International Nuclear Information System (INIS)
Japanese (Jul 1976). Japan Kametani, Katsuaki Tomura, Kayoko . National
Standardisation of "2"1"0Pb by Cerenkov counting
International Nuclear Information System (INIS)
A standard of "2"1"0Pb in solution was produced at the National Physical Laboratory by a novel technique combining Cerenkov counting with the established liquid scintillation efficiency tracing technique known as the CIEMAT/NIST method. Coincidence counting was applied in order to validate the measurements and the activity concentrations of the solution determined with each technique are shown to be in agreement. Radiochemical separation of the "2"1"0Pb from its daughters was also necessary and the scheme for the separation is described. After performing this two-stage standardisation, the uncertainty was successfully lowered to 0.66% (k=1). This uncertainty is approximately a factor of four lower than previously achieved at NPL by the classical method of standardisation of radionuclides, i.e. coincidence counting.
2011-05-01
Isolation and determination of "9"0Sr, "2"2"6Ra, "2"2"8Ra and "2"1"0Pb in food
International Nuclear Information System (INIS)
A procedure is described for the isolation and determination of "9"0Sr, "2"2"6Ra, "2"2"8Ra and "2"1"0Pb in food. These nuclides are highly radiotoxic, above all for babies and children. Samples are dry ashed, alkali metals are removed as carbonates. Separation from other matrix ions and separation of Ra, Sr and Pb can be achieved with a column of Sr-Spec, an immobilized crown ether. For activity measurements membrane filters with SrSO_4, Ba(Ra)SO_4 and PbS are prepared. Ra is determined by gamma-spectrometry, "9"0Sr and "2"1"0Pb are determined by low-level-betacounting. The determination limits are 10 mBq/kg for "9"0Sr and "2"1"0Pb and 50 mBq/kg for "2"2"6Ra and "2"2"8Ra. The procedure is useful for all kinds of foodstuff. (orig.).
Energy Technology Data Exchange (ETDEWEB)
A procedure is described for the isolation and determination of {sup 90}Sr, {sup 226}Ra, {sup 228}Ra and {sup 210}Pb in food. These nuclides are highly radiotoxic, above all for babies and children. Samples are dry ashed, alkali metals are removed as carbonates. Separation from other matrix ions and separation of Ra, Sr and Pb can be achieved with a column of Sr-Spec, an immobilized crown ether. For activity measurements membrane filters with SrSO{sub 4}, Ba(Ra)SO{sub 4} and PbS are prepared. Ra is determined by gamma-spectrometry, {sup 90}Sr and {sup 210}Pb are determined by low-level-betacounting. The determination limits are 10 mBq/kg for {sup 90}Sr and {sup 210}Pb and 50 mBq/kg for {sup 226}Ra and {sup 228}Ra. The procedure is useful for all kinds of foodstuff. (orig.) [Deutsch] Es wird ein Analysengang zur Abtrennung und Bestimmung von {sup 90}Sr, {sup ...
1996-12-31
Alpha radiation sources in low alpha materials and implications for low alpha materials refinement
Energy Technology Data Exchange (ETDEWEB)
Traditionally wafer bumps are made from Pb containing solders. Over 20 years ago IBM recognized that {sup 210}Pb has a decay chain resulting in a 5.4 MeV alpha particle that induces soft errors. A variety of efforts to produce and characterize low alpha Pb ensued. Work at Honeywell over the past several years has shown that low alpha lead activity does not follow the decay signature predicted from {sup 210}Pb secular equilibrium. Data are presented indicating that smelting has a minimal effect on {sup 210}Pb/{sup 210}Po secular equilibrium and that other trace radionuclides are the alpha source. The implications of these data to possible alpha emitter sources in lead free solders are discussed, along with a method developed by Honeywell to remove alpha emitters from lead free solder components.
2004-09-01
International Nuclear Information System (INIS)
At two locations in southern Lake Huron (U.S.A.), twelve 35.5-cm diameter cores of fine-grained sediments were taken for comparison of the vertical distribution of "2"1"0Pb and fallout "1"3"7Cs with the distribution of benthic macroinvertebrates, mainly oligochaete worms (Tubificidae) and the amphipod, Pontoporeia affinis. Locations were selected on the basis of "2"1"0Pb distributions measured a year earlier which indicated contrasting depths of mixing of surface sediments. At one location the activity of "2"1"0Pb is uniform down to about 6 cm and 95% of total invertebrates occur within this zone; at the other location the zone of constant activity is only 3 cm deep but 90% of the invertebrates occur within it. Comparison of published tubificid defecation rates with sediment accumulation rates based on "2"1"0Pb shows that oligochaetes alone can account for mixing in one case while the effects of amphipods may be required in the case of shallower mixing. If mixing is represented as a ...
Environmental radioactivity on Suape (PE) estuary: impact of the installation of an oil refinery
Energy Technology Data Exchange (ETDEWEB)
Nowadays there is a growing interest in the study of natural radioactivity levels, mainly of radionuclides; {sup 238}U, {sup 226}Ra, {sup 232}Th, {sup 40}K, and {sup 210}Pb present in the environment. The environmental radioactivity control is very important to obtain information on exposure of humans and vegetables to potential sources on natural radioactive occurrences. Industrial processes involving mining and extraction and production of oil foster concentration of radionuclides, contributing to the occurrence of what is known as 'TENORM' - Technologically Enhanced Naturally Occurring Radioactive Material. This work aims to assess the environmental radiological impact on the estuarine area of the Industrial Park of SUAPE, due the installation of an oil refinery and the consequent introduction on the environment of natural radioactive materials from other regions in that area. The radioisotopes {sup 238}U, {sup 226}Ra, {sup ...
2009-07-01
British Library Electronic Table of Contents (United Kingdom)
The features of present deposits that form in the vicinity of hot springs can provide clues to the parameters of paleowaters in places of past hydrothermal activity marked by remnant carbonate and/or siliceous sinter. We investigated a large carbonate body at the Garga hot spring developing in the Baikal zone of nitric hydrotherms in the Barguzin Rift Zone valley. The main focus was on the structure of the carbonate mound, as well as on the partitioning of radioactive elements between the cyanobacterial mat and the inorganic component of the body (the issue that has never been explored before). The cyanobacterial community of the Garga spring is an active biosorbent of 226Ra, 228Ra, 210Pb. The radionuclides accumulated by biosorption become preserved in minerals that form within the bacter...
2011-01-01
Application of radiolead to metabolic studies
International Nuclear Information System (INIS)
A review is presented of the literature through 1977 on the uses of radioactive lead isotopes in metabolic studies in man, animals, and plants. These studies have been done mainly with the naturally-occurring, long-lived (22-yr half life) "2"1"0Pb, but a few were with 53-hr "2"0"3Pb or 10.6-hr "2"1"2Pb. Such studies have made possible estimates of the metabolic parameters of lead in man and animals, such as intestinal absorption, the ratio of fecal-to-urinary excretion of endogenous lead, residence time of lead in the body and in various organs, and the distribution in the body (skeleton, liver, kidney, and blood). Subsequently, these parameters and data have been used to trace the sources of lead for man, such as those from the atmosphere, food, cigarette smoke, and automobile exhaust.
11. Preparation of natural radioactive materials
International Nuclear Information System (INIS)
Uranium and thorium ores are the source of natural radionuclides. Briefly described are the original and current methods of long-lived nuclide separation ("2"3"8U, "2"3"5U, "2"2"6Ra, "2"3"0Th, "2"3"1Pa, "2"2"7Ac, "2"3"2Th, "2"2"8Ra+"2"2"8Ac, "2"2"8Th), some short-lived nuclides ("2"3"4Th and "2"2"8Ac), radon, short-lived radon daughter products and long-lived radon daughter products ("2"1"0Pb, "2"1"0Bi, "2"1"0Po). Some nuclides, such as "2"1"0Po or "2"3"1Pa can more easily be producedin reactors. (Ha).
Uncertainties of retrospective radon concentration measurements by multilayer surface trap detector
Energy Technology Data Exchange (ETDEWEB)
The detector for retrospective radon exposure measurements is developed. The detector consists of the multilayer package of solid-state nuclear track detectors LR-115 type. Nitrocellulose films works both as {alpha}-particle detector and as absorber decreasing the energy of {alpha}-particles. The uncertainties of implanted {sup 210}Pb measurements by two- and three-layer detectors are assessed in dependence on surface {sup 210}Po activity and gross background activity of the glass. The generalized compartment behavior model of radon decay products in the room atmosphere was developed and verified. It is shown that the most influencing parameters on the value of conversion coefficient from {sup 210}Po surface activity to average radon concentration are aerosol particles concentration, deposition velocity of unattached {sup 218}Po and air exchange rate. It is demonstrated that with the use of additional information on surface to volume room ...
2006-07-01
Radiotracer study of lead adsorption on glass from very dilute aqueous solutions
Energy Technology Data Exchange (ETDEWEB)
This study deals with the adsorption and desorption of lead (c <= 10/sup -8/ - 10/sup -3/ M), labelled with /sup 212/Pb or /sup 210/Pb, on glass in relation to pH and composition of the solution, concentration of lead and time. The prevailing mechanism of the adsorption in the pH range from 3 to 8 is the ion exchange of Pb/sup 2 +/ and PbOH/sup +/ ions in electric double layer on the surface of glass. At the higher pH values lead (c <= 10/sup -8/ - 10/sup -6/ M) is adsorbed mainly by physical adsorption or chemisorption of its hydrolyzed forms. A rather high adsorption capacity of glass, exceeding 3.10/sup -9/ M/cm/sup 2/, has been found in neutral solutions for the cationic forms of lead. The adsorbed lead can be easily desorbed with the solution of 1 M nitric acid.
1981-01-01
Contamination by depleted uranium (Du) in South Serbia
Energy Technology Data Exchange (ETDEWEB)
The paper present the results of the study on D.U. (depleted uranium) contamination in the environment and possible effects on animal healths in the region o f Bujanovac. Samples of soil, feed, leaves, grass, lichen, moss, honey and water were collected randomly in 2003/2004 in the vicinity of the target area (500-1000 m) and 5 km from the target area. Activity of the radionuclides ({sup 226}Ra, {sup 232}Th, {sup 40}K, {sup 210}Pb, {sup 238}U, {sup 235}U, {sup 137}Cs, {sup 7}Be) in soils, grass, lichen, moss and honey was determined on Hp Ge detector (Canberra, relative efficiency 23%) by standard gamma spectrometry. Total alpha and beta activity in water was determined on proportional alpha/beta counter (Canberra 2400, efficiency for alpha emitters 11%, efficiency for beta emitters 30%). Non significantly higher values of concentrations of {sup 226}Ra, {sup 232}Th, {sup 238}U and {sup 235}U were measured in the immediate vicinity of the ...
2006-07-01
Energy Technology Data Exchange (ETDEWEB)
According to ICRP 60 and European-Directive 96/29, Naturally Occurring Radioactive Materials (NORM) and Technical Enriched Naturally Occurring Radioactive Materials (TENORM) have to take the radiation protection of the general population as well as of workers into account. The German radiation protection regulations stress that particularly. In connection with these regulations, various measurement programs have been and still are performed to investigate the relevant exposure paths. One of these programs is the determination of the intake of natural occurring radionuclides of the uranium decay series in individuals of the public, in exposed regions and houses and also at NORM workplaces by excretion analysis. Excretion analysis surveillance is one of the common tools for internal dosimetry. Sources of primordial radionuclides could be the ingestion of foodstuff and water and the incorporation of (mostly airborne) pollution on work places. The main focus in this report is set upon the ...
2006-07-01
A review of 4 norm industries in Ireland
Energy Technology Data Exchange (ETDEWEB)
Full text: This presentation will review the progress achieved so far by the Irish national regulatory agency, the Radiological Protection Institut e of Ireland (R.P.I.I.) in the investigation of work activities where the presence of natural radiation sources (NORM) could lead to a significant increase in exposure to workers or members of the public which cannot be disregarded from the radiation protection point of view. Since the coming into force in Ma y 2000 of the Radiological Protection Act, 1991 (Ionising Radiation) Order, 2000 (S.I. No. 125 of 2000) which implements the Eu B.S.S. Directive 96/29/EURATOM, four major NORM industries currently active in Ireland have been investigated. According to the literature, they are all considered liable to involve work practices resulting in exposure to NORM. They include: the gas extraction and production industry, the peat- and coal-firing power generation industry and the bauxite/alumina refining industry. For the gas industry, monitoring ...
2006-07-01
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