented by cored elliptical pseudo-isothermal mass distributions, and the cluster member components, parameterized with dual pseudo-isothermal total mass profiles. The latter have total mass-to-light ratios increasing with the galaxy HST/WFC3 near-IR (F160W) luminosities. The measurement of the total enclosed mass within the Einstein radius is accurate to ∼5%, including the systematic uncertainties estimated from six distinct mass models. We emphasize that the use of multiple-image systems with spectroscopic redshifts and knowledge of cluster membership based on extensive spectroscopic information is key to constructing robust high-resolution mass maps. We also produce magnification maps over the central area that is covered with HST observations. We investigate the galaxy contribution, both in terms of total and stellar mass, to the total mass budget of the cluster. When compared with the outcomes of cosmological N-body simulations, our results point to a lack of massive subhalos in the inner regions of simulated clusters with total masses similar to that of MACS J0416.1–2403. Our findings of the location and shape of the cluster dark-matter halo density profiles and on the cluster substructures provide

  2. Rapid And Accurate Technique For Measuring N-15 Of Nitrate Method Development, Calibration And Validation

    A precise and simplified procedure for measuring nitrogen-15 of nitrate in water with moderate ionic strength and moderate to high organic loads is presented. The modified analytical train consists of two main steps: (a) extraction and purification of nitrate from liquid matrix and (b) pyrolysis of purified potassium nitrate. The presented method was evaluated with simulated solutions containing constant amounts of inter-laboratory nitrate standard salt (KNO3 , δ15N = -4.34 ± 0.32 % AirN2) and potentially interfering anions (SO42-, Cl- and HCO3-) as well as dissolved organic carbon (DOC) load. Dowex 1X8 anion exchange resin proved to be a suitable mean and provide accurate and reproducible δ15N values (SD: ± 0.48%).It tolerates high concentrations of chloride and sulfate ions for samples of small volumes (100 ml) of about four folds of the amounts enough to fully saturate the resin column. Rapid, accurate, precise, low-priced and less labour intensive activated graphite based offline pyrolysis technique for measuring N-15 content of nitrate has been developed and implemented. This involves combusting nitrate salt with activated graphite at 550oC for 30 minutes. Dramatic reduction in processing times needed for the analysis of N-15 of nitrate at natural abundance level was achieved. Performance characteristics of the modified analytical cascade showed that 1 to 2 hrs/sample/set of 5 samples processing time is required. The pyrolysis step of the developed method was validated using internationally distributed nitrate stable isotope reference materials. N-15 content of some selected nitrate salts, namely calcium nitrate, sodium nitrate, potassium nitrate and ammonium nitrate fertilizer, was measured using the modified technique, vacuum distillation method, modified ammonia diffusion method, microbial denitrifier method and EA-CF IRMS method at two different laboratories in Egypt and Germany. The results proved the validity and applicability of the modified

  3. Accurate and automatic extrinsic calibration method for blade measurement system integrated by different optical sensors

    He, Wantao; Li, Zhongwei; Zhong, Kai; Shi, Yusheng; Zhao, Can; Cheng, Xu

    2014-11-01

    Fast and precise 3D inspection system is in great demand in modern manufacturing processes. At present, the available sensors have their own pros and cons, and hardly exist an omnipotent sensor to handle the complex inspection task in an accurate and effective way. The prevailing solution is integrating multiple sensors and taking advantages of their strengths. For obtaining a holistic 3D profile, the data from different sensors should be registrated into a coherent coordinate system. However, some complex shape objects own thin wall feather such as blades, the ICP registration method would become unstable. Therefore, it is very important to calibrate the extrinsic parameters of each sensor in the integrated measurement system. This paper proposed an accurate and automatic extrinsic parameter calibration method for blade measurement system integrated by different optical sensors. In this system, fringe projection sensor (FPS) and conoscopic holography sensor (CHS) is integrated into a multi-axis motion platform, and the sensors can be optimally move to any desired position at the object's surface. In order to simple the calibration process, a special calibration artifact is designed according to the characteristics of the two sensors. An automatic registration procedure based on correlation and segmentation is used to realize the artifact datasets obtaining by FPS and CHS rough alignment without any manual operation and data pro-processing, and then the Generalized Gauss-Markoff model is used to estimate the optimization transformation parameters. The experiments show the measurement result of a blade, where several sampled patches are merged into one point cloud, and it verifies the performance of the proposed method.

  4. Accurate measurement of bromine contents in plastic samples by instrumental neutron activation analysis.

    Kim, I J; Lee, K S; Hwang, E; Min, H S; Yim, Y H

    2013-03-26

    Accurate measurements of bromine contents in plastic samples were made by the direct comparator instrumental neutron activation analysis (INAA). Individual factors affecting the measurements were comprehensively evaluated and compensated, including the volatility loss of bromine from standard comparators, the background bromine level in the filter papers used for preparation of the standard comparators, nuclear interference, γ-ray spectral interference and the variance among replicates of the samples. Uncertainty contributions from those factors were thoroughly evaluated and included in the uncertainty budgeting of the INAA measurement. (81)Br was chosen as the target isotope, and the INAA measurements for bromine were experimentally confirmed to exhibit good linearity within a bromine content range of 10-170 μg. The established method has been applied to the analysis of eight plastic samples: four commercially available certified reference materials (CRMs) of polyethylene and polystyrene and four acrylonitrile butadiene styrene (ABS) samples prepared as the candidate reference materials (KRISS CRM 113-01-012, -013, -014 and -015). The bromine contents of the samples were calculated at three different γ-ray energies and compared, showing good agreement. The results of the four CRMs also showed good consistency with their certified values within the stated uncertainties. Finally, the bromine contents of the ABS samples were determined with expanded uncertainties (at a 95% level of confidence) between 2.5% and 5% in a bromine content range of 25-900 mg kg(-1). PMID:23498117

  5. Accurate Measurement of the Effects of All Amino-Acid Mutations on Influenza Hemagglutinin

    Doud, Michael B.; Bloom, Jesse D.

    2016-01-01

    Influenza genes evolve mostly via point mutations, and so knowing the effect of every amino-acid mutation provides information about evolutionary paths available to the virus. We and others have combined high-throughput mutagenesis with deep sequencing to estimate the effects of large numbers of mutations to influenza genes. However, these measurements have suffered from substantial experimental noise due to a variety of technical problems, the most prominent of which is bottlenecking during the generation of mutant viruses from plasmids. Here we describe advances that ameliorate these problems, enabling us to measure with greatly improved accuracy and reproducibility the effects of all amino-acid mutations to an H1 influenza hemagglutinin on viral replication in cell culture. The largest improvements come from using a helper virus to reduce bottlenecks when generating viruses from plasmids. Our measurements confirm at much higher resolution the results of previous studies suggesting that antigenic sites on the globular head of hemagglutinin are highly tolerant of mutations. We also show that other regions of hemagglutinin—including the stalk epitopes targeted by broadly neutralizing antibodies—have a much lower inherent capacity to tolerate point mutations. The ability to accurately measure the effects of all influenza mutations should enhance efforts to understand and predict viral evolution. PMID:27271655

  6. An accurate measurement of the Rosemount 1152 differential pressure cell response time

    The primary heat-transport (PHT) system of a CANDU reactor includes four quadrants of reactor coolant channels, each fed from its own inlet header through a large number of inlet feeders. As part of the safety shutdown system 1 (SDS1) and Reactor Regulating System (RRS) of CANDU reactors, differential-pressure (DP) cells are used to monitor the reactor coolant flows in each quadrant and to register changes with a prescribed response time. This paper describes an accurate in-situ measurement of the response time of two Rosemount 1152 DPA22PB DP cells, one from SDS1 and one from an RRS fully instrumented channel. The response time measurement was done using high-frequency pressure-measurement devises temporarily installed on the high- and low-pressure sides of the DP cells. The results suggest that the actual time constant of the Rosemount DP cell is much faster than indicated in the specification which is based on the traditional instrument-air-step-response measurement method. Furthermore, the actual time constant is much faster than that assumed in the safety analysis report. An examination of the instrument-air-step-response method indicates that is produces conservative estimates of time constants, especially for small time constants. If further work confirms this finding it suggests that the actual time constant may be increased considerably without exceeding the time constant assumed in the safety analysis. (author)

  7. Accurate Estimation of Low Fundamental Frequencies from Real-Valued Measurements

    Christensen, Mads Græsbøll

    2013-01-01

    In this paper, the difficult problem of estimating low fundamental frequencies from real-valued measurements is addressed. The methods commonly employed do not take the phenomena encountered in this scenario into account and thus fail to deliver accurate estimates. The reason for this is that they...... employ asymptotic approximations that are violated when the harmonics are not well-separated in frequency, something that happens when the observed signal is real-valued and the fundamental frequency is low. To mitigate this, we analyze the problem and present some exact fundamental frequency estimators...... that are aimed at solving this problem. These esti- mators are based on the principles of nonlinear least-squares, harmonic fitting, optimal filtering, subspace orthogonality, and shift-invariance, and they all reduce to already published methods for a high number of observations. In experiments, the...

  8. Precision mass measurements of highly charged ions

    Kwiatkowski, A. A.; Bale, J. C.; Brunner, T.; Chaudhuri, A.; Chowdhury, U.; Ettenauer, S.; Frekers, D.; Gallant, A. T.; Grossheim, A.; Lennarz, A.; Mane, E.; MacDonald, T. D.; Schultz, B. E.; Simon, M. C.; Simon, V. V.; Dilling, J.

    2012-10-01

    The reputation of Penning trap mass spectrometry for accuracy and precision was established with singly charged ions (SCI); however, the achievable precision and resolving power can be extended by using highly charged ions (HCI). The TITAN facility has demonstrated these enhancements for long-lived (T1/2>=50 ms) isobars and low-lying isomers, including ^71Ge^21+, ^74Rb^8+, ^78Rb^8+, and ^98Rb^15+. The Q-value of ^71Ge enters into the neutrino cross section, and the use of HCI reduced the resolving power required to distinguish the isobars from 3 x 10^5 to 20. The precision achieved in the measurement of ^74Rb^8+, a superallowed β-emitter and candidate to test the CVC hypothesis, rivaled earlier measurements with SCI in a fraction of the time. The 111.19(22) keV isomeric state in ^78Rb was resolved from the ground state. Mass measurements of neutron-rich Rb and Sr isotopes near A = 100 aid in determining the r-process pathway. Advanced ion manipulation techniques and recent results will be presented.

  9. Cylinder with differential piston for mass measurements

    The paper presents a cylinder with differential piston, adapted for measuring the weight of fixed objects such as: fuel tanks (regardless of their capacity), bunkers and silos for all kind of materials, or mobile objects such as: automobiles, trucks, locomotives and railway cars. Although, the cylinder with differential piston is used on a large scale in hydraulic drive or hydraulic control circuits, till now it was not used as constituent part for weight measurements devices. The novelty of the present paper is precisely the use of the device for such purposes. Based on a computation algorithm, the paper presents the general design (assembly), of the device used for weighing important masses (1…. 100 tones). The fundamental idea consist in the fact that, a mass over 10 tones may be weighted with a helicoidally spring subjected to an axial force between 0 and 3000 N, with a deflection of about 30 mm. Simultaneously with the mechanical part, the electronic recording system is also described. The great advantage of the presented device consist in the fact that it can be used in heavy polluted atmosphere or difficult topographic conditions as a result of both the small dimensions and the protection systems adopted. Keywords: cylinder hydraulic with differential piston, hydrostatic pressure, measuring devices

  10. High resolution/accurate mass (HRMS) detection of anatoxin-a in lake water using LDTD-APCI coupled to a Q-Exactive mass spectrometer.

    Roy-Lachapelle, Audrey; Solliec, Morgan; Sinotte, Marc; Deblois, Christian; Sauvé, Sébastien

    2015-01-01

    A new innovative analytical method combining ultra-fast analysis time with high resolution/accurate mass detection was developed to eliminate the misidentification of anatoxin-a (ANA-a), a cyanobacterial toxin, from the natural amino acid phenylalanine (PHE). This was achieved by using the laser diode thermal desorption-atmospheric pressure chemical ionization (LDTD-APCI) coupled to the Q-Exactive, a high resolution/accurate mass spectrometer (HRMS). This novel combination, the LDTD-APCI-HRMS, allowed for an ultra-fast analysis time (0.999). Enhancement of signal to noise ratios relative to a standard triple-quadrupole method was demonstrated with lower detection and quantification limit values of 0.2 and 0.6 μg/L using the Q-Exactive. Accuracy and interday/intraday relative standard deviations were below 15%. The new method was applied to 8 different lake water samples with signs of cyanobacterial blooms. This work demonstrates the possibility of using an ultra-fast LDTD-APCI sample introduction system with an HRMS hybrid instrument for quantitative purposes with high selectivity in complex environmental matrices. PMID:25476385

  11. Accurate γ-ray spectrometry measurements of the half-life of 92Sr

    Studies of the nuclear fuel cycle require an accurate knowledge of the energy release from the decay of radioactive nuclides produced in a reactor, including precise half-life data for the short-lived radionuclides. Moreover, short-lived fission products are crucial for fission rate distribution measurements performed in low-power facilities, such as EOLE and MINERVE of CEA Cadarache [Fougeras, P., 2005. EOLE, MINERVE and MASURCA facilities and their associated neutron experimental programs. In: 13th International Conference on Nuclear Engineering, Beijing, China, 16-20 May 2005], and their nuclear decay data need to be known to high precision. For these reasons, the half-life of 92Sr has been measured to solve a recently observed inconsistency identified with the quoted value in the main nuclear applications libraries (including JEFF3.1): T1/2=2.71±0.01 h [Parsa, B., Ashari, A., Goolvard, L., Nobar, Y.M., 1971. Decay scheme of 2.71 h 92Sr. Nucl. Phys. A 175, 629-640]. An overestimation of 4.5% has been identified in this work, based on two independent methods. Specific γ-ray spectrometry measurements on activated fissile foils have been carried out, using two HPGe detectors. Influencing factors such as net area measurements of photopeaks, pulse pile-up accuracy and dead time corrections in the presence of decaying activity are discussed. A new value has been obtained by combining eight series of measurements: T1/2=2.594 0.006 h. The uncertainty has been reduced by a factor of two with respect to previous evaluations. This measured value also shows good agreement with the most recent studies of T1/2=2.627±0.009 h [Nir-El, Y., 2003. Private Communications. Soreq Research Centre, Yavne, Israel

  12. Accurate gamma-ray spectrometry measurements of the half-life of 92Sr.

    Leconte, P; Hudelot, J P; Antony, M

    2008-10-01

    Studies of the nuclear fuel cycle require an accurate knowledge of the energy release from the decay of radioactive nuclides produced in a reactor, including precise half-life data for the short-lived radionuclides. Moreover, short-lived fission products are crucial for fission rate distribution measurements performed in low-power facilities, such as EOLE and MINERVE of CEA Cadarache [Fougeras, P., 2005. EOLE, MINERVE and MASURCA facilities and their associated neutron experimental programs. In: 13th International Conference on Nuclear Engineering, Beijing, China, 16-20 May 2005], and their nuclear decay data need to be known to high precision. For these reasons, the half-life of (92)Sr has been measured to solve a recently observed inconsistency identified with the quoted value in the main nuclear applications libraries (including JEFF3.1): T(1/2)=2.71+/-0.01 h [Parsa, B., Ashari, A., Goolvard, L., Nobar, Y.M., 1971. Decay scheme of 2.71 h (92)Sr. Nucl. Phys. A 175, 629-640]. An overestimation of 4.5% has been identified in this work, based on two independent methods. Specific gamma-ray spectrometry measurements on activated fissile foils have been carried out, using two HPGe detectors. Influencing factors such as net area measurements of photopeaks, pulse pile-up accuracy and dead time corrections in the presence of decaying activity are discussed. A new value has been obtained by combining eight series of measurements: T(1/2)=2.594+/-0.006 h. The uncertainty has been reduced by a factor of two with respect to previous evaluations. This measured value also shows good agreement with the most recent studies of T(1/2)=2.627+/-0.009 h [Nir-El, Y., 2003. Private Communications. Soreq Research Centre, Yavne, Israel]. PMID:18456504

  13. Measurement of the W mass at LEP

    Przysiezniak, H

    2000-01-01

    The mass of the W boson is measured using W pair events collected with the ALEPH, DELPHI, L3 and OPAL detectors at LEP2. Three methods are used: the cross section method, the lepton energy spectrum method and the direct reconstruction method, where the latter is described more in detail. For data collected at E/sub cm/=161, 172 and 183 GeV, the following combined preliminary result is obtained: M/sub W//sup LEP/=80.37+or-0.08 GeV/c/sup 2/. (5 refs).

  14. Multiclass semi-volatile compounds determination in wine by gas chromatography accurate time-of-flight mass spectrometry.

    Rodríguez-Cabo, T; Rodríguez, I; Ramil, M; Silva, A; Cela, R

    2016-04-15

    The performance of gas chromatography (GC) with accurate, high resolution mass spectrometry (HRMS) for the determination of a group of 39 semi-volatile compounds related to wine quality (pesticide residues, phenolic off-flavours, phenolic pollutants and bioactive stilbenes) is investigated. Solid-phase extraction (SPE) was used as extraction technique, previously to acetylation (phenolic compounds) and dispersive liquid-liquid microextraction (DLLME) concentration. Compounds were determined by GC coupled to a quadrupole time-of-flight (QTOF) MS system through an electron ionization (EI) source. The final method attained limits of quantification (LOQs) at the very low ng mL(-1) level, covering the range of expected concentrations for target compounds in red and white wines. For 38 out of 39 compounds, performance of sample preparation and determination steps were hardly affected by the wine matrix; thus, accurate recoveries were achieved by using pseudo-external calibration. Levels of target compounds in a set of 25 wine samples are reported. The capabilities of the described approach for the post-run identification of species not considered during method development, without retention time information, are illustrated and discussed with selected examples of compounds from different classes. PMID:26971021

  15. Incentives Increase Participation in Mass Dog Rabies Vaccination Clinics and Methods of Coverage Estimation Are Assessed to Be Accurate.

    Abel B Minyoo

    2015-12-01

    Full Text Available In this study we show that incentives (dog collars and owner wristbands are effective at increasing owner participation in mass dog rabies vaccination clinics and we conclude that household questionnaire surveys and the mark-re-sight (transect survey method for estimating post-vaccination coverage are accurate when all dogs, including puppies, are included. Incentives were distributed during central-point rabies vaccination clinics in northern Tanzania to quantify their effect on owner participation. In villages where incentives were handed out participation increased, with an average of 34 more dogs being vaccinated. Through economies of scale, this represents a reduction in the cost-per-dog of $0.47. This represents the price-threshold under which the cost of the incentive used must fall to be economically viable. Additionally, vaccination coverage levels were determined in ten villages through the gold-standard village-wide census technique, as well as through two cheaper and quicker methods (randomized household questionnaire and the transect survey. Cost data were also collected. Both non-gold standard methods were found to be accurate when puppies were included in the calculations, although the transect survey and the household questionnaire survey over- and under-estimated the coverage respectively. Given that additional demographic data can be collected through the household questionnaire survey, and that its estimate of coverage is more conservative, we recommend this method. Despite the use of incentives the average vaccination coverage was below the 70% threshold for eliminating rabies. We discuss the reasons and suggest solutions to improve coverage. Given recent international targets to eliminate rabies, this study provides valuable and timely data to help improve mass dog vaccination programs in Africa and elsewhere.

  16. Incentives Increase Participation in Mass Dog Rabies Vaccination Clinics and Methods of Coverage Estimation Are Assessed to Be Accurate.

    Minyoo, Abel B; Steinmetz, Melissa; Czupryna, Anna; Bigambo, Machunde; Mzimbiri, Imam; Powell, George; Gwakisa, Paul; Lankester, Felix

    2015-12-01

    In this study we show that incentives (dog collars and owner wristbands) are effective at increasing owner participation in mass dog rabies vaccination clinics and we conclude that household questionnaire surveys and the mark-re-sight (transect survey) method for estimating post-vaccination coverage are accurate when all dogs, including puppies, are included. Incentives were distributed during central-point rabies vaccination clinics in northern Tanzania to quantify their effect on owner participation. In villages where incentives were handed out participation increased, with an average of 34 more dogs being vaccinated. Through economies of scale, this represents a reduction in the cost-per-dog of $0.47. This represents the price-threshold under which the cost of the incentive used must fall to be economically viable. Additionally, vaccination coverage levels were determined in ten villages through the gold-standard village-wide census technique, as well as through two cheaper and quicker methods (randomized household questionnaire and the transect survey). Cost data were also collected. Both non-gold standard methods were found to be accurate when puppies were included in the calculations, although the transect survey and the household questionnaire survey over- and under-estimated the coverage respectively. Given that additional demographic data can be collected through the household questionnaire survey, and that its estimate of coverage is more conservative, we recommend this method. Despite the use of incentives the average vaccination coverage was below the 70% threshold for eliminating rabies. We discuss the reasons and suggest solutions to improve coverage. Given recent international targets to eliminate rabies, this study provides valuable and timely data to help improve mass dog vaccination programs in Africa and elsewhere. PMID:26633821

  17. Incentives Increase Participation in Mass Dog Rabies Vaccination Clinics and Methods of Coverage Estimation Are Assessed to Be Accurate

    Steinmetz, Melissa; Czupryna, Anna; Bigambo, Machunde; Mzimbiri, Imam; Powell, George; Gwakisa, Paul

    2015-01-01

    In this study we show that incentives (dog collars and owner wristbands) are effective at increasing owner participation in mass dog rabies vaccination clinics and we conclude that household questionnaire surveys and the mark-re-sight (transect survey) method for estimating post-vaccination coverage are accurate when all dogs, including puppies, are included. Incentives were distributed during central-point rabies vaccination clinics in northern Tanzania to quantify their effect on owner participation. In villages where incentives were handed out participation increased, with an average of 34 more dogs being vaccinated. Through economies of scale, this represents a reduction in the cost-per-dog of $0.47. This represents the price-threshold under which the cost of the incentive used must fall to be economically viable. Additionally, vaccination coverage levels were determined in ten villages through the gold-standard village-wide census technique, as well as through two cheaper and quicker methods (randomized household questionnaire and the transect survey). Cost data were also collected. Both non-gold standard methods were found to be accurate when puppies were included in the calculations, although the transect survey and the household questionnaire survey over- and under-estimated the coverage respectively. Given that additional demographic data can be collected through the household questionnaire survey, and that its estimate of coverage is more conservative, we recommend this method. Despite the use of incentives the average vaccination coverage was below the 70% threshold for eliminating rabies. We discuss the reasons and suggest solutions to improve coverage. Given recent international targets to eliminate rabies, this study provides valuable and timely data to help improve mass dog vaccination programs in Africa and elsewhere. PMID:26633821

  18. Extracting accurate strain measurements in bone mechanics: A critical review of current methods.

    Grassi, Lorenzo; Isaksson, Hanna

    2015-10-01

    Osteoporosis related fractures are a social burden that advocates for more accurate fracture prediction methods. Mechanistic methods, e.g. finite element models, have been proposed as a tool to better predict bone mechanical behaviour and strength. However, there is little consensus about the optimal constitutive law to describe bone as a material. Extracting reliable and relevant strain data from experimental tests is of fundamental importance to better understand bone mechanical properties, and to validate numerical models. Several techniques have been used to measure strain in experimental mechanics, with substantial differences in terms of accuracy, precision, time- and length-scale. Each technique presents upsides and downsides that must be carefully evaluated when designing the experiment. Moreover, additional complexities are often encountered when applying such strain measurement techniques to bone, due to its complex composite structure. This review of literature examined the four most commonly adopted methods for strain measurements (strain gauges, fibre Bragg grating sensors, digital image correlation, and digital volume correlation), with a focus on studies with bone as a substrate material, at the organ and tissue level. For each of them the working principles, a summary of the main applications to bone mechanics at the organ- and tissue-level, and a list of pros and cons are provided. PMID:26099201

  19. Can structured data fields accurately measure quality of care? The example of falls

    David A. Ganz, MD, PhD

    2012-12-01

    Full Text Available By automating collection of data elements, electronic health records may simplify the process of measuring the quality of medical care. Using data from a quality improvement initiative in primary care medical groups, we sought to determine whether the quality of care for falls and fear of falling in outpatients aged 75 and older could be accurately measured solely from codable (non-free-text data in a structured visit note. A traditional medical record review by trained abstractors served as the criterion standard. Among 215 patient records reviewed, we found a structured visit note in 54% of charts within 3 mo of the date patients had been identified as having falls or fear of falling. The reliability of an algorithm based on codable data was at least good (kappa of at least 0.61 compared with full medical record review for three care processes recommended for patients with two falls or one fall with injury in the past year: orthostatic vital signs, vision test/eye examination, and home safety evaluation. However, the automated algorithm routinely underestimated quality of care. Performance standards based on automated measurement of quality of care from electronic health records need to account for documentation occurring in nonstructured form.

  20. Measuring intermediate mass black hole binaries with advanced gravitational wave detectors

    Veitch, John; Mandel, Ilya

    2015-01-01

    We perform a systematic study to explore the accuracy with which the parameters of intermediate-mass black-hole binary systems can be measured from their gravitational wave (GW) signatures using second-generation GW detectors. We make use of the most recent reduced-order models containing inspiral, merger and ringdown signals of aligned-spin effective-one-body waveforms (SEOBNR) to significantly speed up the calculations. We explore the phenomenology of the measurement accuracies for binaries with total masses between 50 and 500 $M_\\odot$ and mass ratios between 0.1 and 1. We find that (i) at total masses below ~200 $M_\\odot$, where the signal-to-noise-ratio is dominated by the inspiral portion of the signal, the chirp mass parameter can be accurately measured; (ii) at higher masses, the information content is dominated by the ringdown, and total mass is measured more accurately; (iii) the mass of the lower-mass companion is poorly estimated, especially at high total mass and more extreme mass ratios; (iv) sp...

  1. High-Frequency CTD Measurements for Accurate GPS/acoustic Sea-floor Crustal Deformation Measurement System

    Tadokoro, K.; Yasuda, K.; Taniguchi, S.; Uemura, Y.; Matsuhiro, K.

    2015-12-01

    The GPS/acoustic sea-floor crustal deformation measurement system has developed as a useful tool to observe tectonic deformation especially at subduction zones. One of the factors preventing accurate GPS/acoustic sea-floor crustal deformation measurement is horizontal heterogeneity of sound speed in the ocean. It is therefore necessary to measure the gradient directly from sound speed structure. We report results of high-frequency CTD measurements using Underway CTD (UCTD) in the Kuroshio region. We perform the UCTD measurements on May 2nd, 2015 at two stations (TCA and TOA) above the sea-floor benchmarks installed across the Nankai Trough, off the south-east of Kii Peninsula, middle Japan. The number of measurement points is six at each station along circles with a diameter of 1.8 nautical miles around the sea-floor benchmark. The stations TCA and TOA are located on the edge and the interior of the Kuroshio current, respectively, judging from difference in sea water density measured at the two stations, as well as a satellite image of sea-surface temperature distribution. We detect a sound speed gradient of high speeds in the southern part and low speeds in the northern part at the two stations. At the TCA station, the gradient is noticeable down to 300 m in depth; the maximum difference in sound speed is +/- 5 m/s. The sound speed difference is as small as +/- 1.3 m/s at depths below 300 m, which causes seafloor benchmark positioning error as large as 1 m. At the TOA station, the gradient is extremely small down to 100 m in depth. The maximum difference in sound speed is less than +/- 0.3 m/s that is negligible small for seafloor benchmark positioning error. Clear gradient of high speed is observed to the depths; the maximum difference in sound speed is +/- 0.8-0.9 m/s, causing seafloor benchmark positioning error of several tens centimeters. The UCTD measurement is effective tool to detect sound speed gradient. We establish a method for accurate sea

  2. Development and evaluation of a liquid chromatography-mass spectrometry method for rapid, accurate quantitation of malondialdehyde in human plasma.

    Sobsey, Constance A; Han, Jun; Lin, Karen; Swardfager, Walter; Levitt, Anthony; Borchers, Christoph H

    2016-09-01

    Malondialdhyde (MDA) is a commonly used marker of lipid peroxidation in oxidative stress. To provide a sensitive analytical method that is compatible with high throughput, we developed a multiple reaction monitoring-mass spectrometry (MRM-MS) approach using 3-nitrophenylhydrazine chemical derivatization, isotope-labeling, and liquid chromatography (LC) with electrospray ionization (ESI)-tandem mass spectrometry assay to accurately quantify MDA in human plasma. A stable isotope-labeled internal standard was used to compensate for ESI matrix effects. The assay is linear (R(2)=0.9999) over a 20,000-fold concentration range with a lower limit of quantitation of 30fmol (on-column). Intra- and inter-run coefficients of variation (CVs) were 36h at 5°C. Standards spiked into plasma had recoveries of 92-98%. When compared to a common LC-UV method, the LC-MS method found near-identical MDA concentrations. A pilot project to quantify MDA in patient plasma samples (n=26) in a study of major depressive disorder with winter-type seasonal pattern (MDD-s) confirmed known associations between MDA concentrations and obesity (p<0.02). The LC-MS method provides high sensitivity and high reproducibility for quantifying MDA in human plasma. The simple sample preparation and rapid analysis time (5x faster than LC-UV) offers high throughput for large-scale clinical applications. PMID:27437618

  3. Calibration Of X-Ray Imaging Devices For Accurate Intensity Measurement

    National Security Technologies (NSTec) has developed calibration procedures for X-ray imaging systems. The X-ray sources that are used for calibration are both diode type and diode/fluorescer combinations. Calibrating the X-ray detectors is key to accurate calibration of the X-ray sources. Both energy dispersive detectors and photodiodes measuring total flux were used. We have developed calibration techniques for the detectors using radioactive sources that are traceable to the National Institute of Standards and Technology (NIST). The German synchrotron at Physikalische Technische Bundestalt (PTB) is used to calibrate silicon photodiodes over the energy range from 50 eV to 60 keV. The measurements on X-ray cameras made using the NSTec X-ray sources have included quantum efficiency averaged over all pixels, camera counts per photon per pixel, and response variation across the sensor. The instrumentation required to accomplish the calibrations is described. X-ray energies ranged from 720 eV to 22.7 keV. The X-ray sources produce narrow energy bands, allowing us to determine the properties as a function of X-ray energy. The calibrations were done for several types of imaging devices. There were back illuminated and front illuminated CCD (charge coupled device) sensors, and a CID (charge injection device) type camera. The CCD and CID camera types differ significantly in some of their properties that affect the accuracy of X-ray intensity measurements. All cameras discussed here are silicon based. The measurements of quantum efficiency variation with X-ray energy are compared to models for the sensor structure. Cameras that are not back-thinned are compared to those that are.

  4. CALIBRATION OF X-RAY IMAGING DEVICES FOR ACCURATE INTENSITY MEASUREMENT

    Haugh, M J; Charest, M R; Ross, P W; Lee, J J; Schneider, M B; Palmer, N E; Teruya, A T

    2012-02-16

    National Security Technologies (NSTec) has developed calibration procedures for X-ray imaging systems. The X-ray sources that are used for calibration are both diode type and diode/fluorescer combinations. Calibrating the X-ray detectors is key to accurate calibration of the X-ray sources. Both energy dispersive detectors and photodiodes measuring total flux were used. We have developed calibration techniques for the detectors using radioactive sources that are traceable to the National Institute of Standards and Technology (NIST). The German synchrotron at Physikalische Technische Bundestalt (PTB) is used to calibrate silicon photodiodes over the energy range from 50 eV to 60 keV. The measurements on X-ray cameras made using the NSTec X-ray sources have included quantum efficiency averaged over all pixels, camera counts per photon per pixel, and response variation across the sensor. The instrumentation required to accomplish the calibrations is described. X-ray energies ranged from 720 eV to 22.7 keV. The X-ray sources produce narrow energy bands, allowing us to determine the properties as a function of X-ray energy. The calibrations were done for several types of imaging devices. There were back illuminated and front illuminated CCD (charge coupled device) sensors, and a CID (charge injection device) type camera. The CCD and CID camera types differ significantly in some of their properties that affect the accuracy of X-ray intensity measurements. All cameras discussed here are silicon based. The measurements of quantum efficiency variation with X-ray energy are compared to models for the sensor structure. Cameras that are not back-thinned are compared to those that are.

  5. Accurate, in vivo NIR measurement of skeletal muscle oxygenation through fat

    Jin, Chunguang; Zou, Fengmei; Ellerby, Gwenn E. C.; Scott, Peter; Peshlov, Boyan; Soller, Babs R.

    2010-02-01

    Noninvasive near infrared (NIR) spectroscopic measurement of muscle oxygenation requires the penetration of light through overlying skin and fat layers. We have previously demonstrated a dual-light source design and orthogonalization algorithm that corrects for inference from skin absorption and fat scattering. To achieve accurate muscle oxygen saturation (SmO2) measurement, one must select the appropriate source-detector distance (SD) to completely penetrate the fat layer. Methods: Six healthy subjects were supine for 15min to normalize tissue oxygenation across the body. NIR spectra were collected from the calf, shoulder, lower and upper thigh muscles with long SD distances of 30mm, 35mm, 40mm and 45mm. Spectral preprocessing with the short SD (3mm) spectrum preceded SmO2 calculation with a Taylor series expansion method. Three-way ANOVA was used to compare SmO2 values over varying fat thickness, subjects and SD distances. Results: Overlying fat layers varied in thickness from 4.9mm to 19.6mm across all subjects. SmO2 measured at the four locations were comparable for each subject (p=0.133), regardless of fat thickness and SD distance. SmO2 (mean+/-std dev) measured at calf, shoulder, low and high thigh were 62+/-3%, 59+/-8%, 61+/-2%, 61+/-4% respectively for SD distance of 30mm. In these subjects no significant influence of SD was observed (p=0.948). Conclusions: The results indicate that for our sensor design a 30mm SD is sufficient to penetrate through a 19mm fat layer and that orthogonalization with short SD effectively removed spectral interference from fat to result in a reproducible determination of SmO2.

  6. Accurate determination of electric-dipole matrix elements in K and Rb from Stark shift measurements

    Arora, Bindiya; Clark, Charles W

    2007-01-01

    Stark shifts of potassium and rubidium D1 lines have been measured with high precision by Miller et al [1]. In this work, we combine these measurements with our all-order calculations to determine the values of the electric-dipole matrix elements for the 4p_j-3d_j' transitions in K and for the 5p_j-4d_j' transitions in Rb to high precision. The 4p_1/2-3d_3/2 and 5p_1/2-4d_3/2 transitions contribute on the order of 90% to the respective polarizabilities of the np_1/2 states in K and Rb, and the remaining 10% can be accurately calculated using the relativistic all-order method. Therefore, the combination of the experimental data and theoretical calculations allows us to determine the np-(n-1)d matrix elements and their uncertainties. We compare these values with our all-order calculations of the np-(n-1)d matrix elements in K and Rb for a benchmark test of the accuracy of the all-order method for transitions involving nd states. Such matrix elements are of special interest for many applications, such as determi...

  7. Accurately measuring volume of soil samples using low cost Kinect 3D scanner

    van der Sterre, Boy-Santhos; Hut, Rolf; van de Giesen, Nick

    2013-04-01

    The 3D scanner of the Kinect game controller can be used to increase the accuracy and efficiency of determining in situ soil moisture content. Soil moisture is one of the principal hydrological variables in both the water and energy interactions between soil and atmosphere. Current in situ measurements of soil moisture either rely on indirect measurements (of electromagnetic constants or heat capacity) or on physically taking a sample and weighing it in a lab. The bottleneck in accurately retrieving soil moisture using samples is the determining of the volume of the sample. Currently this is mostly done by the very time consuming "sand cone method" in which the volume were the sample used to sit is filled with sand. We show that 3D scanner that is part of the 150 game controller extension "Kinect" can be used to make 3D scans before and after taking the sample. The accuracy of this method is tested by scanning forms of known volume. This method is less time consuming and less error-prone than using a sand cone.

  8. An accurate low current measurement circuit for heavy iron beam current monitor

    Heavy-ion beams at 106 particles per second have been applied to the treatment of deep-seated inoperable tumors in the therapy terminal of the Heavy Ion Research Facility in Lanzhou (HIRFL) which is located at the Institute of Modern Physics, Chinese Academy of Sciences (IMP, CAS). An accurate low current measurement circuit following a Faraday cup was developed to monitor the beam current at pA range. The circuit consisted of a picoammeter with a bandwidth of 1 kHz and a gated integrator (GI). A low input bias current precision amplifier and new guarding and shielding techniques were used in the picoammeter circuit which allowed as to measure current less than 1 pA with a current gain of 0.22 V/pA and noise less than 10 fA. This paper will also describe a novel compensation approach which reduced the charge injection from switches in the GI to 10−18 C, and a T-switch configuration which was used to eliminate leakage current in the reset switch.

  9. How Accurate is Your Sclerostin Measurement? Comparison Between Three Commercially Available Sclerostin ELISA Kits.

    Piec, Isabelle; Washbourne, Christopher; Tang, Jonathan; Fisher, Emily; Greeves, Julie; Jackson, Sarah; Fraser, William D

    2016-06-01

    Sclerostin, bone formation antagonist is in the spotlight as a potential biomarker for diseases presenting with associated bone disorders such as chronic kidney disease (CDK-MBD). Accurate measurement of sclerostin is therefore important. Several immunoassays are available to measure sclerostin in serum and plasma. We compared the performance of three commercial ELISA kits. We measured sclerostin concentrations in serum and EDTA plasma obtained from healthy young (18-26 years) human subjects using kits from Biomedica, TECOmedical and from R&D Systems. The circulating sclerostin concentrations were systematically higher when measured with the Biomedica assay (serum: 35.5 ± 1.1 pmol/L; EDTA: 39.4 ± 2.0 pmol/L; mean ± SD) as compared with TECOmedical (serum: 21.8 ± 0.7 pmol/L; EDTA: 27.2 ± 1.3 pmol/L) and R&D Systems (serum: 7.6 ± 0.3 pmol/L; EDTA: 30.9 ± 1.5 pmol/L). We found a good correlation between the assay for EDTA plasma (r > 0.6; p < 0.001) while in serum, only measurements obtained using TECOmedical and R&D Systems assays correlated significantly (r = 0.78; p < 0.001). There was no correlation between matrices results when using the Biomedica kit (r = 0.20). The variability in values generated from Biomedica, R&D Systems and TECOmedical assays raises questions regarding the accuracy and specificity of the assays. Direct comparison of studies using different kits is not possible and great care should be given to measurement of sclerostin, with traceability of reagents. Standardization with appropriate material is required before different sclerostin assays can be introduced in clinical practice. PMID:26749312

  10. Sitting and standing blood pressure measurements are not accurate for the diagnosis of orthostatic hypotension.

    Cooke, J

    2012-01-31

    INTRODUCTION: Orthostatic hypotension (OH) is associated with troublesome symptoms and increased mortality. It is treatable and deserving of accurate diagnosis. This can be time consuming. The current reference standard for its diagnosis is head-up tilt (HUT) testing with continuous beat-to-beat plethysmography. Our objective was to assess the accuracy of sit-stand testing with semi-automatic sphygmomanometry for the diagnosis of OH. DESIGN: Retrospective test of diagnostic accuracy. METHODS: This was a retrospective study performed using a database maintained by a busy syncope unit. HUT testing was performed using an automated tilt table with Finometer monitoring. A 3 min 70 degrees HUT was performed following 5 min supine. Sitting blood pressure (BP) was measured following 3 min rest. Standing BP was measured within 30 s of assuming the upright posture. The results of sit-stand testing were compared with HUT testing as a reference standard. Both tests happened within 5 min of each other and patients underwent no intervention between tests. RESULTS: From a total of 1452 consecutive HUTs, we identified 730 with pre-test measures of sitting and standing BP. The mean age of this group was 70.57 years (SD = 15.1), 62% were female. The sensitivity of sit-stand testing was calculated as 15.5%, specificity as 89.9%, positive predictive value as 61.7%, negative predictive value as 50.2% and the likelihood ratio as 1.6. The area under the Receiver Operator Curve was 0.564. CONCLUSION: We have demonstrated that sit-stand testing for OH has very low diagnostic accuracy. We recommend that the more time-consuming reference standard method of diagnosis be used if the condition is suspected.

  11. Measurement of the top quark mass

    Varnes, E.W.

    1997-12-31

    This dissertation describes the measurement of the top quark mass m{sub t} using events recorded during a 125 pb{sup -1} exposure of the D0 detector to {radical}s=1.8 TeV {anti p}p collisions. Six events consistent with the hypothesis t{anti t} {yields} bW{sup +}, {anti b}W{sup -} {yields} b{anti l}{nu}, {anti b}l{anti {nu}} form the dilepton sample. The kinematics of such events may be reconstructed for any assumed mt, and the likelihood of each such solution evaluated. A measurement of m{sub t} based on these relative solution likelihoods gives m{sub t} = 169.9 {+-} 14.8 (stat.) {+-} 3. 8 (syst.) GeV/c{sup 2}. A 2C kinematic fit is performed on a sample of 77 events consistent with t{anti t} {yields} bW{sup +}, {anti b}W{sup -} {yields} b{anti l}{nu}, {anti b}q{anti q} , and this, in combination with an estimate on the likelihood that each event is top, yields m{sub t} = 173.3 {+-} 5.6 (stat.) {+-} 6.2 (syst.) GeV/c{sup 2} . A combination of these two measurements gives m{sub t} = 173.1 {+-} 5.2 (stat.) {+-} 5.7 (syst.) GeV/c{sup 2}.

  12. Measurement of the top quark mass

    This dissertation describes the measurement of the top quark mass mt using events recorded during a 125 pb-1 exposure of the D0 detector to √s=1.8 TeV anti pp collisions. Six events consistent with the hypothesis t anti t → bW+, anti bW- → b anti lν, anti bl anti ν form the dilepton sample. The kinematics of such events may be reconstructed for any assumed mt, and the likelihood of each such solution evaluated. A measurement of mt based on these relative solution likelihoods gives mt = 169.9 ± 14.8 (stat.) ± 3. 8 (syst.) GeV/c2. A 2C kinematic fit is performed on a sample of 77 events consistent with t anti t → bW+, anti bW- → b anti lν, anti bq anti q , and this, in combination with an estimate on the likelihood that each event is top, yields mt = 173.3 ± 5.6 (stat.) ± 6.2 (syst.) GeV/c2 . A combination of these two measurements gives mt = 173.1 ± 5.2 (stat.) ± 5.7 (syst.) GeV/c2

  13. Enabling high grayscale resolution displays and accurate response time measurements on conventional computers.

    Li, Xiangrui; Lu, Zhong-Lin

    2012-01-01

    Display systems based on conventional computer graphics cards are capable of generating images with 8-bit gray level resolution. However, most experiments in vision research require displays with more than 12 bits of luminance resolution. Several solutions are available. Bit++ (1) and DataPixx (2) use the Digital Visual Interface (DVI) output from graphics cards and high resolution (14 or 16-bit) digital-to-analog converters to drive analog display devices. The VideoSwitcher (3) described here combines analog video signals from the red and blue channels of graphics cards with different weights using a passive resister network (4) and an active circuit to deliver identical video signals to the three channels of color monitors. The method provides an inexpensive way to enable high-resolution monochromatic displays using conventional graphics cards and analog monitors. It can also provide trigger signals that can be used to mark stimulus onsets, making it easy to synchronize visual displays with physiological recordings or response time measurements. Although computer keyboards and mice are frequently used in measuring response times (RT), the accuracy of these measurements is quite low. The RTbox is a specialized hardware and software solution for accurate RT measurements. Connected to the host computer through a USB connection, the driver of the RTbox is compatible with all conventional operating systems. It uses a microprocessor and high-resolution clock to record the identities and timing of button events, which are buffered until the host computer retrieves them. The recorded button events are not affected by potential timing uncertainties or biases associated with data transmission and processing in the host computer. The asynchronous storage greatly simplifies the design of user programs. Several methods are available to synchronize the clocks of the RTbox and the host computer. The RTbox can also receive external triggers and be used to measure RT with respect

  14. An accurate measurement of the baryonic Tully-Fisher relation with heavily gas-dominated ALFALFA galaxies

    Papastergis, E.; Adams, E. A. K.; van der Hulst, J. M.

    2016-09-01

    We use a sample of 97 galaxies selected from the Arecibo legacy fast ALFA (ALFALFA) 21 cm survey to make an accurate measurement of the baryonic Tully-Fisher relation (BTFR). These galaxies are specifically selected to be heavily gas-dominated (Mgas/M∗ ≳ 2.7) and to be oriented edge-on. The former property ensures that the error on the galactic baryonic mass is small, despite the large systematic uncertainty involved in galactic stellar mass estimates. The latter property means that rotational velocities can be derived directly from the width of the 21 cm emission line, without any need for inclination corrections. We measure a slope for the linewidth-based BTFR of α = 3.75 ± 0.11, a value that is somewhat steeper than (but in broad agreement with) previous literature results. The relation is remarkably tight, with almost all galaxies being located within a perpendicular distance of ± 0.1 dex from the best fit line. The low observational error budget for our sample enables us to establish that, despite its tightness, the measured linewidth-based BTFR has some small (i.e., non-zero) intrinsic scatter. We furthermore find a systematic difference in the BTFR of galaxies with "double-horned" 21 cm line profiles - suggestive of flat outer galactic rotation curves - and those with "peaked" profiles - suggestive of rising rotation curves. When we restrict our sample of galaxies to objects in the former category, we measure a slightly steeper slope of α = 4.13 ± 0.15. Overall, the high-accuracy measurement of the BTFR presented in this article is intended as a reliable observational benchmark against which to test theoretical expectations. Here we consider a representative set of semi-analytic models and hydrodynamic simulations in the lambda cold dark matter (ΛCDM) context, as well as modified Newtonian dynamics (MOND). In the near future, interferometric follow-up observations of several sample members will enable us to further refine the BTFR measurement, and

  15. Recent improvements in chemical dosimetric protocols for accurate measurements of absorbed dose in pulse radiolysis experiments

    This report describes recent improvements made in chemical dosimetric protocols for the Radiation and Photochemistry Division LINAC based pulse radiolysis (PR) experiments, keeping into perspective the current objectives and related machine parameters. In PR studies, accurate measure of absorbed dose based on free radicals' chemistry remains the backbone of all quantitative analyses. Therein, for promptness and convenience, precalibrated secondary chemical dosimeters consisting of aqueous solution of either H2 in alkali, (H2/OH-) or ferrocyanide (Fe(CN)64-), or thiocyanate (CNS-) are employed. Concentration of the free radical species produced as a result (e.g. hydrated electron, eaq-, ferricyanide anion, Fe(CN)63- or thiocyanate dimer radical anion, (SCN)2-) following respective set of chemical reactions is monitored. Amongst these the (SCN)2-) system is in use in RPCD since the machine installation in 1987, due to its sensitivity and ease of use. However, it was realized that rapid partial and variable disappearance of the transient (SCN)2-) species may occur prior to its estimation, introducing significant errors in some cases. Such deviations were searched, analyzed and then quantified, first by mapping the specific time-resolved output electron pulse profiles and the microscopic, random energy variations within each. Secondly, by incorporating such physical irregularities into the opposing set of (SCN)2- radical fast formation and decay chemical reactions, detailed time resolved kinetic analyses of the dosimetric reactions were made separately under all possible scenario. This exercise revealed the varied natures and extents of the hidden inaccuracies in different cases, and consequently also allowed their reduction to negligible levels, by their integration with a user-friendly dosimetry software that was developed in-house, resulting in substantial improvements in the measured dose. (author)

  16. Accurate measurements of {sup 210}Pb in industrial wastes for environmental radiation risk assessment purpose

    Bonczyk, Michal; Michalik, Boguslaw [Central Mining Institute, Silesian Centre for Environmental Radioactivity, Plac Gwarkow 1, 40-166 Katowice (Poland)

    2014-07-01

    Lead {sup 210}Pb is a naturally occurring radioactive nuclide element of the uranium ({sup 238}U) radioactive series. It is produced as a result of the decay of so-called short-lived progenies of {sup 222}Rn, i.e. {sup 214}Po (99.98%) and {sup 214}Bi by {sup 219}Tl (0.02%). Activity concentration of lead {sup 210}Pb could vary independently from parent radionuclides due to its physical and chemical properties, especially, due to its half-life (T{sub 1/2} = 22,3 years). Hence, its behaviour in natural environment is very complex and difficult in forecasting. Lead {sup 210}Pb in substantial amount occurs in mining, gas and oil extraction industry wastes, which are deposited in natural environment very often. Due to lack of secular equilibrium proper radiation risk assessment requires accurate concentration of {sup 210}Pb in such materials. The laboratory measurements seem to be the only reliable method in environmental radioactivity monitoring. One of the methods is gamma-ray spectrometry, which is very fast and cost-effective method to determine {sup 210}Pb concentration. On the other hand, the self-attenuation of gamma ray from {sup 210}Pb (46,5 keV) is significant and not depends only on sample density as well the chemical composition (sample matrix) is crucial. Current work describes how the self-attenuation correction factors in the case of {sup 210}Pb concentration analysis in mining wastes are important when environmental radiation risk assessment is carried out. The measurements were done for such industrial wastes as mine sediments which contain significant amount of elements with high Z-number (Barium, Lead, etc.) Experimentally obtained correction factors range between 0.51-6.96 cm{sup 2}/g. Neglecting this factor can cause a significant error or underestimations in radiological risk assessment. (authors)

  17. MELIFT - A new device for accurate measurements in a snow rich environment

    Dorninger, M.

    2012-04-01

    A deep snow pack, remote locations, no external power supply and very low temperatures are often the main ingredients when it comes to the deployment of meteorological stations in mountainous terrain. The accurate position of the sensor related to the snow surface is normally not known. A new device called METLIFT overcomes the problems. WMO recommends a height between 1.2 m and 2 m above ground level for the measurement of air temperature and humidity. The height above ground level is specified to take care of the possible strong vertical temperature and humidity gradients at the lowest layers in the atmosphere. Especially in snow rich and remote locations it may be hardly possible to follow this advice. Therefore most of the meteorological stations in mountainous terrain are situated at mountain tops where strong winds will blow off the snow or in valleys where a daily inspection of the sensors is possible. In other unpopulated mountainous areas, e.g. basins, plateaus, the distance of the sensor to the snow surface is not known or the sensor will be snow-covered. A new device was developed to guarantee the sensor height above surface within the WMO limits in harsh and remote environments. An ultrasonic snow height sensor measures the distance to the snow surface. If it exceeds certain limits due to snow accumulation or snow melt the lift adapts its height accordingly. The prototype of METLIFT has been installed in Lower Austria at an altitude of 1000m. The lift is 6 m high and can pull out for another 4 m. Sensor arms are mounted every meter to allow the connection of additional sensors or to measure a profile of a certain parameter of the lowest 5 m above surface. Sensors can be added easily since cable wiring is provided to each sensor arm. Horizontal winds are measured at 7 m height above surface. METLIFT is independent of external power supply. Three lead gel accumulators recharged by three solar panels provide the energy necessary for the sensors, the data

  18. Experiment to measure the electron neutrino mass using frozen tritium

    The authors are performing an experiment to determine the electron neutrino mass with the precision of a few eV by measuring the tritium beta decay energy distribution near the endpoint. Key features of the experiment are a 2 eV resolution electrostatic spectometer and a high-activity frozen tritium source. It is important that the source have electronic wavefunctions which can be accurately calculated. These calculations have been made for tritium and the HeT+ daughter ion and allow determination of branching fractions to 0.1% and energy of the excited states to 0.1 eV. The authors discuss the excited final molecular state calculations and describe the experimental apparatus

  19. Accurate determination of ⁴¹Ca concentrations in spent resins from the nuclear industry by accelerator mass spectrometry.

    Nottoli, Emmanuelle; Bourlès, Didier; Bienvenu, Philippe; Labet, Alexandre; Arnold, Maurice; Bertaux, Maité

    2013-12-01

    The radiological characterisation of nuclear waste is essential for managing storage sites. Determining the concentration of Long-Lived RadioNuclides (LLRN) is fundamental for their long-term management. This paper focuses on the measurement of low (41)Ca concentrations in ions exchange resins used for primary fluid purification in Pressurised Water Reactors (PWR). (41)Ca concentrations were successfully measured by Accelerator Mass Spectrometry (AMS) after the acid digestion of resin samples, followed by radioactive decontamination and isobaric suppression through successive hydroxide, carbonate, nitrate and final CaF2 precipitations. Measured (41)Ca concentrations ranged from 0.02 to 0.03 ng/g, i.e. from 0.06 to 0.09 Bq/g. The (41)Ca/(60)Co activity ratios obtained were remarkably reproducible and in good agreement with the current ratio used for resins management. PMID:24144617

  20. Use of niobium for accurate relative fast neutron fluence measurements at the pressure vessel in a WWER-440 NPP

    The reaction 93Nb (n,n') /sup 93m/Nb, with low threshold energy (approximately 0.9 MeV) was used in a novel way to obtain both absolute and accurate, relative experimental estimates for the fast neutron (threshold) fluence at the inner wall of the pressure vessel (PV) in a WWER-440 type PWR reactor. Niobium was separated using chemical methods from steel samples containing 0.5...1% niobium, which had been scraped from the inner wall of the Loviisa NPP. Irradiated niobium foils from the surveillance chains (SC) were also treated in a similar way. Niobium from the liquid samples was then electro-deposited in very thin layers on copper discs. The amount of niobium deposited was determined by spectrophotometry and liquid scintillation measurements. The accuracy of the mass determination was further checked by an additional and independent method. The absolute activity of the niobium deposits was determined by measuring the 16.6 and 18.6 keV X-ray emission with a calibrated Si(Li) detector. The threshold flux PHI/sub T/ (> 0.9 MeV) was then obtained. The results indicate that the relative fluence estimates (PV/SC), which are sufficient for relating the measured embrittlement of the SC steel samples to the embrittlement of the PV, can be obtained with many times reduced in-accuracy (from tens of per cent to less than ten per cent) as compared to separate absolute estimates and estimate obtained by normalizing the calculated fluxes to conform with the measured results at the SC. (author)

  1. Rapid Screening of Bovine Milk Oligosaccharides in a Whey Permeate Product and Domestic Animal Milks by Accurate Mass Database and Tandem Mass Spectral Library.

    Lee, Hyeyoung; Cuthbertson, Daniel J; Otter, Don E; Barile, Daniela

    2016-08-17

    A bovine milk oligosaccharide (BMO) library, prepared from cow colostrum, with 34 structures was generated and used to rapidly screen oligosaccharides in domestic animal milks and a whey permeate powder. The novel library was entered into a custom Personal Compound Database and Library (PCDL) and included accurate mass, retention time, and tandem mass spectra. Oligosaccharides in minute-sized samples were separated using nanoliquid chromatography (nanoLC) coupled to a high resolution and sensitive quadrupole-Time of Flight (Q-ToF) MS system. Using the PCDL, 18 oligosaccharides were found in a BMO-enriched product obtained from whey permeate processing. The usefulness of the analytical system and BMO library was further validated using milks from domestic sheep and buffaloes. Through BMO PCDL searching, 15 and 13 oligosaccharides in the BMO library were assigned in sheep and buffalo milks, respectively, thus demonstrating significant overlap between oligosaccharides in bovine (cow and buffalo) and ovine (sheep) milks. This method was shown to be an efficient, reliable, and rapid tool to identify oligosaccharide structures using automated spectral matching. PMID:27428379

  2. Analysis of the neurotoxic plasticizer n-butylbenzenesulfonamide by gas chromatography combined with accurate mass selected ion monitoring.

    Duffield, P; Bourne, D; Tan, K; Garruto, R M; Duncan, M W

    1994-01-01

    The plasticizer, n-butylbenzenesulfonamide (NBBS), is reported to be neurotoxic when inoculated intracisternally or intraperitoneally into rabbits. Because NBBS is commonly used in the production of polyamide (nylon) plastics and is soluble in water, the disposal of NBBS-containing plastics in landfill sites could result in NBBS appearing in the leachate. Further, NBBS could also be leached from packaging into their contents. To allow us to examine the risks posed by NBBS in the environment, we have developed a quantitative assay for this compound. The assay employs a one-step extraction into dichloromethane followed by gas chromatography with accurate mass selected ion recording. The assay incorporates [13C6]NBBS as an internal standard to allow precise quantitation, and four separate ion chromatograms are recorded. NBBS was found in some Australian domestic solidwaste landfill leachate (from less than 0.3 to 94.6 ng/mL), but ground water in the vicinity of a landfill had only trace quantities of NBBS. NBBS was also quantitated in some bottled and cask wines, and levels varied from not detected to 2.17 ng/mL (n = 14). Additional studies are required to assess the public health risks associated with the use of NBBS as a plasticizer. PMID:7861748

  3. Chemical ionization tandem mass spectrometer for the in situ measurement of methyl hydrogen peroxide

    A new approach for measuring gas-phase methyl hydrogen peroxide [(MHP) CH3OOH] utilizing chemical ionization mass spectrometry is presented. Tandem mass spectrometry is used to avoid mass interferences that hindered previous attempts to measure atmospheric CH3OOH with CF3O- clustering chemistry. CH3OOH has been successfully measured in situ using this technique during both airborne and ground-based campaigns. The accuracy and precision for the MHP measurement are a function of water vapor mixing ratio. Typical precision at 500 pptv MHP and 100 ppmv H2O is ±80 pptv (2 sigma) for a 1 s integration period. The accuracy at 100 ppmv H2O is estimated to be better than ±40%. Chemical ionization tandem mass spectrometry shows considerable promise for the determination of in situ atmospheric trace gas mixing ratios where isobaric compounds or mass interferences impede accurate measurements.

  4. Development of isotope dilution-liquid chromatography/mass spectrometry combined with standard addition techniques for the accurate determination of tocopherols in infant formula

    Graphical abstract: -- Highlights: •ID-LC/MS method showed biased results for tocopherols analysis in infant formula. •H/D exchange of deuterated tocopherols in sample preparation was the source of bias. •Standard addition (SA)-ID-LC/MS was developed as an alternative to ID-LC/MS. •Details of calculation and uncertainty evaluation of the SA-IDMS were described. •SA-ID-LC/MS showed a higher-order metrological quality as a reference method. -- Abstract: During the development of isotope dilution-liquid chromatography/mass spectrometry (ID-LC/MS) for tocopherol analysis in infant formula, biased measurement results were observed when deuterium-labeled tocopherols were used as internal standards. It turned out that the biases came from intermolecular H/D exchange and intramolecular H/D scrambling of internal standards in sample preparation processes. Degrees of H/D exchange and scrambling showed considerable dependence on sample matrix. Standard addition-isotope dilution mass spectrometry (SA-IDMS) based on LC/MS was developed in this study to overcome the shortcomings of using deuterium-labeled internal standards while the inherent advantage of isotope dilution techniques is utilized for the accurate recovery correction in sample preparation processes. Details of experimental scheme, calculation equation, and uncertainty evaluation scheme are described in this article. The proposed SA-IDMS method was applied to several infant formula samples to test its validity. The method was proven to have a higher-order metrological quality with providing very accurate and precise measurement results

  5. Determination of the presence or absence of sulfur materials in drywall using direct analysis in real time in conjunction with an accurate-mass time-of-flight mass spectrometer.

    Curtis, Matthew E; Jones, Patrick R; Sparkman, O David; Cody, Robert B

    2009-11-01

    Based on the concern about the presence of sulfur materials being in drywall (wallboard), a quick and reliable test to confirm the presence or absence of these materials using direct analysis in real time (DART) mass spectrometry in conjunction with an accurate-mass time-of-flight (TOF) mass spectrometer has been developed and is described here. PMID:19700343

  6. Accurate Mass GC/LC-Quadrupole Time of Flight Mass Spectrometry Analysis of Fatty Acids and Triacylglycerols of Spicy Fruits from the Apiaceae Family

    Thao Nguyen

    2015-12-01

    Full Text Available The triacylglycerol (TAG structure and the regio-stereospecific distribution of fatty acids (FA of seed oils from most of the Apiaceae family are not well documented. The TAG structure ultimately determines the final physical properties of the oils and the position of FAs in the TAG molecule affects the digestion; absorption and metabolism; and physical and technological properties of TAGs. Fixed oils from the fruits of dill (Anethum graveolens, caraway (Carum carvi, cumin (Cuminum cyminum, coriander (Coriandrum sativum, anise (Pimpinella anisum, carrot (Daucus carota, celery (Apium graveolens, fennel (Foeniculum vulgare, and Khella (Ammi visnaga, all from the Apiaceae family, were extracted at room temperature in chloroform/methanol (2:1 v/v using percolators. Crude lipids were fractionated by solid phase extraction to separate neutral triacylglycerols (TAGs from other lipids components. Neutral TAGs were subjected to transesterification process to convert them to their corresponding fatty acids methyl esters (FAMES using 1% boron trifluoride (BF3 in methanol. FAMES were analyzed by gas chromatography-quadrupole time of flight (GC-QTOF mass spectrometry. Triglycerides were analyzed using high performance liquid chromatography-quadrupole time of flight (LC-QTOF mass spectrometry. Petroselinic acid was the major fatty acid in all samples ranging from 57% of the total fatty acids in caraway up to 82% in fennel. All samples contained palmitic (16:0, palmitoleic (C16:1n-9, stearic (C18:0, petroselinic (C18:1n-12, linoleic (C18:2n-6, linolinic (18:3n-3, and arachidic (C20:0 acids. TAG were analyzed using LC-QTOF for accurate mass identification and mass spectrometry/mass spectrometry (MS/MS techniques for regiospesific elucidation of the identified TAGs. Five major TAGs were detected in all samples but with different relative concentrations in all of the tested samples. Several other TAGs were detected as minor components and were present in some

  7. Accurate Mass GC/LC-Quadrupole Time of Flight Mass Spectrometry Analysis of Fatty Acids and Triacylglycerols of Spicy Fruits from the Apiaceae Family.

    Nguyen, Thao; Aparicio, Mario; Saleh, Mahmoud A

    2015-01-01

    The triacylglycerol (TAG) structure and the regio-stereospecific distribution of fatty acids (FA) of seed oils from most of the Apiaceae family are not well documented. The TAG structure ultimately determines the final physical properties of the oils and the position of FAs in the TAG molecule affects the digestion; absorption and metabolism; and physical and technological properties of TAGs. Fixed oils from the fruits of dill (Anethum graveolens), caraway (Carum carvi), cumin (Cuminum cyminum), coriander (Coriandrum sativum), anise (Pimpinella anisum), carrot (Daucus carota), celery (Apium graveolens), fennel (Foeniculum vulgare), and Khella (Ammi visnaga), all from the Apiaceae family, were extracted at room temperature in chloroform/methanol (2:1 v/v) using percolators. Crude lipids were fractionated by solid phase extraction to separate neutral triacylglycerols (TAGs) from other lipids components. Neutral TAGs were subjected to transesterification process to convert them to their corresponding fatty acids methyl esters (FAMES) using 1% boron trifluoride (BF₃) in methanol. FAMES were analyzed by gas chromatography-quadrupole time of flight (GC-QTOF) mass spectrometry. Triglycerides were analyzed using high performance liquid chromatography-quadrupole time of flight (LC-QTOF) mass spectrometry. Petroselinic acid was the major fatty acid in all samples ranging from 57% of the total fatty acids in caraway up to 82% in fennel. All samples contained palmitic (16:0), palmitoleic (C16:1n-9), stearic (C18:0), petroselinic (C18:1n-12), linoleic (C18:2n-6), linolinic (18:3n-3), and arachidic (C20:0) acids. TAG were analyzed using LC-QTOF for accurate mass identification and mass spectrometry/mass spectrometry (MS/MS) techniques for regiospesific elucidation of the identified TAGs. Five major TAGs were detected in all samples but with different relative concentrations in all of the tested samples. Several other TAGs were detected as minor components and were present in

  8. Accurate Mass GC/LC-Quadrupole Time of Flight Mass Spectrometry Analysis of Fatty Acids and Triacylglycerols of Spicy Fruits from the Apiaceae Family

    Nguyen, Thao; Aparicio, Mario; Saleh, Mahmoud A.

    2016-01-01

    The triacylglycerol (TAG) structure and the regio-stereospecific distribution of fatty acids (FA) of seed oils from most of the Apiaceae family are not well documented. The TAG structure ultimately determines the final physical properties of the oils and the position of FAs in the TAG molecule affects the digestion; absorption and metabolism; and physical and technological properties of TAGs. Fixed oils from the fruits of dill (Anethum graveolens), caraway (Carum carvi), cumin (Cuminum cyminum), coriander (Coriandrum sativum), anise (Pimpinella anisum), carrot (Daucus carota), celery (Apium graveolens), fennel (Foeniculum vulgare), and Khella (Ammi visnaga), all from the Apiaceae family, were extracted at room temperature in chloroform/methanol (2:1 v/v) using percolators. Crude lipids were fractionated by solid phase extraction to separate neutral triacylglycerols (TAGs) from other lipids components. Neutral TAGs were subjected to transesterification process to convert them to their corresponding fatty acids methyl esters (FAMES) using 1% boron trifluoride (BF3) in methanol. FAMES were analyzed by gas chromatography-quadrupole time of flight (GC-QTOF) mass spectrometry. Triglycerides were analyzed using high performance liquid chromatography-quadrupole time of flight (LC-QTOF) mass spectrometry. Petroselinic acid was the major fatty acid in all samples ranging from 57% of the total fatty acids in caraway up to 82% in fennel. All samples contained palmitic (16:0), palmitoleic (C16:1n-9), stearic (C18:0), petroselinic (C18:1n-12), linoleic (C18:2n-6), linolinic (18:3n-3), and arachidic (C20:0) acids. TAG were analyzed using LC-QTOF for accurate mass identification and mass spectrometry/mass spectrometry (MS/MS) techniques for regiospesific elucidation of the identified TAGs. Five major TAGs were detected in all samples but with different relative concentrations in all of the tested samples. Several other TAGs were detected as minor components and were present in

  9. Accurate offline dispersion measurement of Petawatt-class chirped pulse amplification compressor and stretcher systems

    Complete text of publication follows. The Advanced Radiographic Capability (ARC) on the National Ignition Facility (NIF) is designed to produce energetic x-rays in the range of 10-100 keV for backlighting NIF targets. ARC will convert 4 of the 192 NIF beamlines into 8 split beams, delivering laser pulses with adjustable pulse durations from 1 ps to 50 ps at the kilo-Joule level. Adjustable time delays between the 8 beams enable X-ray 'motion-picture' capture with tens-of-picosecond resolution during the critical phases of an ICF shot. The precise alignment of stretcher-compressor pairs in energetic chirped pulse amplification (CPA) systems is tedious and requires several iterations using advanced temporal diagnostics until the shortest pulse durations and highest peak intensities are achieved. For large, energetic Petawatt laser systems with beam sizes up to 40 cm, diffraction gratings in the compressor reach meter-scale size and are difficult to precisely align. We developed a group delay diagnostic which enables accurate, offline measurements of highly dispersive components such as stretchers or compressors with sub-picosecond accuracy. This diagnostic tool enables us to simply measure each dispersive component offline, and balance the dispersion in each beamline. Furthermore it allows exactly matching the dispersion of ARC's eight, independent four-grating compressors, which is critical for producing eight identical pulses. ARC utilizes a unique, folded compressor design for maximum compactness; two 5.5 m long vacuum vessels house 8 compressors with 91 cm x 45 cm multilayer, dielectric gratings. The group delay diagnostic utilizes the phase-shift technique for measuring the dispersion characteristics of each individual element, e.g. grating stretcher, chirped fiber Bragg grating, grating compressor, material dispersion, or an entire laser system. The system uses an amplitude modulated, highly-stable, single-frequency laser, which is scanned over the spectral

  10. Infrared Thermometer: an accurate tool for temperature measurement during renal surgery

    Giovanni Scala Marchini

    2013-07-01

    Full Text Available Purpose To evaluate infrared thermometer (IRT accuracy compared to standard digital thermometer in measuring kidney temperature during arterial clamping with and without renal cooling. Materials and Methods 20 pigs weighting 20Kg underwent selective right renal arterial clamping, 10 with (Group 1 - Cold Ischemia with ice slush and 10 without renal cooling (Group 2 - Warm Ischemia. Arterial clamping was performed without venous clamping. Renal temperature was serially measured following clamping of the main renal artery with the IRT and a digital contact thermometer (DT: immediate after clamping (T0, after 2 (T2, 5 (T5 and 10 minutes (T10. Temperature values were expressed in mean, standard deviation and range for each thermometer. We used the T student test to compare means and considered p < 0.05 to be statistically significant. Results In Group 1, mean DT surface temperature decrease was 12.6 ± 4.1°C (5-19°C while deep DT temperature decrease was 15.8 ± 1.5°C (15-18°C. For the IRT, mean temperature decrease was 9.1 ± 3.8°C (3-14°C. There was no statistically significant difference between thermometers. In Group 2, surface temperature decrease for DT was 2.7 ± 1.8°C (0-4°C and mean deep temperature decrease was 0.5 ± 1.0°C (0-3°C. For IRT, mean temperature decrease was 3.1 ± 1.9°C (0-6°C. No statistically significant difference between thermometers was found at any time point. conclusions IRT proved to be an accurate non-invasive precise device for renal temperature monitoring during kidney surgery. External ice slush cooling confirmed to be fast and effective at cooling the pig model. IRT = Infrared thermometer DT = Digital contact thermometer D:S = Distance-to-spot ratio

  11. Masses of the components of SB2 binaries observed with Gaia - III. Accurate SB2 orbits for 10 binaries and masses of HIP 87895

    Kiefer, F.; Halbwachs, J.-L.; Arenou, F.; Pourbaix, D.; Famaey, B.; Guillout, P.; Lebreton, Y.; Nebot Gómez-Morán, A.; Mazeh, T.; Salomon, J.-B.; Soubiran, C.; Tal-Or, L.

    2016-05-01

    In anticipation of the Gaia astrometric mission, a large sample of spectroscopic binaries has been observed since 2010 with the Spectrographe pour l'Observation des PHénomènes des Intérieurs Stellaires et des Exoplanètes spectrograph at the Haute-Provence Observatory. Our aim is to derive the orbital elements of double-lined spectroscopic binaries (SB2s) with an accuracy sufficient to finally obtain the masses of the components with relative errors as small as 1 per cent when the astrometric measurements of Gaia are taken into account. In this paper, we present the results from five years of observations of 10 SB2 systems with periods ranging from 37 to 881 d. Using the TODMOR algorithm, we computed radial velocities from the spectra, and then derived the orbital elements of these binary systems. The minimum masses of the components are then obtained with an accuracy better than 1.2 per cent for the 10 binaries. Combining the radial velocities with existing interferometric measurements, we derived the masses of the primary and secondary components of HIP 87895 with an accuracy of 0.98 and 1.2 per cent, respectively.

  12. Masses of the components of SB2 binaries observed with Gaia. III. Accurate SB2 orbits for 10 binaries and masses of HIP 87895

    Kiefer, Flavien; Arenou, Frédéric; Pourbaix, Dimitri; Famaey, Benoit; Guillout, Patrick; Lebreton, Yveline; Gómez-Morán, Ada Nebot; Mazeh, Tsevi; Salomon, Jean-Baptiste; Soubiran, Caroline; Tal-Or, Lev

    2016-01-01

    In anticipation of the Gaia astrometric mission, a large sample of spectroscopic binaries has been observed since 2010 with the SOPHIE spectrograph at the Haute--Provence Observatory. Our aim is to derive the orbital elements of double-lined spectroscopic binaries (SB2s) with an accuracy sufficient to finally obtain the masses of the components with relative errors as small as 1 % when the astrometric measurements of Gaia are taken into account. In this paper we present the results from five years of observations of 10 SB2 systems with periods ranging from 37 to 881 days. Using the TODMOR algorithm we computed radial velocities from the spectra, and then derived the orbital elements of these binary systems. The minimum masses of the components are then obtained with an accuracy better than 1.2 % for the ten binaries. Combining the radial velocities with existing interferometric measurements, we derived the masses of the primary and secondary components of HIP 87895 with an accuracy of 0.98 % and 1.2 % respect...

  13. New Beta-delayed Neutron Measurements in the Light-mass Fission Group

    A new accurate determination of beta-delayed neutron emission probabilities from nuclei in the low mass region of the light fission group has been performed. The measurements were carried out using the BELEN 4π neutron counter at the IGISOL-JYFL mass separator in combination with a Penning trap. The new results significantly improve the uncertainties of neutron emission probabilities for 91Br, 86As, 85As, and 85Ge nuclei

  14. Highly accurate measurements of the spontaneous fission half-life of 240,242Pu

    SALVADOR CASTINEIRA PAULA; BRYS TOMASZ; EYKENS ROGER; Hambsch, Franz-Josef; MOENS Andre; Oberstedt, Stephan; SIBBENS Goedele; VANLEEUW DAVID; Vidali, Marzio; Pretel, C.

    2013-01-01

    Fast spectrum neutron-induced fission cross-section data for transuranic isotopes are of special demand from the nuclear data community. In particular highly accurate data are needed for the new generation IV nuclear applications. The aim is to obtain precise neutron-induced fission cross sections for 240Pu and 242Pu. To do so, accurate data on spontaneous fission half-lives must be available. Also, minimizing uncertainties in the detector efficiency is a key point. We studied both isotopes b...

  15. Mass measurements of exotic nuclei with speg

    Masses of up to know unknown nuclei have been obtained in the present experiment with a total of 13 hours of beam for accumulation of data. Masses of 20N, 21N, 23O, 24F, 25F and 26F are given and compared to predictions from other references

  16. High precision mass measurements in Ψ and Υ families revisited

    High precision mass measurements in Ψ and Υ families performed in 1980-1984 at the VEPP-4 collider with OLYA and MD-1 detectors are revisited. The corrections for the new value of the electron mass are presented. The effect of the updated radiative corrections has been calculated for the J/Ψ(1S) and Ψ(2S) mass measurements

  17. Measurement of Black Hole Mass Radio-Loud Quasars

    Cheng-Yue Su; Z.-F. Chen; R.-L. He; C.-H. Zhang; T.-T. Wang

    2011-03-01

    In this work, we construct a sample of 1585 radio-loud quasars to measure their black hole masses using broad emission lines. We compare our black hole masses with the virial black hole masses measured by Shen et al. (2010).We find that there is a large deviation between them if our black hole mass is measured from the CIV broad emission line. Whereas, if our black hole mass is measured from broad emission line of Mg II or H, both the values are consistent.

  18. In-situ measurements of material thermal parameters for accurate LED lamp thermal modelling

    Vellvehi, M.; Perpina, X.; Jorda, X.; Werkhoven, R.J.; Kunen, J.M.G.; Jakovenko, J.; Bancken, P.; Bolt, P.J.

    2013-01-01

    This work deals with the extraction of key thermal parameters for accurate thermal modelling of LED lamps: air exchange coefficient around the lamp, emissivity and thermal conductivity of all lamp parts. As a case study, an 8W retrofit lamp is presented. To assess simulation results, temperature is

  19. Accurate wavelength prediction of photonic crystal resonant reflection and applications in refractive index measurement

    Hermannsson, Pétur Gordon; Vannahme, Christoph; Smith, Cameron L. C.;

    2014-01-01

    superstrate materials. The importance of accounting for material dispersion in order to obtain accurate simulation results is highlighted, and a method for doing so using an iterative approach is demonstrated. Furthermore, an application for the model is demonstrated, in which the material dispersion of a...

  20. Measurements of the top quark mass with the ATLAS detector

    Brandt, Oleg

    2015-01-01

    The top quark mass is one of the fundamental parameters of the Standard Model. In these proceedings, recent measurements of the top quark mass in $pp$ collisions at centre-of-mass energies of $\\sqrt s=7$ and 8~TeV data in Run I of the Large Hadron Collider using the ATLAS detector are reviewed. A measurement using lepton+jets events is presented, where a multidimensional template fit is used to constrain the uncertainties on the energy measurements of jets. The measurement is combined with a measurement using dilepton events. In addition, novel measurements aiming to measure the mass in a welldefined scheme are presented. These measurements use precision theoretical QCD calculations for both inclusive $\\ttbar$ production and ttbar production with an additional jet to extract the top quark mass in the pole mass scheme.

  1. Accurate extraction of mobility in carbon nanotube network transistors using C-V and I-V measurements

    Yoon, Jinsu; Lee, Dongil; Kim, Chaewon; Lee, Jieun; Choi, Bongsik; Kim, Dong Myong; Kim, Dae Hwan; Lee, Mijung; Choi, Yang-Kyu; Choi, Sung-Jin

    2014-11-01

    The mobility of single-walled carbon nanotube (SWNT) network thin-film transistors (TFTs) is an essential parameter. Previous extraction methods for mobility encountered problems in extracting accurate intrinsic mobility due to the uncertainty of the SWNT density in the network channel and the existence of contact resistance at the source/drain electrodes. As a result, efficient and accurate extraction of the mobility in SWNT TFTs is challenging using previous methods. We propose a direct method of extracting accurate intrinsic mobility in SWNT TFTs by employing capacitance-voltage and current-voltage measurements. Consequently, we simply obtain accurate intrinsic mobility within the ink-jet printed SWNT TFTs without any complicated calculations.

  2. Preservation of the D0 W mass measurement to incorporate future PDF and physics models

    Cúth, Jakub

    2015-01-01

    The D0 experiment at the Fermilab Tevatron Collider provided in recent years one of the most accurate measurements of the W boson mass. The precise knowledge of the W boson mass, to- gether with the mass of the Higgs Boson and the top quark, provides one of the most crucial tests of the Standard Model of particle physics. The uncertainties of this measurement are currently dominated by the limited knowledge of the parton density functions, which will improve in future years. Therefore, a dedicated effort is being made by the D0 Collaboration to preserve the W boson mass analysis for a future reevaluation with improved proton descriptions and other im- provements in the modeling of W boson production and decay. We give an overview of this effort and discuss the underlying technical infrastructure. In addition, we also present a reevaluation of the W boson mass measurement based on R Ldt = 4 : 3 fb...

  3. First direct Penning trap mass measurements on nobelium and lawrencium

    The mass measurements of the three nobelium isotopes 252-254No and the lawrencium isotope 255Lr measured with the Penning trap mass spectrometer SHIPTRAP/GSI have been evaluated. These were the first direct mass measurements of transfermium elements ever performed. The results mark the first step in the exploration of masses of even heavier nuclides which is planned at SHIPTRAP. The main objective is to measure the endpoints of α-decay chains starting from superheavy nuclei in the region of the predicted island of stability. The SHIPTRAP results were compared with previous measurements based on α-decay chains and new literature values were obtained.

  4. Accurate macromolecular structures using minimal measurements from X-ray free-electron lasers

    Hattne, Johan; Echols, Nathaniel; Tran, Rosalie; Kern, Jan; Gildea, Richard J.; Brewster, Aaron S.; Alonso-Mori, Roberto; Glöckner, Carina; Hellmich, Julia; Laksmono, Hartawan; Sierra, Raymond G.; Lassalle-Kaiser, Benedikt; Lampe, Alyssa; Han, Guangye; Gul, Sheraz

    2014-01-01

    X-ray free-electron laser (XFEL) sources enable the use of crystallography to solve three-dimensional macromolecular structures under native conditions and free from radiation damage. Results to date, however, have been limited by the challenge of deriving accurate Bragg intensities from a heterogeneous population of microcrystals, while at the same time modeling the X-ray spectrum and detector geometry. Here we present a computational approach designed to extract statistically...

  5. Development of the Vortex Mass Flowmeter with Wall Pressure Measurement

    Li, Zhiyong; Sun, Zhiqiang

    2013-01-01

    Mass flow measurement is essential to the understanding and control of processes concerning fluid flow. The availability of reliable mass flowmeters, however, is far inadequate to meet the demand. In this paper we developed a practical vortex mass flowmeter with wall pressure measurement. The meter coefficient of mass flow rate was acquired through experiments with air at Reynolds numbers from 1.3×103 to 9.8×103. Here we show that the meter coefficient of mass flow rate is nearly constant at Reynolds numbers greater than 5.5×103. To further extend the lower limit, a correction factor related to the Reynolds number was introduced into the vortex mass flowmeter. The results show that the relative errors of the vortex mass flowmeter developed are basically within ±5%. This device can satisfy a diversity of requirements of mass flow measurement in engineering fields.

  6. Measurement of the W-boson mass

    We have determined mW=79.91±0.39 GeV/c2 from an analysis of W→eν and W→μν data from the Collider Detector at Fermilab in bar pp collisions at a c.m. energy of √s =1.8 TeV. This result, together with the world-average Z mass, determines the weak mixing angle to be sin2θW=0.232±0.008. Bounds on the top-quark mass are discussed

  7. EVALUATION OF OPPORTUNITIES OF SOLAR ENERGETICS ON THE BASIS OF ACCURATE GROUND-BASED MEASUREMENTS OF SOLAR RADIATION

    Aculinin A.

    2008-04-01

    Full Text Available Expected quantity of a solar energy received by solar panel is estimated on the basis of accurate measurements of solar radiation in Kishinev. Optimal orientation of solar panels and apparent volume of the electric power generated by solar panels are determined.

  8. EVALUATION OF OPPORTUNITIES OF SOLAR ENERGETICS ON THE BASIS OF ACCURATE GROUND-BASED MEASUREMENTS OF SOLAR RADIATION

    Aculinin A.; Smikov V.

    2008-01-01

    Expected quantity of a solar energy received by solar panel is estimated on the basis of accurate measurements of solar radiation in Kishinev. Optimal orientation of solar panels and apparent volume of the electric power generated by solar panels are determined.

  9. Accurate determination of Curium and Californium isotopic ratios by inductively coupled plasma quadrupole mass spectrometry (ICP-QMS) in 248Cm samples for transmutation studies

    The French Atomic Energy Commission has carried out several experiments including the mini-INCA (INcineration of Actinides) project for the study of minor-actinide transmutation processes in high intensity thermal neutron fluxes, in view of proposing solutions to reduce the radiotoxicity of long-lived nuclear wastes. In this context, a Cm sample enriched in 248Cm (∼97 %) was irradiated in thermal neutron flux at the High Flux Reactor (HFR) of the Laue-Langevin Institute (ILL). This work describes a quadrupole ICP-MS (ICP-QMS) analytical procedure for precise and accurate isotopic composition determination of Cm before sample irradiation and of Cm and Cf after sample irradiation. The factors that affect the accuracy and reproducibility of isotopic ratio measurements by ICP-QMS, such as peak centre correction, detector dead time, mass bias, abundance sensitivity and hydrides formation, instrumental background, and memory blank were carefully evaluated and corrected. Uncertainties of the isotopic ratios, taking into account internal precision of isotope ratio measurements, peak tailing, and hydrides formations ranged from 0.3% to 1.3%. This uncertainties range is quite acceptable for the nuclear data to be used in transmutation studies.

  10. Accurate determination of Curium and Californium isotopic ratios by inductively coupled plasma quadrupole mass spectrometry (ICP-QMS) in Cm-248 samples for transmutation studies

    The French Atomic Energy Commission has carried out several experiments including the mini-INCA (Incineration of Actinides) project for the study of minor-actinide transmutation processes in high intensity thermal neutron fluxes, in view of proposing solutions to reduce the radiotoxicity of long-lived nuclear wastes. In this context, a Cm sample enriched in 248Cm (similar to 97%) was irradiated in thermal neutron flux at the High Flux Reactor (HFR) of the Laue-Langevin Institute (ILL). This work describes a quadrupole ICP-MS (ICP-QMS) analytical procedure for precise and accurate isotopic composition determination of Cm before sample irradiation and of Cm and Cf after sample irradiation. The factors that affect the accuracy and reproducibility of isotopic ratio measurements by ICP-QMS, such as peak centre correction, detector dead time, mass bias, abundance sensitivity and hydrides formation, instrumental background, and memory blank were carefully evaluated and corrected. Uncertainties of the isotopic ratios, taking into account internal precision of isotope ratio measurements, peak tailing, and hydrides' formations ranged from 0. 3% to 1. 3%. This uncertainties' range is quite acceptable for the nuclear data to be used in transmutation studies. (authors)

  11. Integration of pulsatile gonadotropin secretion by timed urinary measurements: an accurate and sensitive 3-hour test

    The integration of pulsatile gonadotropin secretion by the radioimmunoassay of an acetone precipitation from a short-term urine sample was evaluated. FSH and LH excretion over a 3-h period was compared to the mean level of 10 blood samples obtained every 20 min for a similar time period from 71 patients. A highly significant correlation existed between blood and urine results. In addition, the gonadotropin levels obtained from a 3-h sample correlated well with the 24-h excretion of FSH and LH from the same individual. A 3-h urine collection can provide a simple, sensitive, and accurate means of assessing circulating FSH and LH levels. (U.S.)

  12. Accurate Measurement of the Relative Abundance of Different DNA Species in Complex DNA Mixtures

    Jeong, Sangkyun; Yu, Hyunjoo; Pfeifer, Karl

    2012-01-01

    A molecular tool that can compare the abundances of different DNA sequences is necessary for comparing intergenic or interspecific gene expression. We devised and verified such a tool using a quantitative competitive polymerase chain reaction approach. For this approach, we adapted a competitor array, an artificially made plasmid DNA in which all the competitor templates for the target DNAs are arranged with a defined ratio, and melting analysis for allele quantitation for accurate quantitation of the fractional ratios of competitively amplified DNAs. Assays on two sets of DNA mixtures with explicitly known compositional structures of the test sequences were performed. The resultant average relative errors of 0.059 and 0.021 emphasize the highly accurate nature of this method. Furthermore, the method's capability of obtaining biological data is demonstrated by the fact that it can illustrate the tissue-specific quantitative expression signatures of the three housekeeping genes G6pdx, Ubc, and Rps27 by using the forms of the relative abundances of their transcripts, and the differential preferences of Igf2 enhancers for each of the multiple Igf2 promoters for the transcription. PMID:22334570

  13. Accurate Monitoring and Fault Detection in Wind Measuring Devices through Wireless Sensor Networks

    Komal Saifullah Khan

    2014-11-01

    Full Text Available Many wind energy projects report poor performance as low as 60% of the predicted performance. The reason for this is poor resource assessment and the use of new untested technologies and systems in remote locations. Predictions about the potential of an area for wind energy projects (through simulated models may vary from the actual potential of the area. Hence, introducing accurate site assessment techniques will lead to accurate predictions of energy production from a particular area. We solve this problem by installing a Wireless Sensor Network (WSN to periodically analyze the data from anemometers installed in that area. After comparative analysis of the acquired data, the anemometers transmit their readings through a WSN to the sink node for analysis. The sink node uses an iterative algorithm which sequentially detects any faulty anemometer and passes the details of the fault to the central system or main station. We apply the proposed technique in simulation as well as in practical implementation and study its accuracy by comparing the simulation results with experimental results to analyze the variation in the results obtained from both simulation model and implemented model. Simulation results show that the algorithm indicates faulty anemometers with high accuracy and low false alarm rate when as many as 25% of the anemometers become faulty. Experimental analysis shows that anemometers incorporating this solution are better assessed and performance level of implemented projects is increased above 86% of the simulated models.

  14. Electromagnetic calorimeter and accurate measurement with the ATLAS detector of the LHC collider; Calorimetrie electromagnetique et mesures de precision avec le detecteur ATLAS aupres du collisionneur LHC

    Pralavorio, P

    2007-06-15

    The main purpose of the ATLAS experiment is the understanding of the underlying mechanisms that drive the breaking of the electro-weak symmetry through the discovery of Higgs bosons. An important element to achieve this aim was the design of an electromagnetic calorimeter able to investigate the decay channels: H {yields} {gamma}{gamma} and H {yields} 4e. The high performance of the calorimeter will allow us to get a better accuracy on the measuring values of W and top masses which is essential to indirectly constrain the mass of the Higgs. In the same way, accurate measurements of top and W properties during the decays of top and tWb vertex will be necessary to question the standard model and to see beyond. The author has been working for 9 years in the ATLAS project, he has been involved in the design, construction, qualification and testing phases of the electromagnetic calorimeter of ATLAS. This document is a detailed presentation of the calorimeter, of its qualification and of its expectations when LHC is operating. This document is organized into 4 chapters: 1) assets and weaknesses of the standard model, 2) the ATLAS experiment, 3) the electromagnetic calorimeter, and 4) accurate measurements with ATLAS. This document presented before an academic board will allow its author to manage research works and particularly to tutor thesis students. (A.C.)

  15. New Directions in Mass Communications Research: Physiological Measurement.

    Fletcher, James E.

    Psychophysiological research into the effects of mass media, specifically the music of the masses, promises increased insight into the control the media exert on all their consumers. Attention and retention of mass media messages can be tested by measuring the receiver's electrodernal activity, pupil dilation, peripheral vasodilation, and heart…

  16. Gravitational mass attraction measurement for drag-free references

    Swank, Aaron J.

    Exciting new experiments in gravitational physics are among the proposed future space science missions around the world. Such future space science experiments include gravitational wave observatories, which require extraordinarily precise instruments for gravitational wave detection. In fact, future space-based gravitational wave observatories require the use of a drag free reference sensor, which is several orders of magnitude more precise than any drag free satellite launched to date. With the analysis methods and measurement techniques described in this work, there is one less challenge associated with achieving the high-precision drag-free satellite performance levels required by gravitational wave observatories. One disturbance critical to the drag-free performance is an acceleration from the mass attraction between the spacecraft and drag-free reference mass. A direct measurement of the gravitational mass attraction force is not easily performed. Historically for drag-free satellite design, the gravitational attraction properties were estimated by using idealized equations between a point mass and objects of regular geometric shape with homogeneous density. Stringent requirements are then placed on the density distribution and fabrication tolerances for the drag-free reference mass and satellite components in order to ensure that the allocated gravitational mass attraction disturbance budget is not exceeded due to the associated uncertainty in geometry and mass properties. Yet, the uncertainty associated with mass properties and geometry generate an unacceptable uncertainty in the mass attraction calculation, which make it difficult to meet the demanding drag-free performance requirements of future gravitational wave observatories. The density homogeneity and geometrical tolerances required to meet the overall drag-free performance can easily force the use of special materials or manufacturing processes, which are impractical or not feasible. The focus of

  17. The mass accretion rate of galaxy clusters: a measurable quantity

    De Boni, Cristiano; Diaferio, Antonaldo; Giocoli, Carlo; Baldi, Marco

    2015-01-01

    We explore the possibility of measuring the mass accretion rate of galaxy clusters by using dense galaxy redshift surveys of their outer regions. By approximating the accretion with the infall of a spherical shell, the mass accretion rate only depends on the mass profile of the cluster in a thin shell at radii larger than $R_{200}$. This approximation is rather crude in hierarchical clustering scenarios, where both smooth accretion and aggregation of smaller dark matter haloes contribute to the mass accretion of clusters. Nevertheless, in the redshift range $z=[0,1]$, our prescription returns an average mass accretion rate within $20 \\%$ of the average rate derived with the more realistic merger trees of dark matter haloes extracted from $N$-body simulations. The mass accretion rate of galaxy clusters has been the topic of numerous detailed numerical and theoretical investigations, but so far it has remained inaccessible to measurements in the real Universe. Our result suggests that measuring the mass accreti...

  18. Added mass matrix estimation of beams partially immersed in water using measured dynamic responses

    Liu, Fushun; Li, Huajun; Qin, Hongde; Liang, Bingchen

    2014-09-01

    An added mass matrix estimation method for beams partially immersed in water is proposed that employs dynamic responses, which are measured when the structure is in water and in air. Discrepancies such as mass and stiffness matrices between the finite element model (FEM) and real structure could be separated from the added mass of water by a series of correction factors, which means that the mass and stiffness of the FEM and the added mass of water could be estimated simultaneously. Compared with traditional methods, the estimated added mass correction factors of our approach will not be limited to be constant when FEM or the environment of the structure changed, meaning that the proposed method could reflect the influence of changes such as water depth, current, and so on. The greatest improvement is that the proposed method could estimate added mass of water without involving any water-related assumptions because all water influences are reflected in measured dynamic responses of the structure in water. A five degrees-of-freedom (dofs) mass-spring system is used to study the performance of the proposed scheme. The numerical results indicate that mass, stiffness, and added mass correction factors could be estimated accurately when noise-free measurements are used. Even when the first two modes are measured under the 5 percent corruption level, the added mass could be estimated properly. A steel cantilever beam with a rectangular section in a water tank at Ocean University of China was also employed to study the added mass influence on modal parameter identification and to investigate the performance of the proposed method. The experimental results demonstrated that the first two modal frequencies and mode shapes of the updated model match well with the measured values by combining the estimated added mass in the initial FEM.

  19. Technical Note: PRESAGE three-dimensional dosimetry accurately measures Gamma Knife output factors

    Klawikowski, Slade J.; Yang, James N.; Adamovics, John; Ibbott, Geoffrey S.

    2014-01-01

    Small-field output factor measurements are traditionally very difficult because of steep dose gradients, loss of lateral electronic equilibrium, and dose volume averaging in finitely sized detectors. Three-dimensional (3D) dosimetry is ideal for measuring small output factors and avoids many of these potential challenges of point and two-dimensional detectors. PRESAGE 3D polymer dosimeters were used to measure the output factors for the 4 mm and 8 mm collimators of the Leksell Perfexion Gamma...

  20. Direct mass measurements of 194Hg and 194Au: A new route to the neutrino mass determination?

    The study of nuclear electron capture (EC) offers an exciting alternative for the determination of the neutrino mass. Whereas only tritium and 187Re can be used in the case of β-decay experiments involving the anti-neutrino, a potentially large number of EC-nuclides can be used in experiments involving the monochromatic neutrino. This alternative to β-decay experiments requires an accurate measurement of QEC-values of appropriate candidates. In the present work we initiate a search for such a candidate and determined the QEC-value of the electron capture in 194Hg by direct mass measurements of 194Hg and 194Au. The new QEC-value of 29(4) keV determined by the ISOLTRAP Penning-trap mass spectrometer at ISOLDE/CERN forbids the K-capture for 194Hg. However, it allows a determination of the neutrino mass by a combination of a micro-calorimetric measurement of the de-excitation spectrum from L-capture in 194Hg and a comparable QEC-value remeasurement by high-precision Penning trap mass spectrometry.

  1. Direct mass measurements of {sup 194}Hg and {sup 194}Au: A new route to the neutrino mass determination?

    Eliseev, S., E-mail: sergey.eliseev@mpi-hd.mpg.d [MPI fuer Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany); Boehm, Ch. [MPI fuer Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany); Beck, D. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, Planckstrasse 1, 64291 Darmstadt (Germany); Blaum, K. [MPI fuer Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany); Physikalisches Institut, Ruprecht-Karls-Universitaet, 69120 Heidelberg (Germany); Breitenfeldt, M. [Institut fuer Physik, Ernst-Moritz-Arndt-Universitaet, 17487 Greifswald (Germany); Fedosseev, V.N. [CERN, 1211 Geneva 23 (Switzerland); George, S. [MPI fuer Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany); Herfurth, F. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, Planckstrasse 1, 64291 Darmstadt (Germany); Herlert, A. [CERN, 1211 Geneva 23 (Switzerland); Kluge, H.-J. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, Planckstrasse 1, 64291 Darmstadt (Germany); Physikalisches Institut, Ruprecht-Karls-Universitaet, 69120 Heidelberg (Germany); Kowalska, M. [CERN, 1211 Geneva 23 (Switzerland); Lunney, D.; Naimi, S. [CSNSM-IN2P3-CNRS, Universite de Paris Sud, 91406 Orsay (France); Neidherr, D. [Institut fuer Physik, Johannes Gutenberg-Universitaet, 55099 Mainz (Germany); Novikov, Yu.N. [PNPI, Gatchina, 188300 St. Petersburg (Russian Federation); Rosenbusch, M.; Schweikhard, L. [Institut fuer Physik, Ernst-Moritz-Arndt-Universitaet, 17487 Greifswald (Germany); Schwarz, S. [NSCL, Michigan State University, East Lansing, MI 48824-1321 (United States); Seliverstov, M. [Institut fuer Physik, Johannes Gutenberg-Universitaet, 55099 Mainz (Germany); Zuber, K. [Institut fuer Kern- und Teilchenphysik, Technische Universitaet, 01069 Dresden (Germany)

    2010-10-11

    The study of nuclear electron capture (EC) offers an exciting alternative for the determination of the neutrino mass. Whereas only tritium and {sup 187}Re can be used in the case of {beta}-decay experiments involving the anti-neutrino, a potentially large number of EC-nuclides can be used in experiments involving the monochromatic neutrino. This alternative to {beta}-decay experiments requires an accurate measurement of Q{sub EC}-values of appropriate candidates. In the present work we initiate a search for such a candidate and determined the Q{sub EC}-value of the electron capture in {sup 194}Hg by direct mass measurements of {sup 194}Hg and {sup 194}Au. The new Q{sub EC}-value of 29(4) keV determined by the ISOLTRAP Penning-trap mass spectrometer at ISOLDE/CERN forbids the K-capture for {sup 194}Hg. However, it allows a determination of the neutrino mass by a combination of a micro-calorimetric measurement of the de-excitation spectrum from L-capture in {sup 194}Hg and a comparable Q{sub EC}-value remeasurement by high-precision Penning trap mass spectrometry.

  2. Precision mass measurements of radioactive nuclei at JYFLTRAP

    Rahaman, S; Eronen, T; Hager, U; Hakala, J; Jokinen, A; Kankainen, A; Moore, I D; Pentillä, H; Rinta-Antila, S; Rissanen, J; Saastamoinen, A; Sonoda, T; Weber, C; Äystö, J

    2007-01-01

    The Penning trap mass spectrometer JYFLTRAP was used to measure the atomic masses of radioactive nuclei with an uncertainty better than 10 keV. The atomic masses of the neutron-deficient nuclei around the N = Z line were measured to improve the understanding of the rp-process path and the SbSnTe cycle. Furthermore, the masses of the neutron-rich gallium (Z = 31) to palladium (Z = 46) nuclei have been measured. The physics impacts on the nuclear structure and the r-process paths are reviewed. A better understanding of the nuclear deformation is presented by studying the pairing energy around A = 100.

  3. Archimedes Revisited: A Faster, Better, Cheaper Method of Accurately Measuring the Volume of Small Objects

    Hughes, Stephen W.

    2005-01-01

    A little-known method of measuring the volume of small objects based on Archimedes' principle is described, which involves suspending an object in a water-filled container placed on electronic scales. The suspension technique is a variation on the hydrostatic weighing technique used for measuring volume. The suspension method was compared with two…

  4. W mass and width measurements at the Tevatron

    Nurse, Emily

    2007-01-01

    I present a measurement of the W boson mass (M_W) and width (G_W) using 200 and 350 pb-1 of CDF Run II data respectively. The measurements, performed in both the electron and muon decay channels, rely on a fit to the W transverse mass distribution. We measure M_W = 80413 +/- 48 MeV and G_W = 2032 +/- 71 MeV which represent the world's single most precise measurements to date.

  5. Measuring laser power as a force: a new paradigm to accurately monitor optical power during laser-based machining operations

    Williams, Paul; Simonds, Brian; Sowards, Jeffrey; Hadler, Joshua

    2016-03-01

    In laser manufacturing operations, accurate measurement of laser power is important for product quality, operational repeatability, and process validation. Accurate real-time measurement of high-power lasers, however, is difficult. Typical thermal power meters must absorb all the laser power in order to measure it. This constrains power meters to be large, slow and exclusive (that is, the laser cannot be used for its intended purpose during the measurement). To address these limitations, we have developed a different paradigm in laser power measurement where the power is not measured according to its thermal equivalent but rather by measuring the laser beam's momentum (radiation pressure). Very simply, light reflecting from a mirror imparts a small force perpendicular to the mirror which is proportional to the optical power. By mounting a high-reflectivity mirror on a high-sensitivity force transducer (scale), we are able to measure laser power in the range of tens of watts up to ~ 100 kW. The critical parameters for such a device are mirror reflectivity, angle of incidence, and scale sensitivity and accuracy. We will describe our experimental characterization of a radiation-pressure-based optical power meter. We have tested it for modulated and CW laser powers up to 92 kW in the laboratory and up to 20 kW in an experimental laser welding booth. We will describe present accuracy, temporal response, sources of measurement uncertainty, and hurdles which must be overcome to have an accurate power meter capable of routine operation as a turning mirror within a laser delivery head.

  6. Finding the Density of Objects without Measuring Mass and Volume

    Mumba, Frackson; Tsige, Mesfin

    2007-01-01

    A simple method based on the moment of forces and Archimedes' principle is described for finding density without measuring the mass and volume of an object. The method involves balancing two unknown objects of masses M[subscript 1] and M[subscript 2] on each side of a pivot on a metre rule and measuring their corresponding moment arms. The object…

  7. [Research on accurate measurement of oxygen content in coal using laser-induced breakdown spectroscopy in air environment].

    Yin, Wang-bao; Zhang, Lei; Wang, Le; Dong, Lei; Ma, Wei-guang; Jia, Suo-tang

    2012-01-01

    A technique about accurate measurement of oxygen content in coal in air environment using laser-induced breakdown spectroscopy (LIBS) is introduced in the present paper. Coal samples were excited by the laser, and plasma spectra were obtained. Combining internal standard method, temperature correction method and multi-line methods, the oxygen content of coal samples was precisely measured. The measurement precision is not less than 1.37% for oxygen content in coal analysis, so is satisfied for the requirement of coal-fired power plants in coal analysis. This method can be used in surveying, environmental protection, medicine, materials, archaeological and food safety, biochemical and metallurgy application. PMID:22497159

  8. PRESAGE 3D dosimetry accurately measures Gamma Knife output factors

    Small-field output factor measurements are traditionally very difficult because of steep dose gradients, loss of lateral electronic equilibrium, and dose volume averaging in finitely sized detectors. Three-dimensional (3D) dosimetry is ideal for measuring small output factors and avoids many of these potential challenges of point and 2D detectors. PRESAGE 3D polymer dosimeters were used to measure the output factors for the 4 mm and 8 mm collimators of the Leksell Perfexion Gamma Knife radiosurgery treatment system. Discrepancies between the planned and measured distance between shot centers were also investigated. A Gamma Knife head frame was mounted onto an anthropomorphic head phantom. Special inserts were machined to hold 60 mm diameter, 70 mm tall cylindrical PRESAGE dosimeters. The phantom was irradiated with one 16 mm shot and either one 4 mm or one 8 mm shot, to a prescribed dose of either 3 Gy or 4 Gy to the 50% isodose line. The two shots were spaced between 30 mm and 60 mm apart and aligned along the central axis of the cylinder. The Presage dosimeters were measured using the DMOS-RPC optical CT scanning system. Five independent 4 mm output factor measurements fell within 2% of the manufacturer’s Monte Carlo simulation-derived nominal value, as did two independent 8 mm output factor measurements. The measured distances between shot centers varied by ±0.8 mm with respect to the planned shot displacements. On the basis of these results, we conclude that PRESAGE dosimetry is excellently suited to quantify the difficult-to-measure Gamma Knife output factors. (note)

  9. Energy resolution for accurate measurements of the X-ray linear attenuation coefficient

    At energies below 100keV, measurements of the X-ray linear attenuation coefficient μ, require either a mono-energetic source or a detector with good energy resolution. The majority of X-ray sources contain a spread of energies whilst detectors have finite energy resolution. Beam hardening, arising from the preferential attenuation of lower energy X-rays, introduces systematic errors to μ measurements. These errors are examined for measurements with characteristic X-rays, and for poly-energetic sources in conjunction with energy dispersive detection. Industrial and medical applications are considered, at energies 5-110keV for biological materials, aluminium, iron and copper

  10. Mass Measurement of Single Intact Nanoparticles in a Cylindrical Ion Trap.

    Zhang, Ning; Zhu, Kai; Xiong, Caiqiao; Jiang, Yurong; Chang, Huan-Cheng; Nie, Zongxiu

    2016-06-01

    Accurate nanoparticle mass characterization is a challenging task, especially at a single particle level. To solve this problem, a strategy for the mass measurement of single intact nanoparticle was proposed. A microscopy-based ion trap mass spectrometer was built up. To improve the detection sensitivity, a cylindrical ion trap with transparent conductive end-caps was used to increase the transmission of scattered light, and a vacuum ultraviolet lamp was used to increase the charge state of the isolated nanoparticle. By detecting the scattered light of the isolated nanoparticle, a series of secular frequencies were obtained, from which the corresponding mass-to-charge ratio of the nanoparticle was calculated. Finally, a Labview program was used to help deduce the charge state and absolute mass of the individual nanoparticle. Masses of gold nanoparticles with different sizes were accurately examined, which are (5.08 ± 0.44) × 10(7) Da for 20 nm, (3.55 ± 0.34) × 10(8) Da for 40 nm, and (1.22 ± 0.14) × 10(9) Da for 60 nm, respectively. The mass of MOFs with irregular shapes was also determined, which is (6.48 ± 1.08) × 10(9) Da. This method can provide the mass information on nanomaterials, thus opens up new possibility of characterizing nanoparticles at the single particle level. PMID:27167332

  11. Accurate Ultrasonic Measurement of Surface Profile Using Phase Shift of Echo and Inverse Filtering

    Arihara, Chihiro; Hasegawa, Hideyuki; Kanai, Hiroshi

    2006-05-01

    Atherosclerosis is the main cause of circulatory diseases such as myocardial infarction and cerebral infarction, and it is very important to diagnose atherosclerosis in its early stage. In the early stage of atherosclerosis, the luminal surface of an arterial wall becomes rough because of the injury of the endothelium [R. Ross: New Engl. J. Med. 340 (2004) 115]. Conventional ultrasonic diagnostic equipments cannot detect such roughness on the order of micrometer because of their low resolution of approximately 0.1 mm. In this study, for the accurate detection of surface roughness, an ultrasonic beam was scanned in the direction that is parallel to the surface of an object. When there is a gap on the surface, the phase of the echo from the surface changes because the distance between the probe and the surface changes during the scanning. Therefore, surface roughness can be assessed by estimating the phase shift of echoes obtained during the beam scanning. Furthermore, lateral resolution, which is deteriorated by a finite diameter of the ultrasound beam, was improved by an inverse filter. By using the proposed method, the surface profile of a phantom, which had surface roughness on the micrometer order, was detected, and the estimated surface profiles became more precise by applying the inverse filter.

  12. Accurate on-chip measurement of the Seebeck coefficient of high mobility small molecule organic semiconductors

    C. N. Warwick

    2015-09-01

    Full Text Available We present measurements of the Seebeck coefficient in two high mobility organic small molecules, 2,7-dioctyl[1]benzothieno[3,2-b][1]benzothiophene (C8-BTBT and 2,9-didecyl-dinaphtho[2,3-b:2′,3′-f]thieno[3,2-b]thiophene (C10-DNTT. The measurements are performed in a field effect transistor structure with high field effect mobilities of approximately 3 cm2/V s. This allows us to observe both the charge concentration and temperature dependence of the Seebeck coefficient. We find a strong logarithmic dependence upon charge concentration and a temperature dependence within the measurement uncertainty. Despite performing the measurements on highly polycrystalline evaporated films, we see an agreement in the Seebeck coefficient with modelled values from Shi et al. [Chem. Mater. 26, 2669 (2014] at high charge concentrations. We attribute deviations from the model at lower charge concentrations to charge trapping.

  13. Accurate evaluation of viscoelasticity of radial artery wall during flow-mediated dilation in ultrasound measurement

    Sakai, Yasumasa; Taki, Hirofumi; Kanai, Hiroshi

    2016-07-01

    In our previous study, the viscoelasticity of the radial artery wall was estimated to diagnose endothelial dysfunction using a high-frequency (22 MHz) ultrasound device. In the present study, we employed a commercial ultrasound device (7.5 MHz) and estimated the viscoelasticity using arterial pressure and diameter, both of which were measured at the same position. In a phantom experiment, the proposed method successfully estimated the elasticity and viscosity of the phantom with errors of 1.8 and 30.3%, respectively. In an in vivo measurement, the transient change in the viscoelasticity was measured for three healthy subjects during flow-mediated dilation (FMD). The proposed method revealed the softening of the arterial wall originating from the FMD reaction within 100 s after avascularization. These results indicate the high performance of the proposed method in evaluating vascular endothelial function just after avascularization, where the function is difficult to be estimated by a conventional FMD measurement.

  14. Accurate measurement of the main refractive indices and thermo-optical coefficients of the calcite crystal

    Shuang Zhao; Fuquan Wu; Haifeng Wang; Weigang Zhong; Xiuzhen Li; Hengjing Tang; Meng Shi; Hongyan Deng

    2007-01-01

    The main refractive indices of calcite crystal are measured by the means of auto-collimation, and the thermo-optical coefficients are calculated. The coefficient expression of Sellmeier equation is obtained by solving Sellmeier equation strictly and the refractive indices of different wavelengths are calculated, which accord with experimental esultsery well. The measured main refractive indices of calcite at 488-nm wavelength are identical with the values obtained by Sellmeier equation.

  15. HEASARC Astronomical Archive: GLIESE2MAS - Gliese Catalog Stars with Accurate Coordinates and 2MASS Cross-Identifications

    National Aeronautics and Space Administration — This table contains precise epoch 2000 coordinates and cross-identifications to sources in the 2MASS Point Source Catalog for nearly all stars in the Gliese,...

  16. External urethral sphincter pressure measurement: an accurate method for the diagnosis of detrusor external sphincter dyssynergia?

    Carlos H Suzuki Bellucci

    Full Text Available BACKGROUND: Combined pelvic floor electromyography (EMG and videocystourethrography (VCUG during urodynamic investigation are the most acceptable and widely agreed methods for diagnosing detrusor external sphincter dyssynergia (DESD. Theoretically, external urethral sphincter pressure (EUSP measurement would provide enough information for the diagnosis of DESD and could simplify the urodynamic investigation replacing combined pelvic floor EMG and VCUG. Thus, we evaluated the diagnostic accuracy of EUSP measurement for DESD. PATIENTS #ENTITYSTARTX00026; METHODS: A consecutive series of 72 patients (36 women, 36 men with neurogenic lower urinary tract dysfunction able to void spontaneously was prospectively evaluated at a single university spinal cord injury center. Diagnosis of DESD using EUSP measurement (index test versus combined pelvic floor EMG and VCUG (reference standard was assessed according to the recommendations of the Standards for Reporting of Diagnostic Accuracy Initiative. RESULTS: Using EUSP measurement (index test and combined pelvic floor EMG and VCUR (reference standard, DESD was diagnosed in 10 (14% and in 41 (57% patients, respectively. More than half of the patients presented discordant diagnosis between the index test and the reference standard. Among 41 patients with DESD diagnosed by combined pelvic floor EMG and VCUR, EUSP measurement identified only 6 patients. EUSP measurement had a sensitivity of 15% (95% CI 5%-25%, specificity of 87% (95% CI 76%-98%, positive predictive value of 60% (95% CI 30%-90%, and negative predictive value of 56% (95% CI 44%-68% for the diagnosis of DESD. CONCLUSIONS: For diagnosis of DESD, EUSP measurement is inaccurate and cannot replace combined pelvic floor EMG and VCUR.

  17. A high sensitivity assay is more accurate than a classical assay for the measurement of plasma CRP levels in endometriosis

    Vodolazkaia Alexandra; Bossuyt Xavier; Fassbender Amelie; Kyama Cleophas M; Meuleman Christel; Peeraer Karen; Tomassetti Carla; D'Hooghe Thomas M

    2011-01-01

    Abstract Background Endometriosis is associated with chronic subclinical inflammation. C-reactive protein (CRP), a marker of inflammation, could serve as a biomarker of endometriosis. We tested the hypothesis that a high sensitivity CRP assay (hsCRP) is more accurate than a classical CRP assay in the detection of subclinical inflammation in plasma of women with endometriosis. Methods CRP levels were measured by hsCRP and classical CRP assays in plasma of 204 women with endometriosis and 91 wo...

  18. An accurate measurement of PMT TTS based on the photoelectron spectrum

    Huang, W P; Li, C; Jiang, K; Zhao, X K

    2014-01-01

    The water Cherenkov detector array (WCDA) for the large high altitude air shower observatory(LHAASO) will employ more than 3600 hemisphere 8 inch photomultiplier tubes (PMT). The good time performance of PMT, especially the transit time spread (TTS), is required for WCDA. TTS is usually defined as the TTS of single photoelectron, and usually determined by using single photoelectron counting technique. A method using the photoelectron spectrum is researched for the measurement of TTS. The method is appropriate for multi-photoelectrons and makes it possible to measure the TTS of different photoelectrons at the same time. The TTS of different photoelectrons is measured for Hamamatsu R5912 with the divider circuit designed in specifically. The TTS of single photoelectron is determined to 3.3 ns and satisfies the requirement of WCDA.

  19. Accurate DOSY measure of out-of-equilibrium systems by permutated DOSY (p-DOSY)

    Oikonomou, Maria; Velders, Aldrik H; Delsuc, Marc-André

    2015-01-01

    NMR spectroscopy is a perfect tool for monitoring in-situ chemical reactions. In particular, DOSY measurement is well suited to characterize transient species by the determination of their sizes. However, here we bring to light a difficulty in the DOSY experiments performed on out-of-equilibrium systems. On such a system, the evolution of the concentration of species interferes with the measurement process, and creates a bias on the diffusion coefficient determination that may lead to erroneous interpretations. We show that a random permutation of the series of gradient strengths used during the DOSY experiment allows to average out this bias. This approach, that we name p-DOSY does not require changes in the the pulse sequences nor in the processing software, and restores completely the full accuracy of the measure. This technique is demonstrated on the monitoring of the anomerization reaction of $\\alpha$ to $\\beta$ glucose.

  20. Fast and Accurate Measurement of Entropy Profiles of Commercial Lithium-Ion Cells

    We report on an effective approach to speed up the measurement of thermodynamic characterization curves (entropy of reaction ΔrS(x)) of rechargeable batteries, in particular commercial 18650 lithium ion cells. We propose and demonstrate a measurement and data processing protocol that reduces the time required to record entropy profiles from time scales of weeks to time scales of hours – without loss in accuracy. For time consuming studies such as investigations on ageing of battery cells, entropy profile measurements thus become as feasible as conventional electrochemical characterisation techniques like dV/dQ or cyclic voltammetry. We demonstrate this at the examples of two ageing protocols applied to a commercial high power and a commercial high energy cell, respectively: (i) accelerated calendric aging by storing cells at 100% state of charge at 60 °C and (ii) continuous cycling with a 1C current at 25 °C

  1. Pulsed Frequency Shifted Feedback Laser for Accurate Long Distance Measurements: Beat Order Determination

    Pique, Jean-Paul

    2012-01-01

    Long-distance measurements (10 m - 1000 m) with an accuracy of 10-7 is a challenge for many applications. We show that it is achievable with Frequency Shifted Feedback (FSF) laser interferometry technique, provided that the determination of the radio frequency beat order be made without ambiguity and on a time scale compatible with atmospheric applications. Using the pulsed-FSF laser that we developed for laser guide star application, we propose and test, up to 240 m, a simple method for measuring the beat order in real time. The moving-comb and Yatsenko models are also discussed. The first of these models fails to interpret our long-distance interferometry results. We show that the accuracy of long-distance measurements depends primarily on the stabilization of the acoustic frequency of the modulator.

  2. Inflation model building with an accurate measure of e-folding

    Chongchitnan, Sirichai

    2016-01-01

    We revisit the problem of measuring the number of e-folding during inflation. It has become standard practice to take the logarithmic growth of the scale factor as a measure of the amount of inflation. However, this is only an approximation for the true amount of inflation required to solve the horizon and flatness problems. The aim of this work is to quantify the error in this approximation, and show how it can be avoided. We present an alternative framework for inflation model building using the inverse Hubble radius, aH, as the key parameter. We show that in this formalism, the correct number of e-folding arises naturally as a measure of inflation. As an application, we present an interesting model in which the entire inflationary dynamics can be solved analytically and exactly, and, in special cases, reduces to the familiar class of power-law models.

  3. ACCUWIND - Accurate wind speed measurements in wind energy - Summary report[Cup and sonic anemometers

    Friis Pedersen, T.; Dahlberg, J.Aa.; Cuerva, A.; Mouzakis, F.; Busche, P.; Eecen, P.; Sanz-Andres, A.; Franchini, S.; Markkilde Petersen, S.

    2006-07-15

    The cup anemometer is at present the standard instrument used for mean wind speed measurement in wind energy. It is being applied in high numbers around the world for wind energy assessments. It is also applied exclusively for accredited power performance measurements for certification and verification purposes, and for purposes of optimisation in research and development. The revised IEC standard on power performance measurements has now included requirements for classification of cup anemometers. The basis for setting up such requirements of cup anemometers is two EU projects SITEPARIDEN and CLASSCUP from which the proposed classification method for cup anemometers was developed for the IEC standard. While cup anemometers at present are the standard anemometer being used for average wind speed measurements, sonic anemometers have been developed significantly over the last years, and prices have come down. The application of sonic anemometers may increase in wind energy if they prove to have comparable or better operational characteristics compared to cup anemometers, and if similar requirements to sonic anemometers are established as for cup anemometers. Sonic anemometers have historically been used by meteorologists for turbulence measurements, but have also found a role on wind turbine nacelles for wind speed and yaw control purposes. The report on cup and sonic anemometry deals with establishment of robustness in assessment and classification by focus on methods and procedures for analysis of characteristics of cup and sonic anemometers. The methods and procedures provide a platform, hopefully for use in meeting the requirements of the IEC standard on power performance measurements, as well as for development of improved instruments. (au)

  4. Program package for accurate 3D field reconstruction from boundary measurements

    The problem of the magnetic field reconstruction inside a subregion in R3 from magnetic measurements on the closed boundary of this subregion is considered. The efficiency of the proposed method, algorithm and associated software for the precision magnet system is discussed. The results of the software verification, numerical experiments as well as the ones of the field reconstruction using boundary measurements in the magnet M1 of the separator COMBAS are given. Requirements to the position accuracy of sensors consistent with the required accuracy of the magnetic field reconstruction are defined. Recommendations on the magnetic scheme design for the field mapping are given. (author)

  5. Accurate measurement of the transition dipole moment of self-assembled quantum dots

    Stobbe, Søren; Johansen, Jeppe; Nikolaev, I.S.;

    2007-01-01

    Here we present quantitative measurements of the dipole moment of an ensemble of self-assembled quantum dots employing a modified optical local density of states (LDOS). The LDOS is controlled by varying the distance from the QDs to a semiconductor/air interface.......Here we present quantitative measurements of the dipole moment of an ensemble of self-assembled quantum dots employing a modified optical local density of states (LDOS). The LDOS is controlled by varying the distance from the QDs to a semiconductor/air interface....

  6. Can serum isotope levels accurately measure intestinal calcium absorption compared to gold-standard methods?

    Vreede, Andrew P; Jones, Andrea N; Hansen, Karen E

    2015-01-01

    Background Low fractional calcium absorption (FCA) contributes to osteoporosis but is not measured clinically, as the gold-standard method requires administration of two calcium tracers and a subsequent 24-h urine collection. We evaluated alternate methods to measure FCA, compared to the gold standard method. Methods We administered two stable calcium isotope tracers (~8 mg oral 44Ca and ~3 mg intravenous 42Ca) with breakfast to 20 fasting post-menopausal women (Cohort 1) 59 ± 7 years old wit...

  7. An evaluation of effective radiuses of bulk-wave ultrasonic transducers as circular piston sources for accurate velocity measurements.

    Arakawa, Mototaka; Kushibiki, Jun-ichi; Aoki, Naoya

    2004-05-01

    The effective radius of a bulk-wave ultrasonic transducer as a circular piston source, fabricated on one end of a synthetic silica (SiO2) glass buffer rod, was evaluated for accurate velocity measurements of dispersive specimens over a wide frequency range. The effective radius was determined by comparing measured and calculated phase variations due to diffraction in an ultrasonic transmission line of the SiO2 buffer rod/water-couplant/SiO2 standard specimen, using radio-frequency (RF) tone burst ultrasonic waves. Fourteen devices with different device parameters were evaluated. The velocities of the nondispersive standard specimen (C-7940) were found to be 5934.10 +/- 0.35 m/s at 70 to 290 MHz, after diffraction correction using the nominal radius (0.75 mm) for an ultrasonic device with an operating center frequency of about 400 MHz. Corrected velocities were more accurately found to be 5934.15 +/- 0.03 m/s by using the effective radius (0.780 mm) for the diffraction correction. Bulk-wave ultrasonic devices calibrated by this experimental procedure enable conducting extremely accurate velocity dispersion measurements. PMID:15217227

  8. Fast and Accurate Collocation of the Visible Infrared Imaging Radiometer Suite Measurements with Cross-Track Infrared Sounder

    Likun Wang

    2016-01-01

    Full Text Available Given the fact that Cross-track Infrared Sounder (CrIS and the Visible Infrared Imaging Radiometer Suite (VIIRS are currently onboard the Suomi National Polar-orbiting Partnership (Suomi NPP satellite and will continue to be carried on the same platform as future Joint Polar Satellite System (JPSS satellites for the next decade, it is desirable to develop a fast and accurate collocation scheme to collocate VIIRS products and measurements with CrIS for applications that rely on combining measurements from two sensors such as inter-calibration, geolocation assessment, and cloud detection. In this study, an accurate and fast collocation method to collocate VIIRS measurements within CrIS instantaneous field of view (IFOV directly based on line-of-sight (LOS pointing vectors is developed and discussed in detail. We demonstrate that this method is not only accurate and precise from a mathematical perspective, but also easy to implement computationally. More importantly, with optimization, this method is very fast and efficient and thus can meet operational requirements. Finally, this collocation method can be extended to a wide variety of sensors on different satellite platforms.

  9. An affordable and accurate conductivity probe for density measurements in stratified flows

    Carminati, Marco; Luzzatto-Fegiz, Paolo

    2015-11-01

    In stratified flow experiments, conductivity (combined with temperature) is often used to measure density. The probes typically used can provide very fine spatial scales, but can be fragile, expensive to replace, and sensitive to environmental noise. A complementary instrument, comprising a low-cost conductivity probe, would prove valuable in a wide range of applications where resolving extremely small spatial scales is not needed. We propose using micro-USB cables as the actual conductivity sensors. By removing the metallic shield from a micro-B connector, 5 gold-plated microelectrodes are exposed and available for 4-wire measurements. These have a cell constant ~550m-1, an intrinsic thermal noise of at most 30pA/Hz1/2, as well as sub-millisecond time response, making them highly suitable for many stratified flow measurements. In addition, we present the design of a custom electronic board (Arduino-based and Matlab-controlled) for simultaneous acquisition from 4 sensors, with resolution (in conductivity, and resulting density) exceeding the performance of typical existing probes. We illustrate the use of our conductivity-measuring system through stratified flow experiments, and describe plans to release simple instructions to construct our complete system for around 200.

  10. Measurement of rock mass deformation with grouted coaxial antenna cables

    Dowding, C. H.; Su, M. B.; O'Connor, K.

    1989-01-01

    Techniques presented herein show how reflected voltage pulses from coaxial antenna cable grouted in rock masses can be employed to quantify the type and magnitude of rock mass deformation. This measurement is similar to that obtained from a combined full profile extensometer (to measure local extension) and inclinometer (to measure local shearing). Rock mass movements deform the grouted cable, which locally changes cable capacitance and thereby the reflected wave form of the voltage pulse. Thus, by monitoring changes in these reflection signatures, it is possible to monitor rock mass deformation. This paper presents laboratory measurements necessary to quantitatively interpret the reflected voltage signatures. Cables were sheared and extended to correlate measured cable deformation with reflected voltage signals. Laboratory testing included development of grout mixtures with optimum properties for field installation and performance of a TDR (Time Domain Reflectometry) monitoring system. Finally, the interpretive techniques developed through laboratory measurements were applied to previously collected field data to extract hitherto unrealized information.

  11. An X-band waveguide measurement technique for the accurate characterization of materials with low dielectric loss permittivity

    Allen, Kenneth W.; Scott, Mark M.; Reid, David R.; Bean, Jeffrey A.; Ellis, Jeremy D.; Morris, Andrew P.; Marsh, Jeramy M.

    2016-05-01

    In this work, we present a new X-band waveguide (WR90) measurement method that permits the broadband characterization of the complex permittivity for low dielectric loss tangent material specimens with improved accuracy. An electrically long polypropylene specimen that partially fills the cross-section is inserted into the waveguide and the transmitted scattering parameter (S21) is measured. The extraction method relies on computational electromagnetic simulations, coupled with a genetic algorithm, to match the experimental S21 measurement. The sensitivity of the technique to sample length was explored by simulating specimen lengths from 2.54 to 15.24 cm, in 2.54 cm increments. Analysis of our simulated data predicts the technique will have the sensitivity to measure loss tangent values on the order of 10-3 for materials such as polymers with relatively low real permittivity values. The ability to accurately characterize low-loss dielectric material specimens of polypropylene is demonstrated experimentally. The method was validated by excellent agreement with a free-space focused-beam system measurement of a polypropylene sheet. This technique provides the material measurement community with the ability to accurately extract material properties of low-loss material specimen over the entire X-band range. This technique could easily be extended to other frequency bands.

  12. Measuring the LISA test mass magnetic proprieties with a torsion pendulum

    Hüller, M; Carbone, L; Cavalleri, A; Dolesi, R; Hoyle, C D; Vitale, S; Weber, W J

    2004-01-01

    Achieving the low frequency LISA sensitivity requires that the test masses acting as the interferometer end mirrors are free-falling with an unprecedented small degree of deviation. Magnetic disturbances, originating in the interaction of the test mass with the environmental magnetic field, can significantly deteriorate the LISA performance and can be parameterized through the test mass remnant dipole moment $\\vec{m}_r$ and the magnetic susceptibility $\\chi$. While the LISA test flight precursor LTP will investigate these effects during the preliminary phases of the mission, the very stringent requirements on the test mass magnetic cleanliness make ground-based characterization of its magnetic proprieties paramount. We propose a torsion pendulum technique to accurately measure on ground the magnetic proprieties of the LISA/LTP test masses.

  13. Negative electrospray ionisation of fluorotelomer alcohols (FTOH) and FTOH-derived acrylate surfactants by liquid chromatography coupled to accurate (tandem) mass spectrometry

    Trier, Xenia; Christensen, Jan H.; Niessen, Wilfried M. A.

    Fluorotelomer alcohols (FTOHs) are used to synthesize fluorinated surfactants, which form bioaccumulative perfluorinated degradation products, which are toxic to humans and the environment. To facilitate screening for FTOH-derived surfactants by LC-ESI–-MS, we identified product ions of FTOHs, an...... propose FTOH fragmentation pathways on two MS instruments. By extraction of FTOH basepeak ions from accurate mass spectra, homologues series of peaks showed up in an industrial blend of FTOH-derived fluoroacrylates used in food paper packaging....

  14. Systematic Errors in Black Hole Mass Measurements

    McConnell, Nicholas J.

    2014-01-01

    Compilations of stellar- and gas-dynamical measurements of supermassive black holes are often assembled without quantifying systematic errors from various assumptions in the dynamical modeling processes. Using a simple Monte-Carlo approach, I will discuss the level to which different systematic effects could bias scaling relations between black holes and their host galaxies. Given that systematic errors will not be eradicated in the near future, how wrong can we afford to be?

  15. Simultaneous and accurate measurement of the dielectric constant at many frequencies spanning a wide range

    Pérez-Aparicio, Roberto; Cottinet, Denis; Tanase, Marius; Metz, Pascal; Bellon, Ludovic; Naert, Antoine; Ciliberto, Sergio

    2015-01-01

    We present an innovative technique which allows the simultaneous measurement of the dielectric constant of a material at many frequencies, spanning a four orders of magnitude range chosen between 10 --2 Hz and 10 4 Hz. The sensitivity and accuracy are comparable to those obtained using standard single frequency techniques. The technique is based on three new and simple features: a) the precise real time correction of the amplication of a current amplier; b) the specic shape of the excitation signal and its frequency spectrum; and c) the precise synchronization between the generation of the excitation signal and the acquisition of the dielectric response signal. This technique is useful in the case of relatively fast dynamical measurements when the knowledge of the time evolution of the dielectric constant is needed.

  16. Development of a scattering probability method for accurate vapor fraction measurements by neutron radiography

    Joo, H

    1999-01-01

    Recent test results indicated drawbacks associated with the simple exponential attenuation method (SEAM) as currently applied to neutron radiography measurements to determine vapor fractions in a hydrogenous two-phase flow in a metallic conduit. The scattering component of the neutron beam intensity exiting the flow system is not adequately accounted for by SEAM, and this leads to inaccurate results. To properly account for the scattering effect, a neutron scattering probability method (SPM) is developed. The method applies a neutron-hydrogen scattering kernel to scattered thermal neutrons that leave the incident beam in narrow conduits but eventually show up elsewhere in the measurements. The SPM has been tested with known vapor (void) distributions within an acrylic disk and a water/vapor channel. The vapor (void) fractions deduced by SPM are in good agreement with the known exact values. Details of the scattering correction method and the test results are discussed.

  17. A Procedure for Accurately Measuring the Shaker Overturning Moment During Random Vibration Tests

    Nayeri, Reza D.

    2011-01-01

    Motivation: For large system level random vibration tests, there may be some concerns about the shaker's capability for the overturning moment. It is the test conductor's responsibility to predict and monitor the overturning moment during random vibration tests. If the predicted moment is close to the shaker's capability, test conductor must measure the instantaneous moment at low levels and extrapolate to higher levels. That data will be used to decide whether it is safe to proceed to the next test level. Challenge: Kistler analog formulation for computing the real-time moment is only applicable to very limited cases in which we have 3 or 4 load cells installed at shaker interface with hardware. Approach: To overcome that limitation, a simple procedure was developed for computing the overturning moment time histories using the measured time histories of the individual load cells.

  18. Switched integration amplifier-based photocurrent meter for accurate spectral responsivity measurement of photometers.

    Park, Seongchong; Hong, Kee-Suk; Kim, Wan-Seop

    2016-03-20

    This work introduces a switched integration amplifier (SIA)-based photocurrent meter for femtoampere (fA)-level current measurement, which enables us to measure a 107 dynamic range of spectral responsivity of photometers even with a common lamp-based monochromatic light source. We described design considerations and practices about operational amplifiers (op-amps), switches, readout methods, etc., to compose a stable SIA of low offset current in terms of leakage current and gain peaking in detail. According to the design, we made six SIAs of different integration capacitance and different op-amps and evaluated their offset currents. They showed an offset current of (1.5-85) fA with a slow variation of (0.5-10) fA for an hour under opened input. Applying a detector to the SIA input, the offset current and its variation were increased and the SIA readout became noisier due to finite shunt resistance and nonzero shunt capacitance of the detector. One of the SIAs with 10 pF nominal capacitance was calibrated using a calibrated current source at the current level of 10 nA to 1 fA and at the integration time of 2 to 65,536 ms. As a result, we obtained a calibration formula for integration capacitance as a function of integration time rather than a single capacitance value because the SIA readout showed a distinct dependence on integration time at a given current level. Finally, we applied it to spectral responsivity measurement of a photometer. It is demonstrated that the home-made SIA of 10 pF was capable of measuring a 107 dynamic range of spectral responsivity of a photometer. PMID:27140564

  19. An accurate absolute-scale measurement of bremsstrahlung following absorption of incident X and γ rays

    The spectrum of bremsstrahlung due to photoelectrons ejected by incident photons of energy 59.5 keV was measured. The coincidence setup with two HP germanium detectors was applied, in which the target-detector recorded the energy of ejected photoelectron after it radiated a bremsstrahlung photon, and another (second) detector detected energy of radiated bremsstrahlung photon. A detailed analysis of the measurement was made taking into account various detector-to-detector cross-talk processes. As expected, the experimental method gave a clean spectrum, which can be reliably determined on absolute scale in the low- and mid-energy range. The condition for reliable measurement are that the asymmetry ratio (the ratio of number of incident photons which reached the target detector and the second detector) is higher than approximately 1000 to reduce reverse-Compton scattering, and solid angle is smaller than about 0.15 sr to reduce the influence of double-cross-talk processes. (We name a group of processes double-cross-talk processes in which incident radiation produces secondary radiation in target detector, the secondary radiation escapes it and reaches the second detector where it induces tertiary radiation, which reaches the target detector and is absorbed therein.) Almost any line source of photons can be used even if of a complex spectrum. Therefore, simultaneous measurements at several incident energies are possible in one experiment. Application of a very weak source is possible because of very high signal-to-background ratio and high efficiency of the applied experimental method. The simple theoretical model of bremsstrahlung radiation due to photoelectrons in infinity-thick target gives results in a good agreement with the experimental data. The bremsstrahlung cross-section calculated using the well-known semi-empirical thick-target formula gives also a good agreement with the experimental data. (author)

  20. Accurate measurements and design standards: consistency of design and the travel of 'facts' between heterogeneous groups

    Velkar, Aashish

    2007-01-01

    Design standards are carriers and creators of facts, enabling facts about product value to travel between groups, and assisting in the creation of product value by establishing a reference or comparison against which product attributes are compared. However, when design standards are not consistent, facts about product value may not travel well, even when designs can be expressed or measured with a high degree of precision. Examining the evidence from British iron and steel industry in the ni...

  1. Three-Signal Method for Accurate Measurements of Depolarization Ratio with Lidar

    Reichardt, Jens; Baumgart, Rudolf; McGee, Thomsa J.

    2003-01-01

    A method is presented that permits the determination of atmospheric depolarization-ratio profiles from three elastic-backscatter lidar signals with different sensitivity to the state of polarization of the backscattered light. The three-signal method is insensitive to experimental errors and does not require calibration of the measurement, which could cause large systematic uncertainties of the results, as is the case in the lidar technique conventionally used for the observation of depolarization ratios.

  2. Easy Leaf Area: Automated Digital Image Analysis for Rapid and Accurate Measurement of Leaf Area

    Hsien Ming Easlon; Bloom, Arnold J.

    2014-01-01

    Premise of the study: Measurement of leaf areas from digital photographs has traditionally required significant user input unless backgrounds are carefully masked. Easy Leaf Area was developed to batch process hundreds of Arabidopsis rosette images in minutes, removing background artifacts and saving results to a spreadsheet-ready CSV file. Methods and Results: Easy Leaf Area uses the color ratios of each pixel to distinguish leaves and calibration areas from their background and compares ...

  3. On the Design of Accurate Spatial and Temporal Temperature Measurements in Sea Ice

    Meyer, Karsten

    2012-01-01

    Studies on sea ice have become increasingly popular among researchers in the last decades, due to its effect on the global climate and the challenges it presents for arctic engineering. The research is in demand of reliable data acquisition on various properties, in this case the temperature gradient in forming sea ice.This project continues the development of a spatial temperature instrument, which intends to provide measurements with an accuracy of 0.01°C, making the researchers able t...

  4. A Robust Method of Vehicle Stability Accurate Measurement Using GPS and INS

    Miao Zhibin

    2015-12-01

    Full Text Available With the development of the vehicle industry, controlling stability has become more and more important. Techniques of evaluating vehicle stability are in high demand. Integration of Global Positioning System (GPS and Inertial Navigation System (INS is a very practical method to get high-precision measurement data. Usually, the Kalman filter is used to fuse the data from GPS and INS. In this paper, a robust method is used to measure vehicle sideslip angle and yaw rate, which are two important parameters for vehicle stability. First, a four-wheel vehicle dynamic model is introduced, based on sideslip angle and yaw rate. Second, a double level Kalman filter is established to fuse the data from Global Positioning System and Inertial Navigation System. Then, this method is simulated on a sample vehicle, using Carsim software to test the sideslip angle and yaw rate. Finally, a real experiment is made to verify the advantage of this approach. The experimental results showed the merits of this method of measurement and estimation, and the approach can meet the design requirements of the vehicle stability controller.

  5. A Robust Method of Vehicle Stability Accurate Measurement Using GPS and INS

    Miao, Zhibin; Zhang, Hongtian; Zhang, Jinzhu

    2015-12-01

    With the development of the vehicle industry, controlling stability has become more and more important. Techniques of evaluating vehicle stability are in high demand. Integration of Global Positioning System (GPS) and Inertial Navigation System (INS) is a very practical method to get high-precision measurement data. Usually, the Kalman filter is used to fuse the data from GPS and INS. In this paper, a robust method is used to measure vehicle sideslip angle and yaw rate, which are two important parameters for vehicle stability. First, a four-wheel vehicle dynamic model is introduced, based on sideslip angle and yaw rate. Second, a double level Kalman filter is established to fuse the data from Global Positioning System and Inertial Navigation System. Then, this method is simulated on a sample vehicle, using Carsim software to test the sideslip angle and yaw rate. Finally, a real experiment is made to verify the advantage of this approach. The experimental results showed the merits of this method of measurement and estimation, and the approach can meet the design requirements of the vehicle stability controller.

  6. Investigation of a ten-path ultrasonic flow meter for accurate feedwater measurements

    Tawackolian, K.; Büker, O.; Hogendoorn, J.; Lederer, T.

    2014-07-01

    The flow instruments used in thermal power plants cannot be calibrated directly for the actual process conditions, since no traceable calibration facility with known uncertainty is available. A systematic investigation of the relevant influence parameters is therefore needed. It was found in earlier investigations that the dominant influences on the measurement uncertainty are the flow velocity profile and the temperature. In the present work, we report on our experimental study of the temperature and Reynolds number dependence of a new ten-path ultrasonic flow meter prototype. An improved measuring program is developed that allows for a systematic characterization. Special emphasis was placed on producing and validating well defined velocity profiles on a precision calibration flow rig. It was also for the first time intended and validated to generate fully developed Reynolds-similar velocity profiles for different temperatures so that the two main influence parameters, namely temperature and Reynolds number, can be clearly characterized separately. Since such ideal measurement conditions are not found in practical applications, the approach is also tested for a disturbed flow condition. A well defined disturbance is generated with a new flow disturber.

  7. Optical aperture area determination for accurate illuminance and luminous efficacy measurements of LED lamps

    Dönsberg, Timo; Mäntynen, Henrik; Ikonen, Erkki

    2016-06-01

    The measurement uncertainty of illuminance and, consequently, luminous flux and luminous efficacy of LED lamps can be reduced with a recently introduced method based on the predictable quantum efficient detector (PQED). One of the most critical factors affecting the measurement uncertainty with the PQED method is the determination of the aperture area. This paper describes an upgrade to an optical method for direct determination of aperture area where superposition of equally spaced Gaussian laser beams is used to form a uniform irradiance distribution. In practice, this is accomplished by scanning the aperture in front of an intensity-stabilized laser beam. In the upgraded method, the aperture is attached to the PQED and the whole package is transversely scanned relative to the laser beam. This has the benefit of having identical geometry in the laser scanning of the aperture area and in the actual photometric measurement. Further, the aperture and detector assembly does not have to be dismantled for the aperture calibration. However, due to small acceptance angle of the PQED, differences between the diffraction effects of an overfilling plane wave and of a combination of Gaussian laser beams at the circular aperture need to be taken into account. A numerical calculation method for studying these effects is discussed in this paper. The calculation utilizes the Rayleigh-Sommerfeld diffraction integral, which is applied to the geometry of the PQED and the aperture. Calculation results for various aperture diameters and two different aperture-to-detector distances are presented.

  8. Influence and measurement of mass ablation in ICF implosions

    Spears, B K; Hicks, D; Velsko, C; Stoyer, M; Robey, H; Munro, D; Haan, S; Landen, O; Nikroo, A; Huang, H

    2007-09-05

    Point design ignition capsules designed for the National Ignition Facility (NIF) currently use an x-ray-driven Be(Cu) ablator to compress the DT fuel. Ignition specifications require that the mass of unablated Be(Cu), called residual mass, be known to within 1% of the initial ablator mass when the fuel reaches peak velocity. The specifications also require that the implosion bang time, a surrogate measurement for implosion velocity, be known to +/- 50 ps RMS. These specifications guard against several capsule failure modes associated with low implosion velocity or low residual mass. Experiments designed to measure and to tune experimentally the amount of residual mass are being developed as part of the National Ignition Campaign (NIC). Tuning adjustments of the residual mass and peak velocity can be achieved using capsule and laser parameters. We currently plan to measure the residual mass using streaked radiographic imaging of surrogate tuning capsules. Alternative techniques to measure residual mass using activated Cu debris collection and proton spectrometry have also been developed. These developing techniques, together with bang time measurements, will allow us to tune ignition capsules to meet NIC specs.

  9. A Measurement of the Black-Hole Mass in NGC 1097 using ALMA

    Onishi, Kyoko; Sheth, Kartik; Kohno, Kotaro

    2015-01-01

    We present an estimate of the mass of the supermassive black hole (SMBH) in the nearby type-1 Seyfert galaxy \\object{NGC 1097} using Atacamma Large Millimeter/Submillimeter Array (ALMA) observations of dense gas kinematics. Dense molecular gas dynamics are traced with ${\\rm HCN} (J=1-0)$ and ${\\rm HCO^{+}} (J=1-0)$ emission lines. Assuming a host galaxy inclination of $46^{\\circ}$, we derive a SMBH mass, $M_{\\rm BH}=1.40^{+0.27}_{-0.32} \\times 10^{8}M_{\\odot}$, and an I-band mass to light ratio to be $5.14^{+0.03}_{-0.04}$, using ${\\rm HCN} (J=1-0)$. The estimated parameters are consistent between the two emission lines. The measured SMBH mass is in good agreement with the SMBH mass and bulge velocity dispersion relationship. Our result showcases ALMA's potential for deriving accurate SMBH masses, especially for nearby late-type galaxies. Larger samples and accurate SMBH masses will further elucidate the relationship between the black hole (BH) and host galaxy properties and constrain the coevolutionary growt...

  10. Comparative Ebulliometry: a Simple, Reliable Technique for Accurate Measurement of the Number Average Molecular Weight of Macromolecules. Preliminary Studies on Heavy Crude Fractions Ébulliométrie comparative : technique simple et fiable pour déterminer précisément la masse molaire moyenne en nombre des macromolécules. Etudes préliminaires sur des fractions lourdes de bruts

    Behar E.

    2006-12-01

    Full Text Available This article is divided into two parts. In the first part, the authors present a comparison of the major techniques for the measurement of the molecular weight of macromolecules. The bibliographic results are gathered in several tables. In the second part, a comparative ebulliometer for the measurement of the number average molecular weight (Mn of heavy crude oil fractions is described. The high efficiency of the apparatus is demonstrated with a preliminary study of atmospheric distillation residues and resins. The measurement of molecular weights up to 2000 g/mol is possible in less than 4 hours with an uncertainty of about 2%. Cet article comprend deux parties. Dans la première, les auteurs présentent une comparaison entre les principales techniques de détermination de la masse molaire de macromolécules. Les résultats de l'étude bibliographique sont rassemblés dans plusieurs tableaux. La seconde partie décrit un ébulliomètre comparatif conçu pour la mesure de la masse molaire moyenne en nombre (Mn des fractions lourdes des bruts. Une illustration de l'efficacité de cet appareil est indiquée avec l'étude préliminaire de résidus de distillation atmosphérique et de résines. En particulier, la mesure de masses molaires pouvant atteindre 2000 g/mol est possible en moins de 4 heures avec une incertitude expérimentale de l'ordre de 2 %.

  11. Top-quark mass measurements using jet rates at LHC

    Moch S.

    2013-11-01

    Full Text Available This work presents a new method to measure the top-quark mass in hadronic collisions[1]. The method uses the sensitivity of the tt¯+1$tar t + 1$-jet production on the top-quark mass. In detail we study the ℛ distribution defined as the tt¯+1$tar t + 1$-jet normalized cross section differential in the invariant mass of the total system and calculated at NLO accuracy. We prove that the ℛ distribution has a high sensitivity to the top-quark mass. Furthermore we investigate and quantify the impact of the dominant theoretical and experimental uncertainties. The results obtained show, that the method has the potential to be competitive in precision with established approaches and allows a complementary measurement of the top-quark mass at hadron colliders. We emphasize that in the proposed method the mass parameter is uniquely defined through one-loop renormalization.

  12. Rapid and accurate processing method for amide proton exchange rate measurement in proteins

    Koskela, Harri [University of Helsinki, Finnish Institute for Verification of the Chemical Weapons Convention (VERIFIN) (Finland)], E-mail: Harri.T.Koskela@helsinki.fi; Heikkinen, Outi; Kilpelaeinen, Ilkka; Heikkinen, Sami [University of Helsinki, Laboratory of Organic Chemistry (Finland)

    2007-04-15

    Exchange between protein backbone amide hydrogen and water gives relevant information about solvent accessibility and protein secondary structure stability. NMR spectroscopy provides a convenient tool to study these dynamic processes with saturation transfer experiments. Processing of this type of NMR spectra has traditionally required peak integration followed by exponential fitting, which can be tedious with large data sets. We propose here a computer-aided method that applies inverse Laplace transform in the exchange rate measurement. With this approach, the determination of exchange rates can be automated, and reliable results can be acquired rapidly without a need for manual processing.

  13. Rapid and accurate processing method for amide proton exchange rate measurement in proteins

    Exchange between protein backbone amide hydrogen and water gives relevant information about solvent accessibility and protein secondary structure stability. NMR spectroscopy provides a convenient tool to study these dynamic processes with saturation transfer experiments. Processing of this type of NMR spectra has traditionally required peak integration followed by exponential fitting, which can be tedious with large data sets. We propose here a computer-aided method that applies inverse Laplace transform in the exchange rate measurement. With this approach, the determination of exchange rates can be automated, and reliable results can be acquired rapidly without a need for manual processing

  14. The dark art of light measurement: accurate radiometry for low-level light therapy.

    Hadis, Mohammed A; Zainal, Siti A; Holder, Michelle J; Carroll, James D; Cooper, Paul R; Milward, Michael R; Palin, William M

    2016-05-01

    Lasers and light-emitting diodes are used for a range of biomedical applications with many studies reporting their beneficial effects. However, three main concerns exist regarding much of the low-level light therapy (LLLT) or photobiomodulation literature; (1) incomplete, inaccurate and unverified irradiation parameters, (2) miscalculation of 'dose,' and (3) the misuse of appropriate light property terminology. The aim of this systematic review was to assess where, and to what extent, these inadequacies exist and to provide an overview of 'best practice' in light measurement methods and importance of correct light measurement. A review of recent relevant literature was performed in PubMed using the terms LLLT and photobiomodulation (March 2014-March 2015) to investigate the contemporary information available in LLLT and photobiomodulation literature in terms of reporting light properties and irradiation parameters. A total of 74 articles formed the basis of this systematic review. Although most articles reported beneficial effects following LLLT, the majority contained no information in terms of how light was measured (73%) and relied on manufacturer-stated values. For all papers reviewed, missing information for specific light parameters included wavelength (3%), light source type (8%), power (41%), pulse frequency (52%), beam area (40%), irradiance (43%), exposure time (16%), radiant energy (74%) and fluence (16%). Frequent use of incorrect terminology was also observed within the reviewed literature. A poor understanding of photophysics is evident as a significant number of papers neglected to report or misreported important radiometric data. These errors affect repeatability and reliability of studies shared between scientists, manufacturers and clinicians and could degrade efficacy of patient treatments. Researchers need a physicist or appropriately skilled engineer on the team, and manuscript reviewers should reject papers that do not report beam measurement

  15. Accurate Weak Lensing of Standard Candles. II. Measuring sigma8 with Supernovae

    Quartin, Miguel; Marra, Valerio; Amendola, Luca(Institut für Theoretische Physik, Universität Heidelberg, Philosophenweg 16, D-69120 Heidelberg, Germany)

    2013-01-01

    Soon the number of type Ia supernova (SN) measurements should exceed 100,000. Understanding the effect of weak lensing by matter structures on the supernova brightness will then be more important than ever. Although SN lensing is usually seen as a source of systematic noise, we will show that it can be in fact turned into signal. More precisely, the non-Gaussianity introduced by lensing in the SN Hubble diagram dispersion depends rather sensitively on the amplitude sigma8 of the matter power ...

  16. Accurate measurement of surface areas of anatomical structures by computer-assisted triangulation of computed tomography images

    There is a need for accurate surface area measurement of internal anatomical structures in order to define light dosimetry in adjunctive intraoperative photodynamic therapy (AIOPDT). The authors investigated whether computer-assisted triangulation of serial sections generated by computed tomography (CT) scanning can give an accurate assessment of the surface area of the walls of the true pelvis after anterior resection and before colorectal anastomosis. They show that the technique of paper density tessellation is an acceptable method of measuring the surface areas of phantom objects, with a maximum error of 0.5%, and is used as the gold standard. Computer-assisted triangulation of CT images of standard geometric objects and accurately-constructed pelvic phantoms gives a surface area assessment with a maximum error of 2.5% compared with the gold standard. The CT images of 20 patients' pelves have been analysed by computer-assisted triangulation and this shows the surface area of the walls varies from 143 cm2 to 392 cm2. (Author)

  17. Individual-Based Allometric Equations Accurately Measure Carbon Storage and Sequestration in Shrublands

    Norman W.H. Mason

    2014-02-01

    Full Text Available Many studies have quantified uncertainty in forest carbon (C storage estimation, but there is little work examining the degree of uncertainty in shrubland C storage estimates. We used field data to simulate uncertainty in carbon storage estimates from three error sources: (1 allometric biomass equations; (2 measurement errors of shrubs harvested for the allometry; and (3 measurement errors of shrubs in survey plots. We also assessed uncertainty for all possible combinations of these error sources. Allometric uncertainty had the greatest independent effect on C storage estimates for individual plots. The largest error arose when all three error sources were included in simulations (where the 95% confidence interval spanned a range equivalent to 40% of mean C storage. Mean C sequestration (1.73 Mg C ha–1 year–1 exceeded the margin of error produced by the simulated sources of uncertainty. This demonstrates that, even when the major sources of uncertainty were accounted for, we were able to detect relatively modest gains in shrubland C storage.

  18. Mass measurements near the $r$-process path using the Canadian Penning Trap mass spectrometer

    Van Schelt, J.; Lascar, D.; G. Savard; Clark, J. A.; Caldwell, S.; Chaudhuri, A.; Fallis, J.; Greene, J. P.; Levand, 1 A. F.; Li, G.; Sharma, K. S.; Sternberg, M. G.; Sun, T.; Zabransky, B. J.

    2012-01-01

    The masses of 40 neutron-rich nuclides from Z = 51 to 64 were measured at an average precision of $\\delta m/m= 10^{-7}$ using the Canadian Penning Trap mass spectrometer at Argonne National Laboratory. The measurements, of fission fragments from a $^{252}$Cf spontaneous fission source in a helium gas catcher, approach the predicted path of the astrophysical $r$ process. Where overlap exists, this data set is largely consistent with previous measurements from Penning traps, storage rings, and ...

  19. Uncertainties and re-analysis of glacier mass balance measurements

    Zemp, M.; E. Thibert; Huss, M.; Stumm, D.; Rolstad Denby, C.; Nuth, C.; S. U. Nussbaumer; G. Moholdt; A. Mercer; Mayer, C.; Joerg, P. C.; P. Jansson; B. Hynek; Fischer, A.; Escher-Vetter, H.

    2013-01-01

    Glacier-wide mass balance has been measured for more than sixty years and is widely used as an indicator of climate change and to assess the glacier contribution to runoff and sea level rise. Until present, comprehensive uncertainty assessments have rarely been carried out and mass balance data have often been applied using rough error estimation or without error considerations. In this study, we propose a framework for re-analyzing glacier mass balance series including conceptual and ...

  20. Integration of a silicon-based microprobe into a gear measuring instrument for accurate measurement of micro gears

    The integration of silicon micro probing systems into conventional gear measuring instruments (GMIs) allows fully automated measurements of external involute micro spur gears of normal modules smaller than 1 mm. This system, based on a silicon microprobe, has been developed and manufactured at the Institute for Microtechnology of the Technische Universität Braunschweig. The microprobe consists of a silicon sensor element and a stylus which is oriented perpendicularly to the sensor. The sensor is fabricated by means of silicon bulk micromachining. Its small dimensions of 6.5 mm × 6.5 mm allow compact mounting in a cartridge to facilitate the integration into a GMI. In this way, tactile measurements of 3D microstructures can be realized. To enable three-dimensional measurements with marginal forces, four Wheatstone bridges are built with diffused piezoresistors on the membrane of the sensor. On the reverse of the membrane, the stylus is glued perpendicularly to the sensor on a boss to transmit the probing forces to the sensor element during measurements. Sphere diameters smaller than 300 µm and shaft lengths of 5 mm as well as measurement forces from 10 µN enable the measurements of 3D microstructures. Such micro probing systems can be integrated into universal coordinate measuring machines and also into GMIs to extend their field of application. Practical measurements were carried out at the Physikalisch-Technische Bundesanstalt by qualifying the microprobes on a calibrated reference sphere to determine their sensitivity and their physical dimensions in volume. Following that, profile and helix measurements were carried out on a gear measurement standard with a module of 1 mm. The comparison of the measurements shows good agreement between the measurement values and the calibrated values. This result is a promising basis for the realization of smaller probe diameters for the tactile measurement of micro gears with smaller modules. (paper)

  1. Analysis of Partial Volume Effects on Accurate Measurement of the Hippocampus Volume

    Maryam Hajiesmaeili; Jamshid Dehmeshki; Tim Ellis

    2014-01-01

    Hippocampal volume loss is an important biomarker in distinguishing subjects with Alzheimer’s disease (AD) and its measurement in magnetic resonance images (MRI) is influenced by partial volume effects (PVE). This paper describes a post-processing approach to quantify PVE for correction of the hippocampal volume by using a spatial fuzzyC-means (SFCM) method. The algorithm is evaluated on a dataset of 20 T1-weighted MRI scans sampled at two different resolutions. The corrected volumes for left and right hippocampus (HC) which are 23% and 18% for the low resolution and 6% and 5% for the high resolution datasets, respectively are lower than hippocampal volume results from manual segmentation. Results show the importance of applying this technique in AD detection with low resolution datasets.

  2. Increased profitability in cellulose production through more accurate measurement of the moisture content

    A general report on the project 'Dry Wood' is presented. In this project Noratom-Norcontrol A/S cooperate with the wood-pulp and paper factory Petersen and Soen in the application of Noratom's radiometric moisture gauge and their continuous weighing machine (densimeter) in the continuous measurement of the moisture content of wood chips in cellulose production. Conventional methods give an accuracy of π+ 2% and the objective of this method is an accuracy of π+ 1%. This would have a considerable economic significance. A test unit has been operating in the production line for a year and has attained the objective for short periods. Improved long term stability is the present problem. The system has process outputs which will facilitate future on-line computer process control. (JIW)

  3. Accurate Simulation of 802.11 Indoor Links: A "Bursty" Channel Model Based on Real Measurements

    Agüero Ramón

    2010-01-01

    Full Text Available We propose a novel channel model to be used for simulating indoor wireless propagation environments. An extensive measurement campaign was carried out to assess the performance of different transport protocols over 802.11 links. This enabled us to better adjust our approach, which is based on an autoregressive filter. One of the main advantages of this proposal lies in its ability to reflect the "bursty" behavior which characterizes indoor wireless scenarios, having a great impact on the behavior of upper layer protocols. We compare this channel model, integrated within the Network Simulator (ns-2 platform, with other traditional approaches, showing that it is able to better reflect the real behavior which was empirically assessed.

  4. Radiochromic Plastic Films for Accurate Measurement of Radiation Absorbed Dose and Dose Distributions

    McLaughlin, W. L.; Miller, Arne; Fidan, S.;

    1977-01-01

    Thin radiochromic dye films are useful for measuring large radiation absorbed doses (105–108 rads) and for high-resolution imaging of dose patterns produced by penetrating radiation beams passing through non-homogeneous media. Certain types of amino-substituted triarylmethane cyanides dissolved in...... polymeric solutions can be cast into flexible free-standing thin films of uniform thickness and reproducible response to ultraviolet and ionizing radiation. The increase in optical density versus energy deposited by radiation is linear over a wide range of doses and is for practical purposes independent of...... dose rate (1–1014 rad s−1). Upon irradiation of the film, the profile of the radiation field is registered as a permanent colored image of the dose distribution. Unlike most other types of dyed plastic dose meters, the optical density produced by irradiation is in most cases stable for periods of at...

  5. Combined atomic force microscopy and voltage pulse technique to accurately measure electrostatic force

    Inami, Eiichi; Sugimoto, Yoshiaki

    2016-08-01

    We propose a new method of extracting electrostatic force. The technique is based on frequency modulation atomic force microscopy (FM-AFM) combined with a voltage pulse. In this method, the work that the electrostatic field does on the oscillating tip is measured through the cantilever energy dissipation. This allows us to directly extract capacitive forces including the longer range part, to which the conventional FM-AFM is insensitive. The distance-dependent contact potential difference, which is modulated by local charges distributed on the surfaces of the tip and/or sample, could also be correctly obtained. In the absence of local charges, our method can perfectly reproduce the electrostatic force as a function of the distance and the bias voltage. Furthermore, we demonstrate that the system serves as a sensitive sensor enabling us to check the existence of the local charges such as trapped charges and patch charges.

  6. Accurate plutonium waste measurements using the 252Cf add-a- source technique for matrix corrections

    We have developed a new measurement technique to improve the accuracy and sensitivity of the nondestructive assay (NDA) of plutonium scrap and waste. The 200-ell drum assay system uses the classical NDA method of counting passive-neutron coincidences from plutonium but has added the new features of ''add-a-source'' to improve the accuracy for matrix corrections and statistical techniques to improve the low-level detectability limits. The add-a-source technique introduces a small source of 252Cf (10-8 g) near the external surface of the sample drum. The drum perturbs the rate at which coincident neutrons from the 252Cf are counted. The perturbation provides the data to correct for the matrix and plutonium inside the drum. The errors introduced from matrix materials in 200-ell drums have been reduced by an order of magnitude using the add-a-source technique. In addition, the add-a-source method can detect unexpected neutron-shielding material inside the drum that might hide the presence of special nuclear materials. The detectability limit of the new waste-drum assay system for plutonium is better than prior systems for actual waste materials. For the in-plant installation at a mixed-oxide fabrication facility, the detectability limit is 0.73 mg of 24OPu (or 2.3 mg of high-burnup plutonium) for a 15-min. measurement. For a drum containing 100 kg of waste, this translates to about 7 nCi/g. This excellent sensitivity was achieved using a special low-background detector design, good overhead shielding, and statistical techniques in the software to selectively reduce the cosmic-ray neutron background

  7. An X-Band Waveguide Measurement Technique for the Accurate Characterization of Materials with Low Dielectric Loss Permittivity

    Allen, Kenneth W; Reid, David R; Bean, Jeffrey A; Ellis, Jeremy D; Morris, Andrew P; Marsh, Jeramy M

    2016-01-01

    In this work, we present a new X-band waveguide (WR90) measurement method that permits the broadband characterization of the complex permittivity for low dielectric loss tangent material specimens with improved accuracy. An electrically-long polypropylene specimen that partially fills the cross-section is inserted into the waveguide and the transmitted scattering parameter (S21) is measured. The extraction method relies on computational electromagnetic simulations, coupled with a genetic algorithm, to match the experimental S21 measurement. The sensitivity of the technique to sample length was explored by simulating specimen lengths from 2.54 to 15.24 cm, in 2.54 cm increments. Analysis of our simulated data predicts the technique will have the sensitivity to measure loss tangent values on the order of 10e-3 for materials such as polymers with relatively low real permittivity values. The ability to accurately characterize low-loss dielectric material specimens of polypropylene is demonstrated experimentally. ...

  8. Evapotranspiration: Mass balance measurements compared with flux estimation methods

    Evapotranspiration (ET) may be measured by mass balance methods and estimated by flux sensing methods. The mass balance methods are typically restricted in terms of the area that can be represented (e.g., surface area of weighing lysimeter (LYS) or equivalent representative area of neutron probe (NP...

  9. Rapid and Accurate Identification of Animal Species in Natural Leather Goods by Liquid Chromatography/Mass Spectrometry

    Izuchi, Yukari; Takashima, Tsuneo; Hatano, Naoya

    2016-01-01

    The demand for leather goods has grown globally in recent years. Industry revenue is forecast to reach $91.2 billion by 2018. There is an ongoing labelling problem in the leather items market, in that it is currently impossible to identify the species that a given piece of leather is derived from. To address this issue, we developed a rapid and simple method for the specific identification of leather derived from cattle, horses, pigs, sheep, goats, and deer by analysing peptides produced by the trypsin-digestion of proteins contained in leather goods using liquid chromatography/mass spectrometry. We determined species-specific amino acid sequences by liquid chromatography/tandem mass spectrometry analysis using the Mascot software program and demonstrated that collagen α-1(I), collagen α-2(I), and collagen α-1(III) from the dermal layer of the skin are particularly useful in species identification. PMID:27313979

  10. Accurate weak lensing of standard candles. II. Measuring σ8 with supernovae

    Quartin, Miguel; Marra, Valerio; Amendola, Luca

    2014-01-01

    Soon the number of type Ia supernova (SN) measurements should exceed 100 000. Understanding the effect of weak lensing by matter structures on the supernova brightness will then be more important than ever. Although SN lensing is usually seen as a source of systematic noise, we will show that it can be in fact turned into signal. More precisely, the non-Gaussianity introduced by lensing in the SN Hubble diagram dispersion depends rather sensitively on the amplitude σ8 of the matter power spectrum. By exploiting this relation, we are able to predict constraints on σ8 of 7% (3%) for a catalog of 100 000 (500 000) SNe of average magnitude error 0.12, without having to assume that such intrinsic dispersion and its redshift evolution are known a priori. The intrinsic dispersion has been assumed to be Gaussian; possible intrinsic non-Gaussianities in the data set (due to the SN themselves and/or to other transients) could be potentially dealt with by means of additional nuisance parameters describing higher moments of the intrinsic dispersion distribution function. This method is independent of and complementary to the standard methods based on cosmic microwave background, cosmic shear, or cluster abundance observables.

  11. Accurate measurement of the sticking time and sticking probability of Rb atoms on a polydimethylsiloxane coating

    We present the results of a systematic study of Knudsen’s flow of Rb atoms in cylindrical capillary cells coated with a polydimethylsiloxane (PDMS) compound. The purpose of the investigation is to determine the characterization of the coating in terms of the sticking probability and sticking time of Rb on the two types of coating of high and medium viscosities. We report the measurement of the sticking probability of a Rb atom to the coating equal to 4.3 × 10−5, which corresponds to the number of bounces 2.3 × 104 at room temperature. These parameters are the same for the two kinds of PDMS used. We find that at room temperature, the respective sticking times for high-viscosity and medium-viscosity PDMS are 22 ± 3 μs and 49 ± 6 μs. These sticking times are about million times larger than the sticking time derived from the surface Rb atom adsorption energy and temperature of the coating. A tentative explanation of this surprising result is proposed based on the bulk diffusion of the atoms that collide with the surface and penetrate inside the coating. The results can be important in many resonance cell experiments, such as the efficient magnetooptical trapping of rare elements or radioactive isotopes and in experiments on the light-induced drift effect

  12. EZ-Rhizo: integrated software for the fast and accurate measurement of root system architecture.

    Armengaud, Patrick; Zambaux, Kevin; Hills, Adrian; Sulpice, Ronan; Pattison, Richard J; Blatt, Michael R; Amtmann, Anna

    2009-03-01

    The root system is essential for the growth and development of plants. In addition to anchoring the plant in the ground, it is the site of uptake of water and minerals from the soil. Plant root systems show an astonishing plasticity in their architecture, which allows for optimal exploitation of diverse soil structures and conditions. The signalling pathways that enable plants to sense and respond to changes in soil conditions, in particular nutrient supply, are a topic of intensive research, and root system architecture (RSA) is an important and obvious phenotypic output. At present, the quantitative description of RSA is labour intensive and time consuming, even using the currently available software, and the lack of a fast RSA measuring tool hampers forward and quantitative genetics studies. Here, we describe EZ-Rhizo: a Windows-integrated and semi-automated computer program designed to detect and quantify multiple RSA parameters from plants growing on a solid support medium. The method is non-invasive, enabling the user to follow RSA development over time. We have successfully applied EZ-Rhizo to evaluate natural variation in RSA across 23 Arabidopsis thaliana accessions, and have identified new RSA determinants as a basis for future quantitative trait locus (QTL) analysis. PMID:19000163

  13. The Quick Measure of a Nurbs Surface Curvature for Accurate Triangular Meshing

    Kniat Aleksander

    2014-04-01

    Full Text Available NURBS surfaces are the most widely used surfaces for three-dimensional models in CAD/ CAE programs. When a model for FEM calculation is prepared with a CAD program it is inevitable to mesh it finally. There are many algorithms for meshing planar regions. Some of them may be used for meshing surfaces but it is necessary to take the curvature of the surface under consideration to avoid poor quality mesh. The mesh must be denser in the curved regions of the surface. In this paper, instead of analysing a surface curvature, the method to assess how close is a mesh triangle to the surface to which its vertices belong, is presented. The distance between a mesh triangle and a parallel tangent plane through a point on a surface is the measure of the triangle quality. Finding the surface point whose projection is located inside the mesh triangle and which is the tangency point to the plane parallel to this triangle is an optimization problem. Mathematical description of the problem and the algorithm to find its solution are also presented in the paper.

  14. Accurate Measurements of Free Flight Drag Coefficients with Amateur Doppler Radar

    Courtney, Elya; Courtney, Michael

    2016-01-01

    In earlier papers, techniques have been described using optical chronographs to determine free flight drag coefficients with an accuracy of 1-2%, accomplished by measuring near and far velocities of projectiles in flight over a known distance. Until recently, Doppler radar has been prohibitively expensive for many users. This paper reports results of exploring potential applications and accuracy using a recently available, inexpensive (< $600 US) amateur Doppler radar system to determine drag coefficients for projectiles of various sizes (4.4 mm to 9 mm diameter) and speeds (M0.3 to M3.0). In many cases, drag coefficients can be determined with an accuracy of 1% or better if signal-to-noise ratio is sufficient and projectiles vary little between trials. It is also straightforward to design experiments for determining drag over a wide range of velocities. Experimental approaches and limitations are described. Overall, the amateur radar system shows greater accuracy, ease of use, and simplicity compared with...

  15. Accurate electrical resistance measurement of the crystallization kinetics of amorphous alloys

    WANG; Yaping

    2001-01-01

    [1]Kobayashi, H.?Yasukochi, K., Maximum and minimum heat flux and temperature fluctuation in film-boiling states in superfluid helium, Adv. Cryog. Eng., 1980, 25: 372.[2]Kobayashi, H.?Yasukochi, K., A sample configuration effect on the heat transfer from metal surfaces to pressurized He II, Proc. ICEC, 1980, 8: 217.[3]Schwerdtner, M. V., Stamm, G., Tosi, A. N. et al. The boiling-up process in He II. Optical measurements and visualization, Cryogenics, 1992, 32: 775.[4]Schwerdtner, M. V., Poppes, W., Schmidt, D. W., Distortion of temperature signals in He II due to probe geometry, and a new improved probe, Cryogenics, 1989, 29: 132.[5]Shimazaki, T., Murakami, M.?Iida, T., Second sound wave heat transfer, thermal boundary layer formation and boiling: highly transient heat transport phenomena in He II, Cryogenics, 1995, 35: 645.[6]Zhang, P., Study of physical mechanism of film boiling in He II, Doctoral dissertation, Shanghai Jiaotong University, China, 1998.[7]Arp, V., State equation of liquid helium-4 from 0.8 to 2.5K, J. Low Temp. Phys., 1990, 79: 93.[8]Zhang, P., Kimura, S., Murakami, M. et al., Non-planar and non-linear second sound wave in He II, Chinese Physics Letters, 2000, 17: 43.

  16. Accurate measurement of the HI column density from HI 21cm absorption-emission spectroscopy

    Chengalur, Jayaram N; Roy, Nirupam

    2013-01-01

    We present a detailed study of an estimator of the HI column density, based on a combination of HI 21cm absorption and HI 21cm emission spectroscopy. This "isothermal" estimate is given by $N_{\\rm HI,ISO} = 1.823 \\times 10^{18} \\int \\left[ \\tau_{\\rm tot} \\times {\\rm T_B} \\right] / \\left[ 1 - e^{-\\tau_{\\rm tot}} \\right] {\\rm dV}$, where $\\tau_{\\rm tot}$ is the total HI 21cm optical depth along the sightline and ${\\rm T_B}$ is the measured brightness temperature. We have used a Monte Carlo simulation to quantify the accuracy of the isothermal estimate by comparing the derived $N_{\\rm HI,ISO}$ with the true HI column density $N_{\\rm HI}$. The simulation was carried out for a wide range of sightlines, including gas in different temperature phases and random locations along the path. We find that the results are statistically insensitive to the assumed gas temperature distribution and the positions of different phases along the line of sight. The median value of the ratio of the true H{\\sc i} column density to the...

  17. Report of the working group on precision measurements - measurements of the W boson mass and width.

    Brock, R.; Erler, J.; Kim, Y.-K.; Marciano, W.; Ashmanskas, W.; Baur, U.; Ellison, J.; Lancaster, M.; Nodulman, L.; Rha, J.; Waters, D.; Womersley, J.

    2000-11-29

    We discuss the prospects for measuring the W mass and width in Run II. The basic techniques used to measure M{sub W} are described and the statistical, theoretical and detector-related uncertainties are discussed in detail. Alternative methods of measuring the W mass at the Tevatron and the prospects for M{sub W} measurements at other colliders are also described.

  18. Body Mass Index and the Measurement of Obesity

    Madden, David

    2006-01-01

    This paper proposes a new method of measuring obesity using Body Mass Index (BMI) data. Conventional measures which simply count the number of individuals with BMI in excess of an upper limit ignore the extent by which individuals exceed BMI limits and also the increased risk ratios for various conditions associated very high levels of BMI. This paper suggests that measures currently used in the poverty literature can be usefully applied to measure obesity and provide us with measures which m...

  19. The need for preoperative baseline arm measurement to accurately quantify breast cancer-related lymphedema.

    Sun, Fangdi; Skolny, Melissa N; Swaroop, Meyha N; Rawal, Bhupendra; Catalano, Paul J; Brunelle, Cheryl L; Miller, Cynthia L; Taghian, Alphonse G

    2016-06-01

    Breast cancer-related lymphedema (BCRL) is a feared outcome of breast cancer treatment, yet the push for early screening is hampered by a lack of standardized quantification. We sought to determine the necessity of preoperative baseline in accounting for temporal changes of upper extremity volume. 1028 women with unilateral breast cancer were prospectively screened for lymphedema by perometry. Thresholds were defined: relative volume change (RVC) ≥10 % for clinically significant lymphedema and ≥5 % including subclinical lymphedema. The first postoperative measurement (pseudo-baseline) simulated the case of no baseline. McNemar's test and binomial logistic regression models were used to analyze BCRL misdiagnoses. Preoperatively, 28.3 and 2.9 % of patients had arm asymmetry of ≥5 and 10 %, respectively. Without baseline, 41.6 % of patients were underdiagnosed and 40.1 % overdiagnosed at RVC ≥ 5 %, increasing to 50.0 and 54.8 % at RVC ≥ 10 %. Increased pseudo-baseline asymmetry, increased weight change between baselines, hormonal therapy, dominant use of contralateral arm, and not receiving axillary lymph node dissection (ALND) were associated with increased risk of underdiagnosis at RVC ≥ 5 %; not receiving regional lymph node radiation was significant at RVC ≥ 10 %. Increased pseudo-baseline asymmetry, not receiving ALND, and dominant use of ipsilateral arm were associated with overdiagnosis at RVC ≥ 5 %; increased pseudo-baseline asymmetry and not receiving ALND were significant at RVC ≥ 10 %. The use of a postoperative proxy even early after treatment results in poor sensitivity for identifying BCRL. Providers with access to patients before surgery should consider the consequent need for proper baseline, with specific strategy tailored by institution. PMID:27154787

  20. Distributed Capacitive Sensor for Sample Mass Measurement

    Toda, Risaku; McKinney, Colin; Jackson, Shannon P.; Mojarradi, Mohammad; Manohara, Harish; Trebi-Ollennu, Ashitey

    2011-01-01

    Previous robotic sample return missions lacked in situ sample verification/ quantity measurement instruments. Therefore, the outcome of the mission remained unclear until spacecraft return. In situ sample verification systems such as this Distributed Capacitive (DisC) sensor would enable an unmanned spacecraft system to re-attempt the sample acquisition procedures until the capture of desired sample quantity is positively confirmed, thereby maximizing the prospect for scientific reward. The DisC device contains a 10-cm-diameter pressure-sensitive elastic membrane placed at the bottom of a sample canister. The membrane deforms under the weight of accumulating planetary sample. The membrane is positioned in close proximity to an opposing rigid substrate with a narrow gap. The deformation of the membrane makes the gap narrower, resulting in increased capacitance between the two parallel plates (elastic membrane and rigid substrate). C-V conversion circuits on a nearby PCB (printed circuit board) provide capacitance readout via LVDS (low-voltage differential signaling) interface. The capacitance method was chosen over other potential approaches such as the piezoelectric method because of its inherent temperature stability advantage. A reference capacitor and temperature sensor are embedded in the system to compensate for temperature effects. The pressure-sensitive membranes are aluminum 6061, stainless steel (SUS) 403, and metal-coated polyimide plates. The thicknesses of these membranes range from 250 to 500 m. The rigid substrate is made with a 1- to 2-mm-thick wafer of one of the following materials depending on the application requirements glass, silicon, polyimide, PCB substrate. The glass substrate is fabricated by a microelectromechanical systems (MEMS) fabrication approach. Several concentric electrode patterns are printed on the substrate. The initial gap between the two plates, 100 m, is defined by a silicon spacer ring that is anodically bonded to the glass

  1. Evidence for Broad-Line Region Outflows and Their Impact on Black Hole Mass Measurements

    Denney, K. D.; Assef, R. J.; Horne, K.;

    2012-01-01

    could not be fully and accurately interpreted from the 1D velocity-resolved reverberation signal. From the VDM, an outflow component to the emission remains possible but appears to be in addition to an underlying, disk-like BLR structure consistent in size with the measured reverberation lag. The black...... hole (BH) mass derived from this data is therefore secure from any uncertainties possibly derived from gravitationally unbound gas contributing to the emission. Additionally, we demonstrate that BLR emission from the C IV ¿1549 broad emission line can reliably be used as a virial BH mass estimator...

  2. DISCOVERY AND MASS MEASUREMENTS OF A COLD, 10 EARTH MASS PLANET AND ITS HOST STAR

    We present the discovery and mass measurement of the cold, low-mass planet MOA-2009-BLG-266Lb, performed with the gravitational microlensing method. This planet has a mass of mp = 10.4 ± 1.7 M+ and orbits a star of mass M* = 0.56 ± 0.09 Msun at a semimajor axis of a = 3.2-0.5+1.9 AU and an orbital period of P = 7.6-1.5+7+7 yrs. The planet and host star mass measurements are enabled by the measurement of the microlensing parallax effect, which is seen primarily in the light curve distortion due to the orbital motion of the Earth. But the analysis also demonstrates the capability to measure the microlensing parallax with the Deep Impact (or EPOXI) spacecraft in a heliocentric orbit. The planet mass and orbital distance are similar to predictions for the critical core mass needed to accrete a substantial gaseous envelope, and thus may indicate that this planet is a 'failed' gas giant. This and future microlensing detections will test planet formation theory predictions regarding the prevalence and masses of such planets.

  3. A top quark mass measurement using a matrix element method

    Linacre, Jacob Thomas; /Oxford U.

    2010-02-01

    A measurement of the mass of the top quark is presented, using top-antitop pair (t{bar t}) candidate events for the lepton+jets decay channel. The measurement makes use of Tevatron p{bar p} collision data at centre-of-mass energy {radical}s = 1.96 TeV, collected at the CDF detector. The top quark mass is measured by employing an unbinned maximum likelihood method where the event probability density functions are calculated using signal (t{bar t}) and background (W+jets) matrix elements, as well as a set of parameterised jet-to-parton mapping functions. The likelihood function is maximised with respect to the top quark mass, the fraction of signal events, and a correction to the jet energy scale (JES) of the calorimeter jets. The simultaneous measurement of the JES correction ({Delta}{sub JES}) provides an in situ jet energy calibration based on the known mass of the hadronically decaying W boson. Using 578 lepton+jets candidate events corresponding to 3.2 fb{sup -1} of integrated luminosity, the top quark mass is measured to be m{sub t} = 172.4 {+-} 1.4 (stat+{Delta}{sub JES}) {+-} 1.3 (syst) GeV=c{sup 2}, one of the most precise single measurements to date.

  4. The mass accretion rate of galaxy clusters: a measurable quantity

    De Boni, Cristiano

    2016-01-01

    We are interested in investigating the growth of structures at the nonlinear scales of galaxy clusters from an observational perspective: we explore the possibility of measuring the mass accretion rate of galaxy clusters from their mass profile beyond the virial radius. We derive the accretion rate from the mass of a spherical shell whose infall velocity is extracted from $N$-body simulations. In the redshift range $z=[0,2]$, our prescription returns an average mass accretion rate within $20-40 \\%$ of the average rate derived from the merger trees of dark matter haloes extracted from $N$-body simulations. Our result suggests that measuring the mean mass accretion rate of a sample of galaxy clusters is actually feasible, thus providing a new potential observational test of the cosmological and structure formation models.

  5. A Critical Assessment of Stellar Mass Measurement Methods

    Mobasher, Bahram; Ferguson, Henry C; Acquaviva, Viviana; Barro, Guillermo; Finkelstein, Steven L; Fontana, Adriano; Gruetzbauch, Ruth; Johnson, Seth; Lu, Yu; Papovich, Casey J; Pforr, Janine; Salvato, Mara; Somerville, Rachel S; Wiklind, Tommy; Wuyts, Stijn; Ashby, Matthew L N; Bell, Eric; Conselice, Christopher J; Dickinson, Mark E; Faber, Sandra M; Fazio, Giovanni; Finlator, Kristian; Galametz, Audrey; Gawiser, Eric; Giavalisco, Mauro; Grazian, Andrea; Grogin, Norman A; Guo, Yicheng; Hathi, Nimish; Kocevski, Dale; Koekemoer, Anton M; Koo, David C; Newman, Jeffrey A; Reddy, Naveen; Santini, Paola; Wechsler, Risa H

    2015-01-01

    In this paper we perform a comprehensive study of the main sources of random and systematic errors in stellar mass measurement for galaxies using their Spectral Energy Distributions (SEDs). We use mock galaxy catalogs with simulated multi-waveband photometry (from U-band to mid-infrared) and known redshift, stellar mass, age and extinction for individual galaxies. Given different parameters affecting stellar mass measurement (photometric S/N ratios, SED fitting errors, systematic effects, the inherent degeneracies and correlated errors), we formulated different simulated galaxy catalogs to quantify these effects individually. We studied the sensitivity of stellar mass estimates to the codes/methods used, population synthesis models, star formation histories, nebular emission line contributions, photometric uncertainties, extinction and age. For each simulated galaxy, the difference between the input stellar masses and those estimated using different simulation catalogs, $\\Delta\\log(M)$, was calculated and use...

  6. Measuring Physical Inactivity: Do Current Measures Provide an Accurate View of “Sedentary” Video Game Time?

    Simon Fullerton; Taylor, Anne W.; Eleonora Dal Grande; Narelle Berry

    2014-01-01

    BACKGROUND: Measures of screen time are often used to assess sedentary behaviour. Participation in activity-based video games (exergames) can contribute to estimates of screen time, as current practices of measuring it do not consider the growing evidence that playing exergames can provide light to moderate levels of physical activity. This study aimed to determine what proportion of time spent playing video games was actually spent playing exergames. METHODS: Data were collected via a cross-...

  7. Measuring Physical Inactivity: Do Current Measures Provide an Accurate View of “Sedentary” Video Game Time?

    2014-01-01

    Background. Measures of screen time are often used to assess sedentary behaviour. Participation in activity-based video games (exergames) can contribute to estimates of screen time, as current practices of measuring it do not consider the growing evidence that playing exergames can provide light to moderate levels of physical activity. This study aimed to determine what proportion of time spent playing video games was actually spent playing exergames. Methods. Data were collected via a cross-...

  8. Precision measurement of a particle mass at the linear collider

    Milstene, C.; /Fermilab; Freitas, A.; /Zurich U.; Schmitt, M.; /Northwestern U.; Sopczak, A.; /Lancaster U.

    2007-06-01

    Precision measurement of the stop mass at the ILC is done in a method based on cross-sections measurements at two different center-of-mass energies. This allows to minimize both the statistical and systematic errors. In the framework of the MSSM, a light stop, compatible with electro-weak baryogenesis, is studied in its decay into a charm jet and neutralino, the Lightest Supersymmetric Particle (LSP), as a candidate of dark matter. This takes place for a small stop-neutralino mass difference.

  9. Penning trap mass measurements of transfermium elements with SHIPTRAP

    Penning traps are widely used for high-precision mass measurements of radionuclides related to nuclear astrophysics studies and the evolution of nuclear structure far away from stability. With the stopping of secondary beams in gas cells together with advanced ion-beam manipulation techniques their reach has been extended to rare isotopes of essentially all elements. The Penning trap mass spectrometer SHIPTRAP at GSI Darmstadt has recently demonstrated that even high-precision mass measurements of transfermium elements can be performed despite low production rates of only about one particle per second. This important milestone opens new perspectives for the study of superheavy elements with ion traps.

  10. Measurement of the Higgs boson mass with the ATLAS detector

    Garay Walls F. M.

    2015-01-01

    Full Text Available A summary of the latest results on the combined measurement of the Higgs boson mass in the H → ZZ* → 4l and the H → γγ decay channels with the ATLAS detector is presented. The analysis uses 25 fb−1 of pp collision data recorded by the ATLAS detector at the CERN Large Hadron Collider at centre-of-mass energies of 7TeV and 8 TeV during 2011 and 2012. The combined measured value of the Higgs boson mass is mH = 125.36 ± 0.37 (stat ± 0.18 (syst GeV.

  11. Investigation and Comparison of Localization and Accurate Industrial Measurement through ¬Classic and Modern Mapping Methods

    Seyed Abdolreza Adnani

    2013-01-01

    The purpose of this study is investigation and comparison of localization and accurate industrial measurement through classic and modern mapping methods. in this research and it is proved that if the objective is to determine the coordinates of an event or the geometry of an object, there is no need to align and the coordinates of points on a target, which is generally an ultimate objective of a local mapping project, can be reached and can save the necessary time for aligning and deploying d...

  12. Nuclear Data Measurement Using the Accurate Neutron-Nucleus Reaction Measurement Instrument (ANNRI) in the Japan Proton Accelerator Research Complex (J-PARC)

    A nuclear data measurement project using a spallation neutron source is ongoing at the Japan Proton Accelerator Research Complex (J-PARC). The Accurate Neutron-Nucleus Reaction Measurement Instrument (ANNRI) was built as a beam line for measurement of neutron capture cross sections in J-PARC. The project is aimed to measure the neutron capture cross sections of minor actinides (MA) and long-lived fission products (LLFP) for design of innovative nuclear reactors and study of nuclear transmutation of nuclear waste. The ongoing ANNRI project is overviewed. (author)

  13. Accurate quantification of endogenous androgenic steroids in cattle's meat by gas chromatography mass spectrometry using a surrogate analyte approach

    Determination of endogenous steroids in complex matrices such as cattle's meat is a challenging task. Since endogenous steroids always exist in animal tissues, no analyte-free matrices for constructing the standard calibration line will be available, which is crucial for accurate quantification specially at trace level. Although some methods have been proposed to solve the problem, none has offered a complete solution. To this aim, a new quantification strategy was developed in this study, which is named 'surrogate analyte approach' and is based on using isotope-labeled standards instead of natural form of endogenous steroids for preparing the calibration line. In comparison with the other methods, which are currently in use for the quantitation of endogenous steroids, this approach provides improved simplicity and speed for analysis on a routine basis. The accuracy of this method is better than other methods at low concentration and comparable to the standard addition at medium and high concentrations. The method was also found to be valid according to the ICH criteria for bioanalytical methods. The developed method could be a promising approach in the field of compounds residue analysis

  14. Electron beam CT versus 16-slice spiral CT: how accurately can we measure coronary artery calcium volume?

    The purpose of this study was to investigate how accurately CAC volume we can be measured using electron beam computed tomography (CT) and 16-slice spiral CT. CAC models with known volume attached to a cardiac phantom were scanned. The error of measurement, variability between measured and real volumes, and inter-scan measurement variability were obtained. For spiral CT, seven different parameters were included: (1) slice thickness (0.625 mm, 1.25 mm and 2.5 mm), (2) retrospective spiral electrocardiograph (ECG)-gated or prospective axial ECG-triggering, (3) overlapping or non-overlapping. The error of measurement was 15% on electron beam CT and 8-20% on spiral CT. CAC volumes were underestimated in 92% and overestimated in 8% of the electron beam CT scans. Volumes were underestimated in 79%, correct in 5% and overestimated in 16% of the spiral CT scans. The best measurement and the least variability was observed on 0.625-mm retrospective spiral ECG-gated CT (error of 8%), a significant result (t-test: P<0.01) when compared with electron beam CT. CAC volume measurement on CT scanners may be significantly different and often underestimates the real volume of CAC. For precise evaluation of CAC volume, thin-slice retrospective spiral ECG-gated scan using a spiral CT scanner is desirable. (orig.)

  15. Top Quark Mass Measurements at ATLAS and CMS

    McCarthy, Tom; The ATLAS collaboration

    2016-01-01

    The top quark mass ($m_{top}$) is a fundamental parameter of the Standard Model of Particle Physics (SM). As the heaviest of all known SM particles with a mass close to the EW symmetry breaking scale, the top quark plays a pivotal role in the theory of elementary particles. The exact value of the top quark mass has implications on a number of theoretical predictions, which motivates the need for precision measurements of $m_{top}$. This presentation highlights a number of such precision measurements carried out by the ATLAS and CMS collaborations at centre-of-mass energies of $\\sqrt{s}=7$ and $8$ TeV from the combined LHC Run I datasets. A wide range of analysis strategies are employed in a number of channels. Measurements of both the top quark pole mass and $m_{top}$ as defined by the Monte Carlo generator in simulated signal samples are shown. Finally, a summary of combinations of the LHC measurements is presented, together with a look toward top quark mass measurements at $\\sqrt{s}=13$ TeV.

  16. Using MALDI-TOF mass spectrometry as a rapid and accurate diagnostic tool in infective endocarditis: a case report of a patient with mitral valve infective endocarditis caused by Abiotrophia defectiva

    Holler, Jon Gitz; Pedersen, Line; Calum, Henrik;

    2011-01-01

    A case of infective endocarditis caused by Abiotrophia defectiva is presented. The use of MALDI-TOF mass spectrometry as a rapid and accurate diagnostic tool in infective endocarditis is discussed.......A case of infective endocarditis caused by Abiotrophia defectiva is presented. The use of MALDI-TOF mass spectrometry as a rapid and accurate diagnostic tool in infective endocarditis is discussed....

  17. Self-aliquoting microarray plates for accurate quantitative matrix-assisted laser desorption/ionization mass spectrometry.

    Pabst, Martin; Fagerer, Stephan R; Köhling, Rudolf; Küster, Simon K; Steinhoff, Robert; Badertscher, Martin; Wahl, Fabian; Dittrich, Petra S; Jefimovs, Konstantins; Zenobi, Renato

    2013-10-15

    Matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) is a fast analysis tool employed for the detection of a broad range of analytes. However, MALDI-MS has a reputation of not being suitable for quantitative analysis. Inhomogeneous analyte/matrix co-crystallization, spot-to-spot inhomogeneity, as well as a typically low number of replicates are the main contributing factors. Here, we present a novel MALDI sample target for quantitative MALDI-MS applications, which addresses the limitations mentioned above. The platform is based on the recently developed microarray for mass spectrometry (MAMS) technology and contains parallel lanes of hydrophilic reservoirs. Samples are not pipetted manually but deposited by dragging one or several sample droplets with a metal sliding device along these lanes. Sample is rapidly and automatically aliquoted into the sample spots due to the interplay of hydrophilic/hydrophobic interactions. With a few microliters of sample, it is possible to aliquot up to 40 replicates within seconds, each aliquot containing just 10 nL. The analyte droplet dries immediately and homogeneously, and consumption of the whole spot during MALDI-MS analysis is typically accomplished within few seconds. We evaluated these sample targets with respect to their suitability for use with different samples and matrices. Furthermore, we tested their application for generating calibration curves of standard peptides with α-cyano-4-hdydroxycinnamic acid as a matrix. For angiotensin II and [Glu(1)]-fibrinopeptide B we achieved coefficients of determination (r(2)) greater than 0.99 without the use of internal standards. PMID:24003910

  18. Accurate measurements of carbon monoxide in humid air using the cavity ring-down spectroscopy (CRDS technique

    H. Chen

    2012-09-01

    Full Text Available Accurate measurements of carbon monoxide (CO in humid air have been made using the cavity ring-down spectroscopy (CRDS technique. The measurements of CO mole fractions are determined from the strength of its spectral absorption in the near infrared region (∼1.57 μm after removing interferences from adjacent carbon dioxide (CO2 and water vapor (H2O absorption lines. Water correction functions that account for the dilution and pressure-broadening effects as well as absorption line interferences from adjacent CO2 and H2O lines have been derived for CO2 mole fractions between 360–390 ppm. The line interference corrections are independent of CO mole fractions. The dependence of the line interference correction on CO2 abundance is estimated to be approximately −0.3 ppb/100 ppm CO2 for dry mole fractions of CO. Comparisons of water correction functions from different analyzers of the same type show significant differences, making it necessary to perform instrument-specific water tests for each individual analyzer. The CRDS analyzer was flown on an aircraft in Alaska from April to November in 2011, and the accuracy of the CO measurements by the CRDS analyzer has been validated against discrete NOAA/ESRL flask sample measurements made on board the same aircraft, with a mean difference between integrated in situ and flask measurements of −0.6 ppb and a standard deviation of 2.8 ppb. Preliminary testing of CRDS instrumentation that employs new spectroscopic analysis (available since the beginning of 2012 indicates a smaller water vapor dependence than the models discussed here, but more work is necessary to fully validate the performance. The CRDS technique provides an accurate and low-maintenance method of monitoring the atmospheric dry mole fractions of CO in humid air streams.

  19. The accurate measurement of flow rates in gas and wet-steam systems using a radio-tracer technique

    The utilisation of fluid resources relies heavily on the measurement of flow during processing, transport and custody transfer. To improve and maintain accuracy in industry, periodic calibration against a standard is required. The AAEC's adaptation of the radioisotope dilution method of measuring mass flow in gas systems offers a calibration technique with potentially low cost, accuracy and precision. The method is absolute, independent of pipe diameter and surface condition, and can be applied either in situ or to meters mounted in a calibration facility. The AAEC is constructing a test facility for thorough investigation of the technique over the mass flow range 0.16 - 1.5 kg s-1 using compressed air. A description of the facility is given

  20. First direct mass measurements on nobelium and lawrencium with the Penning trap mass spectrometer SHIPTRAP

    Dworschak, Michael Gerhard

    2009-12-08

    The Penning trap mass spectrometer SHIPTRAP at GSI Darmstadt was set up for high-precision mass measurements of heavy radionuclides produced in fusion evaporation reactions and separated from the primary beam by the velocity filter SHIP. It consists of a gas stopping cell for the deceleration of the high energetic reaction products, an RFQ cooler and buncher for cooling and accumulation of the ions, and a double Penning trap system to perform mass measurements. The mass is determined by measuring the cyclotron frequency of the ion of interest in a strong homogeneous magnetic field and comparing it to the frequency of a well-known reference ion. With this method relative uncertainties in the order of 10{sup -8} can be achieved. Recently, mass measurements of the three nobelium isotopes {sup 252-254}No (Z=102) and the lawrencium isotope {sup 255}Lr (Z=103) were performed successfully. These were the first direct mass measurements of transuranium elements ever per- formed. The production rate of the atoms of interest was about one per second or less. The results of the measurements on nobelium confirm the previous mass values which were deduced from Q{sub {alpha}} values. In the case of {sup 255}Lr the mass excess value, which was previously only estimated from systematic trends, was for the first time directly measured. These results mark the first step in the exploration of the region of transuranium elements which is planned at SHIPTRAP. The main objective is to fix the endpoints of {alpha} decay chains which are originating from superheavy elements close to the predicted island of stability. (orig.)

  1. First direct mass measurements on nobelium and lawrencium with the Penning trap mass spectrometer SHIPTRAP

    The Penning trap mass spectrometer SHIPTRAP at GSI Darmstadt was set up for high-precision mass measurements of heavy radionuclides produced in fusion evaporation reactions and separated from the primary beam by the velocity filter SHIP. It consists of a gas stopping cell for the deceleration of the high energetic reaction products, an RFQ cooler and buncher for cooling and accumulation of the ions, and a double Penning trap system to perform mass measurements. The mass is determined by measuring the cyclotron frequency of the ion of interest in a strong homogeneous magnetic field and comparing it to the frequency of a well-known reference ion. With this method relative uncertainties in the order of 10-8 can be achieved. Recently, mass measurements of the three nobelium isotopes 252-254No (Z=102) and the lawrencium isotope 255Lr (Z=103) were performed successfully. These were the first direct mass measurements of transuranium elements ever per- formed. The production rate of the atoms of interest was about one per second or less. The results of the measurements on nobelium confirm the previous mass values which were deduced from Qα values. In the case of 255Lr the mass excess value, which was previously only estimated from systematic trends, was for the first time directly measured. These results mark the first step in the exploration of the region of transuranium elements which is planned at SHIPTRAP. The main objective is to fix the endpoints of α decay chains which are originating from superheavy elements close to the predicted island of stability. (orig.)

  2. Mass measurements of neutron-rich Rb and Sr isotopes

    Klawitter, R.; Bader, A.; Brodeur, M.; Chowdhury, U.; Chaudhuri, A.; Fallis, J.; Gallant, A. T.; Grossheim, A.; Kwiatkowski, A. A.; Lascar, D.; Leach, K. G.; Lennarz, A.; Macdonald, T. D.; Pearkes, J.; Seeraji, S.; Simon, M. C.; Simon, V. V.; Schultz, B. E.; Dilling, J.

    2016-04-01

    We report on the mass measurements of several neutron-rich Rb and Sr isotopes in the A ≈100 region with the TITAN Penning-trap mass spectrometer. By using highly charged ions in the charge state q =10 + , the masses of Rb,9998 and Sr-10098 have been determined with a precision of 6-12 keV, making their uncertainty negligible for r -process nucleosynthesis network calculations. The mass of 101Sr has been determined directly for the first time with a precision eight times higher than the previous indirect measurement and a deviation of 3 σ when compared to the Atomic Mass Evaluation. We also confirm the mass of 100Rb from a previous measurement. Furthermore, our data indicate the existence of a low-lying isomer with 80 keV excitation energy in 98Rb. We show that our updated mass values lead to minor changes in the r process by calculating fractional abundances in the A ≈100 region of the nuclear chart.

  3. Time-of-flight mass measurements of exotic nuclei

    Atomic masses play an important role in nuclear physics and astrophysics. The need of experimental mass values for unstable nuclides has triggered the development of a wide range of mass measurement techniques, with devices installed at many laboratories around the world. We have implemented a time-of-flight–magnetic-rigidity (TOF-Bρ) technique at the National Superconducting Cyclotron Laboratory (NSCL) that includes a position measurement for magnetic rigidity corrections and uses the A1900 separator and the S800 spectrograph. We performed a successful first experiment measuring masses of neutron-rich isotopes in the region of Z∼ 20–30, important for calculations of processes occurring in the crust of accreting neutron stars. The masses of 16 nuclei were determined, for 61V, 63Cr, 66Mn, and 74Ni for the first time, with atomic mass excesses of −30.510(890) MeV, −35.280(650) MeV, −36.900(790) MeV, and −49.210(990) MeV, respectively. The mass resolution achieved was 1.8×10−4.

  4. Mass measurements of neutron-rich Rb and Sr isotopes

    Klawitter, R; Brodeur, M; Chowdhury, U; Chausdhuri, A; Fallis, J; Gallant, A T; Grossheim, A; Kwiatkowski, A A; Lascar, D; Leach, K G; Lennarz, A; Macdonald, T D; Pearkes, J; Seeraji, S; Simon, M C; Simon, V V; Schultz, B E; Dilling, J

    2015-01-01

    We report on the mass measurements of several neutron-rich $\\mathrm{Rb}$ and $\\mathrm{Sr}$ isotopes in the $A \\approx 100$ region with the TITAN Penning-trap mass spectrometer. Using highly charged ions in the charge state $q=10+$, the masses of $^{98,99}\\mathrm{Rb}$ and $^{98-100}\\mathrm{Sr}$ have been determined with a precision of $6 - 12\\ \\mathrm{keV}$, making their uncertainty negligible for r-process nucleosynthesis network calculations. The mass of $^{101}\\mathrm{Sr}$ has been determined directly for the first time with a precision eight times higher than the previous indirect measurement and a deviation of $3\\sigma$ when compared to the Atomic Mass Evaluation. We also confirm the mass of $^{100}\\mathrm{Rb}$ from a previous measurement. Furthermore, our data indicates the existance of a low-lying isomer with $80\\ \\mathrm{keV}$ excitation energy in $^{98}\\mathrm{Rb}$. We show that our updated mass values lead to minor changes in the r-process by calculating fractional abundances in the $A\\approx 100$ re...

  5. An accurate Rb density measurement method for a plasma wakefield accelerator experiment using a novel Rb reservoir

    Öz, E.; Batsch, F.; Muggli, P.

    2016-09-01

    A method to accurately measure the density of Rb vapor is described. We plan on using this method for the Advanced Wakefield (AWAKE) (Assmann et al., 2014 [1]) project at CERN , which will be the world's first proton driven plasma wakefield experiment. The method is similar to the hook (Marlow, 1967 [2]) method and has been described in great detail in the work by Hill et al. (1986) [3]. In this method a cosine fit is applied to the interferogram to obtain a relative accuracy on the order of 1% for the vapor density-length product. A single-mode, fiber-based, Mach-Zenhder interferometer will be built and used near the ends of the 10 meter-long AWAKE plasma source to be able to make accurate relative density measurement between these two locations. This can then be used to infer the vapor density gradient along the AWAKE plasma source and also change it to the value desired for the plasma wakefield experiment. Here we describe the plan in detail and show preliminary results obtained using a prototype 8 cm long novel Rb vapor cell.

  6. An accurate Rb density measurement method for a plasma wakefield accelerator experiment using a novel Rb reservoir

    Öz, E; Muggli, P

    2015-01-01

    A method to accurately measure the density of Rb vapor is described. We plan on using this method for the Advanced Wakefield (AWAKE)~\\cite{bib:awake} project at CERN , which will be the world's first proton driven plasma wakefield experiment. The method is similar to the hook~\\cite{bib:Hook} method and has been described in great detail in the work by W. Tendell Hill et. al.~\\cite{bib:densitymeter}. In this method a cosine fit is applied to the interferogram to obtain a relative accuracy on the order of $1\\%$ for the vapor density-length product. A single-mode, fiber-based, Mach-Zenhder interferometer will be built and used near the ends of the 10 meter-long AWAKE plasma source to be able to make accurate relative density measurement between these two locations. This can then be used to infer the vapor density gradient along the AWAKE plasma source and also change it to the value desired for the plasma wakefield experiment. Here we describe the plan in detail and show preliminary results obtained using a prot...

  7. Investigation and Comparison of Localization and Accurate Industrial Measurement through ¬Classic and Modern Mapping Methods

    Seyed Abdolreza Adnani

    2013-10-01

    Full Text Available The purpose of this study is investigation and comparison of localization and accurate industrial measurement through classic and modern mapping methods. in this research and it is proved that if the objective is to determine the coordinates of an event or the geometry of an object, there is no need to align and the coordinates of points on a target, which is generally an ultimate objective of a local mapping project, can be reached and can save the necessary time for aligning and deploying device only through measuring the lengths and angles in Theodolite orthogonal framework. Existence of error in measurement and the need for a unit and close-to-truth response for measured quantities are among the most important issues of measurement science, so that it is possible to determine the accuracy and reliability of mapping projects only through these issues and proper application of mathematical language. Observations of total station (Horizontal angle, vertical angle and oblique length are performed in the Local Astronomy Coordinate System which can be time consuming and cause disruption in core activity of industrial sector according to the time required to locate and align device. Alignment in Goniometer and Distance Measurement or Total Station tools are investigated. Numerical results of this research indicate the complete success of presented method. Thus, this paves the ways for application of total station as a quick tool in open industrial environments and provided theory can create the industrial capabilities for ¬classic mapping.

  8. The TITAN mass measurement facility at TRIUMF-ISAC

    The TITAN facility at TRIUMF-ISAC will use four ion traps with the primary goal of determining nuclear masses with high precision, particularly for short lived isotopes with lifetimes down to approximately 10 ms. The design value for the accuracy of the mass measurement is 1 x10-8. The four main components in the facility are an RF cooler/buncher (RFCT) receiving the incoming ion beam, an electron beam ion trap (EBIT) to breed the ions to higher charge states, a cooler Penning trap (CPET) to cool the highly charged ions, and finally the measurement Penning trap (MPET) for the precision mass determination. Additional goals for this system are laser spectroscopy on ions extracted from the RFCT and beta spectroscopy in the EBIT (in Penning trap mode) on ions that are purified using selective buffer gas cooling in the CPET. The physics motivation for the mass measurements are manifold, from unitarity tests of the CKM matrix to nuclear structure very far from the valley of stability, nuclear astrophysics and the study of halo-nuclei. As a first measurement the mass of 11Li will be determined. With a lifetime of 8.7 ms and a demonstrated production rate of 4x104 ions/sec at ISAC the goal for this measurement at TITAN is a relative uncertainty of 5x10-8. This would check previous conflicting measurements and provide information for nuclear theory and models.

  9. Jet calibration and top quark mass measurement in the semi-leptonic channel in the ATLAS experiment

    The main goal of this thesis is to provide a measurement as accurate as possible of the top quark mass in the semi-leptonic decay channel. This experimental measurement is made thanks to the ATLAS detector near LHC, a proton-proton collider. The main interests for this precision measurement are the physics constraints to the theoretical models of fundamental constituents. Besides, the top quark mass is a parameter allowing to have more information on the vacuum stability at the Planck scale within the Standard Model. Jet energy calibration is crucial to this measurement. The impact of real data taking conditions on this calibration and on jet performance is detailed. The top quark mass measurement using 2011 data collected at an energy in the center-of-mass of 7 TeV is presented. It is using a tri dimensional template analysis method. The measured top quark mass is: m(top) = 172.01 ± 0.92 (stat) ± 1.17 (syst) GeV. The 2012 data collected at an energy in the center-of-mass of 8 TeV are also analysed, and a preliminary result for the top quark mass is provided: m(top) = 172.82 ± 0.39 (stat) ± 1.12 (syst) GeV, the combination of both measurements being the most accurate result of this thesis: m(top) = 172.64 ± 0.37 (stat) ± 1.10 (syst) GeV. (author)

  10. Compact Sensitive Piezoelectric Mass Balance for Measurement of Unconsolidated Materials in Space

    Sherrit, Stewart; Trebi-Ollennu, Ashitey; Bonitz, Robert; Bar-Cohen, Yoseph; Yen, Jesse T.

    2010-01-01

    In many in-situ instruments information about the mass of the sample could aid in the interpretation of the data and portioning instruments might require an accurate sizing of the sample mass before dispensing the sample. In addition, on potential sample return missions a method to directly assess the captured sample size would be required to determine if the sampler could return or needs to continue attempting to acquire sample. In an effort to meet these requirements piezoelectric balances were developed using flextensional actuators which are capable of monitoring the mass using two methods. A piezoelectric balance could be used to measure mass directly by monitoring the voltage developed across the piezoelectric which is linear with force, or it could be used in resonance to produce a frequency change proportional to the mass change. In this case of the latter, the piezoelectric actuator/balance would be swept in frequency through its fundamental resonance. If a mass is added to the balance the resonance frequency would shift down proportionally to the mass. By monitoring the frequency shift the mass could be determined. This design would allow for two independent measurements of the mass. In microgravity environments spacecraft thrusters could be used to provide acceleration in order to produce the required force for the first technique or to bring the mass into contact with the balance in the second approach. In addition, the measuring actuators, if driven at higher voltages, could be used to fluidize the powder to aid sample movement. In this paper, we outline some of our design considerations and present the results of a few prototype balances that we have developed.

  11. High frequency body mass measurement, feedback, and health behaviors

    Kooreman, P.; Scherpenzeel, A.

    2014-01-01

    We analyze weight and fat percentage measurements of respondents in an online general population panel in the Netherlands, collected using wireless scales, with an average frequency of 1.6 measurements per week. First, we document the existence of a weekly cycle; body mass is lowest on Fridays and h

  12. Accurate measurements of cross-plane thermal conductivity of thin films by dual-frequency time-domain thermoreflectance (TDTR)

    Jiang, Puqing; Huang, Bin; Koh, Yee Kan

    2016-07-01

    Accurate measurements of the cross-plane thermal conductivity Λcross of a high-thermal-conductivity thin film on a low-thermal-conductivity (Λs) substrate (e.g., Λcross/Λs > 20) are challenging, due to the low thermal resistance of the thin film compared with that of the substrate. In principle, Λcross could be measured by time-domain thermoreflectance (TDTR), using a high modulation frequency fh and a large laser spot size. However, with one TDTR measurement at fh, the uncertainty of the TDTR measurement is usually high due to low sensitivity of TDTR signals to Λcross and high sensitivity to the thickness hAl of Al transducer deposited on the sample for TDTR measurements. We observe that in most TDTR measurements, the sensitivity to hAl only depends weakly on the modulation frequency f. Thus, we performed an additional TDTR measurement at a low modulation frequency f0, such that the sensitivity to hAl is comparable but the sensitivity to Λcross is near zero. We then analyze the ratio of the TDTR signals at fh to that at f0, and thus significantly improve the accuracy of our Λcross measurements. As a demonstration of the dual-frequency approach, we measured the cross-plane thermal conductivity of a 400-nm-thick nickel-iron alloy film and a 3-μm-thick Cu film, both with an accuracy of ˜10%. The dual-frequency TDTR approach is useful for future studies of thin films.

  13. A black-hole mass measurement from molecular gas kinematics in NGC4526.

    Davis, Timothy A; Bureau, Martin; Cappellari, Michele; Sarzi, Marc; Blitz, Leo

    2013-02-21

    The masses of the supermassive black holes found in galaxy bulges are correlated with a multitude of galaxy properties, leading to suggestions that galaxies and black holes may evolve together. The number of reliably measured black-hole masses is small, and the number of methods for measuring them is limited, holding back attempts to understand this co-evolution. Directly measuring black-hole masses is currently possible with stellar kinematics (in early-type galaxies), ionized-gas kinematics (in some spiral and early-type galaxies) and in rare objects that have central maser emission. Here we report that by modelling the effect of a black hole on the kinematics of molecular gas it is possible to fit interferometric observations of CO emission and thereby accurately estimate black-hole masses. We study the dynamics of the gas in the early-type galaxy NGC 4526, and obtain a best fit that requires the presence of a central dark object of 4.5(+4.2)(-3.1) × 10(8) solar masses (3σ confidence limit). With the next-generation millimetre-wavelength interferometers these observations could be reproduced in galaxies out to 75 megaparsecs in less than 5 hours of observing time. The use of molecular gas as a kinematic tracer should thus allow one to estimate black-hole masses in hundreds of galaxies in the local Universe, many more than are accessible with current techniques. PMID:23364690

  14. Measuring Physical Inactivity: Do Current Measures Provide an Accurate View of “Sedentary” Video Game Time?

    Simon Fullerton

    2014-01-01

    Full Text Available Background. Measures of screen time are often used to assess sedentary behaviour. Participation in activity-based video games (exergames can contribute to estimates of screen time, as current practices of measuring it do not consider the growing evidence that playing exergames can provide light to moderate levels of physical activity. This study aimed to determine what proportion of time spent playing video games was actually spent playing exergames. Methods. Data were collected via a cross-sectional telephone survey in South Australia. Participants aged 18 years and above (n=2026 were asked about their video game habits, as well as demographic and socioeconomic factors. In cases where children were in the household, the video game habits of a randomly selected child were also questioned. Results. Overall, 31.3% of adults and 79.9% of children spend at least some time playing video games. Of these, 24.1% of adults and 42.1% of children play exergames, with these types of games accounting for a third of all time that adults spend playing video games and nearly 20% of children’s video game time. Conclusions. A substantial proportion of time that would usually be classified as “sedentary” may actually be spent participating in light to moderate physical activity.

  15. Measuring Physical Inactivity: Do Current Measures Provide an Accurate View of “Sedentary” Video Game Time?

    Fullerton, Simon; Taylor, Anne W.; Dal Grande, Eleonora; Berry, Narelle

    2014-01-01

    Background. Measures of screen time are often used to assess sedentary behaviour. Participation in activity-based video games (exergames) can contribute to estimates of screen time, as current practices of measuring it do not consider the growing evidence that playing exergames can provide light to moderate levels of physical activity. This study aimed to determine what proportion of time spent playing video games was actually spent playing exergames. Methods. Data were collected via a cross-sectional telephone survey in South Australia. Participants aged 18 years and above (n = 2026) were asked about their video game habits, as well as demographic and socioeconomic factors. In cases where children were in the household, the video game habits of a randomly selected child were also questioned. Results. Overall, 31.3% of adults and 79.9% of children spend at least some time playing video games. Of these, 24.1% of adults and 42.1% of children play exergames, with these types of games accounting for a third of all time that adults spend playing video games and nearly 20% of children's video game time. Conclusions. A substantial proportion of time that would usually be classified as “sedentary” may actually be spent participating in light to moderate physical activity. PMID:25002974

  16. Measuring cluster masses with CMB lensing: a statistical approach

    Melin, Jean-Baptiste

    2014-01-01

    We present a method for measuring the masses of galaxy clusters using the imprint of their gravitational lensing signal on the cosmic microwave background (CMB) temperature anisotropies. The method first reconstructs the projected gravitational potential with a quadratic estimator and then applies a matched filter to extract cluster mass. The approach is well-suited for statistical analyses that bin clusters according to other mass proxies. We find that current experiments, such as Planck, the South Pole Telescope and the Atacama Cosmology Telescope, can practically implement such a statistical methodology, and that future experiments will reach sensitivities sufficient for individual measurements of massive systems. As illustration, we use simulations of Planck observations to demonstrate that it is possible to constrain the mass scale of a set of 62 massive clusters with prior information from X-ray observations, similar to the published Planck ESZ-XMM sample. We examine the effect of the thermal (tSZ) and ...

  17. W mass measurements using fully hadronic events at LEP2

    Schmidt-Kärst, S

    2001-01-01

    Since 1996 each LEP experiment recorded data corresponding to an integrated luminosity around 460-500 pb/sup -1/ at centre-of-mass energies between 161 GeV and 202 GeV. The experimental methods to measure the mass of the W boson in the fully hadronic channel are discussed and the preliminary combined value of the four LEP experiments is presented M/sub W/(qqqq) = 80 432 +or- 0 073 GeV. The LEP combined result for the mass of the W boson, obtained from all channels and all data recorded at centre-of-mass energies above the W- pair threshold, is M/sub W/ = 80 427 +or- 0 046 GeV. The width of the W boson is measured to be Gamma /sub W/ = 2 12 +or- 0 11 GeV..

  18. Non-targeted screening for contaminants in paper and board food-contact materials using effect-directed analysis and accurate mass spectrometry

    Bengtström, Linda; Rosenmai, Anna Kjerstine; Trier, Xenia;

    2016-01-01

    commercial mass spectral library for GC-MS (GC-EI-QTOF MS) analysis and an in-house built library of accurate masses for substances known to be used in P&B packaging for UHPLC-QTOF analysis. Of 75 tentatively identified substances, 15 were initially selected for further testing in vitro; however, only seven...... database can provide a fast tentative identification. Pure standards of the seven tentatively identified substances were tested in vitro but could not explain a significant proportion of the AhR-response in the extract. Targeted analyses of dioxins and PCBs, both well-known AhR agonists, was performed....... However, the dioxins could explain approximately 3% of the activity observed in the pizza box extract indicating that some very AhR active substance(s) still remain to be identified in recycled low quality P&B....

  19. Accurate human limb angle measurement: sensor fusion through Kalman, least mean squares and recursive least-squares adaptive filtering

    Inertial sensors are widely used in human body motion monitoring systems since they permit us to determine the position of the subject's limbs. Limb angle measurement is carried out through the integration of the angular velocity measured by a rate sensor and the decomposition of the components of static gravity acceleration measured by an accelerometer. Different factors derived from the sensors' nature, such as the angle random walk and dynamic bias, lead to erroneous measurements. Dynamic bias effects can be reduced through the use of adaptive filtering based on sensor fusion concepts. Most existing published works use a Kalman filtering sensor fusion approach. Our aim is to perform a comparative study among different adaptive filters. Several least mean squares (LMS), recursive least squares (RLS) and Kalman filtering variations are tested for the purpose of finding the best method leading to a more accurate and robust limb angle measurement. A new angle wander compensation sensor fusion approach based on LMS and RLS filters has been developed

  20. Can endocranial volume be estimated accurately from external skull measurements in great-tailed grackles (Quiscalus mexicanus?

    Corina J. Logan

    2015-06-01

    Full Text Available There is an increasing need to validate and collect data approximating brain size on individuals in the field to understand what evolutionary factors drive brain size variation within and across species. We investigated whether we could accurately estimate endocranial volume (a proxy for brain size, as measured by computerized tomography (CT scans, using external skull measurements and/or by filling skulls with beads and pouring them out into a graduated cylinder for male and female great-tailed grackles. We found that while females had higher correlations than males, estimations of endocranial volume from external skull measurements or beads did not tightly correlate with CT volumes. We found no accuracy in the ability of external skull measures to predict CT volumes because the prediction intervals for most data points overlapped extensively. We conclude that we are unable to detect individual differences in endocranial volume using external skull measurements. These results emphasize the importance of validating and explicitly quantifying the predictive accuracy of brain size proxies for each species and each sex.

  1. Nuclear symmetry energy at subnormal densities from measured nuclear masses

    Min LIU; Wang, Ning; Li, Zhuxia; Zhang, Fengshou

    2010-01-01

    The symmetry energy coefficients for nuclei with mass number A=20~250 are extracted from more than 2000 measured nuclear masses. With the semi-empirical connection between the symmetry energy coefficients of finite nuclei and the nuclear symmetry energy at reference densities, we investigate the density dependence of symmetry energy of nuclear matter at subnormal densities. The obtained results are compared with those extracted from other methods.

  2. Mass measurements along the rp-process path

    The path and termination point for the rp-process above 56Ni is uncertain due to a lack of knowledge of nuclear properties, especially masses, near the proton drip line. To address this need we have begun a program to measure masses of nuclei along the rp-process pathway in the A∼60-80 region using β-γ coincidence spectroscopy. Results for 71Se are presented and a preliminary experiment for 72Br is described

  3. Mass improvement of land cadastre data using new measurements

    Ovca, Miha

    2015-01-01

    The diploma thesis represents the land cadastre in Slovenia, which was initially established for the purpose of land taxation. Nowadays, the land cadastre has different functions and is the basis for real property management. Different periods of land cadastre development have been represented, which brought also different approaches to land cadastre maintenance. The emphasis has been given on the procedure of mass new cadastral measurements, which gives the possibility to mass im...

  4. MASS MEASUREMENTS ALONG THE RP-PROCESS PATH

    The path and termination point for the t-p-process above 56Ni is uncertain due to a lack of knowledge of nuclear properties, especially masses, near the proton drip line. To address this need we have begun a program to measure masses of nuclei along the r-p-process pathway in the A∼60-80 region using β-γ coincidence spectroscopy. Results for 71Se are presented and a preliminary experiment for 72Br is described

  5. Direct mass measurements beyond the proton drip-line

    Rauth, C; Blaum, K; Block, M; Chaudhuri, A; Eliseev, S; Ferrer, R; Habs, D; Herfurth, F; Hessberger, F P; Hofmann, S; Kluge, H J; Maero, G; Martin, A; Marx, G; Mukherjee, M; Neumayr, J B; Plass, W R; Quint, W; Rahaman, S; Rodríguez, D; Scheidenberger, C; Schweikhard, L; Thirolf, P G; Vorobjev, G; Weber, C; Di, Z

    2007-01-01

    First on-line mass measurements were performed at the SHIPTRAP Penning trap mass spectrometer. The masses of 18 neutron-deficient isotopes in the terbium-to-thulium region produced in fusion-evaporation reactions were determined with relative uncertainties of about $7\\cdot 10^{-8}$, nine of them for the first time. Four nuclides ($^{144, 145}$Ho and $^{147, 148}$Tm) were found to be proton-unbound. The implication of the results on the location of the proton drip-line is discussed by analyzing the one-proton separation energies.

  6. Measurement of the top quark mass in the dilepton channel

    Abazov, V M; Abolins, M; Acharya, B S; Adams, M; Adams, T; Agelou, M; Aguiló, E; Ahn, S H; Ahsan, M; Alexeev, G D; Alkhazov, G; Alton, A; Alverson, G; Alves, G A; Anastasoaie, M; Andeen, T; Anderson, S; Andrieu, B; Anzelc, M S; Arnoud, Y; Arov, M; Askew, A; Åsman, B; Assis-Jesus, A C S; Atramentov, O; Autermann, C; Avila, C; Ay, C; Badaud, F; Baden, A; Bagby, L; Baldin, B; Bandurin, D V; Banerjee, P; Banerjee, S; Barberis, E; Bargassa, P; Baringer, P; Barnes, C; Barreto, J; Bartlett, J F; Bassler, U; Bauer, D; Beale, S; Bean, A; Begalli, M; Begel, M; Belanger-Champagne, C; Bellantoni, L; Bellavance, A; Benítez, J A; Beri, S B; Bernardi, G; Bernhard, R; Berntzon, L; Bertram, I; Besançon, M; Beuselinck, R; Bezzubov, V A; Bhat, P C; Bhatnagar, V; Binder, M; Biscarat, C; Black, K M; Blackler, I; Blazey, G; Blekman, F; Blessing, S; Bloch, D; Bloom, K; Blumenschein, U; Böhnlein, A; Boeriu, O; Bolton, T A; Borissov, G; Bos, K; Bose, T; Brandt, A; Brock, R; Brooijmans, G; Bross, A; Brown, D; Buchanan, N J; Buchholz, D; Bühler, M; Büscher, V; Burdin, S; Burke, S; Burnett, T H; Busato, E; Buszello, C P; Butler, J M; Calfayan, P; Calvet, S; Cammin, J; Caron, S; Carvalho, W; Casey, B C K; Cason, N M; Castilla-Valdez, H; Chakrabarti, S; Chakraborty, D; Chan, K M; Chandra, A; Charles, F; Cheu, E; Chevallier, F; Cho, D K; Choi, S; Choudhary, B; Christofek, L; Claes, D; Clement, B; Clément, C; Coadou, Y; Cooke, M; Cooper, W E; Coppage, D; Corcoran, M; Cousinou, M C; Cox, B; Crepe-Renaudin, S; Cutts, D; Cwiok, M; Da Motta, H; Das, A; Das, M; Davies, B; Davies, G; Davis, G A; De, K; de Jong, P; De Jong, S J; De La Cruz-Burelo, E; De Oliveira Martins, C; Degenhardt, J D; Déliot, F; Demarteau, M; Demina, R; Demine, P; Denisov, D; Denisov, S P; Desai, S; Diehl, H T; Diesburg, M; Doidge, M; Dominguez, A; Dong, H; Dudko, L V; Duflot, L; Dugad, S R; Duggan, D; Duperrin, A; Dyer, J; Dyshkant, A; Eads, M; Edmunds, D; Edwards, T; Ellison, J; Elmsheuser, J; Elvira, V D; Eno, S; Ermolov, P; Evans, H; Evdokimov, A; Evdokimov, V N; Fatakia, S N; Feligioni, L; Ferapontov, A V; Ferbel, T; Fiedler, F; Filthaut, F; Fisher, W; Fisk, H E; Fleck, I; Ford, M; Fortner, M; Fox, H; Fu, S; Fuess, S; Gadfort, T; Galea, C F; Gallas, E; Galyaev, E; García, C; García-Bellido, A; Gardner, J; Gavrilov, V; Gay, A; Gay, P; Gelé, D; Gelhaus, R; Gerber, C E; Gershtein, Yu; Gillberg, D; Ginther, G; Gollub, N; Gómez, B; Goussiou, A; Grannis, P D; Greenlee, H; Greenwood, Z D; Gregores, E M; Grenier, G; Gris, P; Grivaz, J F; Grünendahl, S; Grünewald, M W; Guo, F; Guo, J; Gutíerrez, G; Gutíerrez, P; Haas, A; Hadley, N J; Haefner, P; Hagopian, S; Haley, J; Hall, I; Hall, R E; Han, L; Hanagaki, K; Hansson, P; Harder, K; Harel, A; Harrington, R; Hauptman, J M; Hauser, R; Hays, J; Hebbeker, T; Hedin, D; Hegeman, J G; Heinmiller, J M; Heinson, A P; Heintz, U; Hensel, C; Herner, K; Hesketh, G; Hildreth, M D; Hirosky, R; Hobbs, J D; Hoeneisen, B; Hoeth, H; Hohlfeld, M; Hong, S J; Hooper, R; Houben, P; Hu, Y; Hubacek, Z; Hynek, V; Iashvili, I; Illingworth, R; Ito, A S; Jabeen, S; Jaffré, M; Jain, S; Jakobs, K; Jarvis, C; Jenkins, A; Jesik, R; Johns, K; Johnson, C; Johnson, M; Jonckheere, A; Jonsson, P; Juste, A; Käfer, D; Kahn, S; Kajfasz, E; Kalinin, A M; Kalk, J M; Kalk, J R; Kappler, S; Karmanov, D; Kasper, J; Kasper, P; Katsanos, I; Kau, D; Kaur, R; Kehoe, R; Kermiche, S; Khalatyan, N; Khanov, A; Kharchilava, A I; Kharzheev, Yu M; Khatidze, D; Kim, H; Kim, T J; Kirby, M H; Klima, B; Kohli, J M; Konrath, J P; Kopal, M; Korablev, V M; Kotcher, J; Kothari, B; Koubarovsky, A; Kozelov, A V; Krop, D; Kryemadhi, A; Kühl, T; Kumar, A; Kunori, S; Kupco, A; Kurca, T; Kvita, J; Lammers, S; Landsberg, G L; Lazoflores, J; Le Bihan, A C; Lebrun, P; Lee, W M; Leflat, A; Lehner, F; Lesne, V; Lévêque, J; Lewis, P; Li, J; Li, Q Z; Lima, J G R; Lincoln, D; Linnemann, J; Lipaev, V V; Lipton, R; Liu, Z; Lobo, L; Lobodenko, A; Lokajícek, M; Lounis, A; Love, P; Lubatti, H J; Lynker, M; Lyon, A L; Maciel, A K A; Madaras, R J; Mättig, P; Magass, C; Magerkurth, A; Magnan, A M; Makovec, N; Mal, P K; Malbouisson, H B; Malik, S; Malyshev, V L; Mao, H S; Maravin, Y; Martens, M; McCarthy, R; Meder, D; Melnitchouk, A; Mendes, A; Mendoza, L; Merkin, M; Merritt, K W; Meyer, A; Meyer, J; Michaut, M; Miettinen, H; Millet, T; Mitrevski, J; Molina, J; Mondal, N K; Monk, J; Moore, R W; Moulik, T; Muanza, G S; Mulders, M; Mulhearn, M; Mundal, O; Mundim, L; Mutaf, Y D; Nagy, E; Naimuddin, M; Narain, M; Naumann, N A; Neal, H A; Negret, J P; Neustroev, P; Nöding, C; Nomerotski, A; Novaes, S F; Nunnemann, T; O'Dell, V; O'Neil, D C; Obrant, G; Oguri, V; Oliveira, N; Onoprienko, D; Oshima, N; Otec, R; Oteroy-Garzon, G J; Owen, M; Padley, P; Parashar, N; Park, S J; Park, S K; Parsons, J; Partridge, R; Parua, N; Patwa, A; Pawloski, G; Perea, P M; Pérez, E; Peters, K; Petroff, P; Petteni, M; Piegaia, R; Piper, J; Pleier, M A; Podesta-Lerma, P L M; Podstavkov, V M; Pogorelov, Y; Pol, M E; Pompos, A; Pope, B G; Popov, A V; Potter, C; Prado da Silva, W L; Prosper, H B; Protopopescu, S D; Qian, J; Quadt, A; Quinn, B; Rangel, M S; Rani, K J; Ranjan, K; Ratoff, P N; Renkel, P; Reucroft, S; Rijssenbeek, M; Ripp-Baudot, I; Rizatdinova, F K; Robinson, S; Rodrigues, R F; Royon, C; Rubinov, P; Ruchti, R; Rud, V I; Sajot, G; Sánchez-Hernández, A; Sanders, M P; Santoro, A F S; Savage, G; Sawyer, L; Scanlon, T; Schaile, A D; Schamberger, R D; Scheglov, Y; Schellman, H; Schieferdecker, P; Schmitt, C; Schwanenberger, C; Schwartzman, A; Schwienhorst, R; Sekaric, J; Sen-Gupta, S; Severini, H; Shabalina, E; Shamim, M; Shary, V; Shchukin, A A; Shephard, W D; Shivpuri, R K; Shpakov, D; Siccardi, V; Sidwell, R A; Simák, V; Sirotenko, V I; Skubic, P L; Slattery, P F; Smith, R P; Snow, G R; Snow, J; Snyder, S; Söldner-Rembold, S; Song, X; Sonnenschein, L; Sopczak, A; Sosebee, M; Soustruznik, K; Souza, M; Spurlock, B; Stark, J; Steele, J; Stolin, V; Stone, A; Stoyanova, D A; Strandberg, J; Strandberg, S; Strang, M A; Strauss, M; Ströhmer, R; Strom, D; Strovink, M; Stutte, L; Sumowidagdo, S; Svoisky, P; Sznajder, A; Talby, M; Tamburello, P; Taylor, W; Telford, P; Temple, J; Tiller, B; Titov, M; Tokmenin, V V; Tomoto, M; Toole, T; Torchiani, I; Towers, S; Trefzger, T; Trincaz-Duvoid, S; Tsybychev, D; Tuchming, B; Tully, C; Turcot, A S; Tuts, P M; Unalan, R; Uvarov, L; Uvarov, S; Uzunyan, S; Vachon, B; vanden Berg, P J; Van Kooten, R; Van Leeuwen, W M; Varelas, N; Varnes, E W; Vartapetian, A H; Vasilyev, I A; Vaupel, M; Verdier, P; Vertogradov, L S; Verzocchi, M; Villeneuve-Séguier, F; Vint, P; Vlimant, J R; Von Törne, E; Voutilainen, M; Vreeswijk, M; Wahl, H D; Wang, L; Wang, M H L; Warchol, J; Watts, G; Wayne, M; Weber, G; Weber, M; Weerts, H; Wermes, N; Wetstein, M; White, A; Wicke, D; Wilson, G W; Wimpenny, S J; Wobisch, M; Womersley, J; Wood, D R; Wyatt, T R; Xie, Y; Xuan, N; Yacoob, S; Yamada, R; Yan, M; Yasuda, T; Yatsunenko, Y A; Yip, K; Yoo, H D; Youn, S W; Yu, C; Yu, J; Yurkewicz, A; Zatserklyaniy, A; Zeitnitz, C; Zhang, D; Zhao, T; Zhou, B; Zhu, J; Zielinski, M; Zieminska, D; Zieminski, A; Zutshi, V; Zverev, E G; al, et

    2007-01-01

    We present a measurement of the top quark mass in the dilepton channel based on approximately 370/pb of data collected by the D0 experiment during Run II of the Fermilab Tevatron collider. We employ two different methods to extract the top quark mass. We show that both methods yield consistent results using ensemble tests of events generated with the D0 Monte Carlo simulation. We combine the results from the two methods to obtain a top quark mass m_t = 178.1 +/- 8.2 GeV. The statistical uncertainty is 6.7 GeV and the systematic uncertainty is 4.8 GeV.

  7. Mass Measurements of Isolated Objects from Space-based Microlensing

    Zhu, Wei; Gould, A; Udalski, A; Han, C; Shvartzvald, Y; Ranc, C; Jorgensen, U G; Poleski, R; Bozza, V; Beichman, C; Bryden, G; Carey, S; Gaudi, B S; Henderson, C B; Pogge, R W; Porritt, I; Wibking, B; Yee, J C; Pawlak, M; Szymanski, M K; Skowron, J; Mroz, P; Kozlowski, S; Wyrzykowski, L; Pietrukowicz, P; Pietrzynski, G; Soszynski, I; Ulaczyk, K; Choi, J Y; Park, H; Jung, Y K; Shin, I -G; Albrow, M D; Park, B -G; Kim, S -L; Lee, C -U; Kim, D -J; Lee, Y; Friedmann, M; Kaspi, S; Maoz, D; Hundertmark, M; Street, R A; Tsapras, Y; Bramich, D M; Cassan, A; Dominik, M; Bachelet, E; Dong, Subo; Jaimes, R Figuera; Horne, K; Mao, S; Menzies, J; Schmidt, R; Snodgrass, C; Steele, I A; Wambsganss, J; Skottfelt, J; Andersen, M I; Burgdorf, M J; Ciceri, S; D'Ago, G; Evans, D F; Gu, S -H; Hinse, T C; Kerins, E; Korhonen, H; Kuffmeier, M; Mancini, L; Peixinho, N; popovas, A; Rabus, M; Rahvar, S; Rasmussen, R T; Scarpetta, G; Southworth, J; Surdej, J; von Essen, C; Wang, Y -B; Wertz, O

    2015-01-01

    We report on the mass and distance measurements of two single-lens events from the 2015 \\emph{Spitzer} microlensing campaign. With both finite-source effect and microlens parallax measurements, we find that the lens of OGLE-2015-BLG-1268 is a $47\\pm7$ $M_{\\rm J}$ brown dwarf at $5.4\\pm1.0$ kpc, and that the lens of OGLE-2015-BLG-0763 is a $0.50\\pm0.04$ $M_\\odot$ star at $6.9\\pm1.0$ kpc. We show that the probability to definitively measure the mass of isolated microlenses, including isolated stellar mass black holes and free floating planets, is dramatically increased once simultaneous ground- and space-based observations are conducted.

  8. Moving to atomic tritium for neutrino mass measurements

    Kazkaz, Kareem; Project8 Collaboration

    2016-03-01

    For direct measurements of the neutrino mass, the tritium-based experiments Mainz and Troitsk have provided the most sensitive measurements to date, with upper limits near 2200 meV. The KATRIN experiment, beginning its first science run in 2016, also uses tritium as its source and has an anticipated ultimate sensitivity of 200 meV. The largest single systematic effect limiting the mass sensitivity beyond KATRIN is the energy sharing between the emitted beta particle and the resulting T-3He molecule. It therefore behooves all future tritium-based experiments to use atomic, rather than molecular, tritium. In this presentation we will outline experimental considerations of atomic tritium: production, purification, inhibiting recombination, and cooling. We will discuss these considerations within the context of Project8, a tritium-based, cyclotron radiation emission spectroscopy neutrino mass measurement with an ultimate target sensitivity of 50 meV. Prepared by LLNL under Contract DE-AC52-07NA27344.

  9. Two old ways to measure the electron-neutrino mass

    De Rújula, A

    2013-01-01

    Three decades ago, the measurement of the electron neutrino mass in atomic electron capture (EC) experiments was scrutinized in its two variants: single EC and neutrino-less double EC. For certain isotopes an atomic resonance enormously enhances the expected decay rates. The favoured technique, based on calorimeters as opposed to spectrometers, has the advantage of greatly simplifying the theoretical analysis of the data. After an initial surge of measurements, the EC approach did not seem to be competitive. But very recently, there has been great progress on micro-calorimeters and the measurement of atomic mass differences. Meanwhile, the beta-decay neutrino-mass limits have improved by a factor of 15, and the difficulty of the experiments by the cube of that figure. Can the "calorimetric" EC theory cope with this increased challenge? I answer this question affirmatively. In so doing I briefly review the subject and extensively address some persistent misunderstandings of the underlying quantum physics.

  10. Measurements of the top quark mass at the tevatron

    Brandt, Oleg

    2012-01-01

    The mass of the top quark (\\mtop) is a fundamental parameter of the standard model (SM). Currently, its most precise measurements are performed by the CDF and D0 collaborations at the Fermilab Tevatron $p\\bar p$ collider at a centre-of-mass energy of $\\sqrt s=1.96 \\TeV$. We review the most recent of those measurements, performed on data samples of up to 8.7 \\fb\\ of integrated luminosity. The Tevatron combination using up to 5.8 fb$^{-1}$ of data results in a preliminary world average top quark mass of $m_{\\rm top} = 173.2 \\pm 0.9$ GeV. This corresponds to a relative precision of about 0.54%. We conclude with an outlook of anticipated precision the final measurement of \\mtop at the Tevatron.

  11. Ultrasonic Measurement of Change in Elasticity due to Endothelium Dependent Relaxation Response by Accurate Detection of Artery-Wall Boundary

    Kaneko, Takuya; Hasegawa, Hideyuki; Kanai, Hiroshi

    2007-07-01

    Ross hypothesized that an endothelial dysfunction is considered to be an initial step in atherosclerosis. Endothelial cells, which release nitric oxide (NO) in response to shear stress from blood flow, have a function of relaxing smooth muscle in the media of the arterial wall. For the assessment of the endothelial function, there is a conventional method in which the change in the diameter of the brachial artery caused by flow-mediated dilation (FMD) is measured with ultrasound. However, despite the fact that the collagen-rich hard adventitia does not respond to NO, the conventional method measures the change in diameter depending on the mechanical property of the entire wall including the adventitia. Therefore, we developed a method of measuring the change in the thickness and the elasticity of the brachial artery during a cardiac cycle using the phased tracking method for the evaluation of the mechanical property of only the intima-media region. In this study, the initial positions of echoes from the lumen-intima and media-adventitia boundaries are determined using complex template matching to accurately estimate the minute change in the thickness and the elasticity of the brachial and radial arteries. The ambiguity in the determination of such boundaries was eliminated using complex template matching, and the change in elasticity measured by the proposed method was larger than the change in inner diameter obtained by the conventional method.

  12. Accurate measurement of the quadratic Zeeman coefficient of 87Rb clock transition based on the Ramsey atom interferometer

    The quadratic Zeeman coefficient was previously measured by using the single pulse spectroscopy method, in which the experimental resolution is limited by the line width of the spectrum of the clock transition. In this paper, an accurate measurement of the quadratic Zeeman coefficient is presented by using the Ramsey atom interferometer. The line width of the central Ramsey fringe of the 87Rb clock transition, which depends on the interrogation time, is much narrower than that of the single pulse spectroscopy method. The measurement uncertainty of less than 1 Hz G−2 is realized, which is much better than the other current existing results. The measured quadratic Zeeman coefficient of the 87Rb clock transition is 575.33±0.36 Hz G−2 by the Raman Ramsey atom interferometer, and 575.48 ± 0.30 Hz G−2 by the microwave Ramsey atom interferometer, which coincides well with the theoretical result of 575.15 Hz G−2 calculated by the Breit–Rabi formula. (paper)

  13. The Mass Accretion Rate of Galaxy Clusters: A Measurable Quantity

    De Boni, C.; Serra, A. L.; Diaferio, A.; Giocoli, C.; Baldi, M.

    2016-02-01

    We explore the possibility of measuring the mass accretion rate (MAR) of galaxy clusters from their mass profiles beyond the virial radius R200. We derive the accretion rate from the mass of a spherical shell whose inner radius is 2R200, whose thickness changes with redshift, and whose infall velocity is assumed to be equal to the mean infall velocity of the spherical shells of dark matter halos extracted from N-body simulations. This approximation is rather crude in hierarchical clustering scenarios where both smooth accretion and aggregation of smaller dark matter halos contribute to the mass accretion of clusters. Nevertheless, in the redshift range z = [0, 2], our prescription returns an average MAR within 20%-40% of the average rate derived from the merger trees of dark matter halos extracted from N-body simulations. The MAR of galaxy clusters has been the topic of numerous detailed numerical and theoretical investigations, but so far it has remained inaccessible to measurements in the real universe. Since the measurement of the mass profile of clusters beyond their virial radius can be performed with the caustic technique applied to dense redshift surveys of the cluster outer regions, our result suggests that measuring the mean MAR of a sample of galaxy clusters is actually feasible. We thus provide a new potential observational test of the cosmological and structure formation models.

  14. High-precision particle mass measurements using the KEDR detector at the VEPP-4M collider

    Levichev, E. B.; Skrinsky, A. N.; Tikhonov, Yu A.; Todyshev, K. Yu

    2014-01-01

    A review is presented of experiments performed using the KEDR detector at the VEPP-4M accelerator complex for the precise measurement of particle masses. The resonant depolarization method, proposed in 1975 at the G I Budker Institute of Nuclear Physics of the RAS Siberian Branch for measuring beam energy, has undergone further development in the experiments described; an unprecedented accuracy of 5\\times 10^{-7} has been achieved. Application of this method together with measurement of the Compton backscattering energy allowed a series of experiments to be carried out which have provided the world's most accurate mass values for the J/{\\rm\\psi}, {\\psi(2S)}, {\\psi(3770)}, and D^{+/- } mesons for the {\\tau}-lepton.

  15. The electron mass from $g$-factor measurements on hydrogen-like carbon $^{12}$C$^{5+}$

    Köhler, Florian; Kracke, Anke; Werth, Günter; Quint, Wolfgang; Blaum, Klaus

    2016-01-01

    The electron mass in atomic mass units has been determined with a relative uncertainty of $2.8\\cdot 10^{-11}$, which represents a 13-fold improvement of the 2010 CODATA value. The underlying measurement principle combines a high-precision measurement of the Larmor-to-cyclotron frequency ratio on a single hydrogen-like carbon ion in a Penning trap with a corresponding very accurate $g$-factor calculation. Here, we present the measurement results in detail, including a comprehensive discussion of the systematic shifts and their uncertainties. A special focus is set on the various sources of phase jitters, which are essential for the understanding of the applied line-shape model for the $g$-factor resonance.

  16. Multiple-Point Mass Flux Measurement System Using Rayleigh Scattering

    Mielke, Amy F.; Elam, Kristie A.; Clem, Michelle M.

    2009-01-01

    A multiple-point Rayleigh scattering diagnostic is being developed to provide mass flux measurements in gas flows. Spectroscopic Rayleigh scattering is an established flow diagnostic that has the ability to provide simultaneous density, temperature, and velocity measurements. Rayleigh scattered light from a focused 18 Watt continuous-wave laser beam is directly imaged through a solid Fabry-Perot etalon onto a CCD detector which permits spectral analysis of the light. The spatial resolution of the measurements is governed by the locations of interference fringes, which can be changed by altering the etalon characteristics. A prototype system has been used to acquire data in a Mach 0.56 flow to demonstrate feasibility of using this system to provide mass flux measurements. Estimates of measurement uncertainty and recommendations for system improvements are presented

  17. Observation and Mass Measurement of the Baryon $\\Xi^-_b$

    Aaltonen, T; Adelman, J; Affolder, T; Akimoto, T; Albrow, M G; Amerio, S; Amidei, D; Anastassov, A; Anikeev, K; Annovi, A; Antos, J; Aoki, M; Apollinari, G; Arisawa, T; Artikov, A; Ashmanskas, W; Attal, A; Aurisano, A; Azfar, F; Azzi-Bacchetta, P; Azzurri, P; Bacchetta, N; Badgett, W; Barbaro-Galtieri, A; Barnes, V E; Barnett, B A; Baroiant, S; Bartsch, V; Bauer, G; Beauchemin, P H; Bedeschi, F; Behari, S; Bellettini, G; Bellinger, J; Belloni, A; Benjamin, D; Beretvas, A; Beringer, J; Berry, T; Bhatti, A; Binkley, M; Bisello, D; Bizjak, I; Blair, R E; Blocker, C; Blumenfeld, B; Bocci, A; Bodek, A; Boisvert, V; Bölla, G; Bolshov, A; Bortoletto, D; Boudreau, J; Boveia, A; Brau, B; Brigliadori, L; Bromberg, C; Brubaker, E; Budagov, Yu; Budd, H S; Budd, S; Burkett, K; Busetto, G; Bussey, P; Buzatu, A; Byrum, K L; Cabrera, S; Campanelli, M; Campbell, M; Canelli, F; Canepa, A; Carrillo, S; Carlsmith, D; Carosi, R; Carron, S; Casal, B; Casarsa, M; Castro, A; Catastini, P; Cauz, D; Cavalli-Sforza, M; Cerri, A; Cerrito, L; Chang, S H; Chen, Y C; Chertok, M; Chiarelli, G; Chlachidze, G; Chlebana, F; Cho, I; Cho, K; Chokheli, D; Chou, J P; Choudalakis, G; Chuang, S H; Chung, K; Chung, W H; Chung, Y S; Cilijak, M; Ciobanu, C I; Ciocci, M A; Clark, A; Clark, D; Coca, M; Compostella, G; Convery, M E; Conway, J; Cooper, B; Copic, K; Cordelli, M; Cortiana, G; Crescioli, F; Cuenca-Almenar, C; Cuevas-Maestro, J; Culbertson, R; Cully, J C; Da Ronco, S; Datta, M; D'Auria, S; Davies, T; Dagenhart, D; De Barbaro, P; De Cecco, S; Deisher, A; De Lentdecker, G; De Lorenzo, G; Dell'Orso, Mauro; Delli Paoli, F; Demortier, L; Deng, J; Deninno, M; De Pedis, D; Derwent, P F; Di Giovanni, G P; Dionisi, C; Di Ruzza, B; Dittmann, J R; D'Onofrio, M; Dorr, C; Donati, S; Dong, P; Donini, J; Dorigo, T; Dube, S; Efron, J; Erbacher, R; Errede, D; Errede, S; Eusebi, R; Fang, H C; Farrington, S; Fedorko, I; Fedorko, W T; Feild, R G; Feindt, M; Fernández, J P; Field, R; Flanagan, G; Forrest, R; Forrester, S; Franklin, M; Freeman, J C; Furic, I; Gallinaro, M; Galyardt, J; García, J E; Garberson, F; Garfinkel, A F; Gay, C; Gerberich, H; Gerdes, D; Giagu, S; Giannetti, P; Gibson, K; Gimmell, J L; Ginsburg, C; Giokaris, N; Giordani, M; Giromini, P; Giunta, M; Giurgiu, G; Glagolev, V; Glenzinski, D; Gold, M; Goldschmidt, N; Goldstein, J; Golossanov, A; Gómez, G; Gómez-Ceballos, G; Goncharov, M; González, O; Gorelov, I; Goshaw, A T; Goulianos, K; Gresele, A; Grinstein, S; Grosso-Pilcher, C; Group, R C; Grundler, U; Guimarães da Costa, J; Gunay-Unalan, Z; Haber, C; Hahn, K; Hahn, S R; Halkiadakis, E; Hamilton, A; Han, B Y; Han, J Y; Handler, R; Happacher, F; Hara, K; Hare, D; Hare, M; Harper, S; Harr, R F; Harris, R M; Hartz, M; Hatakeyama, K; Hauser, J; Hays, C; Heck, M; Heijboer, A; Heinemann, B; Heinrich, J; Henderson, C; Herndon, M; Heuser, J; Hidas, D; Hill, C S; Hirschbuehl, D; Höcker, A; Holloway, A; Hou, S; Houlden, M; Hsu, S C; Huffman, B T; Hughes, R E; Husemann, U; Huston, J; Incandela, J; Introzzi, G; Iori, M; Ivanov, A; Iyutin, B; James, E; Jang, D; Jayatilaka, B; Jeans, D; Jeon, E J; Jindariani, S; Johnson, W; Jones, M; Joo, K K; Jun, S Y; Jung, J E; Junk, T R; Kamon, T; Karchin, P E; Kato, Y; Kemp, Y; Kephart, R; Kerzel, U; Khotilovich, V; Kilminster, B; Kim, D H; Kim, H S; Kim, J E; Kim, M J; Kim, S B; Kim, S H; Kim, Y K; Kimura, N; Kirsch, L; Klimenko, S; Klute, M; Knuteson, B; Ko, B R; Kondo, K; Kong, D J; Konigsberg, J; Korytov, A; Kotwal, A V; Kraan, A C; Kraus, J; Kreps, M; Kroll, J; Krumnack, N; Kruse, M; Krutelyov, V; Kubo, T; Kuhlmann, S E; Kuhr, T; Kulkarni, N P; Kusakabe, Y; Kwang, S; Laasanen, A T; Lai, S; Lami, S; Lammel, S; Lancaster, M; Lander, R L; Lannon, K; Lath, A; Latino, G; Lazzizzera, I; LeCompte, T; Lee, J; Lee, J; Lee, Y J; Lee, S W; Lefèvre, R; Leonardo, N; Leone, S; Levy, S; Lewis, J D; Lin, C; Lin, C S; Lindgren, M; Lipeles, E; Lister, A; Litvintsev, D O; Liu, T; Lockyer, N S; Loginov, A; Loreti, M; Lu, R S; Lucchesi, D; Lujan, P; Lukens, P; Lungu, G; Lyons, L; Lys, J; Lysak, R; Lytken, E; Mack, P; MacQueen, D; Madrak, R; Maeshima, K; Makhoul, K; Mäki, T; Maksimovic, P; Malde, S; Malik, S; Manca, G; Manousakis, A; Margaroli, F; Marginean, R; Marino, C; Marino, C P; Martin, A; Martin, M; Martin, V; Martínez, M; Martinez-Ballarin, R; Maruyama, T; Mastrandrea, P; Masubuchi, T; Matsunaga, H; Mattson, M E; Mazini, R; Mazzanti, P; McFarland, K S; McIntyre, P; McNulty, R; Mehta, A; Mehtälä, P; Menzemer, S; Menzione, A; Merkel, P; Mesropian, C; Messina, A; Miao, T; Miladinovic, N; Miles, J; Miller, R; Mills, C; Milnik, M; Mitra, A; Mitselmakher, G; Miyamoto, A; Moed, S; Moggi, N; Mohr, B; Moon, C S; Moore, R; Morello, M; Movilla-Fernández, P A; Mülmenstädt, J; Mukherjee, A; Müller, T; Mumford, R; Murat, P; Mussini, M; Nachtman, J; Nagano, A; Naganoma, J; Nakamura, K; Nakano, I; Napier, A; Necula, V; Neu, C; Neubauer, M S; Nielsen, J; Nodulman, L; Norniella, O; Nurse, E; Oh, S H; Oh, Y D; Oksuzian, I; Okusawa, T; Oldeman, R; Orava, R; Österberg, K; Pagliarone, C; Palencia, E; Papadimitriou, V; Papaikonomou, A; Paramonov, A A; Parks, B; Pashapour, S; Patrick, J; Pauletta, G; Paulini, M; Paus, C; Pellett, D E; Penzo, Aldo L; Phillips, T J; Piacentino, G; Piedra, J; Pinera, L; Pitts, K; Plager, C; Pondrom, L; Portell, X; Poukhov, O; Pounder, N; Prakoshyn, F; Pronko, A; Proudfoot, J; Ptohos, F; Punzi, G; Pursley, J; Rademacker, J; Rahaman, A; Ramakrishnan, V; Ranjan, N; Redondo, I; Reisert, B; Rekovic, V; Renton, P B; Rescigno, M; Richter, S; Rimondi, F; Ristori, L; Robson, A; Rodrigo, T; Rogers, E; Rolli, S; Roser, R; Rossi, M; Rossin, R; Roy, P; Ruiz, A; Russ, J; Rusu, V; Saarikko, H; Safonov, A; Sakumoto, W K; Salamanna, G; Salto, O; Santi, L; Sarkar, S; Sartori, L; Sato, K; Savard, P; Savoy-Navarro, A; Scheidle, T; Schlabach, P; Schmidt, E E; Schmidt, M P; Schmitt, M; Schwarz, T; Scodellaro, L; Scott, A L; Scribano, A; Scuri, F; Sedov, A; Seidel, S; Seiya, Y; Semenov, A; Sexton-Kennedy, L; Sfyrla, A; Shalhout, S Z; Shapiro, M D; Shears, T G; Shepard, P F; Sherman, D; Shimojima, M; Shochet, M; Shon, Y; Shreyber, I; Sidoti, A; Sinervo, P; Sisakian, A; Slaughter, A J; Slaunwhite, J; Sliwa, K; Smith, J R; Snider, F D; Snihur, R; Söderberg, M; Soha, A; Somalwar, S; Sorin, V; Spalding, J; Spinella, F; Spreitzer, T; Squillacioti, P; Stanitzki, M; Staveris-Polykalas, A; Saint-Denis, R; Stelzer, B; Stelzer-Chilton, O; Stentz, D; Strologas, J; Stuart, D; Suh, J S; Sukhanov, A; Sun, H; Suslov, I; Suzuki, T; Taffard, A; Takashima, R; Takeuchi, Y; Tanaka, R; Tecchio, M; Teng, P K; Terashi, K; Thom, J; Thompson, A S; Thomson, E; Tipton, P; Tiwari, V; Tkaczyk, S; Toback, D; Tokar, S; Tollefson, K; Tomura, T; Tonelli, D; Torre, S; Torretta, D; Tourneur, S; Trischuk, W; Tsuno, S; Tu, Y; Turini, N; Ukegawa, F; Uozumi, S; Vallecorsa, S; Van Remortel, N; Varganov, A; Vataga, E; Vázquez, F; Velev, G; Vellidis, C; Veramendi, G; Veszpremi, V; Vidal, M; Vidal, R; Vila, I; Vilar, R; Vine, T; Vogel, M; Vollrath, I; Volobuev, I P; Volpi, G; Würthwein, F; Wagner, P; Wagner, R G; Wagner, R L; Wagner, J; Wagner, W; Wallny, R; Wang, S M; Warburton, A; Waters, D; Weinberger, M; Wester, W C; Whitehouse, B; Whiteson, D; Wicklund, A B; Wicklund, E; Williams, G; Williams, H H; Wilson, P; Winer, B L; Wittich, P; Wolbers, S; Wolfe, C; Wright, T; Wu, X; Wynne, S M; Yagil, A; Yamamoto, K; Yamaoka, J; Yamashita, T; Yang, C; Yang, U K; Yang, Y C; Yao, W M; Yeh, G P; Yoh, J; Yorita, K; Yoshida, T; Yu, G B; Yu, I; Yu, S S; Yun, J C; Zanello, L; Zanetti, A; Zaw, I; Zhang, X; Zhou, J; Zucchelli, S

    2007-01-01

    We report the observation and measurement of the mass of the bottom, strange baryon $\\Xi^-_b$ through the decay chain $\\Xi^-_b \\to J/\\psi \\Xi^-$, where $J/\\psi \\to \\mu^+ \\mu^-$, $\\Xi^- \\to \\Lambda \\pi^-$, and $\\Lambda \\to p \\pi^-$. Evidence for observation is based on a signal whose probability of arising from the estimated background is $6.6 \\times 10^{-15}$, or 7.7 Gaussian standard deviations. The $\\Xi^-_b$ mass is measured to be $5792.9\\pm 2.5$ (stat.) $\\pm 1.7$ (syst.) MeV/$c^2$.

  18. Measurement of the top mass at the LHC

    Balli, Fabrice; The ATLAS collaboration

    2015-01-01

    The top quark is the most massive fundamental particle ever observed. As such, it plays a particular role in the theories of elementary constituents of matter. The motivation for a precise measurement of the top quark mass ensues from this role. The ATLAS and CMS experiments at the LHC have taken part in this effort and achieve precisions below the GeV, using data collected during the years 2011 and 2012, at a centre-of-mass energy $\\sqrt{s}$ of 7 TeV and 8 TeV respectively. This document reviews the measurements performed by the two collaborations at the time of writing.

  19. Spatially resolved protein hydrogen exchange measured by subzero-cooled chip-based nanoelectrospray ionization tandem mass spectrometry

    Amon, Sabine; Trelle, Morten B; Jensen, Ole N; Jørgensen, Thomas J D

    2012-01-01

    Mass spectrometry has become a valuable method for studying structural dynamics of proteins in solution by measuring their backbone amide hydrogen/deuterium exchange (HDX) kinetics. In a typical exchange experiment one or more proteins are incubated in deuterated buffer at physiological conditions...... optimized mass spectrometric conditions where gas-phase hydrogen scrambling is negligible. Our results show that the known dynamic behavior of ubiquitin in solution is accurately reflected in the deuterium contents of the fragment ions....

  20. Accurate measurements of carbon monoxide in humid air using the cavity ring-down spectroscopy (CRDS technique

    H. Chen

    2013-04-01

    Full Text Available Accurate measurements of carbon monoxide (CO in humid air have been made using the cavity ring-down spectroscopy (CRDS technique. The measurements of CO mole fractions are determined from the strength of its spectral absorption in the near-infrared region (~1.57 μm after removing interferences from adjacent carbon dioxide (CO2 and water vapor (H2O absorption lines. Water correction functions that account for the dilution and pressure-broadening effects as well as absorption line interferences from adjacent CO2 and H2O lines have been derived for CO2 mole fractions between 360–390 ppm and for reported H2O mole fractions between 0–4%. The line interference corrections are independent of CO mole fractions. The dependence of the line interference correction on CO2 abundance is estimated to be approximately −0.3 ppb/100 ppm CO2 for dry mole fractions of CO. Comparisons of water correction functions from different analyzers of the same type show significant differences, making it necessary to perform instrument-specific water tests for each individual analyzer. The CRDS analyzer was flown on an aircraft in Alaska from April to November in 2011, and the accuracy of the CO measurements by the CRDS analyzer has been validated against discrete NOAA/ESRL flask sample measurements made on board the same aircraft, with a mean difference between integrated in situ and flask measurements of −0.6 ppb and a standard deviation of 2.8 ppb. Preliminary testing of CRDS instrumentation that employs improved spectroscopic model functions for CO2, H2O, and CO to fit the raw spectral data (available since the beginning of 2012 indicates a smaller water vapor dependence than the models discussed here, but more work is necessary to fully validate the performance. The CRDS technique provides an accurate and low-maintenance method of monitoring the atmospheric dry mole fractions of CO in humid air streams.

  1. Necessary Conditions for Accurate, Transient Hot-Wire Measurements of the Apparent Thermal Conductivity of Nanofluids are Seldom Satisfied

    Antoniadis, Konstantinos D.; Tertsinidou, Georgia J.; Assael, Marc J.; Wakeham, William A.

    2016-08-01

    The paper considers the conditions that are necessary to secure accurate measurement of the apparent thermal conductivity of two-phase systems comprising nanoscale particles of one material suspended in a fluid phase of a different material. It is shown that instruments operating according to the transient hot-wire technique can, indeed, produce excellent measurements when a finite element method (FEM) is employed to describe the instrument for the exact geometry of the hot wire. Furthermore, it is shown that an approximate analytic solution can be employed with equal success, over the time range of 0.1 s to 1 s, provided that (a) two wires are employed, so that end effects are canceled, (b) each wire is very thin, less than 30 \\upmu m diameter, so that the line source model and the corresponding corrections are valid, (c) low values of the temperature rise, less than 4 K, are employed in order to minimize the effect of convection on the heat transfer in the time of measurement of 1 s, and (d) insulated wires are employed for measurements in electrically conducting or polar liquids to avoid current leakage or other electrical distortions. According to these criteria, a transient hot-wire instrument has been designed, constructed, and employed for the measurement of the enhancement of the thermal conductivity of water when TiO2 or multi-wall carbon nanotubes (MWCNT) are added. These new results, together with a critical evaluation of other measurements, demonstrate the importance of proper implementation of the technique.

  2. Mass measurement of halo nuclides and beam cooling with the mass spectrometer Mistral

    Halo nuclides are a spectacular drip-line phenomenon and their description pushes nuclear theories to their limits. The most critical input parameter is the nuclear binding energy; a quantity that requires excellent measurement precision, since the two-neutron separation energy is small at the drip-line by definition. Moreover halo nuclides are typically very short-lived. Thus, a high accuracy instrument using a quick method of measurement is necessary. MISTRAL is such an instrument; it is a radiofrequency transmission mass spectrometer located at ISOLDE/CERN. In July 2003 we measured the mass of the Li11, a two-neutron halo nuclide. Our measurement improves the precision by a factor 6, with an error of 5 keV. Moreover the measurement gives a two-neutron separation energy 20% higher than the previous value. This measurement has an impact on the radius of the nucleus, and on the state of the two valence neutrons. At the same time, a measurement of the Be11 was performed with an uncertainty of 4 keV, in excellent agreement with previous measurements. In order to measure the mass of the two-neutron halo nuclide Be14, an ion beam cooling system is presently under development which will increase the sensitivity of the spectrometer. The second part of this work presents the development of this beam cooler using a gas-filled Paul trap. (author)

  3. A highly efficient measure of mass segregation in star clusters

    Olczak, C; Henning, Th

    2011-01-01

    Investigations of mass segregation are of vital interest for the understanding of the formation and dynamical evolution of stellar systems on a wide range of spatial scales. Our method is based on the minimum spanning tree (MST) that serves as a geometry-independent measure of concentration. Compared to previous such approaches we obtain a significant refinement by using the geometrical mean as an intermediate-pass. It allows the detection of mass segregation with much higher confidence and for much lower degrees of mass segregation than other approaches. The method shows in particular very clear signatures even when applied to small subsets of the entire population. We confirm with high significance strong mass segregation of the five most massive stars in the Orion Nebula Cluster (ONC). Our method is the most sensitive general measure of mass segregation so far and provides robust results for both data from simulations and observations. As such it is ideally suited for tracking mass segregation in young sta...

  4. Total evaporation measurements of plutonium with a Thermal Quadrupole Mass Spectrometer (THQ)

    On site verification of isotopic distributions of samples prepared at nuclear reprocessing or fuel fabrication plants requires a measurement procedure which is as independent as possible from varying sample preparation procedures or sample concentrations. With conventional peak jumping data collection, mass fractionation effects are dependent upon the total mass of sample taken and amount of that sample evaporated. This requires the sample concentrations to be maintained in a narrow range to allow accurate correction of the fractionation. This effect can be reduced or eliminated if the ion currents or relative ion ratios are summed while the sample is totally evaporated. Measurement of the ion currents for a total evaporation of the sample using a single collector requires a mass spectrometer capable of rapidly scanning or peak jumping the isotopes of interest. This is accomplished using a quadrupole mass spectrometer. A software package written to give a special peak jumping sequence combined with incremental increases of evaporation (sample) filament current makes it possible to evaporate about 98% of the sample. The amount of Pu on the filament is 100 nanograms. Reproducibility of the 240/239 of 0.3% and accuracies of 0.2% (coefficients of variation) have been measured. The measurement is described and results of measurement of standards and actual samples are presented. (author)

  5. A new data evaluation approach for mass measurements of exotic nuclei performed with isochronous mass spectrometry

    The Isochronous Mass Spectrometry (IMS) and Schottky Mass Spectrometry (SMS) are powerful tools to measure masses of rare exotic nuclei in a storage ring. While the SMS method provides very high accuracies it does not give access to rare isotopes with lifetimes in the sub second range because beam cooling has to be performed for a few seconds before the measurements start. As a complementary method IMS can be used without beam cooling to reach isotopes with lifetimes of only a few 10 μs. As a drawback of the IMS method one cannot achieve the high mass accuracy of the SMS method until now. For the data evaluation of the SMS data a correlation matrix method has been successfully applied in the past. In order to improve the accuracy of the IMS measurements the same method will now be used, which will allow to combine and to correlate data from different IMS measurements with each other. Applying this method to the analysis of previous experiments with uranium fission fragments at the FRS-ESR facility at GSI and to future experiments, will increase the accuracy of the IMS method and may lead to new mass values with reasonable accuracies for very rare and important nuclei for nuclear astrophysics such as 130Cd, which were not accessible before.

  6. Measuring Consistent Masses for 25 Milky Way Globular Clusters

    Kimmig, Brian; Ivans, Inese I; Strader, Jay; Caldwell, Nelson; Anderton, Tim; Gregersen, Dylan

    2014-01-01

    We present central velocity dispersions, masses, mass to light ratios ($M/L$s), and rotation strengths for 25 Galactic globular clusters. We derive radial velocities of 1951 stars in 12 globular clusters from single order spectra taken with Hectochelle on the MMT telescope. To this sample we add an analysis of available archival data of individual stars. For the full set of data we fit King models to derive consistent dynamical parameters for the clusters. We find good agreement between single mass King models and the observed radial dispersion profiles. The large, uniform sample of dynamical masses we derive enables us to examine trends of $M/L$ with cluster mass and metallicity. The overall values of $M/L$ and the trends with mass and metallicity are consistent with existing measurements from a large sample of M31 clusters. This includes a clear trend of increasing $M/L$ with cluster mass, and lower than expected $M/L$s for the metal-rich clusters. We find no clear trend of increasing rotation with increasi...

  7. Precise measurement of W and Z masses with UA2

    Since the first observation of W and Z bosons at the CERN SPS Collider, their properties, especially their masses have been the subject of intensive studies. A new improved result is presented for the mass ratio mW/mZ obtained from the recent run of the UA2 detector at the CERN SPS Collider. This provides a new value for the weak mixing parameter sin2ΘW. By combining this result with recent measurements of the Z mass from e+e-colliders a new precise value of the W mass is obtained, mW=80.49±0.43(stat)±0.24(syst) GeV. (R.P.) 6 refs.; 4 figs.; 2 tabs

  8. Dynamical Mass Measurements of Contaminated Galaxy Clusters Using Machine Learning

    Ntampaka, M; Sutherland, D J; Fromenteau, S; Poczos, B; Schneider, J

    2015-01-01

    We study dynamical mass measurements of galaxy clusters contaminated by interlopers and show that a modern machine learning (ML) algorithm can predict masses by better than a factor of two compared to a standard scaling relation approach. We create two mock catalogs from Multidark's publicly-available N-body MDPL1 simulation, one with perfect galaxy cluster membership information and the other where a simple cylindrical cut around the cluster center allows interlopers to contaminate the clusters. In the standard approach, we use a power law scaling relation to infer cluster mass from galaxy line of sight (LOS) velocity dispersion. Assuming perfect membership knowledge, this unrealistic case produces a wide fractional mass error distribution, with width = 0.87. Interlopers introduce additional scatter, significantly widening the error distribution further (width = 2.13). We employ the Support Distribution Machine (SDM) class of algorithms to learn from distributions of data to predict single values. Applied to...

  9. Advances in Radioactive-Isotope Science from Mass Measurements

    Lunney, David

    Mass is a fundamental property that is indispensable for the study of nuclear structure, for applications in stellar nucleosynthesis and neutron-star composition, as well as studies of atomic and weak-interaction physics. We briefly review the mass-measurement programs at radioactive-beam facilities worldwide and examine the wealth of new mass data, compare the strengths of the different installations and reflect on the multitude of physics results. The series of ENAM meetings from 1995 to 2008 saw the rise and subsequent dominance of Penning traps in the field of mass spectrometry, which has continued through the new era of the ARIS meetings. As for the ARIS 2011 conference, we attempt a nomination for "Penning trap of the year."

  10. A Critical Assessment of Stellar Mass Measurement Methods

    Mobasher, Bahram; Dahlen, Tomas; Ferguson, Henry C.; Acquaviva, Viviana; Barro, Guillermo; Finkelstein, Steven L.; Fontana, Adriano; Gruetzbauch, Ruth; Johnson, Seth; Lu, Yu; Papovich, Casey J.; Pforr, Janine; Salvato, Mara; Somerville, Rachel S.; Wiklind, Tommy; Wuyts, Stijn; Ashby, Matthew L. N.; Bell, Eric; Conselice, Christopher J.; Dickinson, Mark E.; Faber, Sandra M.; Fazio, Giovanni; Finlator, Kristian; Galametz, Audrey; Gawiser, Eric; Giavalisco, Mauro; Grazian, Andrea; Grogin, Norman A.; Guo, Yicheng; Hathi, Nimish; Kocevski, Dale; Koekemoer, Anton M.; Koo, David C.; Newman, Jeffrey A.; Reddy, Naveen; Santini, Paola; Wechsler, Risa H.

    2015-07-01

    This is the second paper in a series aimed at investigating the main sources of uncertainty in measuring the observable parameters in galaxies from their spectral energy distributions (SEDs). In the first paper we presented a detailed account of the photometric redshift measurements and an error analysis of this process. In this paper we perform a comprehensive study of the main sources of random and systematic error in stellar mass estimates for galaxies, and their relative contributions to the associated error budget. Since there is no prior knowledge of the stellar mass of galaxies (unlike their photometric redshifts), we use mock galaxy catalogs with simulated multi-waveband photometry and known redshift, stellar mass, age and extinction for individual galaxies. The multi-waveband photometry for the simulated galaxies were generated in 13 filters spanning from U-band to mid-infrared wavelengths. Given different parameters affecting stellar mass measurement (photometric signal-to-noise ratios (S/N), SED fitting errors and systematic effects), the inherent degeneracies and correlated errors, we formulated different simulated galaxy catalogs to quantify these effects individually. For comparison, we also generated catalogs based on observed photometric data of real galaxies in the Great Observatories Origins Deep Survey-South field, spanning the same passbands. The simulated and observed catalogs were provided to a number of teams within the Cosmic Assembly Near-infrared Deep Extragalactic Legacy Survey collaboration to estimate the stellar masses for individual galaxies. A total of 11 teams participated, with different combinations of stellar mass measurement codes/methods, population synthesis models, star formation histories, extinction and age. For each simulated galaxy, the differences between the input stellar masses, Minput, and those estimated by each team, Mest, is defined as {{Δ }}{log}(M)\\equiv {log}({M}{estimated})-{log}({M}{input}), and used to

  11. Measurement of the W mass in $e^+ e^-$ annihilation

    Juste, A

    1998-01-01

    A measurement of the W mass in the fully hadronic decay channel from the data sample collected by ALEPH during 1996 at centre-of-mass energies of 161 and 172 GeV is presented. At 161 GeV, the W mass is derived from the cross-section measurement taking advantage of the high sensitivity close to the production threshold. Due to the presence of large backgrounds, a multidimensional analysis based on Neural Network techniques is developed. By combining the measurements in all decay channels and the four LEP experiments, a precision in the W mass of $\\pm 220$ MeV is finally obtained. At 172 GeV, the W mass is obtained from the direct reconstruction of the final state kinematics. The fully hadronic decay channel becomes particularly difficult due to the large existing background and the important distortions due to fragmentation and detector effects when reconstructing four hadronic jets in the final state. In addition, in this channel there is the intrinsic difficulty associated with the combinatorial background. ...

  12. Using an SLR inversion to measure the mass balance of Greenland before and during GRACE

    Bonin, Jennifer

    2016-04-01

    The GRACE mission has done an admirable job of measuring large-scale mass changes over Greenland since its launch in 2002. However before that time, measurements of large-scale ice mass balance were few and far between, leading to a lack of baseline knowledge. High-quality Satellite Laser Ranging (SLR) data existed a decade earlier, but normally has too low a spatial resolution to be used for this purpose. I demonstrate that a least squares inversion technique can reconstitute the SLR data and use it to measure ice loss over Greenland. To do so, I first simulate the problem by degrading today's GRACE data to a level comparable with SLR, then demonstrating that the inversion can re-localize Greenland's contribution to the low-resolution signal, giving an accurate time series of mass change over all of Greenland which compares well with the full-resolution GRACE estimates. I then utilize that method on the actual SLR data, resulting in an independent 1994-2014 time series of mass change over Greenland. I find favorable agreement between the pure-SLR inverted results and the 2012 Ice-sheet Mass Balance Inter-comparison Exercise (IMBIE) results, which are largely based on the "input-output" modeling method before GRACE's launch.

  13. Skeletal muscle mass and quality: evolution of modern measurement concepts in the context of sarcopenia.

    Heymsfield, Steven B; Gonzalez, M Cristina; Lu, Jianhua; Jia, Guang; Zheng, Jolene

    2015-11-01

    The first reports of accurate skeletal muscle mass measurement in human subjects appeared at about the same time as introduction of the sarcopenia concept in the late 1980s. Since then these methods, computed tomography and MRI, have been used to gain insights into older (i.e. anthropometry and urinary markers) and more recently developed and refined methods (ultrasound, bioimpedance analysis and dual-energy X-ray absorptiometry) of quantifying regional and total body skeletal muscle mass. The objective of this review is to describe the evolution of these methods and their continued development in the context of sarcopenia evaluation and treatment. Advances in these technologies are described with a focus on additional quantifiable measures that relate to muscle composition and 'quality'. The integration of these collective evaluations with strength and physical performance indices is highlighted with linkages to evaluation of sarcopenia and the spectrum of related disorders such as sarcopenic obesity, cachexia and frailty. Our findings show that currently available methods and those in development are capable of non-invasively extending measures from solely 'mass' to quality evaluations that promise to close the gaps now recognised between skeletal muscle mass and muscle function, morbidity and mortality. As the largest tissue compartment in most adults, skeletal muscle mass and aspects of muscle composition can now be evaluated by a wide array of technologies that provide important new research and clinical opportunities aligned with the growing interest in the spectrum of conditions associated with sarcopenia. PMID:25851205

  14. Accurate measurement of extracellular fluid volume from the slope/intercept technique after bolus injection of a filtration marker

    Extracellular fluid volume (ECV) is studied infrequently. The zero-time distribution volume (Vd) generated in the slope-intercept technique for measuring the glomerular filtration rate (GFR) substantially overestimates ECV. The aim was to validate a new technique for measuring ECV from the slope-intercept approach. GFR and ECV were measured using Cr-51-EDTA and iohexol injected into opposite arms in 51 patients undergoing routine measurement of GFR and on 48 occasions in 20 healthy volunteers. Blood samples were obtained bilaterally 20, 40, 60, 120, 180 and 240 min post-injection and assayed for indicator injected contralaterally. Reference ECV (ECV6) was calculated from all six samples as the product of indicator transit time and multi-sample GFR. GFR/ECV was calculated as the rate constant of the exponential fitted to the last three samples (GFR/ECV3). Slope-intercept GFR was calculated from the last three samples using the slope-intercept technique (GFR3). ECV (ECV3) was calculated by dividing GFR3 by GFR/ECV3, having corrected both for their one-compartment assumptions. ECV6EDTA correlated closely with ECV3EDTA (ECV3EDTA = 1.01.ECV6EDTA–0.5 L; r = 0.97; n = 99), but less closely with Vd (Vd = 1.17.ECV6EDTA + 0.7 L; r = 0.86). ECV6iohexol correlated slightly better with ECV6 EDTA (ECV6EDTA = 0.81.ECV6iohexol + 3.3 L; r = 0.86) than with ECV3EDTA (ECV3EDTA = 0.83.ECV6iohexol + 2.9 L; r = 0.84) and had slightly narrower 95% limits of agreement (−3.82 and 2.82 L versus −3.90 to 3.43 L). In conclusion, ECV can be measured from three samples almost as accurately as ECV from multiple samples

  15. A New Top Mass Measurement in The Dilepton Channel

    Trovato, Marco; /INFN, Pisa /Pisa U.

    2008-01-01

    The top quark discovery completed the present picture of the fundamental constituents of the nature. Since then, the Collider Detector at Fermilab and D0 Collaborations have been spending great efforts to measure its properties better. About 30 times larger than the second heaviest quark, the mass of the top has been measured with increased statistic and more and more sophisticated techniques in order to reduce as much as possible its uncertainty. This is because the top is expected to play a fundamental role in the Standard Model. The value of its mass sets boundaries on the mass of the unobserved Higgs boson, and perhaps more appealing, studies of its properties might lead to the discovery of new physics.

  16. Charged Kaon Mass Measurement using the Cherenkov Effect

    Graf, N; Abrams, R J; Akgun, U; Aydin, G; Baker, W; Barnes, P D; Bergfeld, T; Beverly, L; Bujak, A; Carey, D; Dukes, C; Duru, F; Feldman, G J; Godley, A; Gülmez, E; Günaydın, Y O; Gustafson, H R; Gutay, L; Hartouni, E; Hanlet, P; Hansen, S; Heffner, M; Johnstone, C; Kaplan, D; Kamaev, O; Kilmer, J; Klay, J; Kostin, M; Lange, D; Ling, J; Longo, M J; Lu, L C; Materniak, C; Messier, M D; Meyer, H; Miller, D E; Mishra, S R; Nelson, K; Nigmanov, T; Norman, A; Onel, Y; Paley, J M; Park, H K; Penzo, A; Peterson, R J; Raja, R; Rajaram, D; Ratnikov, D; Rosenfeld, C; Rubin, H; Seun, S; Solomey, N; Soltz, R; Swallow, E; Schmitt, R; Subbarao, P; Torun, Y; Tope, T E; Wilson, K; Wright, D; Wu, K

    2009-01-01

    The two most recent and precise measurements of the charged kaon mass use X-rays from kaonic atoms and report uncertainties of 14 ppm and 22 ppm yet differ from each other by 122 ppm. We describe the possibility of an independent mass measurement using the measurement of Cherenkov light from a narrow-band beam of kaons, pions, and protons. This technique was demonstrated using data taken opportunistically by the Main Injector Particle Production experiment at Fermi National Accelerator Laboratory which recorded beams of protons, kaons, and pions ranging in momentum from +37 GeV/c to +63 GeV/c. The measured value is 491.3 +/- 1.7 MeV/c^2, which is within 1.4 sigma of the world average. An improvement of two orders of magnitude in precision would make this technique useful for resolving the ambiguity in the X-ray data and may be achievable in a dedicated experiment.

  17. Improvements to TITAN's mass measurement and decay spectroscopy capabilities

    Lascar, D.; Kwiatkowski, A. A.; Alanssari, M.; Chowdhury, U.; Even, J.; Finlay, A.; Gallant, A. T.; Good, M.; Klawitter, R.; Kootte, B.; Li, T.; Leach, K. G.; Lennarz, A.; Leistenschneider, E.; Mayer, A. J.; Schultz, B. E.; Schupp, R.; Short, D. A.; Andreoiu, C.; Dilling, J.; Gwinner, G.

    2016-06-01

    The study of nuclei farther from the valley of β -stability than ever before goes hand-in-hand with shorter-lived nuclei produced in smaller abundances than their less exotic counterparts. The measurement, to high precision, of nuclear masses therefore requires innovations in technique in order to keep up. TRIUMF's Ion Trap for Atomic and Nuclear science (TITAN) facility deploys three ion traps, with a fourth in the commissioning phase, to perform and support Penning trap mass spectrometry and in-trap decay spectroscopy on some of the shortest-lived nuclei ever studied. We report on recent advances and updates to the TITAN facility since the 2012 EMIS conference. TITAN's charge breeding capabilities have been improved and in-trap decay spectroscopy can be performed in TITAN's Electron Beam Ion Trap (EBIT). Higher charge states can improve the precision of mass measurements, reduce the beam-time requirements for a given measurement, improve beam purity, and open the door to access isotopes not available from the ISOL method via in-trap decay and recapture. This was recently demonstrated during TITAN's mass measurement of 30 Al. The EBIT's decay spectroscopy setup was commissioned with a successful branching ratio and half-life measurement of 124 Cs. Charge breeding in the EBIT increases the energy spread of the ion bunch sent to the Penning trap for mass measurement, so a new Cooler PEnning Trap (CPET), which aims to cool highly charged ions with an electron plasma, is undergoing offline commissioning. Already CPET has demonstrated the trapping and self-cooling of a room-temperature electron plasma that was stored for several minutes. A new detector has been installed inside the CPET magnetic field which will allow for in-magnet charged particle detection.

  18. CLASSIFYING BENIGN AND MALIGNANT MASSES USING STATISTICAL MEASURES

    B. Surendiran

    2011-11-01

    Full Text Available Breast cancer is the primary and most common disease found in women which causes second highest rate of death after lung cancer. The digital mammogram is the X-ray of breast captured for the analysis, interpretation and diagnosis. According to Breast Imaging Reporting and Data System (BIRADS benign and malignant can be differentiated using its shape, size and density, which is how radiologist visualize the mammograms. According to BIRADS mass shape characteristics, benign masses tend to have round, oval, lobular in shape and malignant masses are lobular or irregular in shape. Measuring regular and irregular shapes mathematically is found to be a difficult task, since there is no single measure to differentiate various shapes. In this paper, the malignant and benign masses present in mammogram are classified using Hue, Saturation and Value (HSV weight function based statistical measures. The weight function is robust against noise and captures the degree of gray content of the pixel. The statistical measures use gray weight value instead of gray pixel value to effectively discriminate masses. The 233 mammograms from the Digital Database for Screening Mammography (DDSM benchmark dataset have been used. The PASW data mining modeler has been used for constructing Neural Network for identifying importance of statistical measures. Based on the obtained important statistical measure, the C5.0 tree has been constructed with 60-40 data split. The experimental results are found to be encouraging. Also, the results will agree to the standard specified by the American College of Radiology-BIRADS Systems.

  19. Recent advances in thermal desorption-gas chromatography-mass spectrometery method to eliminate the matrix effect between air and water samples: application to the accurate determination of Henry's law constant.

    Kim, Yong-Hyun; Kim, Ki-Hyun

    2014-05-16

    Accurate values for the Henry's law constants are essential to describe the environmental dynamics of a solute, but substantial errors are recognized in many reported data due to practical difficulties in measuring solubility and/or vapor pressure. Despite such awareness, validation of experimental approaches has scarcely been made. An experimental approach based on thermal desorption-gas chromatography-mass spectrometery (TD-GC-MS) method was developed to concurrently allow the accurate determination of target compounds from the headspace and aqueous samples in closed equilibrated system. The analysis of six aromatics and eight non-aromatic oxygenates was then carried out in a static headspace mode. An estimation of the potential bias and mass balance (i.e., sum of mass measured individually from gas and liquid phases vs. the mass initially added to the system) demonstrates compound-specific phase dependency so that the best results are obtained by aqueous (less soluble aromatics) and headspace analysis (more soluble non-aromatics). Accordingly, we were able to point to the possible sources of biases in previous studies and provide the best estimates for the Henry's constants (Matm(-1)): benzene (0.17), toluene (0.15), p-xylene (0.13), m-xylene (0.13), o-xylene (0.19), styrene (0.27); propionaldehyde (9.26), butyraldehyde (6.19), isovaleraldehyde (2.14), n-valeraldehyde (3.98), methyl ethyl ketone (10.5), methyl isobutyl ketone (3.93), n-butyl acetate (2.41), and isobutyl alcohol (22.2). PMID:24704185

  20. Non-targeted screening for contaminants in paper and board food-contact materials using effect-directed analysis and accurate mass spectrometry.

    Bengtström, Linda; Rosenmai, Anna Kjerstine; Trier, Xenia; Jensen, Lisbeth Krüger; Granby, Kit; Vinggaard, Anne Marie; Driffield, Malcolm; Højslev Petersen, Jens

    2016-06-01

    Due to large knowledge gaps in chemical composition and toxicological data for substances involved, paper and board food-contact materials (P&B FCM) have been emerging as a FCM type of particular concern for consumer safety. This study describes the development of a step-by-step strategy, including extraction, high-performance liquid chromatography (HPLC) fractionation, tentative identification of relevant substances and in vitro testing of selected tentatively identified substances. As a case study, we used two fractions from a recycled pizza box sample which exhibited aryl hydrocarbon receptor (AhR) activity. These fractions were analysed by gas chromatography (GC) and ultra-HPLC (UHPLC) coupled to quadrupole time-of-flight mass spectrometers (QTOF MS) in order tentatively to identify substances. The elemental composition was determined for peaks above a threshold, and compared with entries in a commercial mass spectral library for GC-MS (GC-EI-QTOF MS) analysis and an in-house built library of accurate masses for substances known to be used in P&B packaging for UHPLC-QTOF analysis. Of 75 tentatively identified substances, 15 were initially selected for further testing in vitro; however, only seven were commercially available and subsequently tested in vitro and quantified. Of these seven, the identities of three pigments found in printing inks were confirmed by UHPLC tandem mass spectrometry (QqQ MS/MS). Two pigments had entries in the database, meaning that a material relevant accurate mass database can provide a fast tentative identification. Pure standards of the seven tentatively identified substances were tested in vitro but could not explain a significant proportion of the AhR-response in the extract. Targeted analyses of dioxins and PCBs, both well-known AhR agonists, was performed. However, the dioxins could explain approximately 3% of the activity observed in the pizza box extract indicating that some very AhR active substance(s) still remain to be