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Calibración del separador magnético de alta intensidad magnet-lift mlh (13) 111-5 para su uso en el laboratorio de termocronología de la UCV/ Calibration of a high intensity magnet-lift mlh (13) 111-5 magnetic separator for use in the thermochronology laboratory of the UCV  

Abstract in spanish En este artículo se presenta la calibración del separador magnético de alta intensidad Magnet-lift MLH (13) 111-5 existente en el Laboratorio de Termocronología de la Universidad Central de Venezuela con la finalidad de separar magnéticamente minerales pertenecientes a areniscas y muestras graníticas para su posterior fechado por el método de huellas de fisión. Los resultados obtenidos de esta calibración fueron aplicados a una muestra de 10 kilogramos pertenecie (more) ntes a unaconcentración inicial de minerales de la Formación Betijoque del flanco norte de Los Andes Venezolanos. Se concluye que el Magnet-lift presenta amplias ventajas con respecto a los separadores magnéticos convencionales y además optimiza el tiempo de procesamiento de rocas detríticas que posteriormente serán fechadas por el método de datación empleado eneste laboratorio con el fin de discriminar la edad del último evento tecto-térmico ocurrido en la zona de estudio. Abstract in english In this article we present the calibration of a high intensity Magnet-lift MLH (13) 111-5 magnetic separator located in the Thermochronology Laboratory of the Universidad Central de Venezuela with the purpose of magnetically separating minerals of sandstone and granite samples to be subsequently subjected to the fission track dating method (FTDM). The results of this calibration were applied to 10 kilogram sample belonging to an initial concentration of minerals of Betijo (more) que´s Formation on the north flank of Venezuelans Andes. We conclude that the Magnet-lift presents a number of advantages with regard to conventional magnetic separators as well as optimizing the preparation time of detritic rocks for their dating by the fission track method.

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Magnetic separations: From steel plants to biotechnology  

Magnetic separations have for decades been essential processes in diverse industries ranging from steel production to coal desulfurization. In such settings magnetic fields are used in continuous flow processes as filters to remove magnetic impurities. High gradient magnetic separation (HGMS) has found even broader use in wastewater treatment and food processing. Batch scale magnetic separations are also relevant in industry, particularly biotechnology where fixed magnetic separators are used to purify complex mixtures for protein isolation, cell separation, drug delivery, and biocatalysis. In this review, we introduce the basic concepts behind magnetic separations and summarize a few examples of its large scale application. HGMS systems and batch systems for magnetic separations have been...

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Scalable Magnetic Designs to Achieve Comparable Capture Rates and Capture Efficiency across Multiple Vessel Diameters  

Open gradient magnetic separators utilizing strong permanent magnets are used during a variety of magnetic carrier-based purification and bead coating processes such as protein separations, nucleic acid isolations, and immunodiagnostics. These purification and bead coating processes are often developed on a small, experimental scale before transfer to a functional process scale for use in industrial and manufacturing settings. Accordingly, the strong magnets used for magnetic carrier separation must be scaled to prevent process variation between batch size due to inadequate wash efficiency and discrepant capture times. Magnetic separator scalability may be defined as the consistent capture of magnetic particles as measured by capture time and capture efficiency (>99%) independent of collection vessel diameter. A mathematical relationship between the average magnetic field magnitude and the cross sectional vessel area has been devised for magnetic separators with magnets arranged in quadrature geometry. Using this correlation, the magnet thickness and material for each magnetic separator may be tailored to create the magnetic field strength and gradient required to achieve comparable capture times across different vessel diameters. Accordingly, four magnetic separators ranging in size from 0.125L to 1L were examined and demonstrated equivalent capture times of >99% microparticle capture at 60 seconds for phosphate buffered saline solutions containing 1% solids using Dynabead M-270 carboxylic acid microparticles. In addition, a 5L magnetic separator is also discussed. Magnetic scaling relationships and additional experimental outcomes using magnetic microparticles are described herein for the scaled magnetic separators.

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A feasibility study of magnetic separation of magnetic nanoparticle for forward osmosis.  

It was recently reported that a UK company has developed a naturally non-toxic magnetoferritin to act as a draw solute for drawing water in forward osmosis process. The gist of this technology is the utilization of the magnetic nanoparticle and high-gradient magnetic separation for draw solute separation and reuse. However, any demonstration on this technology has not been reported yet. In this study, a feasibility test of magnetic separation using magnetic nanoparticle was therefore performed to investigate the possibility of magnetic separation in water treatment such as desalination. Basically, a magnetic separation system consisted of a column packed with a bed of magnetically susceptible wools placed between the poles of electromagnet and Fe3O4 magnetic nanoparticle was used as a model nanoparticle. The effect of nanoparticle size to applied magnetic field in separation column was experimentally investigated and the magnetic field distribution in a magnet gap and the magnetic field gradient around stainless steel wool wire were analyzed through numerical simulation. The amount of magnetic nanoparticle captured in the separator column increased as the magnetic field strength and particle size increased. As a result, if magnetic separation is intended to be used for draw solute separation and reuse, both novel nanoparticle and large-scale high performance magnetic separator must be developed. PMID:22097022

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Magnetic separator for chimney dust  

A magnetic separator for separation of magnetic powder (iron trioxide ?-Fe2O3) from the chimney dust of a coal-fired power station is presented. The principle of the new version of separator is based on an iron screw-shaft with square thread which rotates in a dc magnetic field. Design, principle of operation and test results carried out on the magnetic separator are the subjects of the paper.

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Design and test of a 7 T split-pair magnet for magnetic separation  

A 160 mm bore, 7 T split-pair magnet was constructed and tested aiming to mineral processing through HGMS (high gradient magnetic separation) or HCMS (helical channel magnetic separation). This work describes the design and test results of the pair of coils operating under current in parallel mode. In the case of antiparallel current mode large repulsive force between coils is generated and a strong magnetic field gradient outside the magnet is created. A continuous magnetic separation system made with a helical channel magnetic separator for application in TiO2 processing is analyzed.

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Magnetic separation of antibiotics by electrochemical magnetic seeding  

Magnetic separation of several classes of antibiotics was investigated using electrochemical magnetic seeding. Electrocoagulation with a sacrificial anode followed by addition of magnetite particles was applied for the magnetic seeding of antibiotics. With electrochemical magnetic seeding using an iron anode, tetracycline antibiotics (oxytetracycline, chlortetracycline, doxycycline and tetracycline) and cephalosporin antibiotic (cefdinir) were rapidly removed from synthetic wastewater by magnetic separation using a neodymium magnet. Iron and aluminium anodes were suitable for magnetic seeding of the antibiotics. The results indicated that the ability of antibiotics to form strong complex with iron and aluminium allowed the higher removal by magnetic separation. This method would be appropriate for rapid treatment of antibiotics in wastewater.

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Magnetic design considerations for devices and particles used for biological high-gradient magnetic separation (HGMS) systems  

An overview of the magnetic systems used in biological high-gradient magnetic separation (HGMS) is presented. The magnetic design parameters of a range of separation devices are discussed. Such designs have distinct magnetic field characteristics and are usually tailored to meet the needs of particular protocols. The various types of magnets and particles are also discussed, with a comparison of materials available and their magnetic properties.

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Ordered magnetic microdroplets array on magnetic films  

With the development of magnetic droplet-based biochips, the manipulation of magnetic droplets has become an important issue. In this study, deposited magnetic circular films are used to assist the positioning of magnetic microdroplets, which are separated from a mother droplet caused by the Rosensweig instability under a magnetic field. Magnetic microdroplets are attracted by the concentrated magnetic flux density caused by out-of-plane magnetization of the magnetic films, and magnetic films confine the positions of droplets. Through adjusting the applied field strength, droplet arrays with different number densities can be obtained. One-to-one correspondences between droplets and magnetic films can be achieved within specific magnetic field ranges.

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Passive magnetic separator integrated with microfluidic mixer: Demonstration of enhanced capture efficiency  

In this paper, we present two results: (1) a new method for quantifying the efficiency of magnetic bead separators by magnetic measurements, and (2) a new idea for designing efficient magnetic bead separators. For microfluidic magnetic separators, a limiting factor for the capture of magnetic beads is the steep decrease of the magnetic force on the beads as a function of their distance to the magnetic structures. Our idea is to integrate the magnetic separator with a microfluidic mixer to ensure that all beads are brought close to the magnetic structures. We have fabricated a magnetic separator consisting of permalloy elements adjacent to a microfluidic channel. The performance of a system with an integrated surface structured (staggered herringbone) microfluidic mixer is compared to that of an equivalent system without the mixer. It is quantitatively demonstrated that the mixer significantly enhances the bead capture-and-release efficiency.

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MSWI boiler fly ashes: Magnetic separation for material recovery  

Nowadays, ferrous materials are usually recovered from Municipal Solid Waste Incineration (MSWI) bottom ash by magnetic separation. To our knowledge, such a physical technique has not been applied so far to other MSWI residues. This study focuses thus on the applicability of magnetic separation on boiler fly ashes (BFA). Different types of magnet are used to extract the magnetic particles. We investigate the magnetic particle composition, as well as their leaching behaviour (EN 12457-1 leaching test). The magnetic particles present higher Cr, Fe, Mn and Ni concentration than the non-magnetic (NM) fraction. Magnetic separation does not improve the leachability of the NM fraction. To approximate industrial conditions, magnetic separation is also applied to BFA mixed with water by using a pil...

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Magnetic particle dosing and size separation in a microfluidic channel  

Separation of functional magnetic particles or magnetically labeled entities is a key feature for bioanalytical or biomedical applications and therefore also an important component of lab-on-a-chip devices for biological applications. We present a novel integrated microfluidic magnetic bead manipulation device, comprising dosing of magnetic particles, controlled release and subsequent magnetophoretic size separation with high resolution. The system is designed to meet the requirements of specific bioassays, in particular of on-chip agglutination assays for the detection of rare analytes by particle coupling as doublets. Integrated soft-magnetic microtips with different shapes provide the magnetic driving force of the bead manipulation protocol. The magnetic tips that serve as field concent...

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Study on the separation and utilization technology of magnetic bead in fly ash  

This paper describes three methods of separating the magnetic beads within fly ash from the ash itself, using the physical and chemical properties of the beads. Tests were performed on size, density, stability, magnetic material content, specific magnetic susceptibility, medium recovery oxidation resistance, and wear resistance of the magnetic beads from fly ash, in comparison with the magnetic fines currently used in dense media separation. It was shown that magnetic beads from fly ash may substitute for the magnetic fines currently used. 3 refs., 16 tabs.

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Recovery Improvement of Fine Magnetic Particles by Floc Magnetic Separation  

The performance of floc magnetic separation (FMS) has been compared with wet high-intensity magnetic separator (WHIMS). This study was performed on low-grade iron ore slime contained 59.58% Fe with 4.57% silica and 3.78% alumina. Detailed characterization data indicated that a substantial amount of the slime was below 20 µm in size. Beneficiation studies indicated that the FMS process is effective to recover fine hematite and goethite particles, compared with the conventional magnetic separation. In conventional magnetic separation, the extent of the fluid drag force exceeds the magnetic force exerted on ultrafine particles. Thus, ultrafine magnetic particles were usually not recovered effectively by magnetic separators, resulting in the loss of valuable ultrafine slime particles...

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Thick film magnetic nanoparticulate composites and method of manufacture thereof  

Thick film magnetic/insulating nanocomposite materials, with significantly reduced core loss, and their manufacture are described. The insulator coated magnetic nanocomposite comprises one or more magnetic components, and an insulating component. The magnetic component comprises nanometer scale particles (about 1 to about 100 nanometers) coated by a thin-layered insulating phase. While the intergrain interaction between the immediate neighboring magnetic nanoparticles separated by the insulating phase provides the desired soft magnetic properties, the insulating material provides high resistivity, which reduces eddy current loss.

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Bioassay and biomolecular identification, sorting, and collection methods using magnetic microspheres  

The present invention is directed to processes of separating, analyzing and/or collecting selected species within a target sample by use of magnetic microspheres including magnetic particles, the magnetic microspheres adapted for attachment to a receptor agent that can subsequently bind to selected species within the target sample. The magnetic microspheres can be sorted into a number of distinct populations, each population with a specific range of magnetic moments and different receptor agents can be attached to each distinct population of magnetic microsphere.

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Study on magnetic separation system using high Tc superconducting bulk magnets for water purification technique  

The application of superconducting bulk magnets to the magnetic separation techniques has been investigated for the Mn-bearing waste water drained from the university laboratories. The research has been conducted in comparison with the electromagnets, and the cryo-cooled superconducting solenoid magnet. The separation ratios of ferrite precipitates including Mn element in the waste slurry were estimated by means of the high gradient magnetic separation method with ferromagnetic iron filters in the water channel and open gradient magnetic separation without them. As the magnetic force acting on the particles is given by the product of a magnetization of particles and a gradient of magnetic field, and a superconducting bulk magnet shows a sharp gradient of the magnetic field on the surface, the performances of the bulk magnet system were almost equivalent to those of the superconducting solenoid magnet with wide bore with respect to the magnetic separation ratios. The separation ratios for Mn have reached over 80 % for HGMS and 10 % for OGMS under the flow rates less than 3 liter/min.

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MSWI boiler fly ashes: magnetic separation for material recovery.  

Nowadays, ferrous materials are usually recovered from Municipal Solid Waste Incineration (MSWI) bottom ash by magnetic separation. To our knowledge, such a physical technique has not been applied so far to other MSWI residues. This study focuses thus on the applicability of magnetic separation on boiler fly ashes (BFA). Different types of magnet are used to extract the magnetic particles. We investigate the magnetic particle composition, as well as their leaching behaviour (EN 12457-1 leaching test). The magnetic particles present higher Cr, Fe, Mn and Ni concentration than the non-magnetic (NM) fraction. Magnetic separation does not improve the leachability of the NM fraction. To approximate industrial conditions, magnetic separation is also applied to BFA mixed with water by using a pilot. BFA magnetic separation is economically evaluated. This study globally shows that it is possible to extract some magnetic particles from MSWI boiler fly ashes. However, the magnetic particles only represent from 23 to 120 g/kg of the BFA and, though they are enriched in Fe, are composed of similar elements to the raw ashes. The industrial application of magnetic separation would only be profitable if large amounts of ashes were treated (more than 15 kt/y), and the process should be ideally completed by other recovery methods or advanced treatments. PMID:21306886

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Magnetic separation in microfluidic systems  

This Ph.D. thesis presents theory, modeling, design, fabrication, experiments and results for microfluidic magnetic separators. A model for magnetic bead movement in a microfluidic channel is presented, and the limits of the model are discussed. The effective magnetic field gradient is defined, and it is argued that it is a good measure, when comparing the performance of magnetic bead separators. It is described how numeric modelling is used to aid the design of microfluidic magnetic separation systems. An example of a design optimization study is given. A robust fabrication scheme has been developed for fabrication of silicon based systems. This fabrication scheme is explained, and it is shown how, it is applied with variations for several designs of magnetic separators. An experimental setup for magnetic separation experiments has been developed. It has been coupled with an image analysis program to facilitate real-time monitoring of the experiments. The set-up and experimental protocol are described in detail. Results are presented for ’active’ magnetic bead separators, where on-chip microfabricated electromagnets supply the magnetic field and field gradients necessary for magnetic bead separation. It is shown conceptually how such a system can be applied for parallel biochemical processing in a microfluidic system. ’Passive’ magnetic separators are presented, where on-chip soft magnetic elements are magnetized by an external magnetic field and create strong magnetic fields and gradients inside a microfluidic channel. Systems with the elements placed beside the microfluidic channel is combined with hydrodynamic focusing to demonstrate a magnetic bead microarray inside a microfluidic channel. Systems where the on-chip magnetic material is placed underneath the microfluidic channel are also presented. One of these designs feature multiple magnetic length scales, and it is shown that this enhances bead capture ability. A ’hybrid’ magnetic separator design, where the magnetic field from on-chip current lines couples with an externally applied homogenous field to create strong fields and gradients is demonstrated. This gives extra magnetic bead manipulation possibilities compared to the passive designs. It is demonstrated how this can be used for magnetic bead microarrays. Finally, it is discussed, based on the research presented in this thesis, how to further develop magnetic separation systems in microfluidic systems, and recommendations are given for the choice of magnetic design based on the desired application.

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Large Scale Magnetic Separation of Solanum tuberosum Tuber Lectin from Potato Starch Waste Water  

A simple procedure for large scale isolation of Solanum tuberosum tuber lectin from potato starch industry waste water has been developed. The procedure employed magnetic chitosan microparticles as an affinity adsorbent. Magnetic separation was performed in a flow-through magnetic separation system. The adsorbed lectin was eluted with glycine/HCl buffer, pH 2.2. The specific activity of separated lectin increased approximately 27 times during the isolation process.

 
 
 
 
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Design of new heterobifunctional linkers for the covalent binding of biomolecules onto superparamagnetic iron oxide nanoparticles (spions)  

Superparamagnetic Iron Oxide Nanoparticles (SPIONs) are attractive because of some peculiar properties such as selective separation of biomolecules and cells, automated DNA extraction, targeted gene delivery, use as magnetic resonance contrast agent (MRI), and magnetic field induced hyperthermia for...

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by Thomas Je Kuczkowski and Donald He Buckley Cleveland, Ohio  

Gallium is extremely corrosive and forms alloys with most common bearing. 1 ... in an inert environment (argon or vacuum) of binary or ternary systems so ... chamber is mounted a 20-pole magnet, which is separated from a similar magnet ...

23

Ring magnets for the synchrotron x-ray source at ANL  

The designs of the bending, focusing, and correction magnetic for the storage ring are described. The computer-optimized pole-tip contours of the dipole, quadrupole, and sextupole magnets and the construction and assembly techniques keep the field errors within the specified limits. Horizontal and vertical steering corrections are provided by separate magnets in addition to a steering capability included in the sextupole magnets.

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SUPERCONDUCTING MAGNET FOR 60 TONNE/HOUR MINERAL SEPARATOR WITH CLOSED CYCLE 4 KELVIN REFRIGERATION  

Cryogenic Consultants Limited has constructed a superconducting magnet system for magnetic separation, with a three metre long dipole magnet cooled by a closed-cycle refrigerator. This paper considers the design and construction of the magnet system in relation to a theoretical expression for proces...

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A SQUID NDE system for the investigation of pinch welds.  

We present preliminary results for a magnetic flow spectrometer for magnetic microparticle separation, and a magnetic flow cytometer for particle identification. The application of the instrument is to high-throughput bioassay. Here we report on the first application of our magnetic spectrometer to the sorting of ferromagnetic and superparamagnetic microspheres in flow. The system is based on a permanent magnet quadrupole and separates the polymer coated magnetic microspheres based on their magnetic moments. The cryogenic section of our magnetic flow cytometer, which involves SQUID-based detection of the sorted magnetic microspheres based on their magnetic moments, has been re-engineered to permit a smaller standoff between the SQUID array and the flowing magnetic particles. We present preliminary results with the new experimental setup, with an emphasis on both spatial and signal resolution.

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SQUID-Based Bioassay with Magnetic Particles in Flow  

We present preliminary results for a magnetic flow spectrometer for magnetic microparticle separation, and a magnetic flow cytometer for particle identification. The application of the instrument is to high-throughput bioassay. Here we report on the first application of our magnetic spectrometer to the sorting of ferromagnetic and superparamagnetic microspheres in flow. The system is based on a permanent magnet quadrupole and separates the polymer coated magnetic microspheres based on their magnetic moments. The cryogenic section of our magnetic flow cytometer, which involves SQUID-based detection of the sorted magnetic microspheres based on their magnetic moments, has been re-engineered to permit a smaller standoff between the SQUID array and the flowing magnetic particles. We present preliminary results with the new experimental setup, with an emphasis on both spatial and signal resolution.

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The use of a linear Halbach array combined with a step-SPLITT channel for continuous sorting of magnetic species  

The Quadrupole Magnetic Sorter (QMS), employing an annular flow channel concentric with the aperture of a quadrupole magnet, is well established for cell and particle separations. Here we propose a magnetic particle separator comprising a linear array of cylindrical magnets, analogous to the array proposed by Klaus Halbach, mated to a substantially improved form of a parallel plate SPLITT channel, known as the step-SPLITT channel. While the magnetic force and throughput are generally lower than for the QMS, the new separator has advantages in ease of fabrication and the ability to vary the magnetic force to suit the separands. Preliminary experiments yield results consistent with prediction and show promise regarding future separations of cells of biomedical interest. - Research highlights: Novel pairing of an adapted linear Halbach magnet array and step-SPLITT channel is carried out. Unlike QMS, it allows variation in mean magnetic force as well as the gravity component. The magnetic force is easily controlled by varying the channel-magnet distance. Magnetic particle separations behave predictably when varying the flow rate and distance. Separations match prediction with good enrichment of magnetic particles in mixture.

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Application of high temperature superconductors to high-gradient magnetic separation  

High Gradient Magnetic Separation (HGMS) is a powerful technique which can be used to separate widely dispersed contaminants from a host material, This technology can separate magnetic solids from other solids, liquids or gases. As the name implies HGMS uses large magnetic field gradients to separate ferromagnetic and paramagnetic particles. HGMS separators usually consist of a high-field solenoid magnet, the bore of which contains a fine-structured, ferromagnetic matrix material. The matrix material locally distorts the magnetic field and creates large field gradients in the vicinity of the matrix elements. These elements then become trapping sites for magnetic particles and are the basis for the magnetic separation. In this paper we discuss the design and construction of a prototype HGMS unit using a magnet made with high temperature superconductors (HTS). The prototype consists of an outer vacuum vessel which contains the HTS solenoid magnet The magnet is surrounded by a thermal radiation shield and multilayer insulation (MLI) blankets. The magnet, thermal shield and current leads all operate in a vacuum and are cooled by a cryocooler. High temperature superconducting current leads are used to reduce the heat leak from the ambient environment to the HTS magnet.

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Superconducting open-gradient magnetic separation for the pretreatment of radioactive or mixed waste vitrification feeds. 1998 annual progress report  

'The objective is to reduce the volume and cost of high-level waste glass produced during US DOE remediation activities by demonstrating that magnetic separation can separate crystalline, amorphous, and colloidal constituents in vitrification feed streams known to be deleterious to the production of borosilicate glass. Magnetic separation will add neither chemicals nor generate secondary waste streams. The project includes the systematic study of magnetic interactions of waste constituents under controlled physical and chemical conditions (e.g., hydration, oxidation, temperature) to identify mechanisms that control the magnetic properties. Partitioning of radionuclides to determine their sorption mechanisms is also being studied. The identification of fundamental magnetic properties within the microscopic chemical environment in combination with hydrodynamic and electrodynamic models provides insights into the design of a system for optimal separation. Following this, experimental studies using superconducting open-gradient magnetic separation (OGMS) will be conducted to validate its effectiveness as a pretreatment technique.'

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High performance hybrid magnetic structure for biotechnology applications  

The present disclosure provides a high performance hybrid magnetic structure made from a combination of permanent magnets and ferromagnetic pole materials which are assembled in a predetermined array. The hybrid magnetic structure provides means for separation and other biotechnology applications involving holding, manipulation, or separation of magnetic or magnetizable molecular structures and targets. Also disclosed are further improvements to aspects of the hybrid magnetic structure, including additional elements and for adapting the use of the hybrid magnetic structure for use in biotechnology and high throughput processes.

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Particle flocculation and filtration by high-gradient magnetic fields  

Flocculation and filtration of micrometer-sized particles in a high-gradient magnetic field (HGMF) were investigated. Experiments were conducted using a cryogenic magnet of 6 Tesla maximum strength. Hematite particles were used for flocculation and filtration experiments. A new approach of using magnetic fields to enhance separation of weakly magnetic particles was also investigated. This approach is based on magnetic seeding which involves flocculation of existing non-magnetic particles with injected paramagnetic particles. A particle-flocculation model was developed based on trajectory analysis. External forces due to gravity and magnetism, and interparticle forces such as electrostatic, hydrodynamic, magnetic dipole, and van der Waals forces, were taken into consideration in these models.

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Enhancements of Spin and Orbital Magnetic Moments of Submonolayer Co on Cu(001) Studied by X-ray Magnetic Circular Dichroism Using Superconducting Magnet and Liquid He Cryostat  

Magnetic properties of 0.4 monolayer Co grown epitaxially on Cu(001) were investigated by X-ray magnetic circular dichroism (XMCD) using our newly constructed ultrahigh vacuum system equipped with a 7 T superconducting magnet and a liquid He cryostat. The angle-dependent XMCD spectra for the saturated magnetization recorded at 6.0 K allowed us to evaluate separately the spin and orbital magnetic moments along the surface parallel and normal directions. Enhancements of the magnetic moments compared with the corresponding bulk values were clearly elucidated: ?15% for the spin magnetic moment and ?96 and ?53% for the orbital magnetic moments along the surface parallel and normal directions, respectively.   

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Enhancement of separation efficiency on continuous magnetophoresis by utilizing L/T-shaped microchannels  

In this article a novel design of on-chip continuous magnetophoretic separator was proposed by utilizing the magnetic field and L-turning/T-junction effect of the flow field for high throughput applications. The motion of the magnetic bead was simulated based on Lagrangian tracking method and the separation efficiency was calculated according to the trajectories. Impact parameters including geometrical configuration, fluid velocity, magnetic flux density, magnetic bead size, and temperature on separation efficiency were discussed. The results show that both the L- and T-microchannel separators have higher separation efficiency as compared with the conventional straight-microchannel separator because of the L-turning/T-junction effect of the flow field. The separation efficiencies for L- an...

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Magnetic field analysis of high gradient magnetic separator via finite element analysis  

High Gradient Magnetic Separator (HGMS) uses matrix to make high magnetic field gradient so that ferro- or para-magnetic particles can be attracted to them by high magnetic force. The magnetic force generated by the field gradient is several thousand times larger than that by the magnetic flux density alone. So the HGMS shows excellent performance compared with other magnetic separators. These matrices are usually composed of stainless wires having high magnetization characteristics. This paper deals with superconducting HGMS which is aimed for purifying wastewater by using stainless steel matrix. Background magnetic field up to 6T is generated by a superconducting solenoid and the stainless steel matrices are arranged inside of the solenoid. In order to calculate magnetic forces exerting ...

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The Recovery of Electrode Compounds from Waste Nickel Metal Hydride Batteries by Physical Separation Techniques  

A recovery method for electrode compounds from waste nickel metal hydride batteries by physical separation using sizing and distance-variable magnetic separation was investigated. The electrodes are formed by bonding substances of substrate and fine activating agents. Fine particle separation causes increasing costs and decreasing separation efficiency, suggesting a treatment flow where the separation of the anodic compounds from the cathodic compounds is carried out first and then each compound is crushed again for the liberation of activating agents and substrate. There is no suitable magnetic separation equipment to separate ferromagnetic substances using the magnetic property differences in the substrate components and special equipment to achieve this was developed. Using this newly developed equipment resulted in good separation.   

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Clean Up This Mess  

Students are challenged to design a method for separating steel from aluminum based on magnetic properties as is frequently done in recycling operations. To complicate the challenge, the magnet used to separate the steel must be able to be switched off to allow for the recollection of the steel. Students must ultimately design, test, and present an effective electromagnet.

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A Facile Route to Mesoporous Carbon Catalyst Support Modified with Magnetic Nanoparticles  

Magnetically separable ordered mesoporous carbon with Fe3O4 nanoparticles, which were grafted on the outer surface of the mesoporous carbon material CMK-3, was prepared through a facile route. The catalytic performance for hydrogenation of cyclohexene to cyclohexane validates the mesoporous nanocomposite material as a promising magnetically separable catalyst support.   

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Magnetic separation in microfluidic systems using microfabricated electromagnets - Experiments and simulations  

We present experiments and simulations of magnetic separation of magnetic beads in a microfluidic channel. The separation is obtained by microfabricated electromagnets. The results of our simulations using FEMLAB and Mathematica are compared with experimental results obtained using our own microfabricated systems. (c) 2005 Elsevier B.V. All rights reserved.

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High gradient magnetic separation applied to environmental remediation  

High Gradient Magnetic Separation (HGMS) is an application of superconducting magnet technology to the separation of magnetic solids from other solids, liquids, or gases. The production of both high magnetic fields (>4 T) and large field gradients using superconducting magnet technology has made it possible to separate a previously unreachable but large family of paramagnetic materials. This is a powerful technique that can be used to separate widely dispersed contaminants from a host material and may be the only technique available for separating material in the colloidal state. Because it is a physical separation process, no additional waste is generated. We are applying this technology to the treatment of radioactive wastes for environmental remediation. We have conducted tests examining slurries containing nonradioactive, magnetic surrogates. Results from these studies were used to verify our analytical model of the separation process. The model describes the rate process for magnetic separation and is based on a force balance on the paramagnetic species. This model was used to support bench scale experiments and prototype separator design.

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75 FR 28780 - Trade Adjustment Assistance for Farmers  

...Service Trade Adjustment Assistance for Farmers AGENCY: Foreign Agricultural Service...Trade Adjustment Assistance (TAA) for Farmers petitions for Fiscal Year 2011. Petitioners...L. 111-5) reauthorized the TAA for Farmers Program as established by Subtitle C...

 
 
 
 
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Separations technologies  

Separations is a critical element of any pollution prevention technology portfolio because of its applicability to a broad set of problems. The range of technologies included in separations is diverse and ranges from chemical engineering unit operations such as distillation and extraction to gas separation via adsorption and membranes to solids separations via classifiers and magnetic fields. The discussions in this chapter focus on separations technologies as used in pollution prevention.

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Magnetic separation for soil decontamination  

High gradient magnetic separation (HGMS) is a physical separation process that is used to extract magnetic particles from mixtures. The technology is used on a large scale in the kaolin clay industry to whiten or brighten kaolin clay and increase its value. Because all uranium and plutonium compounds are slightly magnetic, HGMS can be used to separate these contaminants from non-magnetic soils. A Cooperative Research and Development Agreement (CRADA) was signed in 1992 between Los Alamos National Laboratory (LANL) and Lockheed Environmental Systems and Technologies Company (LESAT) to develop HGMS for soil decontamination. This paper reports progress and describes the HGMS technology.

43

Magnetic separation for soil decontamination  

High gradient magnetic separation (HGMS) is a physical separation process that is used to extract magnetic particles from mixtures. The technology is used on a large scale in the kaolin clay industry to whiten or brighten kaolin clay and increase its value. Because all uranium and plutonium compounds are slightly magnetic, HGMS can be used to separate these contaminants from non-magnetic soils. A Cooperative Research and Development Agreement (CRADA) was signed in 1992 between Los Alamos National Laboratory (LANL) and Lockheed Environmental Systems and Technologies Company (LESAT) to develop HGMS for soil decontamination. This paper reports progress and describes the HGMS technology.

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Magnetic field analysis of high gradient magnetic separator via finite element analysis  

High Gradient Magnetic Separator (HGMS) uses matrix to make high magnetic field gradient so that ferro- or para-magnetic particles can be attracted to them by high magnetic force. The magnetic force generated by the field gradient is several thousand times larger than that by the magnetic flux density alone. So the HGMS shows excellent performance compared with other magnetic separators. These matrices are usually composed of stainless wires having high magnetization characteristics. This paper deals with superconducting HGMS which is aimed for purifying wastewater by using stainless steel matrix. Background magnetic field up to 6 T is generated by a superconducting solenoid and the stainless steel matrices are arranged inside of the solenoid. In order to calculate magnetic forces exerting on magnetic particles in wastewater, it is important to calculate magnetic field and magnetic field gradient those are proportional to the magnetic force acting on the particle. So we presents magnetic field distribution analysis result and estimates how many times of magnetic force will act on a particle when the matrix are arranged or not. Magnetic field is calculated in 3 dimensions by using Finite Element Method (FEM) and also compared with results obtained from 2 dimensional analysis.

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Harvesting fresh water and marine algae by magnetic separation: screening of separation parameters and high gradient magnetic filtration.  

In this study, the focus is on magnetic separation of fresh water algae Chlamydomonas reinhardtii and Chlorella vulgaris as well as marine algae Phaeodactylum tricornutum and Nannochloropsis salina by means of silica-coated magnetic particles. Due to their small size and low biomass concentrations, harvesting algae by conventional methods is often inefficient and cost-consuming. Magnetic separation is a powerful tool to capture algae by adsorption to submicron-sized magnetic particles. Hereby, separation efficiency depends on parameters such as particle concentration, pH and medium composition. Separation efficiencies of >95% were obtained for all algae while maximum particle loads of 30 and 77 g/g were measured for C. reinhardtii and P. tricornutum at pH 8 and 12, respectively. This study highlights the potential of silica-coated magnetic particles for the removal of fresh water and marine algae by high gradient magnetic filtration and provides critical discussion on future improvements. PMID:22705536

46

Element distribution of high iron-bearing zinc calcine in high gradient magnetic field  

High gradient magnetic separation was conducted in order to separate insoluble zinc ferrite from zinc calcine before acid leaching of hydrometallurgical process. Chemical composition and structural characterization of zinc calcine were studied via inductively coupled plasma (ICP), X-ray diffraction (XRD), Mossbauer spectra, scanning electron microscopy (SEM) and laser particle analysis (LPA). The parameters of magnetic separation which affect the distribution of zinc ferrite and undesired elements, such as calcium, sulfur and lead in magnetic concentrate were investigated. The results of high gradient magnetic separation indicate that more than 85% of zinc ferrite is distributed into magnetic concentrate from the zinc calcine under the magnetic induction of 0.70 T. In addition, about 60% o...

47

Theoretical analysis of a new, efficient microfluidic magnetic bead separator based on magnetic structures on multiple length scales  

We present a theoretical analysis of a new design for microfluidic magnetic bead separation. It combines an external array of mm-sized permanent magnets with magnetization directions alternating between up and down with mu m-sized soft magnetic structures integrated in the bottom of the separation channel. The concept is studied analytically for simple representative geometries and by numerical simulation of an experimentally realistic system geometry. The array of permanent magnets provides long-range magnetic forces that attract the beads to the channel bottom, while the soft magnetic elements provide strong local retaining forces that prevent captured beads from being torn loose by the fluid drag. The addition of the soft magnetic elements increases the maximum retaining force by two orders of magnitude. The design is scalable and provides an efficient and simple solution to the capture of large amounts of magnetic beads on a microsystem platform.

48

Science in Focus: Force in Motion: Workshop 6: "Force Against Force"  

Magnets stick to other magnets and to metal objects made of iron or steel. How much force is required to break the attraction between two magnets? In this workshop, fourth-grade students explore ways to balance the force of magnetism against the force of gravity. A magnet placed in a cup on one side of a pan-balance is stuck to a stationary magnet beneath the cup. When enough washers are placed on the opposite side of the balance, the magnets will separate. Graphical analysis shows some unexpected results.

49

Simultaneous, single particle, magnetization and size measurements of micron sized, magnetic particles  

Single particle magnetization and size measurements of micron and nano sized, magnetic particles were made using a previously described device referred to as Cell Tracking Velocimetry (CTV). Three types of commercially available, and commonly used, magnetic particles were studied in this report. While the CTV instrument provides individual particles measurements, the average magnetization and size measurements were found to have reasonable agreements with reported values from instruments which measure bulk values. In addition, the CTV instrument, using electromagnets, can also determine magnetization curves, which also proved to have reasonable agreement with other published studies. Given that magnetic separation and analysis technology is dependent on the quality of the magnetic particle...

50

Magnetic properties of greigite in the Late Pleistocene sediments of the North Caspian  

The results of magnetic and X-ray studies of the magnetic extracts separated from highly magnetically susceptible horizons of the Late Pleistocene sediments from the North Caspian Basin are presented. Greigite is shown to be the major carrier of magnetic properties in these horizons. Its coercive parameters are characteristic of the predominantly single-domain state of magnetic grains. It is found that the Curie point of greigite is at least 460°C, while the specific magnetization of pure greigite is half the saturation magnetization of magnetite.

51

Freely oriented portable superconducting magnet  

A freely oriented portable superconducting magnet is disclosed. Coolant is supplied to the superconducting magnet from a repository separate from the magnet, enabling portability of the magnet. A plurality of support assemblies structurally anchor and thermally isolate the magnet within a thermal shield. A plurality of support assemblies structurally anchor and thermally isolate the thermal shield within a vacuum vessel. The support assemblies restrain movement of the magnet resulting from energizing and cooldown, as well as from changes in orientation, enabling the magnet to be freely orientable.

52

Energy losses in superconductive DC-electromagnets due to ferromagnetic movement  

A DC-current, superconductive electromagnet is a source of the magnetic field in a separator matrix. This type of separator operates in a cyclic way. Therefore, it appears as very important to ensure the electromagnet stability during operation, i.e., range of parameters` changes that could maintain the magnet winding in the superconductive state. This means selecting parameter changes representing the magnet winding in the superconductive state.

53

Magnetic solids in analytical chemistry: a review.  

Magnetic solids are widely used in detection and analytical systems because of the performance advantages they offer compared to similar solids that lack magnetic properties. These solids can be used to pre-concentrate analytes and for the magnetic separation and molecular identification of biomolecules, and organic and inorganic species. Magnetic solid separation techniques also offer benefits over centrifugation, filtration, and solid-phase extraction. In this review, we describe the synthesis, characterization and applications of a series of solids including silica supports, carbon nanotubes, alumina, organic polymers and other materials, mostly containing magnetite or paramagnetic metals. Also addressed are the future perspectives of magnetic solid applications. PMID:20678625

54

Magnetic solids in analytical chemistry: A review  

Magnetic solids are widely used in detection and analytical systems because of the performance advantages they offer compared to similar solids that lack magnetic properties. These solids can be used to pre-concentrate analytes and for the magnetic separation and molecular identification of biomolecules, and organic and inorganic species. Magnetic solid separation techniques also offer benefits over centrifugation, filtration, and solid-phase extraction. In this review, we describe the synthesis, characterization and applications of a series of solids including silica supports, carbon nanotubes, alumina, organic polymers and other materials, mostly containing magnetite or paramagnetic metals. Also addressed are the future perspectives of magnetic solid applications.

55

Magnetic phase transitions in plasmas and transport barriers  

A model of magnetic phase transitions in plasmas is presented: plasma elements with pressure excess or defect are dia- or paramagnets and move radially under the influence of the background plasma magnetization. It is found that magnetic phase separation could be the underlying mechanism of L to H transitions and drive transport barrier formation. Magnetic phase separation and the associated pedestal build-up, as described here, can be explained by the well-known interchange mechanism, now reinterpreted as a magnetization interchange. The interchange mechanism can drive motion of plasma elements even when stable. A testable necessary criterion for the L to H transition is presented.

56

Ultra highly sensitive method for detecting Flavobacterium psychrophilum using high-gradient immunomagnetic separation with a polymerase chain reaction  

Abstract We attempted to develop an ultrahigh sensitive method for detecting Flavobacterium psychrophilum using high-gradient immunomagnetic separation (HGIMS) with a polymerase chain reaction (PCR). HGIMS is a magnetic separation method in which the magnetic force is strengthened by introducing a magnetic gradient between the magnetic filter and nearby column. Because immunomagnetic beads specifically react with target cells, target cells are collected efficiently. Accumulated beads are released from the filter by removing the external magnetic force. After concentrating the samples using the HGIMS system, DNA was extracted from the samples, and PCR was applied to detect F. psychrophilum. Our primers did not react with reference bacteria and reacted specifically with F. psychrophilum. The...

57

Surface magnetic enhancement for coal cleaning. Quarterly technical progress report no. 11, August 1, 1990--October 31, 1990  

The fundamental chemistry for selective adsorption of magnetizing reagent on coal-associated minerals to enhance the magnetic susceptibilities of minerals have been established in Phase I study. The application of the results to study the feasibility for coal cleaning has been completed in the Phase II study. The most effective approach to clean Illinois No. 6, Ohio Lower Kittanning, and West Virginia Pocahontas coals using the magnetizing method has been determined. Phase III study is in progress during this quarter. Experimental work includes the determination of various separation parameters, including the separator and matrix selection, magnetic reagent dosage, particle size, magnetic field intensity, and retention time.

58

Surface magnetic enhancement for coal cleaning  

The fundamental chemistry for selective adsorption of magnetizing reagent on coal-associated minerals to enhance the magnetic susceptibilities of minerals have been established in Phase I study. The application of the results to study the feasibility for coal cleaning has been completed in the Phase II study. The most effective approach to clean Illinois No. 6, Ohio Lower Kittanning, and West Virginia Pocahontas coals using the magnetizing method has been determined. Phase III study is in progress during this quarter. Experimental work includes the determination of various separation parameters, including the separator and matrix selection, magnetic reagent dosage, particle size, magnetic field intensity, and retention time.

59

Magnetic microstructure of strontium-substituted thulium ferromanganites Tm0.65Sr0.35Mn1 - x Fe x O3 ( x = 0.3-0.4)  

The structural and magnetic properties of the Tm0.65Sr0.35Mn1 - x Fe x O3 ( x = 0.3-0.4) have been studied by methods of magnetic resonance and differential thermomagnetic analysis. A magnetic phase separation has been revealed in structurally single-phase samples.

60

First- and second-order phase transitions between quantum and classical regimes for the escape rate of a biaxial spin system  

The particle Hamiltonian for a biaxial spin system with a transverse or longitudinal magnetic field is investigated. We apply the Hamiltonian to the quantum-classical escape rate transition in small magnets. It is found that the phase boundary separating the first- and second-order transition is greatly influenced by the transverse anisotropy constant as well as the external magnetic field.

 
 
 
 
61

Magnetic susceptibility of escherichia coli  

The magnetic susceptibility of Escherichia coli (E. coli) was measured by the Faraday balance technique using a microcomputer controlled Cahn balance. The volume magnetic susceptibility of E. Coli is determined to be approximately 1X10-6 (SI units). The high gradient magnetic separation (HGMS) method for capturing aerobic E. coli in its supernatant fluid is determined to have a maximum efficiency of 42%.

62

Explosive generation of high magnetic fields in large volumes and solid state applications  

Various methods of producing ultra-high magnetic fields by explosive flux compression are described. A survey is made of the kinds of high magnetic field solid state data obtained in such fields by various groups. Preliminary results are given for the magnetic phase boundary that separates the spin-flop and paramagnetic regions of MnF/sub 2/.

63

Analytical Computation of the Magnetic Field Distribution in a Magnetic Gear  

We propose an analytical computation of the magnetic field distribution in a magnetic gear. The analytical method is based on the resolution of Laplace's and Poisson's equations (by the separation of variables technique) for each subdomain, i.e., magnets, air gap, and slots. The global solution is o...

64

MASS SEPARATION OF HIGH ENERGY PARTICLES  

An apparatus and method are described for separating charged, high energy particles of equal momentum forming a beam where the particles differ slightly in masses. Magnetic lenses are utilized to focus the beam and maintain that condition while electrostatic fields located between magnetic lenses are utilized to cause transverse separation of the particles into two beams separated by a sufficient amount to permit an aperture to block one beam. (AEC)

65

Magnetic circuit for hall effect plasma accelerator  

A Hall effect plasma accelerator includes inner and outer electromagnets, circumferentially surrounding the inner electromagnet along a thruster centerline axis and separated therefrom, inner and outer magnetic conductors, in physical connection with their respective inner and outer electromagnets, with the inner magnetic conductor having a mostly circular shape and the outer magnetic conductor having a mostly annular shape, a discharge chamber, located between the inner and outer magnetic conductors, a magnetically conducting back plate, in magnetic contact with the inner and outer magnetic conductors, and a combined anode electrode/gaseous propellant distributor, located at a bottom portion of the discharge chamber. The inner and outer electromagnets, the inner and outer magnetic conductors and the magnetically conducting back plate form a magnetic circuit that produces a magnetic field that is largely axial and radially symmetric with respect to the thruster centerline.

66

Magnetic molecularly imprinted polymer for aspirin recognition and controlled release  

Core-shell structural magnetic molecularly imprinted polymers (magnetic MIPs) with combined properties of molecular recognition and controlled release were prepared and characterized. Magnetic MIPs were synthesized by the co-polymerization of methacrylic acid (MAA) and trimethylolpropane trimethacrylate (TRIM) around aspirin (ASP) at the surface of double-bond-functionalized Fe{sub 3}O{sub 4} nanoparticles in chloroform. The obtained spherical magnetic MIPs with diameters of about 500 nm had obvious superparamagnetism and could be separated quickly by an external magnetic field. Binding experiments were carried out to evaluate the properties of magnetic MIPs and magnetic non-molecularly imprinted polymers (magnetic NIPs). The results demonstrated that the magnetic MIPs had high adsorption capacity and selectivity to ASP. Moreover, release profiles and release rate of ASP from the ASP-loaded magnetic MIPs indicated that the magnetic MIPs also had potential applications in drug controlled release.

67

Role of centrifugal and charge effects of the mass separation in a plasma centrifuge with crossed fields  

The coefficients of mass separation have been calculated for gas mixtures in crossed electric and magnetic fields. The initial kinetic equations have been derived, and the contribution of centrifugal and charge separation mechanisms to mass separation in a weakly ionized plasma has been assessed.

68

Atomic lithium vapor laser isotope separation  

An atomic vapor laser isotope separation in lithium was performed using tunable diode lasers. The method permits also the separation of the isotopes between the {sup 6} LiD{sub 2} and the {sup 7} LiD{sub 1} lines using a self-made mass separator which includes a magnetic sector and an ion beam designed for lithium. (Author)

69

Atomic lithium vapor laser isotope separation  

An atomic vapor laser isotope separation in lithium was performed using tunable diode lasers. The method permits also the separation of the isotopes between the sup 6 LiD sub 2 and the sup 7 LiD sub 1 lines using a self-made mass separator which includes a magnetic sector and an ion beam designed for lithium. (Author)

70

Cyclical magnetic field flow fractionation  

In this study, a new magnetic field flow fractionation (FFF) system was designed and modeled by using finite element simulations. Other than current magnetic FFF systems, which use static magnetic fields, our system uses cyclical magnetic fields. Results of the simulations show that our cyclical magnetic FFF system can be used effectively for the separation of magnetic nanoparticles. Cyclical magnetic FFF system is composed of a microfluidic channel (length = 5 cm, height = 30 ?m) and 2 coils. Square wave currents of 1 Hz (with 90 deg of phase difference) were applied to the coils. By using Comsol Multiphysics 3.5a, magnetic field profile and corresponding magnetic force exerted on the magnetite nanoparticles were calculated. The magnetic force data were exported from Comsol to Matlab. In Matlab, a parabolic flow profile with maximum flow speed of 0.4 mL/h was defined. Particle trajectories were obtained by the calculation of the particle speeds resulted from both magnetic and hydrodynamic forces. Particle trajectories of the particles with sizes ranging from 10 to 50 nm were simulated and elution times of the particles were calculated. Results show that there is a significant difference between the elution times of the particles so that baseline separation of the particles can be obtained. In this work, it is shown that by the application of cyclical magnetic fields, the separation of magnetic nanoparticles can be done efficiently.

71

Continuous separation of dry crushed coal at one ton per hour by high-gradient magnetic separation  

An earlier experimental program tested the separation of pyritic sulfur and ash-forming minerals from dry crushed coal in a small, cyclic, high-gradient magnetic separator over a range of each of the process parameters. That experimental program defined a band of operating conditions that affected reductions of the mineral contaminants and recoveries of the heating value comparable to gravimetric separations. This report describes the procedures and results of an experimental program to extrapolate from the small, cyclic separations to continuous, pilot-scale separation at a feed rate of 1 ton/h. The program at the Oak Ridge National Laboratory testing magnetic preparation of dry crushed coal has demonstrated that: (1) Dry crushed coal in the size range of about 600 x 45 ..mu.. can be effectively cleaned by magnetic separation techniques; (2) Product quality and heating value recovery by the high-gradient magnetic process approaches that obtained by a laboratory gravimetric separation of the same size fraction; and (3) Separations performed on size fractions from 600 to 45 ..mu.. at a feed rate of 1 ton/h in a continuous, industrial-type high-gradient magnetic separator equal those obtained in a cyclic laboratory separator.

72

Surface magnetic enhancement for coal cleaning. Final report  

The program consisted of a fundamental study to define the chemistry for the interactions between magnetic reagent and mineral and coal particles, a laboratory study to determine the applicability of this technology on coal cleaning, and a parameter study to evaluate the technical and economical feasibility of this technology for desulfurization and de-ashing under various processing schemes. Surface magnetic enhancement using magnetic reagent is a new technology developed at the Institute. This technology can be applied to separate pyrite and other minerals particles from coal with a magnetic separation after adsorbing magnetic reagent on the surface of pyrite and other minerals particles. Particles which have absorbed magnetic reagent are rendered magnetic. The adsorption can be controlled to yield selectivity. Thus, the separation of traditionally nonmagnetic materials with a magnetic separator can be achieved. Experiments have been performed to demonstrate the theoretical fundamentals and the applications of the technology. Adsorbability, adsorption mechanisms, and adsorption selectivity are included in the fundamental study. The effects of particle size, magnetic reagent dosage, solid contents, magnetic matrix, applied magnetic field strengths, retention times, and feed loading capacities are included in the application studies. Three coals, including Illinois No. 6, Lower Kittanning and Pocahontas seams, have been investigated. More than 90% pyritic sulfur and ash reductions have been achieved. Technical and economic feasibilities of this technology have been demonstrated in this study. Both are competitive to that of the froth flotation approach for coal cleaning.

73

Surface magnetic enhancement for coal cleaning  

The program consisted of a fundamental study to define the chemistry for the interactions between magnetic reagent and mineral and coal particles, a laboratory study to determine the applicability of this technology on coal cleaning, and a parameter study to evaluate the technical and economical feasibility of this technology for desulfurization and de-ashing under various processing schemes. Surface magnetic enhancement using magnetic reagent is a new technology developed at the Institute. This technology can be applied to separate pyrite and other minerals particles from coal with a magnetic separation after adsorbing magnetic reagent on the surface of pyrite and other minerals particles. Particles which have absorbed magnetic reagent are rendered magnetic. The adsorption can be controlled to yield selectivity. Thus, the separation of traditionally nonmagnetic materials with a magnetic separator can be achieved. Experiments have been performed to demonstrate the theoretical fundamentals and the applications of the technology. Adsorbability, adsorption mechanisms, and adsorption selectivity are included in the fundamental study. The effects of particle size, magnetic reagent dosage, solid contents, magnetic matrix, applied magnetic field strengths, retention times, and feed loading capacities are included in the application studies. Three coals, including Illinois No. 6, Lower Kittanning and Pocahontas seams, have been investigated. More than 90% pyritic sulfur and ash reductions have been achieved. Technical and economic feasibilities of this technology have been demonstrated in this study. Both are competitive to that of the froth flotation approach for coal cleaning.

74

Dynamic phase separation in La_{5/8-y}Pr_{y}Ca_{3/8}MnO_{3}  

Detailed magnetization measurements in La_{5/8-y}Pr_{y}Ca_{3/8} MnO_{3}, including magnetic relaxation properties, demonstrate the dynamic nature of the phase separated state in manganites. The difference between the field-cooled-cooling and zero-field-cooled magnetization curves signals the existence in the latter of blocked metastable states separated by high energy barriers. Results of the magnetic viscosity show that the system becomes unblocked in a certain temperature window, where large relaxation rates are observed. We propose a simple phenomenological model in which the system evolves through a hierarchy of energy barriers, which separates the coexisting phases. The calculated magnetization curves using this model reproduce all the qualitative features of the experimental data. The overall results allowed us to construct an H-T phase diagram, where frozen and dynamical phase separation regions are clearly distinguished.

75

Microfluidic magnetic separator using an array of soft magnetic elements  

We present the design, fabrication, characterization, and demonstration of a new passive magnetic bead separator. The device operates in an effective state when magnetized by an external magnetic field of only 50 mT, which is available from a tabletop electromagnet. We demonstrate the complete capture of 1.0 mu m fluorescent magnetic beads from a 7.5 mu L sample volume traveling at an average linear fluid velocity of 5 mm/s.

76

Dynamic behaviour of controlled permanent lift magnets in rapid transit systems  

The magnetic flux for the stationary lift force is provided by the permanent magnetic material in controlled permanent magnets. Lift force changes are regulated using auxiliary control ampere turns. The mechanical and electrical processes are described using a system of differential equations in order to simulate digitally the separately suspended magnets. It is shown that the system exhibits a good dynamic lift behaviour, whereby only small winding losses occur during compensation of the disturbances.

77

Theoretical study of in-plane response of magnetic field sensor to magnetic beads magnetized by the sensor self-field  

We present a theoretical study of the spatially averaged in-plane magnetic field on square and rectangular magnetic field sensors from a single magnetic bead, a monolayer of magnetic beads, and a half-space filled with magnetic beads being magnetized by the magnetic self-field due to the applied bias current through the sensor. The analysis of the single bead response shows that beads always contribute positively to the average magnetic field as opposed to the case for an applied homogeneous magnetic field where the sign of the signal depends on the bead position. General expressions and analytical approximations are derived for the sensor response to beads as function of the bead distribution, the bias current, the geometry and size of the sensor, and the bead characteristics. Consequences for the sensor design are exemplified and it is described how the contribution from the self-field experimentally can be separated from that due to static magnetic fields.

78

Theoretical study of in-plane response of magnetic field sensor to magnetic beads magnetized by the sensor self-field  

We present a theoretical study of the spatially averaged in-plane magnetic field on square and rectangular magnetic field sensors from a single magnetic bead, a monolayer of magnetic beads, and a half-space filled with magnetic beads being magnetized by the magnetic self-field due to the applied bias current through the sensor. The analysis of the single bead response shows that beads always contribute positively to the average magnetic field as opposed to the case for an applied homogeneous magnetic field where the sign of the signal depends on the bead position. General expressions and analytical approximations are derived for the sensor response to beads as function of the bead distribution, the bias current, the geometry and size of the sensor, and the bead characteristics. Consequences for the sensor design are exemplified and it is described how the contribution from the self-field experimentally can be separated from that due to static magnetic fields.

79

2-D and 3-D computations of curved accelerator magnets  

In order to save computer memory, a long accelerator magnet may be computed by treating the long central region and the end regions separately. The dipole magnets for the injector synchrotron of the Advanced Photon Source (APS), now under construction at Argonne National Laboratory (ANL), employ magnet iron consisting of parallel laminations, stacked with a uniform radius of curvature of 33.379 m. Laplace's equation for the magnetic scalar potential has a different form for a straight magnet (x-y coordinates), a magnet with surfaces curved about a common center (r-{theta} coordinates), and a magnet with parallel laminations like the APS injector dipole. Yet pseudo 2-D computations for the three geometries give basically identical results, even for a much more strongly curved magnet. Hence 2-D (x-y) computations of the central region and 3-D computations of the end regions can be combined to determine the overall magnetic behavior of the magnets. 1 ref., 6 figs.

80

Unusual magnetization suppression induced by higher magnetic field in (La0.83Bi0.17)0.67Ca0.33MnO3  

Magnetization behavior of (La0.83Bi0.17)0.67Ca0.33MnO3 has been investigated in the temperature range from 100 to 180 K. A metamagnetic transition was observed in the temperature region, where the magnetization was measured after a zero-field-cooling from room temperature to a selected temperature. Experimental results show that, after a higher magnetization route, the field-increasing branches of the magnetization curves shows an unusual training effect: below a magnetic field H0, the applied magnetic field enhances the value of magnetization; however, above H0 the magnetic field suppresses the value, and the behavior cannot be totally attributed to the enhancement effect of the applied magnetic field on ferromagnetic phase fraction. It is proposed that, in the two-phase coexistence region, the higher magnetic field promotes the phase separation and leads to both the fraction of ferromagnetic domain and the stabilization of antiferromagnetic domain increase.

 
 
 
 
81

Magnetic energy harvesting and concentration at distance by transformation optics  

Magnetic energy is one the main agents powering our society: generating energy in power plants, keeping information in magnetic memories, moving our devices with motors. All of these applications require a certain spatial distribution of magnetic energy, for example concentrating it in a transformer core or in a magnetic sensor. We introduce in this work a way to collect magnetic energy and distribute it in space with unprecedented efficiency and flexibility, allowing very large concentration of magnetic energy in a free space region, an enhanced magnetic coupling between two magnetic sources, and the transfer of magnetic energy from a source to a given distant point separated by empty space. All these features are achieved with a single device, a magnetic shell designed by transformation optics.

82

Preparation of magnetic nanoparticles embedded in polystyrene microspheres  

Superparamagnetic particles are widely used for biological applications such as cell separation. The size of the particles is normally in the range of 10 - 20 nm which is much smaller than the size of a cell. Therefore small particles create small force which is not strong enough to separate the cells from solution. Superparamagnetic nanoparticles embedded in Polystyrene microspheres (magnetic beads) are very useful for cell separation. Magnetic beads have been prepared by solvent evaporation of an emulsion. The beads with size of 0.2 ?m - 1.0 ?m have a saturation magnetization of 10 - 25 emu/g. The change of the amount of surfactants, volatile solvent, magnetic particles resulted to the change of size, magnetic properties of the magnetic beads.

83

CFD simulation for biomagnetic separation involving dilute suspensions  

Abstract Full-Eulerian simulation of the separation of magnetic particles carried by a Newtonian fluid through a planar channel under the influence of a magnetic field is presented. The simulation is based on the application of the Navier-Stokes and concentration equations. The scheme for the magnetic separation of particles is achieved by applying an external magnetic dipole field. The hydrodynamic and magnetophoretic interactions between the particles and the carrier fluid are analysed. Analysis of the competing tendencies of mass transfer indicates that the magnetophoresis migration of magnetic particles is dominant over the molecular diffusion. This dominance becomes more evident at lower diffusivities leading to a drastic magnetic separation confined within a small region in the proxi...

84

Magnetically modulated nanosystems: a unique drug-delivery platform  

Magnetic nanoparticles are attractive targets owing to their unique characteristics that are not shared by bulk materials. Magnetic particles, ranging from nanometer-sized to 1 m in size, are being used in an increasing number of medical applications. The important properties of magnetic particles for medical applications are nontoxicity, biocompatiblilty, injectability and high-level accumulation in the target tissue or organ. Magnetic nanoparticles modified with organic molecules have been widely used for biotechnological and biomedical applications as their properties can be magnetically controlled by applying an external magnetic field. They offer high potential for numerous biomedical applications, such as cell separation, automated DNA extraction, gene targeting, drug delivery, MRI a...

85

Surface magnetic enhancement for coal cleaning. Quarterly technical progress report no. 4, November 1, 1988--January 31, 1989  

The progress achieved during this quarter includes the ten months shelf life study of magnetizing reagent, the effect of cation regulators on minerals and coals, the combination effect of depressant and activator on the adsorption of magnetizing reagent, optimum magnetite size for magnetizing reagent, and the magnetic field strength for separating magnetic enhanced minerals. The work is generally on schedule with the original plan. The Phase I study (a fundamental study) is nearly completed. Selective conditions for adsorbing magnetizing reagent on minerals have been identified. The work for the next quarter will be mainly on the Phase II study. Coal will be selected, procured, characterized, and processed.

86

Surface magnetic enhancement for coal cleaning  

The progress achieved during this quarter includes the ten months shelf life study of magnetizing reagent, the effect of cation regulators on minerals and coals, the combination effect of depressant and activator on the adsorption of magnetizing reagent, optimum magnetite size for magnetizing reagent, and the magnetic field strength for separating magnetic enhanced minerals. The work is generally on schedule with the original plan. The Phase I study (a fundamental study) is nearly completed. Selective conditions for adsorbing magnetizing reagent on minerals have been identified. The work for the next quarter will be mainly on the Phase II study. Coal will be selected, procured, characterized, and processed.

87

Present status of electro-magnetic shield technology. Pt. 1. Electro-magnetic shielding materials; Denji shield gijutsu no genjo. 1. Denji shield zairyo to jiki shield zairyo  

We use electromagnetic and magnetic shielding materials to protect environment from EMI or to obtain lower electromagnetic field room. Magnetic materials are used for shielding magnetic field that is the electromagnetic field less than 10 kHz. Electromagnetic shielding is for the field over 10kHz. The shielding principle by electromagnetic shielding materials is to reflect or absorb electromagnetic wave, whereas that by magnetic shielding materials is to collect and flow magnetic flux. Here, we explain electromagnetic and magnetic shielding materials in separated sections on basic properties and examples for practical use. (author)

88

Magnetic and electrostatic deflecting devices  

A short description is given of a number of deflecting devices in use at CERN, with emphasis on some of their technological aspects. In particular, the cyclotron magnet, the Split-Field Magnet at the ISR, and the magnet of the 2 m Liquid-Hydrogen Bubble Chamber are discussed, as well as the magnets of the synchrotron lattices of the Proton Synchrotron, Intersecting Storage Rings, and Super Proton Synchrotron. In addition, some remarks are made on the technology of septum magnets and fast pulsed magnets. Finally, the application and the technology of electrostatic separators and electrostatic septa are described.

89

Batch extracting process using magneticparticle held solvents  

A process for selectively removing metal values which may include catalytic values from a mixture containing same, wherein a magnetic particle is contacted with a liquid solvent which selectively dissolves the metal values to absorb the liquid solvent onto the magnetic particle. Thereafter the solvent-containing magnetic particles are contacted with a mixture containing the heavy metal values to transfer metal values into the solvent carried by the magnetic particles, and then magnetically separating the magnetic particles. Ion exchange resins may be used for selective solvents.

90

Materials Separation from Pulverized Waste Printed Circuit Boards  

Pulverized waste printed circuit board powder is a complex mix of organic epoxy resin, glass fiber, and several different metals. The aim of this study was to investigate the feasibility of separating the components of the powder and then efficiently recovering the metals by magnetic separation. The organic resin was first decomposed by pyrolysis in an inert atmosphere. The pyrolysis gas was subject to chemical analysis, and the toxic components were successfully trapped. Magnetic and nonmagnetic components in the residue were then separated by magnetic force.   

91

Microstripes for transport and separation of magnetic particles  

We present a simple technique for creating an on-chip magnetic particle conveyor based on exchange-biased permalloy microstripes. The particle transportation relies on an array of stripes with a spacing smaller than their width in conjunction with a periodic sequence of four different externally applied magnetic fields. We demonstrate the controlled transportation of a large population of particles over several millimeters of distance as well as the spatial separation of two populations of magnetic particles with different magnetophoretic mobilities. The technique can be used for the controlled selective manipulation and separation of magnetically labelled species. (C) 2012 American Institute of Physics.

92

Small but mighty: How the MACS-technology based on nanosized superparamagnetic particles has helped to analyze the immune system within the last 20 years  

Today, magnetic cell sorting and flow cytometric cell sorting both are state-of-the-art technologies, with a plethora of applications in biology and biomedicine. Both technologies have their stand-alone applications, but they also perfectly complement each other, in particular for the analysis and isolation of fragile and rare cells. The technological evolution from simple magnets and steel wool separation columns to sophisticated instrumentation and automated procedures has paved the way for magnetic cell separation in the scientific community. This review will focus on applications of magnetic cell sorting with commercially available paramagnetic MACS-nanoparticles (Miltenyi Biotech, Bergisch-Gladbach, Germany) that have allowed unprecedented approaches to the exploration of the immune s...

93

Non-magnetic insulator state in Na1CoO2 and phase separation of Na vacancies  

Crystallographic, magnetic and NMR properties of a NaxCoO2 single crystal with x~1 are presented. We identify the stoichiometric Na1CoO2 phase, which is shown to be a non-magnetic insulator, as expected for homogeneous planes of Co3+ ions with S=0. In addition, we present evidence that, because of slight average Na deficiency, chemical and electronic phase separation leads to a segregation of Na vacancies into the well-defined, magnetic, Na0.8CoO2 phase. The importance of phase separation is discussed in the context of magnetic order for x~0.8 and the occurrence of a metal-insulator transition for x->1.

94

Magnetically modified spent coffee grounds for dyes removal  

Large amounts of spent coffee grounds are discharged from food industries, for example, during the instant coffee manufacture. Although part of them is reused as compost and animal feed, most of the coffee grounds are burned as a waste. However, this material can be used as a biosorbent for xenobiotics removal. Spent coffee grounds were magnetically modified by contact with water-based magnetic fluid. This new type of magnetically responsive biocomposite materials can be easily separated by means of commercially available magnetic separators or strong permanent magnets. Magnetic coffee grounds can be used as an inexpensive magnetic adsorbent for the removal of water-soluble dyes. Seven dyes (crystal violet, malachite green, amido black 10B, Congo red, Bismarck brown Y, acridine orange and ...

95

Comparative Studies on the Magnetic Separation of Carbon Nanotubes and Carbon Nanofibers Suspended in Aqueous Solution  

Because of their extremely large surface area, carbon nano tubes (CNTs) and carbon nano fibers (CNFs) have been widely used to remove heavy metals from water. But the removal of such CNTs and CNFs from water is another important aspect in water purification process. In the present work, we discuss CNT and CNF separation from water using a magnetic separation technique. In order to compare the separation efficiencies, CNTs and CNFs having wide variation in their magnetic properties were selected. The effects of CNT and CNF concentrations in untreated water and water flow velocity on the separation efficiency were investigated systematically.   

96

Enrichment of the metallic components from waste printed circuit boards by a mechanical separation process using a stamp mill.  

Printed circuit boards incorporated in most electrical and electronic equipment contain valuable metals such as Cu, Ni, Au, Ag, Pd, Fe, Sn, and Pb. In order to employ a hydrometallurgical route for the recycling of valuable metals from printed circuit boards, a mechanical pre-treatment step is needed. In this study, the metallic components from waste printed circuit boards have been enriched using a mechanical separation process. Waste printed circuit boards shredded to 5.0mm. The fractions of milled printed circuit boards of size zig-zag classifier. The >5.0mm fraction and the heavy fraction were subjected to two-step magnetic separation. Through the first magnetic separation at 700 Gauss, 83% of the nickel and iron, based on the whole printed circuit boards, was recovered in the magnetic fraction, and 92% of the copper was recovered in the non-magnetic fraction. The cumulative recovery of nickel-iron concentrate was increased by a second magnetic separation at 3000 Gauss, but the grade of the concentrate decreased remarkably from 76% to 56%. The cumulative recovery of copper concentrate decreased, but the grade increased slightly from 71.6% to 75.4%. This study has demonstrated the feasibility of the mechanical separation process consisting of milling/size classification/gravity separation/two-step magnetic separation for enriching metallic components such as Cu, Ni, Al, and Fe from waste printed circuit boards. PMID:18835149

97

Asymmetric Two-dimensional Magnetic Lattices for Ultracold Atoms Trapping and Confinement  

A new method to implement an asymmetrical two-dimensional magnetic lattice is proposed. The asymmetrical two-dimensional magnetic lattice can be created by periodically distributing magnetic minima across the surface of magnetic thin film where the periodicity can be achieved by milling $n\\times n$ square holes on the surface of the film. The quantum device is proposed for trapping and confining ultracold atoms and quantum degenerate gases prepared in the low magnetic field seeking-state at low temperature, such as the Bose-Einstein Condensate (BEC) and ultracold fermions. We present detailed analysis of the analytical expressions and the numerical simulation procedure used to calculate the external magnetic field. We also, describe the magnetic band gap structure exhibited by the asymmetric effect of the magnetic minima and show some of the possible application. We analyze the effect of changing the characteristic parameters of the magnetic lattice, such as the separating periodicity length and the hole size...

98

Polymerase chain reaction system using magnetic beads for analyzing a sample that includes nucleic acid  

A polymerase chain reaction system for analyzing a sample containing nucleic acid includes providing magnetic beads; providing a flow channel having a polymerase chain reaction chamber, a pre polymerase chain reaction magnet position adjacent the polymerase chain reaction chamber, and a post pre polymerase magnet position adjacent the polymerase chain reaction chamber. The nucleic acid is bound to the magnetic beads. The magnetic beads with the nucleic acid flow to the pre polymerase chain reaction magnet position in the flow channel. The magnetic beads and the nucleic acid are washed with ethanol. The nucleic acid in the polymerase chain reaction chamber is amplified. The magnetic beads and the nucleic acid are separated into a waste stream containing the magnetic beads and a post polymerase chain reaction mix containing the nucleic acid. The reaction mix containing the nucleic acid flows to an analysis unit in the channel for analysis.

99

Functional Magnetic Particles for Medical Application  

Magnetic particles for medical applications have been developed by many researchers. Since magnetic particles have unique magnetic features not present in other materials, they can be applied to special medical techniques. Separation, immunoassay, magnetic resonance imaging (MRI), drug delivery, and hyperthermia are enhanced by the use of magnetic particles. Magnetite cationic liposomes (MCLs), one of the group of cationic magnetic particles, can be used as carriers to introduce DNA into cells since their positively charged surface associates with the negatively charged DNA. They can also be used as heat mediators for cancer therapy. Magnetic particles conjugated with tumor-specific antibodies have enabled tumor-specific contrast enhancement in MRI. In addition, antibody-conjugated magnetic particles were shown to target renal cell carcinoma cells, and are applicable to the hyperthermic treatment of carcinomas. The use of magnetic particles with their unique features will further improve medical techniques.   

100

Interaction forces between soft magnetic particles in uniform and non-uniform magnetic fields  

The influence of the magnetization of a soft magnetic sphere on the surrounding magnetic field is measured and characterized. The interaction force between two soft magnetic particles is directly measured using an ultra precision load sensor in uniform and non-uniform magnetic fields. The interaction force largely follows an inverse fourth power law as a function of separation distance between particle centers. At small distances, the effect of magnetization of one particle on the magnetization of its adjacent particle causes the attractive (repulsive) force to be larger (smaller) than that predicted by the inverse fourth power law. The theoretical prediction based on a modified dipole model, that takes into account the coupling effect of the magnetization among soft magnetic particles, gi...

 
 
 
 
101

Three-dimensional modeling of a portable medical device for magnetic separation of particles from biological fluids.  

A portable separator has been developed to quantitatively separate blood-borne magnetic spheres in potentially high-flow regimes for the human detoxification purpose. In the separator design, an array of biocompatible capillary tubing and magnetizable wires is immersed in an external magnetic field that is generated by two permanent magnets. The wires are magnetized and the high magnetic field gradient from the magnetized wires helps to collect blood-borne magnetic nano/micro-spheres from the blood flow. In this study, a 3D numerical model was created and the effect of tubing-wire configurations on the capture efficiency of the system was analyzed using COMSOL Multiphysics 3.3{reg_sign}. The results showed that the configuration characterized by bi-directionally alternating wires and tubes was the best design with respect to the four starting configurations. Preliminary in vitro experiments verified the numerical predictions. The results helped us to optimize a prototype portable magnetic separator that is suitable for rapid sequestration of magnetic nano/micro-spheres from the human blood stream while accommodating necessary clinical boundary conditions.

102

Hydrolysis of Sugars Using Magnetic Silica Nanoparticles with Sulfonic Acid Groups  

CoFe2O4-embedded silica nanoparticles containing sulfonic acid groups were found to be highly active solid acid catalysts for hydrolysis of disaccharides (sucrose and cellobiose) and polysaccharides (starch and cellulose) with facile magnetic separation.   

103

Harvesting fresh water and marine algae by magnetic separation: Screening of separation parameters and high gradient magnetic filtration  

In this study, the focus is on magnetic separation of fresh water algae Chlamydomonas reinhardtii and Chlorella vulgaris as well as marine algae Phaeodactylum tricornutum and Nannochloropsis salina by means of silica-coated magnetic particles. Due to their small size and low biomass concentrations, harvesting algae by conventional methods is often inefficient and cost-consuming. Magnetic separation is a powerful tool to capture algae by adsorption to submicron-sized magnetic particles. Hereby, separation efficiency depends on parameters such as particle concentration, pH and medium composition. Separation efficiencies of >95% were obtained for all algae while maximum particle loads of 30 and 77g/g were measured for C. reinhardtii and P. tricornutum at pH 8 and 12, respectively. This study ...

104

Separation of Solid Polymers by Magneto-Archimedes Levitation  

Solid polymers, including polystyrene, poly(ethylene terephthalate), poly(methyl methacrylate), and so forth, suspended in a paramagnetic aqueous solution were levitated in different vertical positions under a magnetic field gradient. This phenomenon will be used for separating solid polymers.   

105

On Space-Time Inversion Invariance and its Relation to Non ...  

QED. As such, the property Eq. (3.7) is shared by any solver of Eq. (1.1) which ...... Bed (SMB) Chromatographic Separation Problems, Chemical Engineering ... tions Without Special Treatment for Divergence-Free Magnetic Field, AIAA J., ...

106

The first interconnection of the LHC  

A welder is seen making the very first interconnection between two cryomagnets for the LHC. The 1700 interconnections between superconducting magnets for the whole collider will require 123 000 separate welding and assembly operations.

107

I 1 | K V I I  

NASA, the alternator windings will operate in a helium-xenon gas mixture which may .... alumina (AlgOo) slot liners and separators and Anadur insulated nickel magnet .... therefore measured with the alternator placed inside a shielded test ...

108

NASA Lunar Dust Filtration and Separations Workshop Report  

filter media and filtration and gas-phase separation technologies. The aim of the ..... -Sticky tape or materials wipes. -Magnetic or ..... techniques, which include (in order of increasing efficiency): dry laid, spun bond, melt blown, glass blanket ...

109

Linear Birefringence and Optical Activity in a Magnetized Plasma.  

Linear birefringence and optical activity are considered separately for electromagnetic wave propagation in magnetized cold plasma, using frequency approximation much bigger than plasma frequency. It is shown that in some interesting cases, those phenomen...

110

Attractive Forces between Cation Condensed DNA Double Helices  

By combining single-molecule magnetic tweezers and osmotic stress on DNA assemblies, we separate attractive and repulsive components of the total intermolecular interaction between multivalent cation condensed DNA. Based on measurements of several different cations, we identify two invariant propert...

111

Annual Report as of 31 January 1972 Prepared for: NASA Manned ...  

magnetic separation, Mossbauer spectroscopy, and microscopic examination. R. M. Housley, R. W. ..... Since this sample was composed largely of glass- welded ... optically resolvable metallic phase can be found in the majority of particles in ...

112

Rhizobium fredii and Rhizobium meliloti produce 3-deoxy-D-manno-2-octulosonic acid-containing polysaccharides that are structurally analogous to group II K antigens (capsular polysaccharides) found in Escherichia coli.  

The polysaccharide components from cultured cells of Rhizobium fredii USDA205 and Rhizobium meliloti AK631 were extracted with hot phenol-water and separated by repetitive gel filtration chromatography. Polyacrylamide gel electrophoresis, nuclear magnetic resonance spectrometry, and gas chromatograp...

113

N 9 1  

oxidation at 11UK and 114OK and the reduction of pseudobrookite (Fe2TiOs) ...... stony fraction through magnetic and gaseous digestion separation techniques. ..... tains ores of chromium and Pt-group metals, illustrates the sort of dry-magma ...

114

Cerium moment collapse in ternary silicides CePd[sub 2[minus][ital x  

Cerium [ital L][sub 3] XANES (x-ray-absorption near-edge-structure) spectra were analyzed to separate Ce moment contributions and mixed valence (MV) in complex magnetic silicides CePd[sub 2[minus][ital x

115

New cleaning technologies advance coal. Part 2. Agglomeration, biological and chemical cleaning processes  

The second part of this paper is concerned with techniques of oil agglomeration, high gradient magnetic separation, biological oxidation and chemical cleaning. Brief descriptions of several of the processes are given.

116

A Technique for Automated Determination of Flare-ribbon Separation and Energy Release  

We present a technique for automatic determination of flare-ribbon separation and the energy released during the course of two-ribbon flares. We have used chromospheric H$\\alpha$ filtergrams and photospheric line-of-sight magnetograms to analyse flare-ribbon separation and magnetic-field structures, respectively. Flare-ribbons were first enhanced and then extracted by the technique of "region growing", i.e., a morphological operator to help resolve the flare-ribbons. Separation of flare-ribbons was then estimated from magnetic polarity reversal line using an automatic technique implemented into Interactive Data Language (IDL\\tm) platform. Finally, the rate of flare-energy release was calculated using photospheric magnetic-field data and the corresponding separation of the chromospheric H$\\alpha$ flare-ribbons. This method could be applied to measure the motion of any feature of interest (e.g., intensity, magnetic, Doppler) from a given point of reference.

117

History of early atomic clocks  

This review of the history of early atomic clocks includes early atomic beam magnetic resonance, methods of separated and successive oscillatory fields, microwave absorption, optical pumping and atomic masers. (author)

118

A near-earth optical communications terminal with a corevolving ...  

an outward thrust or tether tension T directed away from the two massive bodies. .... wires would maintain their separation by the magnetic field, and the voltage ... The taper required for constant ... and the tether could be a plastic filament.

119

Separation of impurities in coal by magnetic separation: a study of the desulfurization and deashing of coal  

A high-gradient magnetic separator was used in tests of Nishiyama, Miller and Tatung coals. It was discovered that pyrite and siderite could be removed; that calcite and feldspar, which contain iron and other impurities, could be concentrated; and that incomplete separation of clay minerals was possible. The relation between magnetic field strength, coal solution flow rate, percentage ash removal and coal yield was clarified, and light was also thrown on the relation between flow rate and magnetic field strength, both of which affect the percentage pyrite removal. Considerations of yield lead the authors to recommend low magnetic field separation followed by cleaning of impurities which have not adhered to the magnet. 6 references.

120

Magnetic Separations with Magnetite: Theory, Operation, and Limitations  

This dissertation documents the theory development and experimental plan followed to describe how a magnetite-based column under the influence of an external magnetic field functions as a magnetic separator. Theoretical simulations predict that weekly paramagnetic particles in the sub-micron range can be magnetically separated while diamagnetic particles as large as 2 microns in diameter may pass. Magnetite-based columns were evaluated as magnetically-controllable enhanced filtration devices. There was no evidence of enhanced filtration for diamagnetic particles by the magnetite-based bed. Magnetite-based magnetic separators have proven to be effective in specific laboratory experiments, indicating a potential feasibility for scale-up operations. Column media-filter type filtration effects indicate a magnetite-based column would not be suitable for treatment of a waste stream with a high diamagnetic solids content or high volume throughput requirements. Specific applications requiring removal of sub-micron para- or ferromagnetic particles under batch or Stokes flow conditions would be most applicable.

 
 
 
 
121

A study on the rare earth ore containing scandium by high gradient magnetic separation  

Scandium (Sc) concentration from the rare earth ore by high gradient magnetic separation (HGMS) was determined on the basis of Sc content, geophysical parameter determination and the magnetic analyses of the ore. Based on the condition experiments, expanding experiments were carried out. The results showed that the ore had a Sc grade of 48.90 g/t, and after removing iron by low-intensity magnetic separation, a Sc concentrate of 314.89 g/t grade and with 77.53% recovery was obtained by one-stage roughing-one-stage cleaning of high gradient magnetic separation. Most of the rare earth elements were enriched in the Sc concentrate, and some could be comprehensively recovered during Sc extraction. It was therefore concluded that most of the rare earth elements in the weakly magnetic minerals cou...

122

Technical Challenges for the Head-on Collisions and Extraction at the ILC  

An interaction region with head-on collisions is considered as an alternative to the baseline ILC configuration. Progress in the final focus optics design includes engineered large bore superconducting final doublet magnets and their 3D magnetic integration in the detector solenoids. Progress on the beam separation optics is based on technical designs of electrostatic separator and special extraction quadrupoles. The spent beam extraction is realized by a staged collimation scheme relying on realistic collimators.

123

Optics of mass separator I  

The ion optics of an existing mass separator are documented. The elctrostatic and magnetic stages are analyzed theoretically, both separately and in combination, by paying particular attention to the ion trajectories, the linear and angular magnifications, and the dispersion. The possibility of converting the magnet into a tunable unit by means of current-carrying elements in the gap is demonstrated. The feasibility of correction coils constructed from printed circuit board is shown.

124

Self-assembled magnetic filter for highly efficient immunomagnetic separation.  

We have developed a compact and inexpensive microfluidic chip, the self-assembled magnetic filter, to efficiently remove magnetically tagged cells from suspension. The self-assembled magnetic filter consists of a microfluidic channel built directly above a self-assembled NdFeB magnet. Micrometre-sized grains of NdFeB assemble to form alternating magnetic dipoles, creating a magnetic field with a very strong magnitude B (from the material) and field gradient ?B (from the configuration) in the microfluidic channel. The magnetic force imparted on magnetic beads is measured to be comparable to state-of-the-art microfabricated magnets, allowing for efficient separations to be performed in a compact, simple device. The efficiency of the magnetic filter is characterized by sorting non-magnetic (polystyrene) beads from magnetic beads (iron oxide). The filter enriches the population of non-magnetic beads to magnetic beads by a factor of >10(5) with a recovery rate of 90% at 1 mL h(-1). The utility of the magnetic filter is demonstrated with a microfluidic device that sorts tumor cells from leukocytes using negative immunomagnetic selection, and concentrates the tumor cells on an integrated membrane filter for optical detection. PMID:20949198

125

Affinity separation in magnetically stabilized fluidized beds: synthesis and performance of packing materials  

A magnetically stabilized fluidized-bed separator designed to test the use of pellicular, ferromagnetic affinity chromatography packing materials has been developed. A wire wound solenoid was used to produce the magnetic field. The ferromagnetic packing material is comprised of a magnetite-containing, polyurethane gel coated onto polystyrene beads. The gel contains free carboxyl groups. These were carbodiimide-coupled to soy trypsin inhibitor and the material used for trypsin purification. Narrow-band affinity chromatography was carried out in packed-bed, fluidized-bed, and magnetically stabilized, fluidized-bed separators. Pressure drop, capacity, dilution, and peak asymmetry were evaluated for each type of separator. The three types provide comparable efficiency but the fluidized separators exhibit a much lower pressure drop. As might be expected, fluidized-bed separators perform well for affinity chromatography (large k') but poorly for size exclusion chromatography.

126

Removal of algal blooms from freshwater by the coagulation-magnetic separation method.  

This research investigated the feasibility of changing waste into useful materials for water treatment and proposed a coagulation-magnetic separation technique. This technique was rapid and highly effective for clearing up harmful algal blooms in freshwater and mitigating lake eutrophication. A magnetic coagulant was synthesized by compounding acid-modified fly ash with magnetite (Fe(3)O(4)). Its removal effects on algal cells and dissolved organics in water were studied. After mixing, coagulation, and magnetic separation, the flocs obtained from the magnet surface were examined by SEM. Treated samples were withdrawn for the content determination of chlorophyll-a, turbidity, chemical oxygen demand (COD), total nitrogen, and total phosphorus. More than 99 % of algal cells were removed within 5 min after the addition of magnetic coagulant at optimal loadings (200 mg L(-1)). The removal efficiencies of COD, total nitrogen, and phosphorus were 93, 91, and 94 %, respectively. The mechanism of algal removal explored preliminarily showed that the magnetic coagulant played multiple roles in mesoporous adsorption, netting and bridging, as well as high magnetic responsiveness to a magnetic field. The magnetic-coagulation separation method can rapidly and effectively remove algae from water bodies and greatly mitigate eutrophication of freshwater using a new magnetic coagulant. The method has good performance, is low cost, can turn waste into something valuable, and provides reference and directions for future pilot and production scale-ups. PMID:22767355

127

Ramp rate testing of an HTS high gradient magnetic separation magnet  

The authors report on the ramp rate testing of a prototype high temperature superconducting (HTS) high gradient magnetic separation (HGMS) magnet. HGMS magnets are ramped from full field to zero field to clean the separation matrix. The time spent ramping the magnet is unavailable for processing and must therefore be kept to a minimum. Existing commercial low temperature superconducting HGMS magnets are immersed in a liquid helium bath and are designed to ramp from zero to full current in one minute. The HTS magnet in the system is conductively cooled and operates in a vacuum at a temperature of approximately 30 K. Heat generated during ramping is not as readily removed from the conductively cooled magnet as a bath cooled magnet. To verify that the conductive cooling can adequately remove heat generated during ramping they recorded magnet temperatures and voltages while ramping at rates of up to 4.8 A/second. The magnet can accommodate ramps from zero to 100 A (1.6 Tesla) in 21 seconds with no degradation in performance. The average magnet temperature rises a maximum of 1 K during ramping. Using temperatures recorded during ramps they have made rough estimates of the ac losses generated in the magnet.

128

Direct imaging of the coexistence of ferromagnetism and superconductivity at the LaAlO3/SrTiO3 interface  

LaAlO3 and SrTiO3 are insulating, non-magnetic oxides, yet the interface between them exhibits a two-dimensional electron system with high electron mobility, superconductivity at low temperatures and electric-field-tuned metal?insulator and superconductor?insulator phase transitions. Bulk magnetization and magnetoresistance measurements also indicate some form of magnetism depending on preparation conditions and a tendency towards nanoscale electronic phase separation. Here we use local imaging of the magnetization and magnetic susceptibility to directly observe a landscape of ferromagnetism, paramagnetism and superconductivity. We find submicrometre patches of ferromagnetism in a uniform background of paramagnetism, with a non-uniform, weak diamagnetic superconducting susceptibility at lo...

129

Electronic structure and magnetism of CuNi coherent modulated structures  

The electronic structure and magnetism of coherent modulated structures of CuNi for varying numbers of Cu and Ni layers modulated along (111) and (100) directions has been determined theoretically by means of self-consistent spin polarized LMTO energy band studies and compared with experiment and with theoretical results separately obtained for bulk fcc and tetragonally distorted Ni metal. The magnetic moments in the Ni layers in CuNi are found to be reduced relative to that of fcc Ni indicating that the enhanced magnetism deduced from earlier ferromagnetic resonance observations must arise from other sources. These predictions have been confirmed recently by direct magnetization and neutron magnetic scattering studies.

130

Novel Electromagnetic Structure with Bypass Magnetic Path for Reset Switch  

This paper presents a novel magnetic structure for a switch equipped with an electromagnetic reset function. This structure contains a bypass magnetic path which is separated from the main magnetic path for the permanent magnet so that the magnetic flux excited by the current can increase substantially to improve the efficiency when the reset operation is performed. The characteristics of the attractive force of this model are calculated by the 3-D finite element method and are compared with a usual rocker switch with the reset function. The calculation results clarify the effectiveness of this structure.   

131

Numerical simulation for hydrogen magnetic refrigeration  

We have built active magnetic regenerator (AMR) test apparatuses operated with a gas displacer to transfer the heat from magnetic material unit (AMR bed). Because finding an optimum parameter by experiment is not easy, numerical simulation is necessary to confirm the experimental conditions. As the first step of the project, we developed a 1-dimensional porous media model for hydrogen magnetic refrigerator with a Brayton-likeoperation cycle. This model has been calculated separately for heat exchange fluid and magnetic material. The results using two different magnetic materials have been compared.We confirmed that the simulation results agreed with experimental data of the internal gas displacer system.

132

Measurement of Magnetic Susceptibility of a Particle Suspended in a Liquid Phase  

It was proposed that a method to measure the magnetic susceptibility of a particle such as the biological cell suspended in a liquid phase without any kind of contact with the apparatus. This method utilizes the magnetic force acting on the particle under the high magnetic field gradient, which is balanced by the viscous force controlled by the fluid velocity. The magnetic susceptibility can be determined from the value of the fluid velocity when the suspended particle is stopped against the fluid motion by the magnetic force. An experimental result for a polystyrene micro-sphere proved a possibility of the in vivo assay and separation of the living cells by using this method.   

133

The role of cobalt ferrite magnetic nanoparticles in medical science  

The nanotechnology industry is rapidly growing and promises that the substantial changes that will have significant economic and scientific impacts be applicable to a wide range of areas, such as aerospace engineering, nano-electronics, environmental remediation and medical healthcare. In this area, cobalt ferrite nanoparticles have been regarded as one of the competitive candidates because of their suitable physical, chemical and magnetic properties like the high anisotropy constant, high coercivity and high Curie temperature, moderate saturation magnetization and ease of synthesis. This paper introduces the magnetic properties, synthesis methods and some medical applications, including the hyperthermia, magnetic resonance imaging (MRI), magnetic separation and drug delivery of cobalt fer...

134

Break Arcs Driven by Transverse Magnetic Field in a DC48V/6-24A Resistive Circuit  

Silver electrical contacts are separated to generate break arcs in a DC48V/6-24A resistive circuit. The transverse magnetic field formed by a permanent magnet is applied to the break arcs. A series of experiments are carried out for two different experimental conditions. One condition is a constant contact separating speed while the magnetic flux density is changed to investigate the shortening effect of the arc duration. Another condition is a constant magnetic flux density while the contact separating speed is changed to investigate the changes in the arc duration and the contact gap when the break arc is extinguished. As a result, with constant separating speed, it is confirmed that the duration of break arcs is shortened by the transverse magnetic field and the break arcs are extinguished when the arc length reaches a certain value L. Under the condition of constant transverse magnetic field, (i) the arc duration is shortened by increasing the separation speed; (ii) the contact gap when the break arc is extinguished is almost constant when the separating speed v is sufficiently faster than 5mm/s.   

135

Superconducting superferric dipole magnet with cold iron core for the VLHC  

The magnet system of the Very Large Hadron Collider (VLHC) Stage I is based on a superconducting 2 Tesla magnetic field combined function magnets. These magnets will have a room temperature iron core with two 20 mm air gaps. Magnetic field in both horizontally separated air gaps is excited by a single turn 100 kA superconducting transmission line. The alternative design with cold iron core, horizontally or vertically separated air gaps is under investigation. The cold iron option with horizontally separated air gaps reduces the amount of iron, which is one of the main cost driver for 233 km length magnet system of the future accelerator. The vertical beam separation decreases volume superconductor, heat load from synchrotron radiation and eliminates fringing field from a return bus. But the horizontal beam separation has lowest volume of iron core and as a result lower heat load for cryosystem during cooling down. All these options are discussed and comparison is made. Superconducting correction system, combined with the magnet, allowing to increase the maximum field is also under discussion. Preliminary cost analysis are made for all options.

136

Magnetic field enhanced cake filtration of superparamagnetic PVAc-particles  

The combination of two classical separation methods, cake filtration and magnetic field driven separation, for superparamagnetic nanocomposites results in positive synergetic effects and in extension of the field of application of the cake filtration process. In inhomogeneous magnetic fields magnetic particles experience a magnetic force. Experimental results show that two different effects of the magnetic field influence the cake building process. A special configuration of the magnet system leads to a slow down of the cake built-up. Due to changes of the structure the cake itself has a higher permeability. The result is an increase of the overall filtrate mass flow and therefore an improvement of filtration kinetics.This new process could be applied to the emerging field of biotechnology...

137

Ultrafast magnetization enhancement in metallic multilayers driven by superdiffusive spin current  

Uncovering the physical mechanisms that govern ultrafast charge and spin dynamics is crucial for understanding correlated matter as well as the fundamental limits of ultrafast spin-based electronics. Spin dynamics in magnetic materials can be driven by ultrashort light pulses, resulting in a transient drop in magnetization within a few hundred femtoseconds. However, a full understanding of femtosecond spin dynamics remains elusive. Here we spatially separate the spin dynamics using Ni/Ru/Fe magnetic trilayers, where the Ni and Fe layers can be ferro- or antiferromagnetically coupled. By exciting the layers with a laser pulse and probing the magnetization response simultaneously but separately in Ni and Fe, we surprisingly find that optically induced demagnetization of the Ni layer transiently enhances the magnetization of the Fe layer when the two layer magnetizations are initially aligned parallel. Our observations are explained by a laser-generated superdiffusive spin current between the layers.

138

Charge-magnetic interference resonant scattering studies of ferromagnetic crystals and thin films  

The element- and site-specificity of X-ray resonant magnetic scattering (XRMS) makes it an ideal tool for furthering our understanding of complex magnetic systems. In the hard X-rays, XRMS is readily applied to most antiferromagnets where the relatively weak resonant magnetic scattering (10â?????2â??????10â?????6 I c ) is separated in reciprocal space from the stronger, Bragg charge scattered intensity, I c . In ferro(ferri)magnetic materials, however, such separation does not occur and measurements of resonant magnetic scattering in the presence of strong charge scattering are quite challenging. We discuss the use of charge-magnetic interference resonant scattering for studies of ferromagnetic (FM) crystals and layered films. We review the challenges and opportunities afforded by this ...

139

Magnetic Materials  

Students begin working on the grand challenge of the unit by thinking about the nature of metals and quick, cost-effective means of separating different metals, especially steel. They arrive at the idea, with the help of input from relevant sources, to use magnets, but first they must determine if the magnets can indeed isolate only the steel.

140

Magnetocaloric effect in phase separated manganite probed by differential thermal analysis  

Differential thermal analysis is used to measure the temperature change (DELTAT) due to the application of an external magnetic field in a manganite with phase separation. The temperature dependence of DELTAT is compared with the expected from magnetization measurements. A phenomenological model for the enthalpy change is used to obtain DELTAT during the metamagnetic transition.

 
 
 
 
141

Magnetocaloric effect in phase separated manganite probed by differential thermal analysis  

Differential thermal analysis is used to measure the temperature change (?T) due to the application of an external magnetic field in a manganite with phase separation. The temperature dependence of ?T is compared with the expected from magnetization measurements. A phenomenological model for the enthalpy change is used to obtain ?T during the metamagnetic transition.

142

Novel multifunctional iron oxide and poly(amidomine)s based nanoparticles  

In the last decade magnetic nanoparticles (NPs), had a large impact in many areas of biomedicine, including contrast agents for magnetic resonance imaging, drug targeting, diagnostics, molecular biology, cell separation and purification, and hyperthermia therapy. In this widespread scenario we start...

143

Latching relay switch assembly  

A latching relay switch assembly which includes a coil section and a switch or contact section. The coil section includes at least one permanent magnet and at least one electromagnet. The respective sections are, generally, arranged in separate locations or cavities in the assembly. The switch is latched by a permanent magnet assembly and selectively switched by an overriding electromagnetic assembly.

144

Functionalization of magnetic gold/iron-oxide composite nanoparticles with oligonucleotides and magnetic separation of specific target  

Magnetic composite nanoparticles of gold and iron-oxide synthesized with gamma-rays or ultrasonics were functionalized with thiol-modified oligonucleotides. The amount of oligonucleotides bound to the functionalized nanoparticle probes via hybridization was quantified with fluorescently-labeled target oligonucleotides. Our composite nanoparticles magnetically separated the specific target oligonucleotides without the non-specific adsorption.

145

Magnetic separation of amino acids by gold/iron-oxide composite nanoparticles synthesized by gamma-ray irradiation  

Amounts of amino acids adsorbed onto the Au/{gamma}-Fe{sub 2}O{sub 3} composite nanoparticles synthesized by gamma-ray irradiation were measured using magnetic separation technique. Cystine and methionine, which are sulfur-containing amino acids, connected to Au by a Au-S bond could be selectively picked up by a magnet.

146

Giant entropy change at the co-occurrence of structural and magnetic transitions in the Ni2.19Mn0.71Ga Heusler alloy  

In this paper we report the existence of a giant magnetocaloric effect (MCE) in a intermetallic compound non-containing rare-earth. This effect is associated with the concomitant occurrence of a structural and a magnetic transition. The result has been compared with that obtained in a parent compound in which magnetic and structural transition occur separately.

147

CONTINUOUS FLOW SEPARATION, AN APPLICATION OF SELECTIVE MAGNETOSEDIMENTATION  

A Continuous Flow Separation (CFS) technique is introduced, which operates uninterruptedly, without the use of a magnetic filter matrix. CFS is based on selective magnetosedimentation, in a field gradient introduced by the processing magnet itself. A laboratory scale continuous flow system has been ...

148

A co-crystal of polyoxometalates exhibiting single-molecule magnet behavior: the structural origin of a large magnetic anisotropy.  

A polyoxometalate-based {Mn(III)(3)Mn(IV)} single-molecule magnet exhibits a large axial anisotropy (D = -0.86 cm(-1)) resulting from a near-parallel alignment of Jahn-Teller axes. Its rigorous three-fold symmetry (i.e. rhombicity E? 0) and increased intercluster separation via co-crystallization effectively hamper quantum tunnelling of the magnetization. PMID:22510784

149

Manipulation of Magnetic Domain Walls and Vortices by Current Injection  

This thesis deals with the interaction of spin-polarized currents with the spin configuration in magnetic wires and disks. The samples are studied by high resolution X-ray magnetic circular dichroism - photo emission electron microscopy and the experiments can be separated in two groups. The study o...

150

Spin Dependent Transport in Magnetic Nanostructures  

Recent progress in physics on spin dependent transport in magnetic nanostructures is reviewed. Special attention is paid on the spin accumulation and spin current caused by spin injection into non-magnetic metals and semiconductors and superconductors. A variety of phenomena induced in nano-superconductor/ferromagnet devices are proposed, examining the spin-charge separation in superconductors.

151

Chemical species in fly ash from coal-burning power plants  

Fly ash specimens from four power plants in the Tennessee Valley Authority system have been separated into three matrices: glass, mullite-quartz, and magnetic spinel. Chemical species of trace elements are defined to a large extent by the matrices that contain them. The magnetic component of fly ash is ferrite. The mullit-quartz phase is relatively pure and can be recovered as a resource.

152

Highly selective fluorescent chemosensor for Zn2+ derived from inorganic-organic hybrid magnetic core/shell Fe3O4@SiO2 nanoparticles  

Magnetic nanoparticles with attractive optical properties have been proposed for applications in such areas as separation and magnetic resonance imaging. In this paper, a simple and novel fluorescent sensor of Zn2+ was designed with 3,5-di-tert-butyl-2-hydroxybenzaldehyde [DTH] covalently grafted on...

153

Ferrimagnetic [CoII3(micro3-OH)2(RCO2)4] chains embedded in a laminar hybrid material exhibiting single-chain magnet behaviour.  

The ligand, benzophenone-2,4'-dicarboxylate, was used as a polytopic linker and magnetic separator to bridge the inorganic hydroxide-bridged cobat(ii) chain motifs into a laminar inorganic-organic hybrid materials with nearest inter-chain Co(ii)Co(ii) distance of ca. 8.14 A, which exhibits single-chain magnet behaviour. PMID:19259557

154

A Multifunctional Heterogeneous Catalyst: Titanium-containing Mesoporous Silica Material Encapsulating Magnetic Iron Oxide Nanoparticles  

Magnetic iron oxide nanoparticles coated with mesoporous silica involving single-site titanium oxide moiety have been first developed by adopting a two-step coating method. The catalytic performance and magnetically separable ability were demonstrated in the oxidation of 2,6-di-tert-butylphenol using hydrogen peroxide.   

155

Colossal enhancement of magnetoresistance in La(0.67)Sr(0.33)MnO(3) thin films: possible evidence of electronic phase separation.  

A gigantic three orders of magnitude change of resistivity in La(0.67)Sr(0.33)MnO(3) (LSMO) thin film, on application of magnetic field, has been observed. The transport and magnetic properties are characteristic of electronic phase separation between ferromagnetic metallic and antiferromagnetic charge-ordered insulating regions, unusual for a canonical double exchange system such as LSMO. PMID:21814010

156

Preliminary analysis of the MER magnetic properties experiment using a computational fluid dynamics model  

Motivated by questions raised by the magnetic properties experiments on the NASA Mars Pathfinder and Mars Exploration Rover (MER) missions, we have studied in detail the capture of airborne magnetic dust by permanent magnets using a computational fluid dynamics (CFD) model supported by laboratory simulations. The magnets studied are identical to the capture magnet and filter magnet on MER, though results are more generally applicable. The dust capture process is found to be dependent upon wind speed, dust magnetization, dust grain size and dust grain mass density. Here we develop an understanding of how these parameters affect dust capture rates and patterns on the magnets and set bounds for these parameters based on MER data and results from the numerical model. This results in a consistent picture of the dust as containing varying amounts of at least two separate components with different physical properties.

157

Method of manufacturing motor  

In manufacturing a DC motor body including a motor magnet by conventional processes, a magnet is fitted to the cylindrical molding core and a motor body is injection-molded within a cavity formed between a motor-body-forming mold and a cylindrical molding core to which the magnet is attached. Therefore, the magnet has to be molded and stocked before molding the motor body, thus being inapplicable to mass-production processes. To overcome these problems, the motor magnet and the motor body are molded in sequence in accordance with two separate molding steps by the use of the same molding core. This method can eliminate troublesome magnet fitting work and the need of magnet stock, and enhance the dimensional precision of motor magnet, thus being applicable to mass-production process while increasing the energy transduction efficiency of the DC motor.

158

Magnetic solid-phase extraction based on magnetic carbon nanotube for the determination of estrogens in milk  

Abstract In this work, a novel method for the fabrication of magnetic carbon nanotubes based on -aggregation wrap- was proposed. When carbon nanotubes and magnetic nanoparticles were vortically mixed in a solvent, the magnetic nanoparticles were wrapped into the carbon nanotube bundles that formed during the aggregation process, leading to the formation of magnetic carbon nanotubes. Thus, the resultant material can be separated from the solvent rapidly and conveniently by a magnet. Our investigation demonstrated that the -aggregation wrap- mechanism for the preparation of magnetic composite is also applicable to other self-aggregated micro/nanomaterials, including graphene, graphite, C60, etc. To testify the feasibility of the magnetic composites in sample preparation, the resultant magnet...

159

Relationships between magnetic foot points and G-band bright structures  

Magnetic elements are thought to be described by flux tube models, and are well reproduced by MHD simulations. However, these simulations are only partially constrained by observations. We observationally investigate the relationship between G-band bright points and magnetic structures to clarify conditions, which make magnetic structures bright in G-band. The G-band filtergrams together with magnetograms and dopplergrams were taken for a plage region covered by abnormal granules as well as ubiquitous G-band bright points, using the Swedish 1-m Solar Telescope (SST) under very good seeing conditions. High magnetic flux density regions are not necessarily associated with G-band bright points. We refer to the observed extended areas with high magnetic flux density as magnetic islands to separate them from magnetic elements. We discover that G-band bright points tend to be located near the boundary of such magnetic islands. The concentration of G-band bright points decreases with inward distance from the boundar...

160

Nano-aggregates of hexacyanoferrate (II)-loaded magnetite for removal of cesium from radioactive wastes  

Nano-sized magnetic sorbents can be promising candidate materials for treatment of low-level effluents resulting in effective decontamination and very high volume reduction of radioactive wastes. Preparation of magnetite-hexacyanoferrate composite was based upon wet-dispersion and in situ precipitation for synthesizing coatings on magnetite. Superior magnetic properties were rendered to potassium nickel (II) hexacyanoferrate (II), a sorbent with high specificity for cesium uptake, by loading to magnetite. The magnetic complex showed same apparent sorption capability for cesium as potassium nickel (II) hexacyanoferrate (II). Transmission electron microscope revealed a particle size distribution of 8-30 nm for these magnetic particles. Large moment possessed by particles was responsible for high uptake of magnetic separator column at low background magnetic field. Low residual magnetism favored magnetic filter regeneration parameter requirement.

 
 
 
 
161

Strength and directionality of surface Ruderman–Kittel–Kasuya–Yosida interaction mapped on the atomic scale  

Ruderman–Kittel–Kasuya–Yosida interaction is an indirect magnetic coupling between localized spins in a non-magnetic host mediated by conduction electrons. In diluted systems it is often the dominating magnetic interaction and has played a key part in the development of giant magnetoresistance devices, drives ferromagnetism in heavy rare-earth elements as well as in diluted magnetic semiconductors and gives rise to complex magnetic phases such as spin glasses. For bulk systems, an isotropic and continuous model of Ruderman–Kittel–Kasuya–Yosida interaction is often sufficient. However, it can be misleading in magnetic nanostructures consisting of separate magnetic atoms adsorbed on the surface of a non-magnetic material. Here, an atomically precise map of...

162

Removal of radioactive materials and heavy metals from water using magnetic resin  

Magnetic polymer resins capable of efficient removal of actinides and heavy metals from contaminated water are disclosed together with methods for making, using, and regenerating them. The resins comprise polyamine-epichlorohydrin resin beads with ferrites attached to the surfaces of the beads. Markedly improved water decontamination is demonstrated using these magnetic polymer resins of the invention in the presence of a magnetic field, as compared with water decontamination methods employing ordinary ion exchange resins or ferrites taken separately. 9 figs.

163

Magnetic Composite Nanoparticle of Au/?-Fe2O3 Synthesized by Gamma-Ray Irradiation  

Magnetic composite nanoparticle of Au/?-Fe2O3 was synthesized in an aqueous phase using gamma-ray. Connection between gold and ?-Fe2O3 was confirmed by the magnetic separation technique. TEM observation shows that 5-nm gold particles were dispersed on 20-nm ?-Fe2O3 particles. The nanoparticles adsorbed a water-soluble mercaptan, glutathione, and was manipulated by an external magnetic field.   

164

Magnetic fields near overhead distribution lines; Measurements and estimating technique  

This paper summarizes the measurements and the analysis of magnetic fields in the vicinity of 51 separate overhead distribution lines. Data obtained covered a wide range of loads up to nearly 300 Amps. Results of measurements as well as the correlation between the magnetic field and the phase currents at various distances from the line are discussed. A method of estimating the magnetic field exposure based on the load history of the distribution circuits is presented.

165

The metal-nonmetal transition in ionic liquids  

The metal-nonmetal transition in ionic liquids is reviewed with special emphasis on alkali metal-alkali halide solutions and the ionic alloy Cs-Au. Magnetic measurements, especially nuclear magnetic resonance, are discussed in relation to the nature of localized electronic states at low concentrations of excess metal and electron dynamics in the metal-nonmetal transition region. It is suggested that the stability of non-magnetic species governs the occurrence of a continuous metal-nonmetal transition or, alternatively, liquid-liquid phase separation.

166

MTN magnet for the SPS extracted beam.  

This type of dipole magnet was used in the extracted beam lines of the North Area. It shows an opening for three different proton beam lines: a primary extracted proton beam, split by an upstream magnetic beam splitter (see photo 7612017) into three separated beams passes through different parts of its aperture: right, left up, left down. These magnets were designed to be concrete-insulated for radiation resistance. F. Streun stands on the right.

167

Removal of radioactive materials and heavy metals from water using magnetic resin  

Magnetic polymer resins capable of efficient removal of actinides and heavy metals from contaminated water are disclosed together with methods for making, using, and regenerating them. The resins comprise polyamine-epichlorohydrin resin beads with ferrites attached to the surfaces of the beads. Markedly improved water decontamination is demonstrated using these magnetic polymer resins of the invention in the presence of a magnetic field, as compared with water decontamination methods employing ordinary ion exchange resins or ferrites taken separately.

168

Method for regenerating magnetic polyamine-epichlorohydrin resin  

Magnetic polymer resins capable of efficient removal of actinides and heavy metals from contaminated water are disclosed together with methods for making, using, and regenerating them. The resins comprise polyamine-epichlorohydrin resin beads with ferrites attached to the surfaces of the beads. Markedly improved water decontamination is demonstrated using these magnetic polymer resins of the invention in the presence of a magnetic field, as compared with water decontamination methods employing ordinary ion exchange resins or ferrites taken separately.

169

Interpretation of Magnetic Anomalies and Estimation of Depth of Magnetic Crust in Slovakia  

The magnetic map of Slovakia used in the paper was compiled as part of a project titled Atlas of Geophysical maps and profiles in 2001. The residual magnetic data were analyzed to produce Curie point estimates. To remove distortion of magnetic anomalies caused by the Earth’s magnetic field, reduction to pole transformation was applied to the magnetic anomalies using the magnetization angle of the induced magnetization. Anomalies reduced to the pole tend to be better correlated with tectonic structures. We applied a 3-km upward continuation to the residually compiled magnetic anomalies in order to remove effects of topography. The depth of magnetic dipoles was calculated by an azimuthally averaged power spectrum method for the entire area. Such estimates can be indicative of temperatures in the crust, since magnetic minerals lose their spontaneous magnetization according to Curie temperature of the dominant magnetic minerals in the rocks. The computed Curie point depths in the Slovakia region vary between 15.2 km and 20.9 km. Heat flow higher than 100 mWm-2 occurs at the central volcanics and eastern part of Slovakia, where the Curie point depths values are shallow. The correlation between Curie point depths, heat flow and crust depth was investigated for two E-W cross sections. Heat flow and Curie point depth values are correlated with each other however, these values could not be correlated with crust depth. The Curie point isotherm, which separates magnetic and non-magnetic parts of the crust, is represented in two cross sections.

170

RF-tests on deflecting cavities for a superconducting particle separator  

A superconducting S-band RF particle separator is under construction which will be used at the CERN 300 GeV proton synchrotron. It is foreseen to separate particles up to at least 30 GeV/c momentum. A summary of quality factors- (Q) and peak magnetic field (H/sub p/) measurements on several test-deflectors is given. (14 refs).

171

Importance of Coulomb Corrections In Extraction of the Proton Form Factors  

Results of recent polarization transfer experiments indicate that the ratio of the proton's electric to magnetic form factor decreases with increasing momentum transfer, yet the polarization transfer results are in sharp disagreement with the many Rosenbluth separation results. In this paper, it will be shown that the inclusion of a Coulomb correction to the Rosenbluth separation data slightly reduces this discrepancy.

172

Role of centrifugal and ion mechanisms of separation in a plasma centrifuge with crossed fields  

Calculation of element separation coefficients in crossed electrical and magnetic fields in gaseous mixtures are presented. Initial kinetic equations have been derived; the contribution of centrifugal and ion mechanisms determining the mass separation effect in slightly ionized plasma under the above conditions has been analyzed.

173

Mass separation in a rotating weakly ionized plasma  

A study is made of the processes responsible for the spatial separation by mass in a weakly ionized plasma in a radial electric field crossed with a longitudinal magnetic field. The separation processes associated with cataphoresis and with transfer of radial momentum from ions to the neutral particles are studied for the case of unmagnetized ions.

174

A PRACTICAL PROCESS FOR THE SEPARATION OF MONAZITE AND ASSOCIATED MINERALS FROM LOW GRADE ORES  

A process is presented for the separation of monazite sands from magnetite, eliminite, zircon, and other heavy minerals by using electrostatic and magnetic separators alternatively. Wilfley tables were used for the complete removal of siliceous sand as a preliminary treatment. (W.L.H.)

175

The ISOLDE on-line isotope separator at the 600 MeV Synchro-Cyclotron  

Is at present being thoroughly modified and improved, in order to allow for the increased proton beam intensities, resulting from the SC improvement programme. This photograph, taken before the dismantinling of the facility in June 1973, shows the separator analysing magnet (centre background), the collector chamber of the mass-separated ion.

176

Preliminary Design of the Vacuum System for FAIR Super FRS Quadrupole Magnet Cryostat  

The Super-Conducting Fragment Separator (Super FRS) of the Facility for Antiproton and Ion Research (FAIR) at GSI Darmstadt is a large-acceptance superonducting fragment separator. The separator consists of large dipole, quadrupole and hexapole superconducting magnets. The long quadrupole magnet cryostat houses the helium chamber, which has the magnet iron and NbTi superconducting coil. The magnet weighs about 30 tons. The helium chamber is enclosed in vacuum inside the magnet cryostat. Multilayer Insulation (MLI) will be wrapped around the thermal shield to reduce radiation loss. Polyster of MLI comprises the major component responsible for outgassing. In order to reduce outgassing, pumping at elevated temperatures has to be carried out. In view of the large size and weight of the magnet, a seal off approach might not be operationally feasible. Continuous pumping of the cryostat has also been examined. Pump has been kept at a distance from the magnet considering the effect of stray magnetic fields. Oil free turbo molecular pump and scroll pump combination will be used to pump down the cryostat. The ultimate heat load of the cryostat will be highly dependent on the pressure attained. Radiation and conduction plays an important role in the heat transfer at low temperatures. This paper presents the vacuum design of the long quadrupole magnet cryostat and estimates the heat load of the cryostat.

177

Traveling wave magnetophoresis for high resolution chip based separations.  

A new mode of magnetophoresis is described that is capable of separating micron-sized superparamagnetic beads from complex mixtures with high sensitivity to their size and magnetic moment. This separation technique employs a translating periodic potential energy landscape to transport magnetic beads horizontally across a substrate. The potential energy landscape is created by superimposing an external, rotating magnetic field on top of the local fixed magnetic field distribution near a periodic arrangement of micro-magnets. At low driving frequencies of the external field rotation, the beads become locked into the potential energy landscape and move at the same velocity as the traveling magnetic field wave. At frequencies above a critical threshold, defined by the bead's hydrodynamic drag and magnetic moment, the motion of a specific population of magnetic beads becomes uncoupled from the potential energy landscape and its magnetophoretic mobility is dramatically reduced. By exploiting this frequency dependence, highly efficient separation of magnetic beads has been achieved, based on fractional differences in bead diameter and/or their specific attachment to two microorganisms, i.e., B. globigii and S. cerevisiae. PMID:18030387

178

Normal Conducting Separation Dipoles For The Lhc Beam Cleaning Insertions  

In the Large Hadron Collider (LHC), two straight sections, IR3 and IR7, will be dedicated to beam cleaning [1]. These cleaning insertions will be equipped with normal conducting magnets. MBW magnets are dipole magnets used to increase the separation of the two beams. They have a core length of 3.4 m and a gap height of 52 mm and will operate at a magnetic field ranging from 0.09 T to 1.53 T. Limitations on the dimensions and total weight of the magnet resulted in a special design with a common yoke for the two beams. The orbits of the two beams will be separated horizontally by a distance between 194 mm and 224 mm in the gap of the magnet. The magnet was designed in collaboration between CERN and BINP. The report presents the main design issues and results of the pre-series acceptance tests including mechanical, electrical and magnetic field measurements. Index terms - LHC, normal conducting magnet, twin aperture design, separation dipole

179

Production of short lived radioactive beams of radium  

Short lived $^{212,213,214}$Ra isotopes have been produced at the TRI$\\mu$P facility in inverse kinematics via the fusion-evaporation reaction $^{206}$Pb+$^{12}$C at 8 MeV/u. Isotopes are separated from other reaction products online using the TRI$\\mu$P magnetic separator. The energetic radium (Ra) isotopes at the exit of the separator were converted into low energy ions with a thermal ionizer. Ra isotopes have been identified by observing their $\\alpha$ decay and life times.

180

Ultrasonication-assisted synthesis of molecularly imprinted polymer-encapsulated magnetic nanoparticles for rapid and selective removal of 17-estradiol from aqueous environment  

Abstract Molecularly imprinting technique was combined with magnetic nanoparticles to synthesize molecularly imprinted polymer-encapsulated particles for selective removal and efficient separation of estrogenic compounds from water. The core-shell-structured particles were successfully prepared by a novel 2-h ultrasonication-assisted synthesis in a mixture of water and organic solvent using dual-layer surfactant-modified magnetic particles as core, the most physiologically active estrogenic compound (17-estradiol) as template, and widely adapted methacrylic acid as functional monomer. Ultraviolet-visible spectroscopy, Fourier transform infrared spectroscopy, scanning electron microscopy, and magnetic separation were used to characterize the particles. High-performance liquid chromatography...

 
 
 
 
181

Application of derivatized magnetic materials to the separation and the preconcentration of pollutants in water samples  

Monitoring pollutants in water samples is a challenge to analysts. In recent years, separation technology based on magnetic materials has received considerable attention. This article reviews the literature dealing with the application of magnetic materials, combined with other materials (e.g., silica, octadecylsilane, polymers and surfactants), to the separation and the preconcentration of pollutants in water samples. The magnetic extraction method is not only convenient, economical and highly efficient, but it also overcomes problems with conventional solid-phase extraction, (e.g., packing of sorbent into the column and time-consuming loading of large-volume samples).

182

Continuous-flow ferrohydrodynamic sorting of particles and cells in microfluidic devices  

A new sorting scheme based on ferrofluid hydrodynamics (ferrohydrodynamics) was used to separate mixtures of particles and live cells simultaneously. Two species of cells, including Escherichia coli and Saccharomyces cerevisiae, as well as fluorescent polystyrene microparticles were studied for their sorting throughput and efficiency. Ferrofluids are stable magnetic nanoparticles suspensions. Under external magnetic field gradients, magnetic buoyancy forces exerted on particles and cells lead to size-dependent deflections from their laminar flow paths and result in spatial separation. We report the design, modeling, fabrication and characterization of the sorting device. This scheme is simple, low-cost and label-free compared to other existing techniques.

183

Microfluidic Device for Continuous Magnetophoretic Separation of Red Blood Cells  

This paper presents a microfluidic device for magnetophoretic separation red blood cells from blood under contionous flow. The separation method consist of continous flow of a blood sample (diluted in PBS) through a microfluidic channel which presents on the bottom "dots" of feromagnetic layer. By appling a magnetic field perpendicular on the flowing direction, the feromagnetic "dots" generates a gradient of magnetic field which amplifies the magnetic force. As a result, the red blood cells are captured on the bottom of the microfluidic channel while the rest of the blood is collected at the outlet. Experimental results show that an average of 95 % of red blood cells are trapped in the device

184

Magnetic Phase transitions in Plasmas and Transport Barriers  

A model of magnetic phase transitions in plasmas is presented: plasma blobs with pressure excess or defect are magnetised and will move radially under the influence of the background plasma magnetisation. It is found that magnetic phase separation could be the underlying mechanism of L to H transitions and transport barrier formation. Magnetic phase separation and associated pedestal build up can be driven by the well known interchange mechanism, now reinterpreted as a magnetisation interchange which remains relevant even when stable or saturated. A testable necessary criterion for the L to H transition is presented.

185

Device for continuous extracorporeal blood purification using target-specific metal nanomagnets  

Background. The present work illustrates how magnetic separation-based blood purification using ultra-strong iron nanomagnets can be implemented into an extracorporeal blood purification circuit. By this promising technique, today's blood purification may be extended to specifically filter high-molecular compounds without being limited by filter cut-offs or column surface saturation. Methods. Blood spiked with digoxin (small molecule drug) and interleukin-1b (inflammatory protein) was circulated ex vivo through a device composed of approved blood transfusion lines. Target-specific nanomagnets were continuously injected and subsequently recovered with the aid of a magnetic separator before recirculating the blood. Results. Magnetic blood purification was successfully carried out under flow ...

186

Stability of Einstein-Yang-Mills monopoles and dyons  

The stabilities of Yang-Mills magnetic and Coulomb charges have been studied separately before, without laying much emphasis on the singular nature of the effective potential in the resulting radial equation. We investigate an analysis that is valid simultaneously for both Yang-Mills magnetic monopoles and dyons in flat as well as curved spacetime. We find the instability modes with their qualitative behaviour determined completely by the large distance behaviour of the radial equation. One of the results for the dyon is that we could get unstable modes even if there were no such modes for the constituent Yang-Mills ''electric'' and ''magnetic'' charges separately.

187

A new way of utilizing pole face windings and magnetic field corrections for independent tuning of betatron wave numbers and chromaticities in the CERN Proton Synchrotron  

Precise control of the quadrupole and sextupole components of the magnetic fields in focusing and defocusing sectors respectively was achieved by the combined use of pole-face and yoke windings with three separate power supplies synchronously programmed by a computer. Experience of this technique led to a new philosophy in the design of pole-face windings, in which they become an integral and active part of the magnet. With the arrangement described, focusing and guiding functions are partially separated and an old combined-function accelerator can be transformed effectively into a more flexible separate-function machine without any decrease in available straight- section space. (5 refs).

188

Use of high-gradient magnetic fields for the separation of macromolecules  

High gradient magnetic field separation (HGMS) has been used to separate several types of > 1 ..mu..m sized ferro- or paramagnetic particles from bulk streams. The majority of the studies have been carried out using a single ferromagnetic wire or wire mesh to produce the field gradients necessary for particle capture. The purpose of this paper is to examine the possibility of using HGMS on < 1 ..mu..m entities for the purpose of macromolecular separations. Preliminary experimental results demonstrate that HGMS techniques can be used to capture 0.1 ..mu..M diam latex beads from a paramagnetic salt solution passing through a columnar bed of ferro-magnetic spheres.

189

Use of high-gradient magnetic fields for the separation of macromolecules  

High gradient magnetic field separation (HGMS) has been used to separate several types of > 1 ..mu..m sized ferro- or paramagnetic particles from bulk streams. The majority of the studies have been carried out using a single ferromagnetic wire or wire mesh to produce the field gradients necessary for particle capture. The purpose of this paper is to examine the possibility of using HGMS on < 1 ..mu..m entities for the purpose of macromolecular separations. Preliminary experimental results demonstrate that HGMS techniques can be used to capture 0.1 ..mu..m diam latex beads from a paramagnetic salt solution passing through a columnar bed of ferro- magnetic spheres. 10 refs., 3 figs.

190

Phase separation and magnetic properties in Gd-(Hf,Ti,Y)-Co-Al metallic glasses  

The phase-separation behavior of the Gd-(Hf,Ti,Y)-Co-Al system has been investigated. The Gd-(Hf,Ti)-Co-Al system undergoes liquid-liquid phase separation during quenching and solidifies into either a Gd-rich phase or a Hf-rich phase (or a TiCo crystalline phase) while the Gd-Y-Co-Al alloy forms a monolithic amorphous state. To investigate the influences of the feature of phase separation and the role of alloying elements on the magnetic properties, the temperature and field dependence of magnetization have also been measured.

191

Aligning effect of magnetic field on PDLC films during the phase separation  

The results ofthe study ofthe uniaxially oriented PDLC films prepared by solvent induced phase separation (SIPS) method are presented. The samples were obtained applying a longitudinal magnetic field while the phase separation of the liquid crystal and polymer occurs due to the evaporation of common solvent from the uniform solution. In the presence of magnetic field the nematic liquid crystals 4-n-pentyl-4' -cyanophenylcyclohexane (5PCH), the 4-n-pentyl-4'- cyanobiphenyl (SCB) and nematic mixture LN-394 form the separate droplets in polyvinylbutyral (PVB) matrix. At that, the nematics 5PCH and LN-394 form always the stable bipolar structures with the order parameter of the droplet axes depending on the value of the applied field. In 5CB droplets the bipolar structure is realized only in a weak magnetic field and the radial one is formed in a strong magnetic field. At intermediate field the non-equilibrium structures are appeared that are characterized by the flickering textures.

192

Magnetisation effects of multicore magnetite nanoparticles crystallised from a silicate glass  

Magnetic multicore nanoparticles were produced by crystallisation of a glass with the composition Na2O?Al2O3?B2O3?SiO2?Fe2O3. During cooling of the melt, in a first step, phase separation occurred and droplets enriched in boron and iron oxide were formed. These droplets crystallised spontaneously during cooling. The phase-separated droplets had sizes in the range from 200 to 800?nm. Inside the droplets, magnetite crystals with a mean size of 33?nm occurred. Magnetometer measurements showed the occurrence of a small hysteresis which indicates predominantly superparamagnetic behaviour of the magnetite crystals. The magnetic domains of the phase-separated droplets were studied by magnetic force microscopy. In this article, a glass which is exposed to a magnetic field shows droplet-shape phase...

193

Coal preparation using magnetic separation. Volume 2. Final report  

Wet magnetic separation tests have been performed on two coals (Eastern Associated Delmont coal and Old Ben coal) using a superconducting magnet. Pyritic sulfur reductions in excess of 86% were achieved for both coals with corresponding yields of 60% by weight of clean coal product. Ash reductions in the range from 60 to 80% were also obtained. These results were obtained with flow velocities ranging from 1 to 4 cm/sec, slurry concentrations between 10 and 33% and magnetic field strengths of 20 and 50 kilogauss with a stainless steel wool matrix for generating high gradients. A conceptual design for a 110 ton/h superconducting magnetic separator is presented. Capital cost for the equipment for this separator is estimated to be $600,000.

194

Precise measurement of remanent magnetism of rocks under non-magnetic fields; Mujikaika deno ganseki zanryu jiki no seimitsu sokutei  

Various magnetic information data from solidification or deposition up to date are contained in rocks. For the analysis of remanent magnetism, in general, the stable thermal remanent magnetization and the secondary magnetization are separately evaluated using vector variations determined by the location changes of magnetic pole from ac demagnetization or thermal demagnetization. Especially, in geothermal fields, the remanent magnetism in rocks is complicated due to the predominant alteration. When the remanent magnetism of rocks can be precisely measured and the primary and secondary magnetization can be evaluated, important data can be obtained, which represent oriented core samples required for evaluating the geothermal reservoirs. A rock remanent magnetism measuring system using superconductive magnetic shield has been developed, to evaluate the location of magnetic pole. This system can distinguish the remanent magnetization in rocks, and can be applied to the remanent magnetism in rocks in which the location of dipole model is shifted from the center of core. Important basic data of orientation information in rocks can be provided. 6 figs.

195

Development of water-bloom removal system by using a superconductive magnetic separation technique; Chodendo jiki bunri gijutsu ni yoru aoko jokyo sochi no kaihatsu  

Purification techniques are expected to be developed in order to remove a huge amount of water-bloom at high speed, which is a kind of plankton generated in summer due to the eutrophication of lakes and marshes. This paper describes a newly developed water-bloom removal system by means of a magnetic separation technique utilizing superconductivity. Magnetic powders and flocculants are mixed and agitated in the raw water for several minutes, to form floc. Since the magnetic powders are mixed in the floc, the floc is sucked and separated at the magnetic filter by injecting this pre-treated water into the magnetic separator. Thus, purified water is drained. The trial system is wholly cooled through the conduction by cooling an edge of superconductive magnet with the very low temperature gas of a small helium refrigerator. The intensity of magnetic field is 1 tesla, and the demand is 7 kW. Purification tests were conducted using water-bloom raw water of the Kasumigaura, collected in summer, 1995. As a result, it was confirmed that 95% of the water-bloom can be separated and removed at a high speed. This system has a small size and can be mounted on a vehicle. 2 refs., 4 figs., 2 tabs.

196

A PURPOSE ORIENTED MAGNETIC SEPARATOR: SKIMMER  

A magnetic separator was designed to selectively separate fine-liberated magnetite. The conceptual design was simulated using CFD techniques. A separator tank was fabricated and a magnetic drum was used to capture magnetic particles. The initial tank design was modified to eliminate application oriented problems. The new separator was able to produce a fine product as a concentrate at relatively high feed rates. A plant simulation showed that such a device could lower circulating loads around ball mills by 16%, thereby creating room for a 5-8% increase in throughput at the same energy level. However, it was concluded that further improvements in terms of both size and mineral selectivity are needed to have a marketable product.

197

Integrating flotation to improve the performance of an HMC circuit treating a low-rank fine coal  

One reason that heavy media cyclone (HMC) circuits suffer from the inadvertent loss of magnetite and fine coal is the presence of nonmagnetic material in the magnetic separator feed. In this study, flotation was applied to the undersize fractions of the HMC drain-and-rinse screens to minimize these problems. These fractions, which contain 17.9% nonmagnetic material, are currently sent to magnetic separators and the nonmagnetic portion from the separators contains 39.1% ash. Applying flotation resulted in a clean coal product with an ash content of 8.7% and a calorific value of 6,300 kcal/kg. The refuse from flotation, which will be sent to the magnetic separators, contains 7.7% nonmagnetics.

198

Magnetic force control technique in industrial application  

Techniques of the magnetic force control have been examined for industrial application. The problems and the technique are different in dispersion medium of gas and that of liquid. In addition, the method is different depending on the magnetic characteristic of the target objects. In case of the liquid, the dispersion medium having different viscosity was examined. The separation speed is decided with the magnitude of the magnetic force because a drag force increases with the viscosity. When the water is the dispersion medium, magnetic seeding is possible and hence the nonmagnetic materials can be separated and even the dissolved material could be separated. The separation technique has been used for purifying the waste water form paper mill or wash water of drum. On the other hand when the water is not dispersion medium, mainly the ferromagnetism particle becomes the target object because the magnetic seeding becomes difficult. The iron fragments have been separated from the slurry of slicing machine of solar battery. It has been clarified high gradient magnetic separation (HGMS) can be applied for the viscous fluid of which viscosity was as high as 10 Pa s. When the dispersion medium is gaseous material, the air is important. The drag force from air depends greatly on Reynolds number. When speed of the air is small, the Reynolds number is small, and the drag force is calculated by the Stokes' law of resistance. The study with gaseous dispersion medium is not carried out much. The magnetic separation will discuss the possibility of the industrial application of this technique.

199

Magnetic force control technique in industrial application  

Techniques of the magnetic force control have been examined for industrial application. The problems and the technique are different in dispersion medium of gas and that of liquid. In addition, the method is different depending on the magnetic characteristic of the target objects. In case of the liquid, the dispersion medium having different viscosity was examined. The separation speed is decided with the magnitude of the magnetic force because a drag force increases with the viscosity. When the water is the dispersion medium, magnetic seeding is possible and hence the nonmagnetic materials can be separated and even the dissolved material could be separated. The separation technique has been used for purifying the waste water form paper mill or wash water of drum. On the other hand when the water is not dispersion medium, mainly the ferromagnetism particle becomes the target object because the magnetic seeding becomes difficult. The iron fragments have been separated from the slurry of slicing machine of solar battery. It has been clarified high gradient magnetic separation (HGMS) can be applied for the viscous fluid of which viscosity was as high as 10 Pa s. When the dispersion medium is gaseous material, the air is important. The drag force from air depends greatly on Reynolds number. When speed of the air is small, the Reynolds number is small, and the drag force is calculated by the Stokes’ law of resistance. The study with gaseous dispersion medium is not carried out much. The magnetic separation will discuss the possibility of the industrial application of this technique.

200

Study on control method of running velocity for the permanent magnet-HTSC hybrid magnetically levitated conveyance system  

We have developed the magnetically levitated carrying system. In this system, pinning force of high temperature bulk super conductor (HTSC) is used for the levitation and guidance. Four HTSCs are installed on the carrier. The magnetic rail is set on the ground, and flux from the magnetic rail is pinned by HTSCs. To increase levitation force, repulsive force of the permanent magnet is used. The hybrid levitation system is composed. The permanent magnet is installed under the load stage of the carrier. Repulsive force by the permanent magnet between the load stage on the carrier and the magnetic rail on the ground is used to support the load weight. Levitation and guidance one by pinning effect of the YBaCuO HTSC in the carrier is used to levitate the carrier body. The load stage is separate...

 
 
 
 
201

Purification of condenser water in thermal power station by superconducting magnetic separation  

Thermal power station is made up of a steam turbine and a steam condenser which need a lot of water. The water of steam condenser should be replaced, since scales consisting of iron oxide mainly are accumulated on the surface of condenser pipes as it goes. Superconducting high gradient magnetic separation (HGMS) system has merits to remove paramagnetic substance like iron oxides because it can generate higher magnetic field strength than electromagnet or permanent magnet. In this paper, cryo-cooled Nb-Ti superconducting magnet that can generate up to 6T was used for HGMS systems. Magnetic filters were designed by the analysis of magnetic field distribution at superconducting magnets. The result of X-ray analysis showed contaminants were mostly a-Fe2O3 (hematite) and g-Fe2O3 (maghemite). Th...

202

Magnetic-field-induced supercurrent enhancement in hybrid superconductor/magnetic metal structures  

The dc transport properties of the (S/M)I(M/S) tunnel structure - proximity coupled superconductor (S) and magnetic (M) layers separated by an insulator (I) - in a parallel magnetic field have been investigated. We choose for the M metal the one in which the effective magnetic interaction, whether it arises from direct exchange interaction or due to configuration mixing, aligns spins of the conducting electrons antiparallel to the localized spins of magnetic ions. For tunnel structures under consideration, we predict that there are the conditions when the destructive action of the internal and applied magnetic fields on Cooper pairs is weakened and the increase of the applied magnetic field causes the field-induced enhancement of the tunnel critical current. The experimental realization of the novel interesting effect of the interplay between superconducting and magnetic orders is also discussed.

203

Characterization of domain wall-based traps for magnetic beads separation  

We characterize the magnetic behavior of an array of magnetic bead traps based on domain walls (DWs) formed in zig-zag permalloy wires patterned on a Si substrate. Using magnetic force and magneto-optical Kerr effect microscopy, we study the nucleation and annihilation of DWs for two different wire widths. Through scanning electron microscopy with polarization analysis, we analyze in detail the magnetization configuration of the DWs in the presence of a magnetic bead previously trapped by the DW stray field. Finally, we patterned the magnetic nanostructures directly on a polydimethylsiloxane (PDMS) substrate, and we show that the functionality of the device is completely maintained. These results pave the way to the integration of DW-based devices in a PDMS lab-on-a-chip system for magnetic bead separation.

204

Superconducting phase diagram of NaxCoO2.yH2O  

We synthesized Nax(H3O)zCoO2yH2O samples with various Na/H3O ratios but with the constant Co valence of s = +3.40, and measured their magnetic properties to draw phase diagrams of the system. The superconductivity is very sensitive to the Na/H3O ratio. With varying x under fixed s of +3.40, magnetically ordered phase appears in the intermediate range of x sandwiched by two separated superconducting phases, suggesting that the superconductivity is induced by moderately strong magnetic interactions. In the vicinity of the magnetic phase, transition from the superconducting state to the magnetically ordered state was induced by applying high magnetic field. This transition is of the second order, at least, above 1.8 K. The upper-critical field is expected to be much higher than the Pauli limit for a phase located far away from the magnetic phase regarding the Na/H3O ratio.

205

Magnetically induced separation of stable emulsions  

Experiments were conducted to demonstrate the feasibility of recovering oil from fine, stable oil-in- water emulsions by magnetic means. Emulsions in which the oil phase was rendered magnetically responsive by the addition of a ferrofluid were passed through packed beds (containing magnetic particles and/or screens) placed in a magnetic field. The oil content of the effluent stream was typically 2 to 3 orders of magnitude lower than the oil content of the feed emulsion. The influence of various operating parameters including bed height, flow rate, oil magnetization, and magnetic field strength were systematically evaluated. The results demonstrated that it is possible to attain virtually complete removal of particles of the order of one micron in diameter with a static separation device (magnetic demulsifier) using residence times of the order of a fraction of a minute.

206

Continuous Magnetophoretic Separation of Blood Cells from Plasma at the Microscale  

We present a method for the direct and continuous separation of red and white blood cells from plasma at the microscale. The method is implemented in a microfluidic system with magnetic functionality. The fluidic structure within the microsystem consists of an inlet and a single microfluidic channel with multiple outlets. The magnetic functionality is provided by an array of integrated soft-magnetic elements that are embedded transverse and adjacent to the microchannel. The elements are magnetized using an external field, and once magnetized they produce a magnetic force on blood cells as they flow through the microchannel. In whole blood, white blood cells (WBCs) behave as diamagnetic microparticles, while red blood cells (RBCs) exhibit diamagnetic or paramagnetic behavior depending on the oxygenation of their hemoglobin. We study the motion of blood cells through the microchannel using a mathematical model that takes into account the magnetic, fluidic and gravitational forces on the cells. We use the model ...

207

Out-of-plane magnetization reversal processes of (Ga,Mn)As with two different hole concentrations  

We study magnetization reversal processes of in-plane magnetized (Ga,Mn)As epilayers with different hole concentrations in out-of-plane magnetic fields using magnetotransport measurements. A clear difference in the magnetization process is found in two separate samples with hole concentrations of 10^20 cm^-3 and 10^21 cm^-3 as the magnetization rotates from the out-of-plane saturation to the in-plane remanence. Magnetization switching process from the in-plane remanence to the out-of-plane direction, on the other hand, shows no hole concentration dependence, where the switching process occurs via domain wall propagation. We show that the balance of cubic magnetocrystalline anisotropy and uniaxial [110] anisotropy gives an understanding of the difference in the out-of-plane magnetization processes of (Ga,Mn)As epilayers.

208

Novel magnetic cross-linked enzyme aggregates (magnetic CLEAs) of alpha amylase  

Novel magnetic cross-linked enzyme aggregates of alpha amylase were prepared by chemical cross-linking of enzyme aggregates with amino functionalized magnetite nanoparticles which can be separated from reaction mixture using magnetic field. Of the initially applied alpha amylase activity 100% was recovered in magnetic CLEAs, whereas only 45% was recovered in CLEAs due to the low content of Lys residues in alpha amylase. Scanning electron microscopy analysis showed that CLEAs and magnetic CLEAs were spherical structures. The CLEAs and magnetic CLEAs displayed a shift in optimal pH towards the acidic side, whereas optimal temperature of magnetic CLEAs was improved compared to free enzyme and CLEAs. Although Vmax of enzyme in CLEAs and magnetic CLEAs did not change, substrate affinity of the ...

209

Photo-electric conversion system and its production method; Koden henkan sochi to sono seizo hoho  

This invention provides a photo-electric conversion system which is able to supply the energy to the system such as micromachine requiring the electric energy without employing any electric wire. The system consists of magnetic core member and coil of primary coil side of thin film laminate transformer composing of photo-electric conversion system made on separate substrates, and magnetic core member and coil of secondary coil side. Both magnetic core members face to each other closely to construct the common magnetic core in which the magnetic fluxes are chain-crossed. By combining magnetically the first coil and the second coil through the above-said magnetic coil, the integrated circuit driven by the output of the thin film laminate transformer and driving member such as actuator or sensor can be constructed. As a result, a compact and multi-functional micromachine can be realized. 5 figs.

210

Removal of less biodegradable dissolved organic matters in water by superconducting magnetic separation with magnetic mesoporous carbon  

Less biodegradable dissolved organic matters in water as typified by humic substances are known as precursors of carcinogenic trihalomethanes, and are removed about 60% by current advanced water treatments. However, further increase of the removal ratio is demand. In this study, magnetic mesoporous carbon (MMPC), which can adsorb the substances physically and be efficiently collected by using superconducting high gradient magnetic separation (HGMS), has been synthesized with coconut-shell-based activated carbon and ferric nitrate solution by the gas activation method. The MMPC has the maximum magnetization value of 30.7emu/g and an adsorption ability of 87% to 10mg/L humic acid in a short time. The standard MMPC having a magnetization of 6.43emu/g was able to be separated at magnetic field...

211

Surface magnetic enhancement for coal cleaning. Quarterly technical progress report no. 7, August 1--October 31, 1989  

The fundamental chemistry for selective adsorption of magnetizing reagent on coal-associated minerals to enhance the magnetic susceptibilities of minerals have been established in Phase I study. The application of the results on coal cleaning is in progress in the Phase II study. Illinois No. 6, Ohio Lower Kittanning, and West Virginia Pocahontas coals have been prepared(simulating the industrial operations) and characterized. The adsorption conditions for {minus}48 mesh ROM coals and flotation concentrates have been optimized. Magnetic separation of the reagent conditioned coals shows that both ash and pyritic sulfur can be significantly reduced. Comparing with the repeated flotation approach for coal cleaning, the magnetizing reagent enhanced magnetic separation method shows better performance on cleaning the flotation concentration at {minus}48 mesh.

212

Surface magnetic enhancement for coal cleaning  

The fundamental chemistry for selective adsorption of magnetizing reagent on coal-associated minerals to enhance the magnetic susceptibilities of minerals have been established in Phase I study. The application of the results on coal cleaning is in progress in the Phase II study. Illinois No. 6, Ohio Lower Kittanning, and West Virginia Pocahontas coals have been prepared(simulating the industrial operations) and characterized. The adsorption conditions for {minus}48 mesh ROM coals and flotation concentrates have been optimized. Magnetic separation of the reagent conditioned coals shows that both ash and pyritic sulfur can be significantly reduced. Comparing with the repeated flotation approach for coal cleaning, the magnetizing reagent enhanced magnetic separation method shows better performance on cleaning the flotation concentration at {minus}48 mesh.

213

170 Nanometer Nuclear Magnetic Resonance Imaging using Magnetic Resonance Force Microscopy  

We demonstrate one-dimensional nuclear magnetic resonance imaging of the semiconductor GaAs with 170 nanometer slice separation and resolve two regions of reduced nuclear spin polarization density separated by only 500 nanometers. This is achieved by force detection of the magnetic resonance, Magnetic Resonance Force Microscopy (MRFM), in combination with optical pumping to increase the nuclear spin polarization. Optical pumping of the GaAs creates spin polarization up to 12 times larger than the thermal nuclear spin polarization at 5 K and 4 T. The experiment is sensitive to sample volumes containing $\\sim 4 \\times 10^{11}$ $^{71}$Ga$/\\sqrt{Hz}$. These results demonstrate the ability of force-detected magnetic resonance to apply magnetic resonance imaging to semiconductor devices and other nanostructures.

214

Study of magnetic moments of nuclear excited states at TRISTAN  

Measurement of the static magnetic dipole moments of nuclear excited states are of interest since they reveal information on nuclear structure not available by other means. A system has been constructed at the TRISTAN separator to measure magnetic dipole moments of excited states in neutron-rich nuclei using the method of perturbed angular correlations (PAC). High magnetic fields are not available through the use of a superconducting magnet. The capability of the TRISTAN system is discussed and the PAC measuring apparatus is described. Final results from recent g factor measurements at TRISTAN on 4/sup +/ states in the N = 82 isotones are discussed in some detail. Studies in progress are briefly outlined.

215

Rapid magnetic flux variability on the flare star CN Leonis  

We present UVES/VLT observations of the nearby flare star CN Leo covering the Wing-Ford FeH band near 1mu with high spectral resolution. Some of the FeH absorption lines in this band are magnetically sensitive and allow a measurement of the mean magnetic flux on CN Leo. Our observations, covering three nights separated by 48 hours each, allow a clear detection of a mean magnetic field of Bf~2.2kG. The differential flux measurements show a night-to-night variability with extremely high significance. Finally, our data strongly suggest magnetic flux variability on time scales as low as 6 hours in line with chromospheric variability.

216

Effects of the randomly distributed magnetic field on the phase diagrams of Ising nanowire I: Discrete distributions  

The effect of the random magnetic field distribution on the phase diagrams and ground state magnetizations of Ising nanowire is investigated using effective field theory with correlations. Trimodal distribution has been chosen as a random magnetic field distribution. The variation of the phase diagrams with that distribution parameters has been obtained and some interesting results have been found such as reentrant behavior and first order transitions. Also for the trimodal distribution, ground state magnetizations for different distribution parameters have been determined which can be regarded as separate partially ordered phases of the system.

217

Effects of the randomly distributed magnetic field on the phase diagrams of Ising nanowire I: Discrete distributions  

The effect of the random magnetic field distribution on the phase diagrams and ground state magnetizations of Ising nanowire is investigated using effective field theory with correlations. Trimodal distribution has been chosen as a random magnetic field distribution. The variation of the phase diagrams with that distribution parameters has been obtained and some interesting results have been found such as reentrant behavior and first order transitions. Also for the trimodal distribution, ground state magnetizations for different distribution parameters have been determined which can be regarded as separate partially ordered phases of the system.

218

Core-shell and magnetic structure of barium hexaferrite fluids studied by SANS  

We report on small angle neutron scattering measurements with polarised neutrons on ferrofluids (FF) based on barium hexaferrite. The combination of magnetic and isotopic H/D contrast variation of the carrier liquid, dodecane, allows to identify and separate between magnetic and non-magnetic components. In the FF a core-shell structure was found where the shell of surfactants was found to be impenetrable for the carrier liquid. Additionally, magnetic aggregates and isolated surfactant molecules were detected. As results the sizes of the structural parts were given.

219

The creation of a geophysical observatory at the Aleksandrovka research base of the geological faculty of Moscow State University in the Kaluga region  

Since May 2011, long-period magnetotelluric (MT) data have been collected in the non-magnetic pavilion at the geophysical base of Moscow University in the Kaluga Region. The non-magnetic pavilion was constructed in compliance with the following conditions: selection of non-magnetic materials, control of local magnetic field anomalies, and setting the basement for magnetometers separately from the main building. Recording equipment with fluxgate and optomechanical magnetometers with three sets of electric lines with different electrodes was installed. The parallel testing of channels was performed. Currently, the seismo-logical equipment and meteorological station are being prepared for installation.

220

Multipartite Entanglement in a Discrete Magnetic Bands Magnetic Lattice  

Using magneto-optical materials, an asymmetric multi-quantum state magnetic lattice is proposed to host an entangled multipartite system formed by using a quantum degenerate gas of ultracold atoms in a Bose Einstein Condensate (BEC). The discrete magnetic bands magnetic lattice is devised to locate a controllable long-range entanglement of a many harmonic oscillator system well separated in space. The confinement of the coupled magnetic quantum well (CMQW) system may significantly improve the condition for the long-range entanglement of the multipartite (multi-qubits) to be used in quantum information processors.

 
 
 
 
221

Observation of Laser Induced Magnetization Dynamics in Co/Pd Multilayers with Coherent X-ray Scattering  

We report on time-resolved coherent x-ray scattering experiments of laser induced magnetization dynamics in Co/Pd multilayers with a high repetition rate optical pump x-ray probe setup. Starting from a multi-domain ground state, the magnetization is uniformly reduced after excitation by an intense 50 fs laser pulse. Using the normalized time correlation, we study the magnetization recovery on a picosecond timescale. The dynamic scattering intensity is separated into an elastic portion at length scales above 65 nm which retains memory of the initial domain magnetization, and a fluctuating portion at smaller length scales corresponding to domain boundary motion during recovery.

222

Investigation of the process of diamagnetic particle separation in a high-gradient ordered-structure magnetic field  

On the basis of the model of a flow-type magnetic filter with a transversely magnetized ordered system of long ferromagnetic rods of rectangular cross section, the process of high-gradient magnetic separation of microscopic diamagnetic particles (potato starch granules of sizes 8-30 ?m) from a liquid suspension has been investigated. The registered laws of change in the concentration and size distribution of particles at the suspension outlet from the filter agree with the theoretical conclusions obtained from the analysis of the magnetic field structure and thecharacter of the particle motion in the filter volume.

223

Investigation of the process of diamagnetic particle separation in a high-gradient ordered-structure magnetic field  

On the basis of the model of a flow-type magnetic filter with a transversely magnetized ordered system of long ferromagnetic rods of rectangular cross section, the process of high-gradient magnetic separation of microscopic diamagnetic particles (potato starch granules of sizes 8?30 ?m) from a liquid suspension has been investigated. The registered laws of change in the concentration and size distribution of particles at the suspension outlet from the filter agree with the theoretical conclusions obtained from the analysis of the magnetic field structure and thecharacter of the particle motion in the filter volume.

224

Magnetic Field Dependence of Magnetic Clusters in the Random Magnet Fe65(Ni0.78Mn0.22)35  

A neutron scattering study on a concentrated spin-glass alloy Fe65(Ni0.78Mn0.22)35 has been performed under magnetic field. The amplitude of the magnetic diffuse scattering pattern arising from short-range ferromagnetic correlations is markedly reduced by increasing magnetic field. On the other hand, the effect of external field on the diffuse scattering pattern arising from antiferromagnetic short-range correlations is small. These results show that the regions of ferromagnetic and antiferromagnetic short-range correlations (ferromagnetic and antiferromagnetic clusters) coexist separately in this random magnetic material.   

225

Ion acceleration by the space charge electric force arising from the radiation pressure in a magnetized electron-positron plasma  

It is shown that ions can be accelerated by the space charge electric force arising from the separation of electrons and positrons due to the ponderomotive force of the magnetic field-aligned circularly polarized electromagnetic (CPEM) wave in a magnetized electron-positron-ion plasma. The ion acceleration critically depends on the external magnetic field strength. The result is useful in understanding differential ion acceleration in magnetized electron-positron-ion plasmas, such as those in magnetars and in some laboratory experiments that aim to mimic astrophysical environments.

226

Physical separation of useful materials from industrial and municipal wastes; Haikibutsu kara no yuyo busshitsu no bunri kaishu  

This paper introduces a municipal wastes recycling flow proposed by the Aachen Engineering University in Germany referring to technologies to separate and recover useful materials from industrial and municipal wastes and an assembling method of the wastes separation and recovery flows. The flow is targeted to achieve complete recovery of useful materials. Municipal wastes are first sieved and separated from coarse particles. Fine particles which contain organic matters at high rates are utilized as compost materials after having ferrous materials separated by magnetic sorting. Coarse particles are pulverized to sizes smaller than 100 mm, subjected to wind sorting, and separated into: (1) papers, textiles and plastics with low density, (2) organic matters, and (3) organic matters and plastics with high density. The materials in (1) are further treated to make regenerated papers, followed by magnetic sorting to recover ferrous materials. Materials that have not been recovered by the magnetic sorting are sorted into non-ferrous metals, ceramics, stones, and glass materials going through a two-stage dense media separation. Glass materials are separated into colorless and colored glass materials by color sorting. Progress is expected in technologies to separate and recover useful materials from industrial and municipal wastes. 15 refs., 13 figs., 2 tabs.

227

Mechanism of chain formation in nanofluid based MR fluids  

Mechanism of structure formation in bidispersed colloids is important for its physical and optical properties. It is microscopically observed that the mechanism of chain formation in magnetic nanofluid based magnetorheological (MR) fluid is quite different from that in the conventional MR fluid. Under the application of magnetic field the magnetic nanoparticles are filled inside the structural microcavities formed due to the association of large magnetic particles, and some of the magnetic nanoparticles are attached at the end of the chains formed by the large particles. The dipolar energy of the large particles in a magnetic nanofluid matrix becomes effective magnetic permeability ({mu}{sub eff}) times smaller than that of the neutral medium. Inclusion of magnetic nanoparticles ({approx}10 nm) with large magnetic particles ({approx}3-5 {mu}m) restricts the aggregation of large particles, which causes the field induced phase separation in MR fluids. Hence, nanofluid based MR fluids are more stable than conventional MR fluids, which subsequently increase their application potentiality. - Research highlights: In bidispersed magnetic colloids nanoparticles are attached at the end of the chains formed by the large particles. Inclusion of magnetic nanoparticles ({approx}10 nm) with large magnetic particles ({approx}3-5 m) restricts the aggregation of large particles. Nanofluid based MR fluids are more stable than conventional MR fluids.

228

77 FR 11595 - Notice of Buy American Waiver under the American Recovery and Reinvestment Act of 2009  

...of section 1605 of the American Recovery and Reinvestment Act of 2009 (Recovery Act), Public Law 111-5, 123 Stat. 115, 303 (2009), with respect to the purchase of the quiet seawater system balancing valves that will be used in the Alaska...

229

77 FR 11161 - Notice of Buy American Waiver Under the American Recovery and Reinvestment Act of 2009  

...of section 1605 of the American Recovery and Reinvestment Act of 2009 (Recovery Act), Public Law 111-5, 123 Stat. 115, 303 (2009), with respect to the purchase of the propulsion shaft bulkhead seals that will be used in the Alaska Region...

230

77 FR 11163 - Notice of Buy American Waiver Under the American Recovery and Reinvestment Act of 2009  

...of section 1605 of the American Recovery and Reinvestment Act of 2009 (Recovery Act), Public Law 111-5, 123 Stat. 115, 303 (2009), with respect to the purchase of the superior holding power balanced anchors that will be used in the Alaska...

231

75 FR 66760 - Notice of a Regional Waiver of Section 1605 (Buy American Requirement) of the American Recovery...  

...to the City for the purchase and use of four rotary screw air compressors to provide...This action permits the purchase of rotary screw air compressors for Palmer's...Public Law 111-5 for the purchase and use of four rotary screw air compressors...

232

Regular Array of L-Tyrosine Molecules on Si(111)-Au Superstructures  

Studies of adsorption of organic molecules on metal-induced super-reconstructed silicon surfaces are important for future Si-based organic electronic device. We investigated the adsorption dynamics of L-tyrosine on Si-Au surface by in situ reflection high-energy electron diffraction. Si(111)5×2-Au and Si(111) ?3×?3-Au coexisting surface was exposed to L-tyrosine and the intensities of diffraction spots from corresponding domains were monitored. L-tyrosine was found to adsorb onto the Si(111)5×2-Au domains preferentially, while the Si(111) ?3×?3-Au domains were found to be less active. Adsorption sites were revealed by using scanning tunneling microscopy. The molecular adsorption site on the ?3×?3-Au was found to be on domain boundary suggesting that the adsorption probability is small on this domain. On the other hand, the adsorbates ordering in 2.3 unit cell distance along [-110] rows were found to create the similar structure as the Si(111)5×2-Au surface. These results suggest that the Si(111)5×2-Au superstructure can be used for the control of the molecular adsorption geometry and ordering effectively. [DOI: 10.1380/ejssnt.2010.303]   

233

Some effects of chemical irritants on the membrane of the giant amoeba.  

1 The effects of chemical irritants on the membrane potential and input resistance of the giant amoeba, Chaos carolinense, have been investigated. The membrane potential and input resistance were -111.5 mV and 8.6 M pi respectively. 2 In the resting state the cell membrane of Chaos carolinense was f...

234

Orthodontic magnets. A study of force and field pattern, biocompatibility and clinical effects.  

Magnetic forces have been incorporated into orthodontic mechanics during recent years. However, the biocompatibility of magnet alloys and the possible risk of harmful or unusual reactions in tissues exposed to static magnetic fields have been characterized as inconsistent and often contradictory. It has also been questioned whether magnetic forces have significant advantages over traditional mechanics. The present series of studies aimed to analyse the force and field properties, the biocompatibility and the clinical effects of rare earth magnets as well as to compare the efficiency of tooth movement between magnets and another force system. Samarium-cobalt magnets for molar distalization were tested in experimental models for force and field properties. The cytotoxicity of different magnet alloys (rare earth types) as well as of clinically used and recycled magnets was assessed by two in vitro methods, the millipore filter method and an extraction method. The effect of static magnetic fields on human gingival tissue and dental pulp was examined histologically for alterations in cell pattern and cell morphology. The effects of using repelling samarium-cobalt magnets for simultaneous distalization of maxillary first and second molars were analysed in individuals with Class II malocclusion. The efficiency of molar distalization was also intra-individually compared between repelling magnets and superelastic NiTi-coils in individuals with Class II malocclusion and deep bite. The magnet forces decreased approximately with the reciprocal square of the separation distance between the magnets. No fatigue of force over time could be seen. The static magnetic fields were weak and had a limited extent and the flux density dropped exponentially in all directions with increased distance from the magnets, implying a small exposure area when the magnets are used clinically. Rare earth magnets showed good biocompatibility, particularly coated magnets. However, uncoated samarium-cobalt magnets showed significant cytotoxicity. It was also found that stainless-steel-coated samarium-cobalt magnets could be recycled with maintained good biocompatibility. After exposure to static magnetic fields, normal clinical and histological conditions in the human gingival tissue and normal histological features in the human dental pulp were found. Repelling magnets were effective in producing maxillary molar distalization but some side effects like anchorage loss and molar tipping were found. The superelastic coils were shown to be even more efficient than the repelling magnets for maxillary molar distalization in individuals with Class II malocclusion and deep bite. PMID:7801229

235

The performance and on-line monitoring of dense medium wet drum magnetic separators  

Experimental work using a wet drum magnetic separator has shown this piece of equipment to be extremely robust. Magnetic separators tend to be overlooked by both maintenance and metallurgical personnel. They appear to work with no attention other than the occasional shot of grease. In surveys conducted it was commonly observed that the separator physical settings were not as they should have been. Poor performance of wet drum magnetic separators commonly observed in industrial situations is usually due to their being operated well outside their design envelope. This paper briefly describes the pilot plant experimental programme and considers the reasons for the considerably inferior results obtained in the real world. The findings have clearly shown that a device to continually monitor magnetite losses in magnetic separator tailings, either installed permanently as part of the plant instrumentation, or temporarily as a trouble shooting device, would be of considerable value to producers and have motivated the development of the Magnetics Loss Monitor (MLM). The operation of this monitor and the first field trials are also described. (author). 17 figs., 10 refs.

236

First spatial isotopic separation of relativistic uranium projectile fragments  

Spatial isotopic separation of relativistic uranium projectile fragments has been achieved for the first time. The fragments were produced in peripheral nuclear collisions and spatially separated in-flight with the fragment separator FRS at GSI. A two-fold magnetic-rigidity analysis was applied exploiting the atomic energy loss in specially shaped matter placed in the dispersive central focal plane. Systematic investigations with relativistic projectiles ranging from oxygen up to uranium demonstrate that the FRS is a universal and powerful facility for the production and in-flight separation of monoisotopic, exotic secondary beams of all elements up to Z=92. This achievement has opened a new area in heavy-ion research and applications. (orig.)

237

A proof-of-principle experiment of a novel harmonics separation optics for synchrotron facilities.  

A proof-of-principle experiment of a novel harmonics separation optics for synchrotron facilities is presented. The harmonic separator is a Si crystal cut in an inclined geometry in which the impinging beam undergoes a diffractive-refractive effect owing to the dispersive nature of X-ray refraction. A polychromatic beam containing higher-order energies is spatially separated behind the separator into individual monochromatic diffraction spots. A synchrotron experiment at a bending-magnet beamline with 7?keV fundamental energy is presented. The spot of the third-order harmonic of 21?keV is deviated from the fundamental by 0.35?mm at a distance 1?m behind the device. PMID:23093763

238

A proof-of-principle experiment of a novel harmonics separation optics for synchrotron facilities  

A proof-of-principle experiment of a novel harmonics separation optics for synchrotron facilities is presented. The harmonic separator is a Si crystal cut in an inclined geometry in which the impinging beam undergoes a diffractive-refractive effect owing to the dispersive nature of X-ray refraction. A polychromatic beam containing higher-order energies is spatially separated behind the separator into individual monochromatic diffraction spots. A synchrotron experiment at a bending-magnet beamline with 7-keV fundamental energy is presented. The spot of the third-order harmonic of 21-keV is deviated from the fundamental by 0.35-mm at a distance 1-m behind the device.

239

Coagulation Using Kerosene for Magnetic Deinking of Waste Office Paper  

A method for disintegrating waste office paper using kerosene was reported in our previous paper, which achieved almost a 100% liberation of toner from paper fibers. The liberated toner must be completely separated to realize effective deinking. Recently, a new method for deinking waste officer paper by magnetic separation after hetero-coagulation of magnetic and non-magnetic toner by 1-octadecanol was reported by Augusta et al. Under this method, coagulation was carried out at 72°C. The 1-octadecanol liquid was then cooled to produce strong solid coagulates. As reported in our previous paper, kerosene has the ability to soften toner, and strong coagulates for magnetic separation may be produced by their adhesion when used as a flocculant. The present study investigated the size of toner particles liberated by the kerosene disintegration method, and compared the bonding strength between the toner particles coagulated by the addition of kerosene as a flocculant to those coagulated with 1-octadecanol. After these investigations, the coagulating and deinking properties of kerosene and 1-octadecanol were compared by rejecting toner coagulates with a neodymium-boron magnet. The results showed that nearly perfect deinking can be achieved with little paper loss, even in ambient temperature, due to the large and strong coagulates produced by this method. When kerosene was used in the disintegration and coagulation stages, the average coagulate size was 1114??m, and a deinking percentage of 98.4% was attained through separation with a neodymium-boron magnet.   

240

Waste remediation using in situ magnetically assisted chemical separation  

The magnetically assisted chemical separation process (MACS) combines the selective and efficient separation afforded by chemical sorption with the magnetic recovery of ferromagnetic particles. This process is being developed for treating the underground storage tanks at Hanford. These waste streams contain cesium, strontium, and transuranics (TRU) that must be removed before this waste can be disposed of as grout. The separation process uses magnetic particles coated with either (1) a selective ion exchange material or an organic extractant containing solvent (for cesium and strontium removal) or (2) solvents for selective separation of TRU elements (e.g., TRUEX process). These coatings, by their chemical nature, selectively separate the contaminants onto the particles, which can then be recovered from the tank using a magnet. Once the particles are removed, the contaminants can either be left on the loaded particles and added to the glass feed slurry or stripped into a small volume of solution so that the extracting particles can be reused. The status of chemistry and separation process is discussed in this paper.

 
 
 
 
241

Magma transport beneath La Palma: inferences based on fluid inclusion and mineral-melt thermobarometry  

La Palma (Canary Islands) represents a hotspot island with an active rift zone, inferred to have formed during the last 800 ka following southward growth of the former radial-symmetrical stratovolcano Taburiente /1/. The aim of our study is to model the magmatic evolution of the rift system from its early stage (Cumbre Nueva) through the short Bejenado volcano phase which followed the Cumbre Nueva collapse (560-549 ka) to the presently active rift zone (Cumbre Vieja). Clinopyroxene-melt thermobarometry and microthermometry of fluid inclusions were applied to constrain magma pathways and major levels of magma stagnation. CO2- dominated fluid inclusions in olivine and clinopyroxene in Taburiente picrites show density distributions with maxima at 0.7-0.85 g/cm-3. These values correspond to equilibrium pressures of 400-600 MPa, in accordance with other Taburiente data /2/. Inclusion data of a Cumbre Nueva ankaramite give pressure estimates of 200-300 MPa. In comparison, fluid inclusions in Recent Cumbre Vieja rocks yield a pronounced pressure estimate at 200-400 MPa, which overlaps with the Cumbre Nueva data but is shallower than that for Taburiente. Clinopyroxene-melt barometry of phenocryst rims and glassy groundmass yield pressure maxima between 600 and 900 MPa for Taburiente, Bejenado and Cumbre Nueva. This pressure range partly overlaps with that for Cumbre Vieja (maximum between 500 and 800 MPa) but has a tendency to higher pressures. The combined data indicate that two separate magma stagnation levels are distinct for each rift phase: (1) a main fractionation level within the upper mantle which is common to all phases, and (2) intermittent stagnation close to the Moho for the Taburiente volcano and above the Moho for both the Cumbre Nueva and Cumbre Vieja. Observing that the present rift system and the early stages of the rift show different levels of fractionation and magma stagnation and also show compositional differences between the lavas, we suggest that the present rift configuration does not reflect continuous growth of the Taburiente shield during the last 800 ka. We thus propose that Taburiente/Cumbre Nueva and Cumbre Vieja represent two distinct volcanoes with separate magma plumbing systems. This model is supported by the overall morphology. /1/ Carracedo et al. (1999), Geol Soc Am Bull 111 (5), 755-768 /2/ Nikogosian et al., (2002), Chem Geol 183, 169-193

242

Development of extrusion molded Nd-Fe-B magnets  

A new manufacturing process for extrusion molded magnets, composed of isotropic Nd-Fe-B powder and Nylon-12, has been developed. This newly developed extrusion molding process has several interesting features. First, the extruded product contains 72% by volume magnetic powder and yields a (BH)[sub max] of 8.0 MGO[sub e]. Second, through the addition of an anti-oxidant, the viscosity of the magnetic powder-nylon compound remains almost constant during molding. Third, by means of a specially cooled outlet, which is separated from the heated die by a thermal insulator, an optimized temperature profile is obtained which yields uniformly smooth extrusion molded magnets. Both long thin-walled magnets and small arc-shaped (kawala) magnets are easily molded by this new process.

243

Computational Fluid Dynamics Simulation of a Quadrupole Magnetic Sorter Flow Channel: Effect of Splitter Position on Nonspecific Crossover.  

In the Quadrupole Magnetic Sorter (QMS) magnetic particles enter a vertical flow annulus and are separated from non-magnetic particles by radial deflection into an outer annulus where the purified magnetic particles are collected via a flow splitter. The purity of magnetically isolated particles in QMS is affected by the migration of nonmagnetic particles across transport lamina in the annular flow channel. Computational Fluid Dynamics (CFD) simulations were used to predict the flow patterns, pressure drop and nonspecific crossover in QMS flow channel for the isolation of pancreatic islets of Langerhans. Simulation results were compared with the experimental results to validate the CFD model. Results of the simulations were used to show that one design gives up to 10% less nonspecific crossover than another and this model can be used to optimise the flow channel design to achieve maximum purity of magnetic particles. PMID:21984840

244

Intersubband resistance oscillations in crossed electric and magnetic fields  

Quantum oscillations of nonlinear resistance are investigated in response to electric current and magnetic field applied perpendicular to single GaAs quantum wells with two populated subbands. At small magnetic fields current-induced oscillations appear as Landau-Zener transitions between Landau levels inside the lowest subband. The period of these oscillations is proportional to the magnetic field. At high magnetic fields, a different kind of quantum oscillations emerges with a period that is independent of the magnetic field. At a fixed current the oscillations are periodic in inverse magnetic field with a period that is independent of the dc bias. The proposed model considers these oscillations as a result of spatial variations of the energy separation between two subbands induced by the electric current.

245

Surface magnetic enhancement for coal cleaning. Quarterly technical progress report no. 3, August 1, 1988--October 31, 1988  

The progress achieved during this quarter includes the reagent shelf life study, the evaluation and selection of magnetizing reagents, an experimental database for activating and depressing the adsorption of magnetizing reagents in the presence of various chemicals, an adsorption regulator investigation, the establishment of a coal surface controlling theory, and a magnetite size effect study for the separation of magnetic enhanced minerals. The work is on schedule with the original plan. Modifications include the addition of a regulator study to help proving the selectivity controlling theory. The fundamentals for applying the magnetizing reagent technology on coal cleaning are generally established during this quarter. Selective magnetic enhancement of minerals through the adsorption of magnetizing reagents has been experimentally proved. The work for the next quarter will be mainly on optimizing the selective adsorption conditions and the continuation on magnetite size effect study.

246

Surface magnetic enhancement for coal cleaning  

The progress achieved during this quarter includes the reagent shelf life study, the evaluation and selection of magnetizing reagents, an experimental database for activating and depressing the adsorption of magnetizing reagents in the presence of various chemicals, an adsorption regulator investigation, the establishment of a coal surface controlling theory, and a magnetite size effect study for the separation of magnetic enhanced minerals. The work is on schedule with the original plan. Modifications include the addition of a regulator study to help proving the selectivity controlling theory. The fundamentals for applying the magnetizing reagent technology on coal cleaning are generally established during this quarter. Selective magnetic enhancement of minerals through the adsorption of magnetizing reagents has been experimentally proved. The work for the next quarter will be mainly on optimizing the selective adsorption conditions and the continuation on magnetite size effect study.

247

Design and implementation of LQG\\LTR controller for a magnetic telemanipulation system-performance evaluation and energy saving  

This paper deals with designing a telemanipulation system (TMS) for microrobotics applications. The TMS uses magnetic levitation technology for the three-dimensional (3-D) manipulation of a microrobot. The TMS is made up of two separate components: a magnetic drive unit and a microrobot. The magnetic drive unit is developed to generate the magnetic field for propelling the microrobot in an enclosed environment. The drive unit consists of electromagnets, a disc pole-piece for connecting the magnetic poles, and a yoke. To handle the 3-D high precision motion control of the microrobot, experimental magnetic field measurements coupled with numerical analysis were done to identify the dynamic model of levitation. This approach leads to the design of a linear quadratic gaussian (LQG) control sys...

248

Cryo-magnets transport vehicles and transfer table sets  

About 1800 LHC cryo-magnets will be installed in the LHC tunnel. The transport and installation of the LHC cryo-magnets in the LEP tunnels originally designed for smaller, lighter LEP magnets have required development of completely new handling solutions. The severe space constraints combined with the long, heavy loads meant that solutions had to be very sophisticated. The equipment needed has been procured using two separate contracts, one for the vehicles to transport the cryo-magnets to their place of installation, and one for transfer tables to place cryo-magnets on their support jacks. The key phases of the contract are described, starting from conceptual design, through manufacture, testing and training of operators, to the installation of the first cryo-magnet. The paper includes conclusions and some lessons learnt.

249

Rapid extraction of low concentration heavy metal ions by magnetic fluids in high gradient magnetic separator  

A novel method for the extraction of low concentration heavy metal ions from aqueous solution by using magnetic fluids in the high gradient magnetic separator (HGMS) has been constructed. We dissolved the extractant tributyl phosphate (TBP) in the magnetic fluids, and selected the Au3+ as the model of heavy metal ion to research the extraction efficiency of magnetic fluids containing TBP in this article. The magnetic fluids containing TBP, as stationary phase in the form of liquid-droplet, were immobilized on the surface of steel wires in the HGMS; the low concentration Au3+, as mobile phase, flowed through the HGMS and was extracted from aqueous solution. The experiments investigated the dependence of the Au3+ extraction efficiency of magnetic fluids on the pH value of aqueous solution, T...

250

Flavoured Large N Gauge Theory on a Compact Space with an External Magnetic Field  

The phase structure of flavoured N=2 SYM on a three sphere in an external magnetic field is studied. The binding effect the magnetic field competes with the dissociating effect of the Casimir free energy, leading to an interesting phase structure of confined and deconfined phases separated by a critical curve of a first order quantum phase transition. At vanishing magnetic field the phase transition is of a third order. For sufficiently strong magnetic field, the only stable phase is the confined phase and magnetic catalysis of chiral symmetry breaking is realized. The meson spectra of the theory exhibit Zeeman splitting and level crossing and feature a finite jump at the phase transition between the confined and deconfined phases. At strong magnetic field the ground state has a massless mode corresponding to the Goldstone boson associated with the spontaneously broken U(1) R-symmetry analogous to the eta' meson in QCD.

251

Crustal structure across the San Andreas Fault at the SAFOD site from potential field and geologic studies  

We present newly compiled magnetic, gravity, and geologic datasets from the Parkfield region around the San Andreas Fault Observatory at Depth (SAFOD) pilot hole in order to help define the structure and geophysical setting of the San Andreas Fault (SAF). A 2-D cross section of the SAF zone at SAFOD, based on new, tightly spaced magnetic and gravity observations and surface geology, shows that as drilling proceeds NE toward the SAF, it is likely that at least 2 fault bounded magnetic slivers, possibly consisting of magnetic granitic rock, serpentinite, or unusually magnetic sandstone, will be encountered. The upper 2 km of the model is constrained by an order of magnitude increase in magnetic susceptibility at 1400 m depth observed in pilot hole measurements. NE of the SAF, a flat lying, tabular body of serpentinite at 2 km depth separates two masses of Franciscan rock and truncates against the SAF.

252

Capture of metallic copper by high gradient magnetic separation system  

Valence copper was recovered from wastewater by chemical reduction and use of a high gradient magnetic separation (HGMS) system. Ammonia (NH3) and sodium dithionate (Na2S2O4) at a molar ratio of [Cu]:[NH3]:[Na2S2O4] = 1:4:3 at pH = 9.5 were used first to chemically reduce copper ion to metallic copper; the resultant metal solids were captured in an upflowing reactor space equipped with a permalloy matrix net under a high gradient magnetic field. The captured solids were predominantly 6-20 µm in diameter, with Cu2O and CuO present among the solids. Four treatment configurations with and without the use of magnetic field and metal alloy as the matrix net were tested and their effects evaluated: (1) no magnetic field or matrix, (2) no magnetic field but with matrix, (3) with magnetic fie...

253

Digital lock-in detection of site-specific magnetism in magnetic materials  

The polarization and diffraction characteristics of x-rays incident upon a magnetic material are manipulated to provide a desired magnetic sensitivity in the material. The contrast in diffracted intensity of opposite helicities of circularly polarized x-rays is measured to permit separation of magnetic signals by element type and by atomic environment. This allows for the direct probing of magnetic signals from elements of the same species in nonequivalent atomic environments to better understand the behavior and characteristics of permanent magnetic materials. By using known crystallographic information together with manipulation of the polarization of x-rays having energies tuned near element-specific electronic excitations and by detecting and comparing the incident and diffracted photons at the same frequency, more accurate magnetic measurements can be made over shorter observation periods.

254

MR safety: simultaneous B 0, d?/dt, and dB/dt measurements on MR-workers up to 7 T  

Object The EU directive on safety requirements (2004/40/EC) limits the exposure to time varying magnetic fields to dB /dt = 200 mT/s. This action value is not clearly defined as it considers only the temporal change of the magnitude of Formula Not Shown . Thus, only the translational motion in the magnet?s fringe field is considered and rotations are neglected. Materials and methods A magnetic field probe was constructed to simultaneously record the magnetic flux density Formula Not Shown (x, y, z) with a 3-axis Hall sensor and the induced voltage due to movements with a set of three orthogonal coils. Voltages were converted into time-varying magnetic flux d ?(x, y, z)/dt serving as an exposition parameter for both translations and rotations. To separate the two types of motion, d B/dt was...

255

Acceleration of Particles at the Termination Shock of a Relativistic Striped Wind  

The relativistic wind of obliquely-rotating pulsars consists of toroidal stripes of opposite magnetic field polarity, separated by current sheets of hot plasma. By means of two- and three-dimensional particle-in-cell simulations, we investigate particle acceleration and magnetic field dissipation at the termination shock of a relativistic striped wind. At the shock, the flow compresses and the alternating fields annihilate by driven magnetic reconnection. Irrespective of the stripe wavelength "lambda" or the wind magnetization "sigma" (in the regime sigma>>1 of magnetically-dominated flows), shock-driven reconnection transfers all the magnetic energy of alternating fields to the particles, whose average Lorentz factor increases by a factor of sigma with respect to the pre-shock value. The shape of the post-shock spectrum depends primarily on the ratio lambda/(r_L*sigma), where r_L is the relativistic Larmor radius in the wind. The spectrum becomes broader as the value of lambda/(r_L*sigma) increases, passing ...

256

Size distribution of magnetic iron oxide nanoparticles using Warren-Averbach XRD analysis  

We use the Fourier transform based Warren-Averbach (WA) analysis to separate the contributions of X-ray diffraction (XRD) profile broadening due to crystallite size and microstrain for magnetic iron oxide nanoparticles. The profile shape of the column length distribution, obtained from WA analysis, is used to analyze the shape of the magnetic iron oxide nanoparticles. From the column length distribution, the crystallite size and its distribution are estimated for these nanoparticles which are compared with size distribution obtained from dynamic light scattering measurements. The crystallite size and size distribution of crystallites obtained from WA analysis are explained based on the experimental parameters employed in preparation of these magnetic iron oxide nanoparticles. The variation of volume weighted diameter (Dv, from WA analysis) with saturation magnetization (Ms) fits well to a core shell model wherein it is known that Ms=Mbulk(1-6g/Dv) with Mbulk as bulk magnetization of iron oxide and g as magnetic shell disorder thickness.

257

High speed maglev design  

A propulsion and stabilization system for an inductive repulsion type magnetically levitated vehicle which is propelled and suspended by a system which includes dividing the superconducting magnets into two types: a strong field magnet which is located vertically below the vehicle for propulsion and guidance and a weak field superconducting magnet located at the ends of the vehicle for levitation and added guidance. Several proposed embodiments exist for the placement of the magnetic field shielding: locating the shielding on the vehicle, locating the shielding on the guideway, and locating the shielding on the guideway and adding shielding to the vertical undercarriage. In addition, the separation between the vehicle and the guideway can be controlled to reduce the exposure of the passenger cabin to magnetic fields.

258

Modeling high gradient magnetic separation from biological fluids.  

A proposed portable magnetic separator consists of an array of biocompatible capillary tubing and magnetizable wires immersed in an externally applied homogeneous magnetic field. While subject to the homogeneous magnetic field, the wires create high magnetic field gradients, which aid in the collection of blood-borne magnetic nanospheres from blood flow. In this study, a 3-D numerical model was created using COMSOL Multiphysics 3.2 software to determine the configuration of the wire-tubing array from two possible configurations, one being an array with rows alternating between wires and tubing, and the other being an array where wire and tubing alternate in two directions. The results demonstrated that the second configuration would actually capture more of the magnetic spheres. Experimental data obtained by our group support this numerical result.

259

Anode activating agent recovery by magnetic separation from the <0.075mm fraction of crushed nickel metal hydride batteries from hybrid vehicles  

Nickel metal hydride batteries of hybrid vehicles contain rare metals such as Ni, Co, and rare-earth elements as electrode components. A direct smelting method has been used to recover Ni from waste batteries, but the Co and rare-earth elements are difficult to extract with this conventional method. To recycle Co and rare-earth elements, physical pretreatment is necessary to separate the anode and cathode compounds before smelting. This study investigated the magnetic separation of anode and cathode activating agents in the <0.075mm fraction of crushed cylindrical and prismatic types batteries. In the cylindrical type anode activating agent concentrated in the non-magnetic product of the Davis tube tester, separated at low magnetic fields (0.1T), while in the prismatic type anode activatin...

260

Speciation of inorganic arsenic in environmental waters using magnetic solid phase extraction and preconcentration followed by ICP-MS  

A new method was developed for the speciation of inorganic arsenic in environmental water by using selective magnetic solid-phase extraction followed by inductively coupled plasma mass spectrometry. It is found that As(V) selectively adsorbed on amino-modified silica-coated magnetic nanoparticles (MNPs) in the pH range from 3 to 8, while As(III) is not be retained. The As(V)-loaded MNPs can be separated easily from the aqueous sample solution by simply applying an external magnetic field. The adsorbed As(V) was quantitatively recovered from the MNPs using using 1?M nitric acid. Total inorganic As was extracted after the permanganate oxidation of As(III) to As(V). Parameters affecting the separation were investigated systematically, and the optimal separation conditions were established. Un...

 
 
 
 
261

Reversible solid-state hydrogen-pump driven by magnetostructural transformation in the prototype system La(Fe,Si)13Hy  

In magnetocaloric La(Fe,Si)13 alloys, it is known that hydrogen addition shifts the magnetic transition temperature TC near room temperature. By partial hydrogen desorption, TC can be adjusted precisely towards the working temperature of a magnetic cooling device. In this work, we studied the stability of partially desorbed LaFe11.6Si1.4Hy and show that the large volume difference of ferro- and para-magnetic phases drives the system from a single phase to a stable two-phase configuration. The hydrogen concentration separates on a macroscopic scale. The phase-coexistence is visualized by Kerr Microscopy. Differential scanning calorimetry measurements show that hydrogen can be reversibly recombined and separated again. We explain the separation by the coexistence of a high-volume ferromagnetic and low-volume paramagnetic phase that can be induced either by temperature or other external stimuli. This phenomenon can be applied to material systems that show a coupling of physical and structural transitions.

262

Design and construction of a Wien velocity filter for AMS facilities  

Many experiments in atomic and nuclear physics using accelerated particles require accurate ion beams with respect to their atomic number, mass number and ion charge. These requirements have special important for experiments of accelerated mass spectrometry. Double focussing analyzing magnets perform the mass selection of charged ions. However, the magnetic analyzer cannot distinguish between particles with equal charge and having the same mass-velocity product. A simple way of resolving this degeneracy is to use a Wien velocity filter, WVF, in conjunction with the magnet analyzers. The design and construction of a WVF is presented together with experiments performed to determine the separation power. A velocity separation DELTA v/v = 1/100 was obtained. The design in this separate arrangements of fields is simple and straightforward. The construction can be achieved in a usual workshop. The applications of the WVF are manifold, e.g., AMS, ERDA, RBS, etc. (authors)

263

Effect of reverse flotation on magnetic separation concentrates  

Reverse flotation studies on magnetite samples have revealed that the use of starch as a depressant of Fe-oxides has a hydrophilic effect on the surface of Fe-bearing silicates and significantly decreases Fe in the silica-rich stream when used in combination with an amine (Lilaflot D817M). In this study, the effect of reverse flotation on the optimization of products obtained from magnetic separation was investigated. Two different magnetic samples, zones 1 and 2, were milled to separation (LIMS). The LIMS test conducted on the separation. Reverse flotation tests were conducted on the agitated magnetic concentrate feed, and the result shows a significant upgrade of Fe compared to that obtained from the non-agitated feed. Iron concentrations greater than 69%, and SiO2 concentrations less than 2% with overall magnetite recoveries greater than 67% and 71% were obtained for zones 1 and 2, respectively.

264

Microstructure and magnetic properties of Gd-Hf-Co-Al phase separated metallic glasses  

Microstructure and magnetic properties of phase separating Gd"5"5"-"xHf"xCo"2"5Al"2"0 metallic glasses are investigated for x = 0, 10, 20, 27.5, 35, 45 and 55 at. %. The Gd-Hf-Co-Al alloy system undergoes typical liquid-liquid phase separation during quenching and decomposes into Gd-rich and Hf-rich amorphous phases. The microstructural features such as length scale and volume fraction of separated phases and the occurrence of secondary precipitation strongly depend on composition and cooling rate. In particular for the Gd"2"7"."5Hf"2"7"."5Co"2"5Al"2"0 alloy, a strong dependence of microstructural features on the local cooling rate could be observed. The Gd-containing alloys exhibit soft magnetic behavior (H"c < 100 Oe) and a magnetic transition from paramagnetic to ferromagnetic in the te...

265

Spin-orbit induced electronic spin separation in semiconductor nanostructures  

The demonstration of quantized spin splitting by Stern and Gerlach is one of the most important experiments in modern physics. Their discovery was the precursor of recent developments in spin-based technologies. Although electrical spin separation of charged particles is fundamental in spintronics, in non-uniform magnetic fields it has been difficult to separate the spin states of charged particles due to the Lorentz force, as well as to the insufficient and uncontrollable field gradients. Here we demonstrate electronic spin separation in a semiconductor nanostructure. To avoid the Lorentz force, which is inevitably induced when an external magnetic field is applied, we utilized the effective non-uniform magnetic field which originates from the Rashba spin-orbit interaction in an InGaAs-based heterostructure. Using a Stern-Gerlach-inspired mechanism, together with a quantum point contact, we obtained field gradients of 108 T m-1 resulting in a highly polarized spin current.

266

Effect of carrier doping on the formation and collapse of magnetic polarons in lightly hole-doped La1-xSrxCoO3  

We investigate the doping dependence of the nanoscale electronic and magnetic inhomogeneities in the hole-doping range 0.002?x?0.1 of cobalt based perovskites, La1-xSrxCoO3. Using single-crystal inelastic neutron scattering and magnetization measurements we show that the lightly doped system exhibits magnetoelectronic phase separation in the form of spin-state polarons. Higher hole doping leads to a decay of spin-state polarons in favor of larger scale magnetic clusters, due to competing ferromagnetic correlations of Co3+ ions which are formed by neighboring polarons. The present data give evidence for two regimes of magnetoelectronic phase separation in this system: (i) x?0.05, dominated by ferromagnetic intrapolaron interactions, and (ii) x?0.05, dominated by Co3+-Co3+ intracluster interactions. Our conclusions are in good agreement with a recently proposed model of the phase separation in cobalt perovskites [C. He , Europhys. Lett.EULEEJ0295-507510.1209/0295-5075/87/27006 87, 27006 (2009)].

267

The gas filled separator as a separation method to detect transuranic elements; Der gasgefuellte Separator als Separationsmethode zum Nachweis von Transuranen  

The mass spectrometer NASE (NAchSEparator) built as a post-separator and located behind the velocity filter SHIP at the GSI in Darmstadt, was taken into operation as a gas-filled separator, and its separation properties for fusion products from heavy ion reactions were studied. Chapter 2 describes the principle of separation in a gas-filled magnet. The technical specifications of the separator, the detectors and the setup of detection electronics are outlined in chapter 3. The studies of separation properties are described in chapter 4, and chapter 5 deals with preliminary applications of the gas-filled separator to detect isotopes poor in neutrons, with an atomic number Z = 92, 93. Chapter 6 is concerned with preliminary tests to detect heavy nuclei with an atomic number Z > = 100 by means of light radiation and actinide targets. The experimental results of comparative measurements between the velocity filter SHIP and the gas-filled separator are pointed out in chapter 7, and future application possibilities of gas-filled separators for synthesis of heaviest nuclei through asymmetric reactions are discussed. (orig./BBR). [Deutsch] Das als NAchSEparator gebaute Massenspektrometer NASE, das sich hinter dem Geschwindigkeitsfilter SHIP bei der GSI in Darmstadt befindet, wurde als gasgefuellter Separator in Betrieb genommen und seine Separationseigenschaften fuer Fusionsprodukte aus Schwerionenreaktionen wurden untersucht. In Kapitel 2 wird das Prinzip der Trennung in einem gasgefuellten Magneten beschrieben. Die technischen Spezifikationen des Separators, die Detektoren und der Aufbau der Nachweiselektronik werden in Kapitel 3 skizziert. Die Untersuchungen der Separationseigenschaften werden im Kapitel 4 beschrieben und im Kapitel 5 erste Anwendungen des gasgefuellten Separators zum Nachweis neutronenarmer Isotope mit einer Ordnungszahl Z = 92, 93. Kapitel 6 befasst sich mit den ersten Versuchen schwere Kerne mit einer Ordnungszahl Z > = 100 mit leichten Strahlen und Aktinidentargets nachzuweisen. Die experimentellen Ergebnisse der Vergleichsmessungen zwischen dem Geschwindigkeitsfilter SHIP und dem gasgefuellten Separator werden im Kapitel 7 aufgezeigt sowie zukuenftige Einsatzmoeglichkeiten des gasgefuellten Separators zur Synthese schwerster Kerne ueber asymmetrische Reaktionen diskutiert. (orig./BBR).

268

Process parametric study for the recovery of very-fine size uranium values on super-conducting high gradient magnetic separator  

This paper discusses the application of super-conducting high gradient magnetic separator for the recovery of very-fine size uranium bearing mineral values present in the flotation tailings of an Indian copper ore. The U3O8 content of the tailings is 0.009%. The focus of this study is centered on determining the effect of various process variables like applied magnetic field, wool filling factor in the canister, wool diameter, loading capacity of the matrix, feed flow-rate and slurry pH on the recovery of uranium values in the magnetized matrix. The results indicate significant improvement in the recovery of <10mm size uranium bearing particles, to the extent of 60-65% in SCHGMS as against mere 20% in other high intensity magnetic separators. The enrichment ratio of U3O8 values in the magn...

269

A novel technique for in situ aggregation of Gluconobacter oxydans using bio-adhesive magnetic nanoparticles.  

Here, we present a novel technique to immobilize magnetic particles onto whole Gluconobacter oxydans in situ via a synthetic adhesive biomimetic material inspired by the protein glues of marine mussels. Our approach involves simple coating of a cell adherent polydopamine film onto magnetic nanoparticles, followed by conjugation of the polydopamine-coated nanoparticles to G. oxydans which resulted in cell aggregation. After optimization, 21.3?mg (wet cell weight) G. oxydans per milligram of nanoparticle was aggregated and separated with a magnet. Importantly, the G. oxydan aggregates showed high specific activity and good reusability. The facile approach offers the potential advantages of low cost, easy cell separation, low diffusion resistance, and high efficiency. Furthermore, the approach is a convenient platform technique for magnetization of cells in situ by direct mixing of nanoparticles with a cell suspension. Biotechnol. Bioeng. 2012; 109: 2970-2977. © 2012 Wiley Periodicals, Inc. PMID:22729662

270

Jet confinement by magneto-torsional oscillations  

Many quasars and active galactic nuclei (AGN) appear in radio, optical, and X-ray maps, as a bright nuclear sources from which emerge single or double long, thin jets. When observed with high angular resolution these jets show structure with bright knots separated by relatively dark regions. Nonthermal nature of a jet radiation is well explained as the synchrotron radiation of the relativistic electrons in an ordered magnetic field. We consider magnetic collimation, connected with torsional oscillations of a cylinder with elongated magnetic field, and periodically distributed initial rotation around the cylinder axis. The stabilizing azimuthal magnetic field is created here by torsional oscillations, where charge separation is not necessary. Approximate simplified model is developed. Ordinary differential equation is derived, and solved numerically, what gives a possibility to estimate quantitatively the range of parameters where jets may be stabilized by torsional oscillations.

271

Arsenic removal by magnetic nanocrystalline barium hexaferrite  

Nanoscale magnetite (Fe3O4) (<15 nm) is known to remove arsenic efficiently but is very difficult to separate or require high magnetic fields to separate out from the waste water after treatment. Anisotropic hexagonal ferrite (BaFe12O19, BHF) is a well-known permanent magnet (i.e., fridge magnets) and attractive due to its low cost in making large quantities. BHF offers a viable alternative to magnetite nanocrystals for arsenic removal since it features surfaces similar to iron oxides but with much enhanced magnetism. Herein, we employ BHF nanocrystalline materials for the first time in arsenic removal from wastewater. Our results show better (75 %) arsenic removal than magnetite of the similar sizes. The BHF nanoparticles, 6.06 ± 0.52 nm synthesized by thermolysis method at 320 °C do not ...

272

Titanium-containing magnetic mesoporous silica spheres: effective enrichment of peptides and simultaneous separation of nonphosphopeptides and phosphopeptides.  

Protein phosphorylation is a common posttranslational modification, and involved in many cellular processes. Like endogenous peptides, endogenous phosphopeptides contain many biomarkers of preclinical screening and disease diagnosis. In this work, titanium-containing magnetic mesoporous silica spheres were synthesized and applied for effective enrichment of peptides from both tryptic digests of standard proteins and human serum. Besides, the enriched peptides can be further separated into nonphosphopeptides and phosphopeptides by a simple elution. First, titanium-containing magnetic mesoporous silica spheres were synthesized by a sol-gel method and found to have high surface area, narrow pore size distribution, and useful magnetic responsivity. Then, as the prepared material was used for selective capturing of phosphopeptides, it demonstrated to have higher selectivity than commercial titanium dioxide. Moreover, via combination of size-exclusion mechanism, hydrophobic interaction, and affinity chromatography, titanium-containing magnetic mesoporous silica spheres were successfully applied to simultaneously extract and separate nonphosphopeptides and phosphopeptides from standard protein digestion and human serum. PMID:22740261

273

Superconducting combined function magnets  

Superconducting accelerators and storage rings, presently under construction or in the design phase, are based on separate dipole and quadrupole magnets. It is here suggested that a hybrid lattice configuration consisting of dipoles and combined function gradient magnets would: (1) reduce the number of magnet units and their total cost; and (2) increase the filling factor and thus the energy at a given field. Coil cross sections are presented for the example of the Brookhaven Colliding Beam Accelerator. An asymmetric two-layer cable gradient magnet would have transfer functions of 10.42 G/A and 0.628 G cm/sup -1//A versus 15.77 G/A and 2.03 G cm/sup -1//A of the present separate dipoles and quadrupoles.

274

Simultaneous spectrophotometric determination of trace amount of polycyclic aromatic hydrocarbons in water samples after magnetic solid-phase extraction by using projection pursuit regression.  

Magnetic solid-phase extraction based on coated nano-magnets Fe(3)O(4) was applied for the preconcentration of four polycyclic aromatic hydrocarbons (PAHs; anthracene, phenanthrene, fluorine, and pyrene) in environmental water samples prior to simultaneous spectrophotometric determination using multivariate calibration method. Magnetic nanoparticles, carrying target metals, were easily separated from the aqueous solution by applying an external magnetic field so, no filtration or centrifugation was necessary. After elution of the adsorbed PAHs, the concentration of PAHs was determined spectrophotometrically with the aid of a new and efficient multivariate spectral analysis base on principal component analysis-projection pursuit regression, without separation of analytes. The obtained results revealed that using projection pursuit regression as a flexible modeling approach improves the predictive quality of the developed models compared with partial least squares and least squares support vector machine methods. The method was used to determine four PAHs in environmental water samples. PMID:22684809

275

SUPERCONDUCTING DIPOLE MAGNETS FOR THE LHC INSERTION REGIONS  

Dipole bending magnets are required to change the horizontal separation of the two beams in the LHC. In Intersection Regions (IR) 1, 2, 5, and 8, the beams are brought into collision for the experiments located there. In IR4, the separation of the beams is increased to accommodate the machine's particle acceleration hardware. As part of the US contribution to the LHC Project, BNL is building the required superconducting magnets. Designs have been developed featuring a single aperture cold mass in a single cryostat, two single aperture cold masses in a single cryostat, and a dual aperture cold mass in a single cryostat. All configurations feature the 80 mm diameter, 10 m long superconducting coil design used in the main bending magnets of the Relativistic Heavy Ion Collider recently completed at Brookhaven. The magnets for the LHC, to be built at Brookhaven, are described and results from the program to build two dual aperture prototypes are presented.

276

Effect of reverse flotation on magnetic separation concentrates  

Reverse flotation studies on magnetite samples have revealed that the use of starch as a depressant of Fe-oxides has a hydrophilic effect on the surface of Fe-bearing silicates and significantly decreases Fe in the silica-rich stream when used in combination with an amine (Lilaflot D817M). In this study, the effect of reverse flotation on the optimization of products obtained from magnetic separation was investigated. Two different magnetic samples, zones 1 and 2, were milled to <75 ?m and then subjected to low intensity magnetic separation (LIMS). The LIMS test conducted on the <75 ?m shown an upgrade of 46.40wt% Fe, 28.40wt% SiO2 and 2.61wt% MnO for zone 1 and 47.60wt% Fe, 29.17wt% SiO2 and 0.50wt% MnO for zone 2. Further milling of the ore to <25 ?m resulted in a higher magnetic-rich pr...

277

Simulation of relativistically colliding laser-generated electron flows  

The plasma dynamics resulting from the simultaneous impact, of two equal, ultra-intense laser pulses, in two spatially separated spots, onto a dense target is studied via particle-in-cell (PIC) simulations. The simulations show that electrons accelerated to relativistic speeds, cross the target and exit at its rear surface. Most energetic electrons are bound to the rear surface by the ambipolar electric field and expand along it. Their current is closed by a return current in the target, and this current configuration generates strong surface magnetic fields. The two electron sheaths collide at the midplane between the laser impact points. The magnetic repulsion between the counter-streaming electron beams separates them along the surface normal direction, before they can thermalize through other beam instabilities. This magnetic repulsion is also the driving mechanism for the beam-Weibel (filamentation) instability, which is thought to be responsible for magnetic field growth close to the internal shocks of ...

278

Extraction of uranium from seawater using magnetic adsorbents  

A new process for the extraction of uranium from seawater was developed. In the process, uranium adsorption is effected using powdered magnetic adsorbents; the adsorbents are then separated from seawater using magnetic separation technology. This process is superior to a column method using a granulated hydrous titanium oxide adsorber bed in the following ways: (1) a higher rate of adsorption is realized because smaller particles are used in the uranium adsorption; and (2) blocking, which is inevitable in an adsorber bed, is eliminated. The composite hydrous titanium-iron oxide as a magnetic adsorbent having high uranium adsorption capacity and magnetization can be prepared by adding urea to a mixed solution of titanium sulfate and ferrous sulfate. Adsorption and desoprtion of uranium and the removal of the adsorbent using a small-scale uranium extraction plant (about 15 m/sup 3//d) is reported, and the feasibility of uranium extraction from seawater by this process is demonstrated. 10 figures.

279

Glassy magnetic phase driven by short-range charge and magnetic ordering in nanocrystalline La1/3Sr2/3FeO3-?: Magnetization, Mössbauer, and polarized neutron studies  

The charge ordered La1/3Sr2/3FeO3-? (LSFO) in bulk and nanocrystalline forms are investigated using ac and dc magnetization, Mössbauer, and polarized neutron studies. A complex scenario of short-range charge and magnetic ordering is realized from the polarized neutron studies in nanocrystalline specimen. This short-range ordering does not involve any change in spin state and modification in the charge disproportion between Fe3+ and Fe5+ compared to bulk counterpart as evident in the Mössbauer results. The refinement of magnetic diffraction peaks provides magnetic moments of Fe3+ and Fe5+ are about 3.15 ?B and 1.57 ?B for bulk, and 2.7 ?B and 0.53 ?B for nanocrystalline specimen, respectively. The destabilization of charge ordering leads to magnetic phase separation, giving rise to the robust exchange bias (EB) effect. Strikingly, EB field at 5 K attains a value as high as 4.4 kOe for average size ˜70 nm, which is zero for the bulk counterpart. A strong frequency dependence of ac susceptibility reveals cluster-glass-like transition around ˜65 K, below which EB appears. Overall results propose that finite-size effect directs the complex glassy magnetic behavior driven by unconventional short-range charge and magnetic ordering, and magnetic phase separation appears in nanocrystalline LSFO.

280

Separators for SLAC B-Factory  

In order to separate the beams during injection, a closed vertical bump will be introduced in the B-Factory High Energy Ring (HER) using four dedicated, pulsed magnets. The design field in the magnets is B{sub 0} = 660 G; the field integrals of the magnets are nominally: {integral} Hdl = 0.0450 T{center_dot}m; {integral} Hdl = 0.0420 T{center_dot}m; {integral} Hdl = 0.0756 T{center_dot}m; {integral} Hdl = 0.0832 T{center_dot}m. The magnet apertures are 15 cm horizontal along the field direction and 10 cm in the vertical direction. The beams will be separated with a rise time of about 200 ms at the end of a coast and brought back into collision within about 1 ms. A good-field-region of {+-} 4.1 cm in the horizontal and {+-} 2.1 cm in the vertical direction with field non-uniformity less than 0.2% is aimed for, and fast magnetic field switch-off even through the present steel vacuum pipe of about 4 mm thickness. A 15% variation in each magnet current is done with variable shunts to allow tuning of the bump for different lattice configurations. The magnets have to fit into the existing constrained space of the B-factory. The magnets have been made and tested successfully at BINP and at SLAC. The whole system including pulsed power supply and shunts were also tested successfully.

 
 
 
 
281

Studies on application of fine power materials to the biochemical engineering. Biryushi zairyo no seibutsu kagaku kogaku eno oyo ni kansuru kenkyu  

This paper summarizes studies on the application of fine powder materials to the biochemical engineering, as for the structural analysis of protein molecules on solid phase surface, and the development of functional fine particles and their application to bioproduct separation. The purpose of this series of investigations is to utilize existing fine powder materials by the new ideas, and to newly prepare fine powder materials suitable for the operation. Since ultra fine powder dispersion liquid is transparent and the light is not scattered, the structure of protein on the solid phase surface can be evaluated through the spectroscopic method, such as circular dichroic spectroscopy. By this method, the structural change of protein on the solid phase surface is illustrated. In addition, the magnetic separation method, coagulation separation method, and extraction separation method were investigated as fine powder separation method, and their effectiveness was revealed. Moreover, the affinity separation process of bioproducts using fine powders is introduced. 8 refs., 3 figs.

282

Projectile fragments isotopic separation: Application to the LISE spectrometer at GANIL  

The isotopic separation of intermediate-energy (30 to 100 MeV per nucleon) heavy-ion projectile fragments is theoretically and experimentally investigated. Physical separation of nuclides is achieved through magnetic analysis (A/Z sensitivity) and differential stopping-power effects (Z/sup -2/ sensitivity). Depending on the specific case, a complete mass and charge separation may be achieved or a few nuclides may be selected simultaneously. The projectile fragments isotopic separation method described allows us to obtain an experimental mass separation A/..delta..Aapprox.=100. Simple formulae are given to determine the optimum factors for the best separation and transmission of the device. First applications to the spectroscopy of exotic nuclei lead to the new observation of the beta decay of /sup 37/P at GANIL and /sup 15/B at CERN.

283

Isobar separator for radioactive nuclear beams project  

In order to produce pure beams of radioactive products emanating from the production target/ion source system, both mass and isobar separation is required. A preliminary mass separation with a resolution {triangle}M/M of approximately 10{sup -3} will select the proper mass beam. An isobar separator is needed because the masses of adjacent isobars are usually quite close, especially for beams near stability. In general, a mass resolution of 5 x 10{sup -5} is needed for isobar separation in the A < 120 region, while a resolution of 3 x 10{sup -5} or better is needed for heavier masses. Magnets are used to obtain mass separation. However, in addition to having mass dispersion properties, magnets also have an equal energy dispersion. This means that an energy variation in the beam cannot be distinguished from a mass difference. This is important because ions emerge from the ion source having a small ({approximately} 10{sup -5} - 10{sup -4}) energy spread. In order to make the system respond only to mass differences, it must be made energy dispersion. This is normally accomplished by using a combination of electric and magnetic fields. The most convenient way of doing this is to use an electric deflection following the magnet separator. A preliminary isobar separator which achieves a mass resolution of 2.7 x 10{sup -5} is shown in Figure I-38. It uses two large 60{degrees} bending magnets to obtain a mass dispersion of 140 mm/%, and four electric dipoles with bending angles of 39{degrees} to cancel the energy dispersion. Sextupole and octupole correction elements are used to reduce the geometrical aberrations.

284

Approaches to improve separation efficiency of eddy current separation for recovering aluminum from waste toner cartridges.  

Separation efficiency of eddy current separation (ECS) is low (about 85%) in industrial application for recovering aluminum from crushed waste toner cartridges. Influencing factors of ECS were studied to improve the separation efficiency. Operation factors were researched by orthogonal experiment of ECS on investigating the separation distance between aluminum and plastic flakes. The results indicated the difference (?R-v) between feeding speed (v) and rotation speed (?) of magnetic drum (radius: R) was critical factor of influencing the separation efficiency, feeding speed (v) was general factor, and collecting position (H) was subordinate factor. Separation efficiency decreased as the increasing of v, and increased as the increasing of (?R-v). 0.9 m was the optimal value of H in the orthogonal experiment. Influencing factors of particle characteristics and machine structure were studied by newly established models for computing the separation distance between aluminum and plastic flake in ECS. The results indicated changing of particle size would influence the separation efficiency greater than ? and particle shape. Separation efficiency will increase as the increasing of particle size and ?. Shape of circle is beneficial to improve separation efficiency. Finally, approaches to improve separation efficiency of ECS were presented. PMID:22571825

285

Extraction of Rare Earth Elements as Oxides from a Neodymium Magnetic Sludge  

We propose a simple method for separating rare earth elements as oxides from a neodymium magnetic sludge by focusing on the affinity of oxygen for the rare earth elements (Nd, Dy, and Pr) and Fe. We have conducted separation experiments with a carbon crucible as contact material to confirm that carbon maintains the oxygen potential in the coexistence region of rare earth oxides and metallic Fe. In this work, the oxide phase of the rare earth elements and the alloy phase that primarily consists of Fe were separated clearly when the magnetic sludge in the carbon crucible was kept at 1823 K (1550 °C) under an Ar atmosphere. The purity of the rare earth oxide phase was high and only a small amount of rare earth elements were contained in the alloy phase. We found that the melting temperature of the rare earth oxides is a crucial factor for separation efficiency in our proposed method.

286

Separation and characterization of alkyl phenol formaldehyde resins demulsifier by adsorption chromatography, gel permeation chromatography, infrared spectrometry and nuclear magnetic resonance spectroscopy  

This paper deals with the separation and characterization of alkyl phenol formaldehyde resins demulsifier by infrared spectrometry and nuclear magnetic resonance spectroscopy after separation of the different surfactants and low molecular additives by adsorption chromatography. Firstly, the types of surfactants are identified by methylene blue chloride-chloroform test method and the elemental analysis such as Ca, K, Mg, Na, P, S and N. Then, the different surfactants and low molecular components are separated by adsorption chromatography after parts of low molecular components are dried in an oven, and the molecular weight distribution is measured by gel permeation chromatography also. Finally, the separated surfactants are determined by Fourier transform infrared (FTIR) spectrometry and nuclear magnetic resonance (NMR) spectroscopy. The distortionless enhancement by polarization transfer (DEPT), H, C correlated spectroscopy (H, C-COSY), H, H correlated spectroscopy (H, H-COSY) and heteronuclear multiple-bond correlation (HMBC) spectroscopy are applied to determine the molecular structures.

287

Process and apparatus for cleaning very fine ore  

In an ore cleaning process, the underflow from an ore classifying cyclone is delivered to a heavy medium cyclone where the ore is cleaned. The underflow leaving the classifying cyclone is continually measured for specific gravity and flow rate while the specific gravity of heavy medium that can be applied to the underflow is continually measured. The amount of this heavy medium and the amount of water required to be added to the underflow are continually controlled as functions of the specific gravity and flow rate thus measured, whereby a substantially constant specific gravity and flow rate of the underflow is maintained as it enters the heavy medium cyclone. Magnetic separating means receive the overflow from the heavy medium cyclone and separate the heavy medium from the ore, while other magnetic separating means receive the underflow from the same cyclone and separate the heavy medium from the rejects. The heavy medium is used again. 3 claims, 1 figure.

288

Correlation between magnetic and transport properties of phase separated La$_{0.5}$Ca$_{0.5}$MnO$_{3}$  

The effect of low magnetic fields on the magnetic and electrical transport properties of polycrystalline samples of the phase separated compound La$_{0.5}$Ca$_{0.5}$MnO$_{3}$ is studied. The results are interpreted in the framework of the field induced ferromagnetic fraction enlargement mechanism. A fraction expansion coefficient af, which relates the ferromagnetic fraction f with the applied field H, was obtained. A phenomenological model to understand the enlargement mechanism is worked out.

289

Correlation between magnetic and transport properties of phase-separated La0.5Ca0.5MnO3  

The effect of low-magnetic fields on the magnetic and electrical transport properties of polycrystalline samples of the phase-separated compound La0.5Ca0.5MnO3 is studied. The results are interpreted in the framework of the field-induced ferromagnetic fraction enlargement mechanism. A fraction expansion coefficient ?f, which relates the ferromagnetic fraction f with the applied field /H, was obtained. A phenomenological model to understand the enlargement mechanism is worked out.

290

Arithmetic of the integer quantum Hall effect  

text of abstract (Integer quantum Hall effect (IQHE) has been analysed considering the degeneracies of localized and extended states separately. Occupied localized and extended states are counted and their variation is studied as a function of magnetic field. The number of current carrying electrons is found to have a saw-tooth variation with magnetic field. The analysis attempts to answer certain basic questions besides providing a simple but complete understanding of IQHE.)

291

Curing of polyurethane coatings: Radiation curing. January 1980-November 1989 (A Bibliography from World Surface Coatings Abstracts). Report for January 1980-November 1989  

This bibliography contains citations concerning the curing of urethane and polyurethane coatings by electromagnet radiation. This bibliography is specific to electric and/or magnetic curing as compared to photocuring or ultraviolet curing, which are treated as separate bibliographies. These coatings may be described as inks, paints, lacquers, adhesives, or specialized coatings. Special applications of this technology in the magnetic recording media industry are presented. (Contains 98 citations fully indexed and including a title list.)

292

H/sub 2//sup +/ ion in an intense magnetic field: Improved adiabatic approximations  

We study the ground state binding energy of the H/sub 2//sup +/ ion in an intense magnetic field. Our calculations are based on improved forms of the adiabatic approximation. We calculate the binding energy, the equilibrium internuclear separation and the zero point energies of nuclear vibrations both parallel and perpendicular to the magnetic field. Comparison of our results with those obtained from the static adiabatic approximation and from variational calculations shows a substantial improvement.

293

Magnetic permeability of transparent magnetodielectrics at optical frequencies. Experiment  

The method of waveguide light propagation was applied to carry out direct measurement of non-diagonal components of tensors of dielectric and magnetic permittivity of (YbPr)/sub 3/(FeGa)/sub 5/O/sub 12/ ferrite-garnet. Separate measurement of non-diagonal components of tensors of dielectric and magnetic permittivity can be conducted at waveguide light propagation in ferrite-garnet epitaxial films; the non-diagonal components of the tensor appear to be different from zero in the optical frequency range.

294

Excitons in Carbon Nanotubes with Broken Time-Reversal Symmetry  

Near-infrared magneto-optical spectroscopy of single-walled carbon nanotubes reveals two absorption peaks with an equal strength at high magnetic fields ($>$ 55 T). We show that the peak separation is determined by the Aharonov-Bohm phase due to the tube-threading magnetic flux, which breaks the time-reversal symmetry and lifts the valley degeneracy. This field-induced symmetry breaking thus overcomes the Coulomb-induced intervalley mixing which is predicted to make the lowest exciton state optically inactive (or "dark'').

295

Magnetic field programming in quadrupole magnetic field-flow fractionation  

Magnetic field-flow fractionation (MgFFF) is a technique for the separation and characterization of magnetic nanoparticles. It is explained that the analysis of polydisperse samples requires a programmed decay of field and field gradient during sample elution. A procedure for achieving reproducible field decay with asymptotic approach to zero field using a quadrupole electromagnet is described. An example of an analysis of a polydisperse sample under programmed field decay is given.

296

Evolution in the split-peak structure across the Peak Effect region in single crystals of $2H$-NbSe$_2$  

We have explored the presence of a two-peak feature spanning the peak effect (PE) region in the ac susceptibility data and the magnetization hysteresis measurements over a wide field-temperature regime in few weakly pinned single crystals of $2H$-NbSe$_2$, which display reentrant characteristic in the PE curve near $T_c$(0). We believe that the two-peak feature evolves into distinct second magnetization peak anomaly well separated from the PE with gradual enhancement in the quenched random pinning.

297

Exact solution of Dirac equation in 2+1 dimensional gravity  

We find exact solutions of the Dirac equation in the 2+1 dimensional curved background by separation of variables. These solutions are given in terms of hypergeometric functions. We also perform the Gordon decomposition for the Dirac current to discuss the time dependence of the polarization densities and the magnetization density, and to show that the polarization densities are more effective than the magnetization density in the pair production in finite time intervals.

298

Fabrication of magnetic Ni nanoparticles functionalized water-soluble graphene sheets nanocomposites as sorbent for aromatic compounds removal  

The magnetic Ni nanoparticles functionalized water-soluble graphene sheets nanocomposites (NiGSs-C(CH3)2COONa) were fabricated via a facile and mild strategy. We designed a simple and efficient approach (the addition of cyano radicals) to improve the water solubility of nanocomposites. The NiGSs-C(CH3)2COONa nanocomposites had great potential as an effective absorbent for removing aromatic compounds from waste water owing to their rapid absorption rate, high absorption capacity, convenient magnetic separation and re-use property.

299

Electromagnetic ion separator  

In this paper we study the dynamics of charged particles interacting with a space homogeneous but time oscillating magnetic field of arbitrary amplitude and frequency. We analyze the stability of the particles orbits as functions of the magnetic field parameters and their masses. Based on the fact for a given magnitude field, the particles trajectories may become unstable depending on their masses, that we propose this system as an isotopic separator. (Author)

300

Adiabatic demagnetization and generation of entanglement in spin systems  

We study the entanglement emergence in a dipolar-coupled nuclear spin-1/2 system cooled using the adiabatic demagnetization technique. The unexpected behavior of entanglement for the next- and next-next-neighbor spins is revealed: entangled states of a spin system appear in two distinct temperature and magnetic field regions separated by a zero-concurrence area. The magnetic field dependence of the concurrence can have two maximums which positions are determined by the initial conditions and number of spins in a chain.

 
 
 
 
301

Asymptotic form of the Gordeyev function for initial-value problems  

An asymptotic representation is given of the Gordeyev transcendental function appearing in the elements of the dielectric tensor of a hot nonrelativistic Vlasov plasma in a magnetic field. It is valid for large values of the Larmor radius parameter and for initial-value problems in the finding of the dispersion relation roots. This formula shows, in the limit, a clear separation between magnetic and nonmagnetic effects.

302

Double-donor complex in vertically coupled quantum dots in a threading magnetic field.  

ABSTRACT: We consider a model of hydrogen-like artificial molecule formed by two vertically coupled quantum dots in the shape of axially symmetrical thin layers with on-axis single donor impurity in each of them and with the magnetic field directed along the symmetry axis. We present numerical results for energies of some low-lying levels as functions of the magnetic field applied along the symmetry axis for different quantum dot heights, radii, and separations between them. The evolution of the Aharonov-Bohm oscillations of the energy levels with the increase of the separation between dots is analyzed. PMID:23013550

303

Low-Q: proton electric and magnetic form factors  

An extensive measurement of the elastic H(e,e?)p reaction in the Q 2-region from 0.003 to 1?(GeV/c)2 has been performed with the three-spectrometer set-up of the A1 collaboration at the Mainz Microtron. The data set consists of about 3,000 overlapping cross-section measurements with a high level of internal redundancy, which allow for a determination of the electric and magnetic form factors with strict control over statistical and systematic errors, in particular also of the charge and magnetization radii of the proton. Besides the classical Rosenbluth separation, the form factors are separated by direct, global fits of different sufficiently flexible models.

304

Core-shell silica magnetic microspheres supported proline as a recyclable organocatalyst for the asymmetric aldol reaction  

l-4-Hydroxyproline has been successfully grafted onto the core-shell structural silica magnetic microspheres and characterized by elemental analysis, thermo gravimetric analysis (TGA), vibrating sample magnetometry (VSM), high resolution transmission electron microscopy (HRTEM) and Fourier transform infrared (FT-IR). The chiral immobilized catalyst demonstrated high catalytic activity (up to 92%), diastereoselectivity (up to 85:15) and enantioselectivity (up to 80%) in the asymmetric aldol reaction between aldehyde acceptors and ketone donors. On the other hand, the synthesized catalyst could be rapidly separated from the reaction mixture through an external magnetic field and reused up to five runs without any obvious loss of activity, indicating its easy-separated property and excellent ...

305

Use of high-gradient magnetic fields for the separation of macromolecules  

High gradient magnetic field separation (HGMS) has been used to separate several types of > 1 ..mu..m sized ferro- or paramagnetic particles from bulk streams. The majority of the studies have been carried out using a single ferromagnetic wire or wire mesh to produce the field gradients necessary for particle capture. The purpose of this paper is to examine the possibility of using HGMS on HGMS techniques can be used to capture 0.1 ..mu..m diam latex beads from a paramagnetic salt solution passing through a columnar bed of ferro- magnetic spheres. 10 refs., 3 figs.

306

Removal, preconcentration and spectrophotometric determination of picric acid in water samples using modified magnetic iron oxide nanoparticles as an efficient adsorbent  

A simple, fast and sensitive spectrophotometric method is developed for removal, preconcentration and determination of trace amounts of picric acid in water samples. Magnetic iron oxide nanoparticles (MIONPs) were synthesized and characterized by transmission electron microscopy (TEM). The magnetic nanoparticles were coated with cetyltrimethylammonium bromide (CTAB) and were applied for fast separation, preconcentration and spectrophotometric determination of picrate anion (the ion of picric acid) in an aqueous solution. The separation, preconcentration procedure is fast and will be completed in 2min. Methanol is used for desorption of adsorbed picrate anion. The effects of important parameters such as pH of aqueous medium, CTAB dosage, adsorbent amount, temperature, electrolyte concentrat...

307

Invert sugar formation with Saccharomyces cerevisiae cells encapsulated in magnetically responsive alginate microparticles  

Invert sugar (an equimolar mixture of glucose and fructose prepared by sucrose hydrolysis) is a very important food component. We have prepared magnetically responsive alginate microbeads containing entrapped Saccharomyces cerevisiae cells and magnetite microparticles which can be easily separated in an appropriate magnetic separator. The microbeads (typical diameter between 50 and 100 ?m) were prepared using the water-in-oil emulsification process. The prepared microbeads containing yeast cells with invertase activity enabled efficient sucrose conversion. The biocatalyst was quite stable; the same catalytic activity was observed after one month storage at 4 °C and the microbeads could be used at least six times.

308

Invert sugar formation with Saccharomyces cerevisiae cells encapsulated in magnetically responsive alginate microparticles  

Invert sugar (an equimolar mixture of glucose and fructose prepared by sucrose hydrolysis) is a very important food component. We have prepared magnetically responsive alginate microbeads containing entrapped Saccharomyces cerevisiae cells and magnetite microparticles which can be easily separated in an appropriate magnetic separator. The microbeads (typical diameter between 50 and 100 {mu}m) were prepared using the water-in-oil emulsification process. The prepared microbeads containing yeast cells with invertase activity enabled efficient sucrose conversion. The biocatalyst was quite stable; the same catalytic activity was observed after one month storage at 4 deg. C and the microbeads could be used at least six times.

309

Ultrafine 316L stainless steel particles with frozen-in magnetic structures characterized by means of electron backscattered diffraction  

Electron Backscatter Diffraction (EBSD) studies clearly revealed a different crystallographic structure of the smallest particle size fraction of gas-atomized AISI 316L stainless steel powder (<4mm) compared with larger sized fractions of the same powder (<45mm). Despite similar chemical compositions, the predominating structure of the smallest particle size fraction was ferritic (i.e., has ferromagnetic properties) whereas the larger sized particle fractions and massive 316L revealed an expected austenitic and non-magnetic structure. From these findings, it follows that direct magnetic separation can be applied to separate very fine sized particles. These structural differences explain previously observed dissimilarities from corrosion and metal release perspectives.

310

An RFQ injection system for the HRIBF  

At the Holifield Radioactive Ion Beam Facility (HRIBF) at Oak Ridge National Laboratory (ORNL), molecular ions extracted from a positive ion source and subsequently broken up in a charge exchange cell produce Radioactive Ion Beams (RIBs) with several hundred eV energy spread, preventing effective magnetic isobar separation. In order to perform magnetic isobar separation prior to charge exchange, a multi-harmonic buncher and a 12 MHz RFQ (Radio-Frequency Quadrupole) is proposed to supplement the present 300 kV injection system for the 25 MV tandem electrostatic accelerator. The RFQ will be mounted on a variable high voltage platform to accelerate ions with masses from 10 to 150 amu.

311

Magnetic iron oxide chestnutlike hierarchical nanostructures: preparation and their excellent arsenic removal capabilities.  

To obtain adsorbents with high As(V) removal capacity and quick magnetic separation simultaneously, we have fabricated maghemite (?-Fe(2)O(3)) and magnetite (Fe(3)O(4)) chestnutlike hierarchical nanostructures (CHNs) with strong ferromagnetic property by annealing the Fe(2)O(3) chestnutlike amorphous core/?-phase shell hierarchical nanoarchitectures (CAHNs) at different temperatures in a nitrogen atmosphere. Compared to the Fe(2)O(3) CAHNs, the saturated magnetization of the as-obtained ?-Fe(2)O(3) CHNs is enhanced over 10 times, while the As(V) removal capacity is maintained 74% and reaches 101.4 mg·g(-1). Both of the as-obtained ?-Fe(2)O(3) and Fe(3)O(4) CHNs can be separated simply and rapidly from treated water by magnetic separation after As(V) adsorption treatment. The As(V) adsorption process of the as-obtained ?-Fe(2)O(3) CHNs obeys well the Freundlich isotherm model rather than the Langmuir one, suggesting that a multilayered adsorption occurs on the surface of the ?-Fe(2)O(3) CHNs. Taking advantages of the high adsorption capacity, fast adsorption rate and quick magnetic separation from treated water, the ?-Fe(2)O(3) CHNs developed in the present study is expected to be an efficient magnetic adsorbent for As(V) removal from aqueous solutions. PMID:22796758

312

Evaluation of extractant-coated ferromagnetic microparticles for the recovery of hazardous metals from waste solution.  

A magnetically assisted chemical separation (MACS) process was developed earlier at Argonne National Laboratory (ANL). This compact process was designed for the separation of transuranics (TRU) and radionuclides from the liquid waste streams that exist at many DOE sites, with an overall reduction in waste volume requiring disposal. The MACS process combines the selectivity afforded by solvent extractant/ion exchange materials with magnetic separation to provide an efficient chemical separation. Recently, the MACS process has been evaluated with acidic organophosphorus extractants for hazardous metal recovery from waste solutions. Moreover, process scale-up design issues have been addressed with respect to particle filtration and recovery. Two acidic organophosphorus compounds have been investigated for hazardous metal recovery, bis(2,4,4-trimethylpentyl) phosphinic acid (Cyanex{reg_sign} 272) and bis(2,4,4-trimethylpentyl) dithiophosphinic acid (Cyanex{reg_sign} 301). Coated onto magnetic microparticles, these extractants demonstrated superior recovery of hazardous metals from solution, relative to what was expected on the basis of results from solvent extraction experiments. The results illustrate the diverse applications of MACS technology for dilute waste streams. Preliminary process scale-up experiments with a high-gradient magnetic separator at Oak Ridge National Laboratory have revealed that very low microparticle loss rates are possible.

313

Magnetic solid-phase extraction based on magnetic carbon nanotube for the determination of estrogens in milk.  

In this work, a novel method for the fabrication of magnetic carbon nanotubes based on 'aggregation wrap' was proposed. When carbon nanotubes and magnetic nanoparticles were vortically mixed in a solvent, the magnetic nanoparticles were wrapped into the carbon nanotube bundles that formed during the aggregation process, leading to the formation of magnetic carbon nanotubes. Thus, the resultant material can be separated from the solvent rapidly and conveniently by a magnet. Our investigation demonstrated that the 'aggregation wrap' mechanism for the preparation of magnetic composite is also applicable to other self-aggregated micro/nanomaterials, including graphene, graphite, C(60), etc. To testify the feasibility of the magnetic composites in sample preparation, the resultant magnetic carbon nanotubes were applied as sorbents for magnetic solid-phase extraction (MSPE) of estrogens in milk samples. Under optimized conditions, a rapid, convenient and efficient method for the determination of estrogens in milk samples was established by the combination of MSPE with high-performance liquid chromatography with fluorescence detector. The linearity range of the proposed method was 5-2000 ?g/L with correlation coefficients (R) of 0.9983-0.9994. The limit of detection (LOD) for three estrogens ranged from 1.21 to 2.35 ?g/L. The intra- and inter-day relative standard deviations (RSDs) were <9.3%. The reproducibility of the MSPE with different batches of magnetic carbon nanotubes was acceptable with RSD values <3.6%. PMID:21780288

314

Magnetic orientation and navigation in marine turtles, lobsters, and molluscs: concepts and conundrums.  

The Earth's magnetic field provides a pervasive source of directional information used by phylogenetically diverse marine animals. Behavioral experiments with sea turtles, spiny lobsters, and sea slugs have revealed that all have a magnetic compass sense, despite vast differences in the environment each inhabits and the spatial scale over which each moves. For two of these animals, the Earth's field also serves as a source of positional information. Hatchling loggerhead sea turtles from Florida responded to the magnetic fields found in three widely separated regions of the Atlantic Ocean by swimming in directions that would, in each case, facilitate movement along the migratory route. Thus, for young loggerheads, regional magnetic fields function as navigational markers and elicit changes in swimming direction at crucial geographic boundaries. Older turtles, as well as spiny lobsters, apparently acquire a "magnetic map" that enables them to use magnetic topography to determine their position relative to specific goals. Relatively little is known about the neural mechanisms that underlie magnetic orientation and navigation. A promising model system is the marine mollusc Tritonia diomedea, which possesses both a magnetic compass and a relatively simple nervous system. Six neurons in the brain of T. diomedea have been identified that respond to changes in magnetic fields. At least some of these appear to be ciliary motor neurons that generate or modulate the final behavioral output of the orientation circuitry. These findings represent an encouraging step toward a holistic understanding of the cells and circuitry that underlie magnetic orientation behavior in one model organism. PMID:21676799

315

High gradient magnetic particle separation in viscous flows by 3D BEM  

The boundary element method was applied to study the motion of magnetic particles in fluid flow under the action of external nonuniform magnetic field. The derived formulation combines the velocity-vorticity resolved Navier-Stokes equations with the Lagrange based particle tracking model, where the one-way coupling with fluid phase was considered. The derived algorithm was used to test a possible design of high gradient magnetic separation in a narrow channel by computing particles trajectories in channel flow under the influence of hydrodynamic and magnetic forces. Magnetic field gradient was obtained by magnetization wires placed outside of the channel. Simulations with varying external magnetic field and flow rate were preformed in order to asses the collection efficiency of the proposed device. We found that the collection efficiency decreases linearly with increasing flow rate. Also, the collection efficiency was found to increase with magnetic field strength only up a saturation point. Furthermore, we found that high collection efficiently is not feasible at high flow velocity and/or at weak magnetic field. Recommendation for optimal choice of external magnetic field and flow rate is discussed.

316

CFD simulation of the magnetophoretic separation in a microchannel  

The CFD simulation of the separation of labeled biospecies from a native fluid flowing through a planar microchannel, mediated by a magnetic field is presented in this study. The fluid flow, coupled with Eulerian advection-convection concentration equation, is utilized to model the transport of the magnetic biospecies. A moderate-gradient magnetic field caused accumulation of the magnetic labeled species in the vicinity of the higher magnetic field region. The re-distribution of the magnetically labeled species in the region close to the highest magnetic field zone presents a scheme for the focusing or collection of these species from the heterogeneous samples under the simulation conditions. The magnetic-fluidic interactions and interplay between the magnetophoretic mass transfer and molecular diffusion for different throughputs are analyzed. The study found out that the axial magnetic forces, created from a dipole-like magnetic field, is playing a major role in the vortex formation, and this complements the downward vertical force in confining the particles to a small region near the point with the highest magnetic strength. Also, the study predicts that the generated viscous shear stress levels in the interior region of the channel provide a safe transport mechanism for the biological cells in the solution. - Highlights: > Transport of magnetic microparticles through a planar microchannel is modeled and simulated. > Full Eulerian approach is used to solve the flow and concentration fields. > Simulations show a practical scheme for the collection of magnetically labeled biospecies. > Vortex formation as related to the magnetic force and flow fields is analyzed.

317

The design of a new gas-filled separator at JYFL  

A new gas-filled recoil separator, intended mainly for the study of reaction products in mass region of 100-200 produced in symmetric or nearly symmetric reactions, is under design at the Department of Physics in the University of Jyvaeskylae. The separator will be of the type DQQ where a horizontally focusing dipole (D) is followed by a quadrupole (Q) doublet. The bending radius of the dipole magnet will be 1850 mm and the bending angle 50 deg.

318

The design of a new gas-filled separator at JYFL  

A new gas-filled recoil separator, intended mainly for the study of reaction products in mass region of 100-200 produced in symmetric or nearly symmetric reactions, is under design at the Department of Physics in the University of Jyvaeskylae. The separator will be of the type DQQ where a horizontally focusing dipole (D) is followed by a quadrupole (Q) doublet. The bending radius of the dipole magnet will be 1850 mm and the bending angle 50 deg. .

319

Separation of variables in the classical integrable SL(3) magnetic chain  

There are two fundamental problems studied by the theory of hamiltonian integrable systems: integration of equations of motion, and construction of action-angle variables. The third problem, however, should be added to the list: separation of variables. Though much simpler than two others, it has important relations to the quantum integrability. Separation of variables is constructed for the $SL(3)$ magnetic chain --- an example of integrable model associated to a nonhyperelliptic algebraic curve.

320

Very low energy conversion electron detection system at the ISOCELE on-line isotope separator, Orsay  

A system designed and installed at the on-line isotope separator ISOCELE II allows the high resolution detection of low energy conversion electrons (down to 1 keV) emitted by mass separated radioactive sources: The use of a special tape transport permits both the slowing down of the incoming beam of radioactive ions up to a collection point and the acceleration of the electrons emitted by the 'collected sources' brought to a flat magnetic spectrograph. Typical spectra thus obtained are presented.

 
 
 
 
321

Method for recovery of materials from small batteries. Verfahren zur Ausarbeitung von Klein-Batterien  

In the main, only the metal casing of the small batteries is burst in a mechanical destruction. The destroyed material is roasted under motion in an oxidizing atmosphere at a temperature of 500 to 1000/sup 0/C and the evaporated mercury is extracted from the waste gas. The roasted material is separated by screening and magnetic separation into a scrap metal fraction containing brass and a collection fraction containing manganese, zinc and silver.

322

Mineral and coal processing  

Discusses recent developments in mineral and coal processing. Aspects covered are: computers; comminution and liberation; grinding; screening and classification; gravity; magnetic and electrostatic separation; froth flotation (including theory and reagents, flotation practice and machines and solid-liquid separation); and the treatment of specific ores, i.e., sulphide ores, oxide ores, industrial minerals and coal. The discussion of coal preparation includes gravity processing froth flotation, oil-agglomeration and other beneficiation techniques. 101 refs., 2 figs.

323

Ca0.85Sm0.15MnO3 A mixed antiferromagnet with unusual properties  

We investigated electrical and magnetic properties of the electron-doped manganites Ca1-xSmxMnO3 (0separation in electron doped manganites. The compounds with x = 0.13-0.15 show unusual difference between zero-field cooled and field-cooled resistivities which are not observed in lower compositions. Our results suggest that electronic phase separation alone is insufficient to understand the origin of the resistivity irreversibilities.

324

Evidence of glassy ferromagnetic phase and kinetic arrest of electronic phase in Sm0.35Pr0.15Sr0.5MnO3 manganites  

The effect of doping of rare earth Pr3+ ion as a replacement of Sm3+ in Sm0.5Sr0.5MnO3 is investigated. Temperature dependent dc and ac magnetic susceptibility, resistivity, magnetoresistance measurements on chemically synthesized (Sm0.5-xPrx)Sr0.5MnO3 show various unusual features with doping level x=0.15. The frequency independent ferromagnetic to paramagnetic transition at higher temperature (˜191 K) followed by a frequency dependent reentrant magnetic transition at lower temperature (˜31 K) has been observed. The nature of this frequency dependent reentrant magnetic transition is described by a critical slowing down model of spin glasses. From non-linear ac susceptibility measurements it has been confirmed that the finite size ferromagnetic clusters are formed as a consequence of intrinsic phase separation, and undergo spin glass-like freezing below a certain temperature. There is an unusual observation of a 2nd harmonic peak in the non-linear ac susceptibility around this reentrant magnetic transition at low temperature (˜31 K). Arrott plots at 10 and 30 K confirm the existence of glassy ferromagnetism below this low temperature reentrant transition. Electronic- and magneto-transport measurements show a strong magnetic field—temperature history dependence and strong irreversibility with respect to the sweeping of magnetic field. These results are attributed to the effect of phase separation and kinetic arrest of the electronic phase in this phase separated manganite at low temperatures.

325

Effect of interatomic distances on magnetic ordering of RMnSi (R = La, Y, Sm, Gd) compounds  

One determined dependence of nature of magnetic ordering of RMnSi compounds on d sub M sub n sub - sub M sub n distance between manganese atoms inside magnetic layers located in planes perpendicular to c axis. With that point in view one investigated into SmMnSi and GdMnSi compounds where the mentioned distances were near d sub M sub n sub - sub M sub n critical value separating the range of ferromagnetic and antiferromagnetic ordering of RMnSi compounds. Admission of lanthanum and yttrium (which respectively increase and decrease dimensions of crystalline cell) into rare-earth sublattice results in occurrence of magnetic phase transitions in these compounds

326

Z_3 Quantum Criticality in a spin-1/2 chain model  

The stability of the magnetization $m=1/3$ plateau phase of the XXZ spin-1/2 Heisenberg chain with competing interactions is investigated upon switching on a staggered transverse magnetic field. Within a bosonization approach, it is shown that the low-energy properties of the model are described by an effective two-dimensional XY model in a three-fold symmetry-breaking field. A phase transition in the three-state Potts universality class is expected separating the $m=1/3$ plateau phase to a phase where the spins are polarized along the staggered magnetic field. The Z$_3$ critical properties of the transition are determined within the bosonization approach.

327

Bose-Einstein condensates on a permanent magnetic film atom chip  

We present a permanent magnetic film atom chip based on perpendicularly magnetized TbGdFeCo films. This chip routinely produces a Bose-Einstein condensate (BEC) of 10^5 87Rb atoms using the magnetic film potential. Fragmentation observed near the film surface provides unique opportunities to study BEC in a disordered potential. We show this potential can be used to simultaneously produce multiple spatially separated condensates. We exploit part of this potential to realize a time-dependent double well system for splitting a condensate.

328

Bacteria capture, lysate clearance, and plasmid DNA extraction using pH-sensitive multifunctional magnetic nanoparticles  

A multifunctional magnetic nanoparticle (MNP)-assisted bioseparation method was developed to isolate plasmid DNA (pDNA) from Escherichia coli culture. Using the pH-sensitive carboxyl-modified magnetic nanoparticles, both cell capture and the subsequent removal of genomic DNA/protein complex after lysis can be achieved simply by magnetic separation. Furthermore, the yield and purity of pDNA extracted by MNPs are comparable to those obtained using organic solvents or commercial kits. This time- and cost-effective protocol does not require centrifugation or precipitation steps and has the potential for automated DNA extraction, especially within miniaturized lab chip applications.

329

Bacteria capture, lysate clearance, and plasmid DNA extraction using pH-sensitive multifunctional magnetic nanoparticles.  

A multifunctional magnetic nanoparticle (MNP)-assisted bioseparation method was developed to isolate plasmid DNA (pDNA) from Escherichia coli culture. Using the pH-sensitive carboxyl-modified magnetic nanoparticles, both cell capture and the subsequent removal of genomic DNA/protein complex after lysis can be achieved simply by magnetic separation. Furthermore, the yield and purity of pDNA extracted by MNPs are comparable to those obtained using organic solvents or commercial kits. This time- and cost-effective protocol does not require centrifugation or precipitation steps and has the potential for automated DNA extraction, especially within miniaturized lab chip applications. PMID:19903448

330

Synthesis and design of functionalized magnetic nanocolloids for water pollution remediation  

This work focus on the potential applications of magnetic nanoparticles on pollution remediation. We draw attention to the chemical design of functionalized magnetic colloids based on tartrate ligands to be used in magnetic separation of heavy metals from wastewater. Coupling the speciation diagrams of nanoferrites particles surface with that of the tartaric acid, it was possible to provide a theoretical prediction of the optimal pH for particle surface-ligand complexation. Finally, from an electrochemical approach based on simultaneous potentiometric and conductimetric titrations it was possible to determine the saturation value of the surface charge density of the functionalized nanoparticles and its pH dependence.

331

Automated processing integrated with a microflow cytometer for pathogen detection in clinical matrices  

A spinning magnetic trap (MagTrap) for automated sample processing was integrated with a microflow cytometer capable of simultaneously detecting multiple targets to provide an automated sample-to-answer diagnosis in 40min. After target capture on fluorescently coded magnetic microspheres, the magnetic trap automatically concentrated the fluorescently coded microspheres, separated the captured target from the sample matrix, and exposed the bound target sequentially to biotinylated tracer molecules and streptavidin-labeled phycoerythrin. The concentrated microspheres were then hydrodynamically focused in a microflow cytometer capable of 4-color analysis (two wavelengths for microsphere identification, one for light scatter to discriminate single microspheres and one for phycoerythrin bound t...

332

Layer-by-layer assembly of a magnetic nanoparticle shell on a thermoresponsive microgel core  

We describe the surface modification of magnetic nanoparticles (MNPs), the coverage of poly(N-isopropylacrylamide) (PNiPAM) microgel with the MNPs and the inductive heating of these carriers. PNiPAM surface itself was modified using the layer-by-layer (LbL) assembly of polyelectrolytes to facilitate the deposition of surface-modified MNPs. One advantage of this concept is it allows the tuning of the magnetic and thermoresponsive properties of individual components (nanoparticles and microgels) separately before assembling them. Characterisations of the hybrid core-shell are discussed. In particular, it is shown that (i) each layer is successfully deposited and, more importantly, (ii) the coated microgel retains its thermoresponsive and magnetic behaviour.

333

Testing of the large bore single aperture 1-meter superconducting dipoles made with phenolic inserts  

Two identical single aperture 1-metre superconducting dipoles have been built in collaboration with HMA Power Systems and tested at CERN. The 87.8 mm aperture magnets feature a single layer coil wound using LHC main dipole outer layer cable, phenolic spacer type collars, and a keyed two part structural iron yoke. The magnets are designed as models of the D1 separation dipole in the LHC experimental insertions, whose nominal field is 4.5 T at 4.5 K. In this report we present the test results of the two magnets at 4.3 K and 1.9 K.

334

Magnetic lumped parameter modeling of rotor eccentricity in brushless permanent-magnet motors  

Vibration, giving rise to acoustical noise, is an important index of motor performance. The unbalanced force due to rotor eccentricity caused by manufacturing imprecision or bearing defects is one possible source of excitation to vibration. The previously developed fast design package for permanent magnet motors, based on magnetic lumped parameter modeling, is modified to predict the influence of rotor eccentricity. Both static and dynamic cases are investigated. Magnetic material nonlinearity is taken into consideration. A two-dimensional relative permeance function is derived by conformal transformation followed by the modification of permeances modeling the air gap. Static and dynamic rotor eccentricity bring different effects to symmetric and asymmetric motors and are discussed separately.

335

A search for integrable four-dimensional nonlinear accelerator lattices  

Integrable nonlinear motion in accelerators has the potential to introduce a large betatron tune spread to suppress instabilities and to mitigate the effects of space charge and magnetic field errors. To create such an accelerator lattice one has to find magnetic and/or electric field combinations leading to a stable integrable motion. This paper presents families of lattices with one invariant where bounded motion can be easily created in large volumes of the phase space. In addition, it presents two examples of integrable nonlinear accelerator lattices, realizable with longitudinal-coordinate-dependent magnetic or electric fields with the stable nonlinear motion, which can be solved in terms of separable variables.

336

A search for integrable four-dimensional nonlinear accelerator lattices  

Integrable nonlinear motion in accelerators has the potential to introduce a large betatron tune spread to suppress instabilities and to mitigate the effects of space charge and magnetic field errors. To create such an accelerator lattice one has to find magnetic and/or electric field combinations leading to a stable integrable motion. This paper presents families of lattices with one invariant where bounded motion can be easily created in large volumes of the phase space. In addition, it presents two examples of integrable nonlinear accelerator lattices, realizable with longitudinal-coordinate-dependent magnetic or electric fields with the stable nonlinear motion, which can be solved in terms of separable variables.

337

Temperature rise in the lambertsen septum magnet associated with the positron target  

This note presents the results of EGS calculations and simple analytic models for the temperature rise in a spoiler, and magnet iron following such a spoiler, for a 33 GeV electron beam. Temperature rises in both spoiler and magnet iron of less than 100/sup 0/C/pulse are possible for 100..mu.. (Gaussian sigma) beams of 5 x 10/sup 10/e/sup -//pulse. The results should allow for easy optimization of spoiler thickness and spoiler-to-magnet separation distances. 3 references, 9 figures.

338

Unconventional magnetoresistance in long InSb nanowires  

Magnetoresistance in long correlated nanowires of degenerate semiconductor InSb in asbestos matrix (wire diameter of around 5 nm, length 0.1 - 1 mm) is studied over temperature range 2.3 - 300 K. At zero magnetic field the electric conduction $G$ and the current-voltage characteristics of such wires obey the power laws $G\\propto T^\\alpha$, $I\\propto V^\\beta$, expected for one-dimensional electron systems. The effect of magnetic field corresponds to a 20% growth of the exponents $\\alpha$, $\\beta$ at H=10 T. The observed magnetoresistance is caused by the magnetic-field-induced breaking of the spin-charge separation and represents a novel mechanism of magnetoresistance.

339

Interplay of Rashba, Zeeman and Landau splitting in a magnetic two dimensional electron gas  

The transport properties of a magnetic two dimensional electron gas consisting of a modulation doped n type HgMnTe/HgCdTe quantum well, QW, have been investigated. By analyzing the Shubnikov-de Haas oscillations and the node positions of their beating patterns, we have been able to separate the gate voltage dependent Rashba spin-orbit splitting from the temperature dependent giant Zeeman splitting. It has been experimentally demonstrated that the Rashba spin-orbit splitting is larger than or comparable to the $sp-d$ exchange interaction induced giant Zeeman splitting in this magnetic 2DEG even at moderately high magnetic fields.

340

High-strength metal nanomagnets for diagnostics and medicine: carbon shells allow long-term stability and reliable linker chemistry  

The rapidly growing applications of nanomagnets in magnetic drug delivery and separation in clinical diagnostics require strong and reliable magnetic vehicles. Strength conveys rapid processing, high delivery/targeting yield and rapid results when used in clinics. Reliability enables recycling of nanomagnets, regulatory-conforming drug formulations and efficient use of (expensive) antibodies in diagnostics, combined with reduced leaching (reagent loss). The present work illustrates how metal-based nanomagnets provide a two-three-times stronger magnetic particle than conventional magnetite-based materials. Ligands, antibodies or drugs can be anchored to such carbon/metal core/shell nanomagnets over covalent, hydrolysis-resistant carbon-carbon bonds. This linker chemistry resists strong acid...

 
 
 
 
341

Magnetic Silyl Scaffold Enables Efficient Recycling of Protecting Groups  

Abstract A novel organic/inorganic hybrid material comprising carbon-coated cobalt nanoparticles and a poly(benzylchloride)styrene shell is the first magnetic support that complies with important requirements for immobilized reagents and scavengers, that is, stability under harsh conditions (e.g., acids), sufficient loading (up to 2-mmol-g-1), and satisfying magnetization. The durability of the scaffold was demonstrated by immobilization of a trialkylsilane reagent, which served as a -magnetic- protecting group for a number of primary and secondary alcohols. Importantly, the scaffold could be efficiently separated, recycled, and reused after alcohol cleavage (HF-pyridine) via regeneration of the silyl chloride moiety with BCl3.

342

Current-driven Magnetization Reversal and Spin Wave Excitations in Co/Cu/Co Pillars  

Using thin film pillars ~100 nm in diameter, containing two ferromagnetic Co layers of different thicknesses separated by a paramagnetic Cu spacer, we examine effects of torques due to spin-polarized currents flowing perpendicular to the layers. In accordance with spin-transfer theory, spin-polarized electrons flowing from the thin to the thick Co layer can switch the magnetic moments of the layers antiparallel, while a reversed electron flow causes switching to a parallel state. When large magnetic fields are applied, the current no longer fully reverses the magnetic moment, but instead stimulates spin-wave excitations.

343

The Magnetic Casimir Effect  

The Casimir effect results from alterations of the zero-point electromagnetic energy introduced by boundary-conditions. For ferromagnetic layers separated by vacuum (or a dielectric) such boundary-conditions are influenced by the magneto-optical Kerr effect. We will show that this gives rise to a long-range magnetic interaction and discuss the effect for two different configurations (magnetization parallel and perpendicular to the layers). Analytical expressions are derived for two models and compared to numerical calculations. Numerical calculations of the effect for Fe are also presented and the possibility of an experimental observation of the Casimir magnetic interaction is discussed.

344

AC susceptibility of magnetic markers in suspension for liquid phase immunoassay  

AC susceptibility of magnetic markers in solution was studied for biosensor applications. First, frequency dependence of the susceptibility was measured, and size distribution of the markers was estimated by analyzing the experimental result with the so-called singular value decomposition (SVD) method. The size distribution estimated with the magnetic measurement agreed with that obtained from conventional optical measurement. Next, susceptibility measurement was applied to the liquid-phase immunoassay without bound/free (B/F) separation. We performed the detection of biotin-coated polymer beads in suspension using avidin-coated magnetic markers. Changes of the susceptibility and the size distribution caused by the binding reaction were shown.

345

AC susceptibility of magnetic markers in suspension for liquid phase immunoassay  

AC susceptibility of magnetic markers in solution was studied for biosensor applications. First, frequency dependence of the susceptibility was measured, and size distribution of the markers was estimated by analyzing the experimental result with the so-called singular value decomposition (SVD) method. The size distribution estimated with the magnetic measurement agreed with that obtained from conventional optical measurement. Next, susceptibility measurement was applied to the liquid-phase immunoassay without bound/free (B/F) separation. We performed the detection of biotin-coated polymer beads in suspension using avidin-coated magnetic markers. Changes of the susceptibility and the size distribution caused by the binding reaction were shown.

346

Specific bloch wall area of tape wound cores of amorphous and crystalline material  

At low magnetizing frequencies not the total available domain wall area is instantaneously in motion. A method is presented to separate the simultaneously irreversibly moved domain wall area (specific area Sirr) from that wall area which is elastically attached at pinning centres. For tape wound cores of iron silicon and of metallic glass Sirr was determined as function of the magnetizing frequency by measuring the complex core impedance and applying a simple domain model. At very low magnetizing frequencies fm<10-2s-1 the quantity Sirr is found to be approximately proportional to f0.8m.

347

Testing chiral magnetic effect with central U+U collisions  

Quark interaction with topologically non-trivial gluonic fields, instantons and sphalerons, violates \\P~ and \\CP~ symmetry. In the strong magnetic field of a non-central nuclear collision such interactions lead to the charge separation along the magnetic field, the so called chiral magnetic effect (CME). Recent results from STAR collaboration on charge dependent correlations are consistent with theoretical expectations for CME but may have contributions from other effects, which prevents definitive interpretation of the data. Here I propose to use central body-body U+U collisions to disentangle correlations due to CME from possible background correlations due to elliptic flow. Further more quantitative studies can be performed with collision of isobaric beams.

348

The Septa for LEIR Extraction and PS Injection  

The Low Energy Ion Ring (LEIR) is part of the CERN LHC injector chain for ions. The LEIR extraction uses a pulsed magnetic septum, clamped around a metallic vacuum chamber. Apart from separating the ultra high vacuum in the LEIR ring from the less good vacuum in the transfer line to the PS this chamber also serves as magnetic screen and retains the septum conductor in place. The PS ion injection septum consists of a pulsed laminated magnet under vacuum, featuring a single-turn water cooled coil and a remote positioning system. The design, the construction and the commissioning of both septa are described.

349

Particle Energization in 3D Magnetic Reconnection of Relativistic Pair Plasmas  

We present large scale 3D particle-in-cell simulations to examine particle energization in magnetic reconnection in relativistic electron-positron (pair) plasmas. These simulations are large enough to accommodate a sufficient number of tearing and kink modes. We find that the magnetic energy dissipation is first facilitated by the tearing instability and followed by the secondary kink instability. Particles are mostly energized inside the magnetic islands during the tearing stage due to the spatially varying electric fields produced by the outflows from reconnection. Secondary kink instability also leads to some particle acceleration due to the electric fields caused by space charge separation. Accelerated particles are, however, observed to be thermalized.

350

Method for oxidation of pyrite in coal to magnetite and low field magnetic separation  

A method is described for reducing the sulfur concentration of pyrite-containing pulverized coal comprising the steps of: converting at least a fraction of the pyrite in the coal to magnetite for increasing the magnetization of the coal; and magnetically separating at least a portion of the pyrite from the coal in a low-strength magnetic field; the step of converting pyrite to magnetite including heating the coal in an atmosphere having an inert gas that is inert to pyrite containing 3 to 60 torr partial pressure of air to a temperature in the range 390/sup 0/C to 455/sup 0/C for at least two minutes.

351

Intercalibration of Boreal and Tethyan time scales: the magnetobiostratigraphy of the Middle Triassic and the latest Early Triassic from Spitsbergen, Arctic Norway  

Abstract An integrated biomagnetostratigraphic study of the latest Early Triassic to the upper parts of the Middle Triassic, at Milne Edwardsfjellet in central Spitsbergen, Svalbard, allows a detailed correlation of Boreal and Tethyan biostratigraphies. The biostratigraphy consists of ammonoid and palynomorph zonations, supported by conodonts, through some 234 m of succession in two adjacent sections. The magnetostratigraphy consists of 10 substantive normal-reverse polarity chrons, defined by sampling at 150 stratigraphic levels. The magnetization is carried by magnetite and an unidentified magnetic sulphide, and is difficult to fully separate from a strong present-day-like magnetization. The biomagnetostratigraphy from the late Olenekian (Vendomdalen Member) is supplemented by data from ...

352

Coercive Field and Magnetization Deficit in Ga(1-x)Mn(x)As Epilayers  

We have studied the field dependence of the magnetization in epilayers of the diluted magnetic semiconductor Ga(1-x)Mn(x)As for 0.0135 < x < 0.083. Measurements of the low temperature magnetization in fields up to 3 T show a significant deficit in the total moment below that expected for full saturation of all the Mn spins. These results suggest that the spin state of the non-ferromagnetic Mn spins is energetically well separated from the ferromagnetism of the bulk of the spins. We have also studied the coercive field (Hc) as a function of temperature and Mn concentration, finding that Hc decreases with increasing Mn concentration as predicted theoretically.

353

Nanostructured thin manganite films in megagauss magnetic field  

We report on the use of the colossal magnetoresistance (CMR) effect in manganites for the measurement of pulsed magnetic fields up to the megagauss limit. To increase the application range in a magnetic field, we fabricated nanostructured La-Sr-Mn-O films consisting of nanocrystallites cummulated into clusters separated by highly amorphous inter-cluster boundaries. We demonstrate that the CMR effect does not saturate in these films at 77 K up to 91.4 T. Moreover, the magnetoresistance behavior at 290 K shows that nanostructured manganite films are promising candidates for the development of magnetic field scalar sensors operating in wide field and temperature ranges.

354

Magnetic nanoparticles grafted with b-cyclodextrin-polyurethane polymer as a novel nanomagnetic polymer brush catalyst for nucleophilic substitution reactions of benzyl halides in water  

The polymer coated magnetic nanoparticles has gained significant attention for potential applications in biomedicine, separations, and magnetic storage. In this study, b-cyclodextrin-polyurethane polymer coated Fe3O4 magnetic nanoparticle as a novel class of hybrid organic/inorganic molecular catalyst was successfully prepared and evaluated as solid-liquid phase-transfer catalyst and molecular host system for nucleophilic substitution reactions. The nanocomposite has demonstrated the ability to catalytic the nucleophilic substitution reaction of benzyl halides with thiocyanate, azide, cyanide and acetate anions in water. No evidence for the formation of by-products for example isothiocyanate or alcohol was observed and the products obtained in pure form without further purification. The na...

355

Novel Coexistence of Superconductivity with Two Distinct Magnetic Orders  

The heavy fermion Ce(Rh,Ir)In5 system exhibits properties that range from an incommensurate antiferromagnet on the Rh-rich end to an exotic superconductor on the Ir-rich end of the phase diagram. At intermediate composition where antiferromagnetism coexists with superconductivity, two types of magnetic order are observed: the incommensurate one of CeRhIn5 and a new, commensurate antiferromagnetism that orders separately. The coexistence of f-electron superconductivity with two distinct f-electron magnetic orders is unique among unconventional superconductors, adding a new variety to the usual coexistence found in magnetic superconductors.

356

Finite-Size Scaling in the Diluted Two-Dimensional Heisenberg Antiferromagnet  

Ground state properties of the randomly diluted two-dimensional Heisenberg antiferromagnet are discussed. Quantum Monte Carlo (stochastic series expansion) data for L × L lattices, with L up to 64, are extrapolated to infinite size for dilution fractions p between 0 (clean system) and p* (the percolation threshold). The sublattice magnetization is calculated using a decomposition into a classical and a quantum mechanical factor, which are evaluated separately. The quantum mechanical factor (the sublattice magnetization of the largest connected cluster of magnetic sites) remains finite at the percolation threshold, implying that the dilution driven order-disorder transition is a classical percolation transition. The spin stiffness is calculated using the winding number fluctuations.   

357

Quantum phase transitions in the itinerant ferromagnet ZrZn{sub 2}  

We report a study of the pressure p, temperature T and magnetic field B phase diagram of ZrZn{sub 2}, the most promising material to exhibit ferromagnetic quantum criticality. We find that the ordered ferromagnetic moment disappears discontinuously at p{sub c}=16.5kbar. Thus, a tricritical point separates a line of first-order ferromagnetic transitions from second-order (continuous) transitions at higher temperature. We also identify two lines of transitions of the magnetization isotherms up to 12T in the p-T plane where the derivative of the magnetization changes rapidly.

358

Time-of-flight flow imaging using NMR remote detection  

A time-of-flight imaging technique is introduced to visualize fluid flow and dispersion through porous media using NMR. As the fluid flows through a sample, the nuclear spin magnetization is modulated by RF pulses and magnetic field gradients to encode the spatial coordinates of the fluid. When the fluid leaves the sample, its magnetization is recorded by a second RF coil. This scheme not only facilitates a time-dependent imaging of fluid flow, it also allows a separate optimization of encoding and detection subsystems to enhance overall sensitivity. The technique is demonstrated by imaging gas flow through a porous rock.

359

Nonlinear traveling waves in confined ferrofluids  

We study the development of nonlinear traveling waves on the interface separating two viscous fluids flowing in parallel in a vertical Hele-Shaw cell. One of the fluids is a ferrofluid and a uniform magnetic field is applied in the plane of the cell, making an angle with the initially undisturbed interface. We employ a mode-coupling theory that predicts the possibility of controlling the speed of the waves by purely magnetic means. The influence of the tilted magnetic field on the waves shape profile and the establishment of stationary traveling wave structures are investigated.

360

CLASHING BEAM PARTICLE ACCELERATOR  

A charged-particle accelerator of the proton synchrotron class having means for simultaneously accelerating two separate contra-rotating particle beams within a single annular magnet structure is reported. The magnet provides two concentric circular field regions of opposite magnetic polarity with one field region being of slightly less diameter than the other. The accelerator includes a deflector means straddling the two particle orbits and acting to collide the two particle beams after each has been accelerated to a desired energy. The deflector has the further property of returning particles which do not undergo collision to the regular orbits whereby the particles recirculate with the possibility of colliding upon subsequent passages through the deflector.

 
 
 
 
361

Quantum Dynamics of Spin Wave Propagation Through Domain Walls  

Through numerical solution of the time-dependent Schrodinger equation, we demonstrate that magnetic chains with uniaxial anisotropy support stable structures, separating ferromagnetic domains of opposite magnetization. These structures, domain walls in a quantum system, are shown to remain stable if they interact with a spin wave. We find that a domain wall transmits the longitudinal component of the spin excitations only. Our results suggests that continuous, classical spin models described by LLG equation cannot be used to describe spin wave-domain wall interaction in microscopic magnetic systems.

362

Kelvin-Helmholtz instability of an anisotropic pressure plasma with generalized polytrope laws  

The Kelvin-Helmholtz instability (K.H.) of two magnetized compressible fluids flowing in opposite direction is investigated. The anisotropic pressures are considered in the description of plasma using MHD set of equations. The magnetic field is assumed in the direction of flow and perpendicular to the direction of separation of two fluids. The pressure relations with polytropic index are used and using boundary conditions a general dispersion relation for K.H. instability is obtained. It is found that the condition of K.H. instability depends upon magnetic field, parallel and perpendicular pressures and polytropic index. The condition of K.H. instability for MHD and CGL system is also obtained. (author)

363

The ferromagnetic and antiferromagnetic phases in anion deficient La0.5-xPrxBa0.5CoO3-? cobaltites  

Neutron powder diffraction studies of crystal and magnetic structures, magnetization and magnetotransport measurements have been performed for La0.5-xPrxBa0.5CoO3-? (xstate. The compositions with antiferromagnetic component show structural phase separation, strong increase of the unit cell volume upon cooling, and anomalous magnetization behavior. It is suggested that these phenomena are associated with stabilization of Co3+ ions in high/low spin state at low temperature. The high/low spin state corresponds antiferromagnetic phase, whereas in the ferromagnetic one, the Co3+ and Co4+ ions adopt intermediate spin state.

364

Crystalline electric fields and the ground state of Ce$_{3}$Rh$_{4}$Pb$_{13}$  

We have succeeded in synthesizing of single crystals of a new intermetallic compound, Ce$_{3}$Rh$_{4}$Pb$_{13}$. Magnetic susceptibility measurements indicate that the Ce moments are highly localized, despite the metallic character of the electrical resistivity. Heat capacity measurements reveal that the cubic crystal electric field lifts the six-fold degeneracy of the Ce$^{3+}$ ground state, with the quartet state separated by approximately 60 K from the doublet ground state. The magnetic field dependence of the heat capacity at low temperature indicates a further splitting of the doublet, but no sign of magnetic order was found above 0.35 K.

365

A study on the beneficiation of sericitic pottery stone for a white ware  

For the application of the Chojeon pottery stone to white ware, flotation and magnetic separation were carried out to remove iron minerals in it. To obtain the optimum conditions for flotation, the effects of particle size, the kinds and dosage of collector, the pH of the slurry, the scavenging times and the pulp density on the yield and rejection rate were investigated. The Chojeon pottery stone contained 1.26 wt.% Fe{sub 2}O{sub 3}. The raw ore mainly consisted of quartz(SiO{sub 2}), sericite(K{sub 2}Al{sub 4}Si{sub 6}Al{sub 2}O{sub 20}(OH,F){sub 4}) and dolomite(CaMg(CO{sub 3}){sub 2}). In addition, fine grained pyrite(FeS{sub 2}) and siderite(FeCO{sub 3}) existed as iron bearing minerals in the sample. The results of characterization for Chojeon pottery stone suggest that flotation and magnetic separation are more effective for removing fine grained iron minerals from the sample. The optimum condition for the flotation was obtained at particle size: 65mesh, dosage of AP-404 as first promoter: 637gr./t, dosage of AP-404 as second promoter: 127gr./t, frother: 18gr./t, scavenging: 2 times, cleaning: 1 time, pulp density: 24% solids, pH: 5, and pulp density: 10% solids and feed rate: 1 l/min., magnetic density: 10,000 gauss for the magnetic separation, the 1.26 wt.% Fe{sub 2}O{sub 3} content of raw ore decreased to 0.30 wt.% after the flotation and subsequent magnetic separation at the optimum condition. The calcined whiteness of the final product increased from 74.25 to 91.73 and plasticity and subsequent magnetic separation process was effective for the removal of iron minerals in the sample. It was also evident that the beneficiated pottery stone can be used as a raw material for high grade ceramics. (author). 5 refs., 4 tabs., 8 figs.

366

Cryo magnetic separation adaptation to environment technologies: application to industrial effluents; Adaptation de la separation cryomagnetique aux technologies de l`environnement: application a l`epuration d`effluents liquides industriels  

Cryomagnetic separation adaptation to environment technologies application to industrial liquid effluents. The performance, obtained by superconducting high filed - high gradient magnetic separation, permitted to foresee the magnetic treatment of heavy metals in rinse waters, derived from the surface finishing industry. The paramagnetic ions, precipitated in basic media as hydroxides, present a very hydrated amorphous structure, which masks their subjacent magnetic properties. Coprecipitation of a `magnetic carrier`, jointly with the heavy metals, has been studied: ferric chloride forms in basic media, an hydrated iron oxide. Its structure is of the goethite type, and it stabilizes as hematite. The magnetic susceptibility of the obtained product is still weak and its crystalline structure is not enough affirmative to utilize magnetic filtration with efficiency. Mixture of ferrous sulphate and ferric chloride forms, in a basic media, an hydrated magnetite. Initial ideal ratio between divalent iron and trivalent iron, varies between 0,5 and 1,2. This mixture, coprecipitated with the heavy metals, permits to optimize the magnetic cleaning of the fluids in a high field - high gradient filter. (author)

367

Magnetic hetero-flocculation of paramagnetic colloidal particles  

The feasibility of a high-gradient magnetic separation process, utilizing magnetite as the energizable element in lieu of stainless steel wool, is evaluated by means of an equilibrium, two-particle, magnetic hetero-flocculation model. The model calculates the net force, defined as the sum of the magnetic, electrostatic, and van der Waals forces, exerted on a paramagnetic nanoparticle that is in the proximity of a fixed magnetite particle. Since the nanoparticle-magnetite system is assumed to be in direct contact with the moving fluid, the influence of the hydrodynamic force on the magnetic attractive force between the two particles is also explored. This model clearly reveals the ranges and conditions over which each of these various forces contributes to the net force relative to Brownian (thermal) motion. The model also reveals the feasibility of using magnetite particles instead of stainless steel as the energizable element for high-gradient magnetic separation. Important variables investigated include the size and surface charge of the particles, the magnetic field, the flow velocity, the electrolyte concentration, and the magnetic susceptibility of the nanoparticle.

368

M13 bacteriophage-activated superparamagnetic beads for affinity separation.  

The growth of the biopharmaceutical industry has created a demand for new technologies for the purification of genetically engineered proteins.The efficiency of large-scale, high-gradient magnetic fishing could be improved if magnetic particles offering higher binding capacity and magnetization were available. This article describes several strategies for synthesizing microbeads that are composed of a M13 bacteriophage layer assembled on a superparamagnetic core. Chemical cross-linking of the pVIII proteins to a carboxyl-functionalized bead produces highly responsive superparamagnetic particles (SPM) with a side-on oriented, adherent virus monolayer. Also, the genetic manipulation of the pIII proteins with a His(6) peptide sequence allows reversible assembly of the bacteriophage on a nitrilotriacetic-acid-functionalized core in an end-on configuration. These phage-magnetic particles are successfully used to separate antibodies from high-protein concentration solutions in a single step with a >90% purity. The dense magnetic core of these particles makes them five times more responsive to magnetic fields than commercial materials composed of polymer-(iron oxide) composites and a monolayer of phage could produce a 1000 fold higher antibody binding capacity. These new bionanomaterials appear to be well-suited to large-scale high-gradient magnetic fishing separation and promise to be cost effective as a result of the self-assembling and self-replicating properties of genetically engineered M13 bacteriophage. PMID:22619210

369

Recovery of iron from cyanide tailings with reduction roasting-water leaching followed by magnetic separation.  

Cyanide tailing is a kind of solid waste produced in the process of gold extraction from gold ore. In this paper, recovery of iron from cyanide tailings was studied with reduction roasting-water leaching process followed by magnetic separation. After analysis of chemical composition and crystalline phase, the effects of different parameters on recovery of iron were chiefly introduced. Systematic studies indicate that the high recovery rate and grade of magnetic concentrate of iron can be achieved under the following conditions: weight ratios of cyanide tailings/activated carbon/sodium carbonate/sodium sulfate, 100:10:3:10; temperature, 50 °C; time, 60 min at the reduction roasting stage; the liquid to solid ratio is 15:1 (ml/g), leaching at 60 °C for 5 min and stirring speed at 20 r/min at water-leaching; exciting current is 2A at magnetic separation. The iron grade of magnetic concentrate was 59.11% and the recovery ratio was 75.12%. The mineralography of cyanide tailings, roasted product, water-leached sample, magnetic concentrate and magnetic tailings were studied by X-ray powder diffraction (XRD) technique. The microstructures of above products except magnetic tailings were also analyzed by scanning electron microscope (SEM) and energy disperse spectroscopy (EDS) to help understand the mechanism. PMID:22333161

370

Dielectric response to the low-temperature magnetic defect structure and spin state transition in polycrystalline LaCoO3  

The dielectric and magnetic properties and their correlations were investigated in polycrystalline perovskite LaCoO3-? . The intrinsic bulk and grain-boundary (GB) dielectric relaxation processes were deconvoluted using impedance spectroscopy between 20 and 120 K, and resistivity and capacitance were analyzed separately. A thermally induced magnetic transition from a Co3+ low-spin (LS) (S=0;t2g6eg0) to a higher spin state occurs at Ts1?80K , which is controversial in nature and has been suggested to be an intermediate-spin (IS) state (S=1;t2g5eg1) or a high-spin (HS) state (S=2;t2g4eg2) transition. This spin state transition was confirmed by magnetic-susceptibility measurements and was reflected in the impedance by a split of the single GB relaxation process into two coexisting contributions. This apparent electronic phase coexistence at T>80K was interpreted as a reflection of the coexistence of magnetic LS and IS/HS states. At lower temperatures (T?40K) perceptible variation in bulk dielectric permittivity with temperature appeared to be correlated with the magnetic susceptibility associated with a magnetic defect structure. At 40Kseparated GB and bulk resistivity vs T curves were consistent with localized polaron Mott variable-range hopping (VRH) based on impurity conduction. Below 40 K, a crossover from impurity Mott’s VRH to another type of thermally activated charge transport was detected, which was correlated with the appearance of the defect-related magnetism.

371

Magma flow directions inferred from field evidence and magnetic fabric studies of the Streitishvarf composite dike in east Iceland  

Anisotropy of magnetic susceptibility (AMS) and rock magnetic studies have been made on three outcrops separated by 12km along strike (NNE-SSW) on the Streitishvarf composite dike in east Iceland. Samples for this study have been collected from the inner quartz-porphyry part of the dike, which show clear field evidence of a lateral flow component from north to south at one of the sites. This flow component is consistent with margin AMS results from all three sites. The quartz-porphyry has a substantial bulk magnetic susceptibility (10^-^2 SI) mainly carried by magnetically soft titanium-poor titanomagnetite (MDF ~15mT). The ferrimagnetic grains yield a characteristic remanent magnetization in all three sites which gives a virtual geomagnetic pole at latitude 52.6^o S and longitude 319.6^o ...

372

Magnetoconvection and dynamo coefficients Dependence of the alpha-effect on rotation and magnetic field  

We present numerical simulations of three-dimensional compressible magnetoconvection in a rotating rectangular box that represents a section of the solar convection zone. The box contains a convectively unstable layer, surrounded by stably stratified layers with overshooting convection. The magnetic Reynolds number, Rm, is chosen subcritical, thus excluding spontaneous growth of the magnetic field through dynamo action, and the magnetic energy is maintained by introducing a constant magnetic field into the box, once convection has attained a statistically stationary state. Under the influence of the Coriolis force, the advection of the magnetic field results in a non-vanishing contribution to the mean electric field, given by uxb. From this electric field, we calculate the alpha-effect, separately for the stably and the unstably stratified layers, by averaging over time and over suitably defined volumes. From the variation of alpha we derive an error estimate, and the dependence of alpha on rotation and magne...

373

Network numerical analysis of hydromagnetic squeeze film flow dynamics between two parallel rotating disks with induced magnetic field effects  

We study numerically the hydromagnetic squeeze film between two rotating disks using the numerical network simulation method. The external magnetic field, H, generates an induced magnetic field, B, with radial (Br), tangential (B?) and axial (Bz) components between the two disks, which rotate with different angular velocities, ?1 and ?2, and at time t are separated by a distance D(1??t)1/2. The applied magnetic field at the lower disk is assumed to be zero. The conservation equations for mass, momentum and induced magnetic field are reduced to a set of ordinary differential equations using a series of transformations, in terms of four dependent variables, f (axial velocity), g (azimuthal velocity), m (axial magnetic field component) and n (azimuthal ...

374

Application of Upgraded X-ray Magnetic Diffraction Experimental System to 3d- and 4f-Electron Ferromagnets  

An experimental system of X-ray magnetic diffraction (XMD) is developed on BL3C at the Photon Factory (PF) of High Energy Research Organization (KEK). We applied this upgraded XMD experimental system to 3d- and 4f-electron ferromagnet, YTiO3 and CeRh3B2, respectively. In YTiO3 we successfully obtained spin magnetic form factor for 31 reciprocal lattice points. The observed spin magnetic form factor suggests anisotropic spin density distribution in real space. In CeRh3B2 we succeeded in measuring spin and orbital magnetic form factor separately. We found that the dominant part of the magnetic moment is the orbital component in CeRh3B2. [DOI: 10.1380/ejssnt.2011.134]   

375

Study of the Morin transition in nearly perfect crystals of hematite by diffraction and topography. [Fe sub 2 O sub 3  

The spin reorientational magnetic Morin transition is investigated on nearly perfect crystals of hematite by combining neutron diffraction, neutron and synchrotron radiation topography, and magnetization measurements. The samples are platelet shaped crystals, with their main surface parallel to the (111) basal plane. The magnetization measurements show that the main part of the transition occurs over a rather narrow temperature range (about 3 K), whereas this range appears broadened to about 13 K on the neutron diffraction curves. Neutron topographs show the whole crystal image during transition and X-ray topographs show zone contrast when modifying the applied magnetic field. These experimental facts indicate that the interfaces which separate the weakly ferromagnetic and the antiferromagnetic phases are parallel to the main surfaces of the crystals. This is the basis for a very simple model which explains, through severe extinction effects, the apparent contradiction between neutron diffraction and magnetization measurements, and leads to an estimation of the crystal perfection parameters. (orig.).

376

Twisted magnetic structures emerging from buoyancy instabilities  

We here report calculations of magnetic buoyancy instabilities of a sheared magnetic layer where two separate zones are unstable. The idea is to study the possible generation of large-scale helical structures which could then rise through a stellar convection zone and emerge at the surface to create active regions. The calculations shown here are a follow-up of the work of Favier et al. (2012) where the instability developed in a weakly magnetized atmosphere, consisting of a uniform field oriented in a different direction from the unstable layer below. Here, the top layer representing the atmosphere is itself unstable to buoyancy instabilities and thus quickly creates a more complex magnetic configuration with which the layer below will interact. We also find in this case that the accumulation of magnetic tension between the two unstable layers favors the creation of large-scale helical structures.

377

Magnetic microstructure of candidates for epitaxial dual Heusler magnetic tunnel junctions  

Heusler alloys are considered as interesting ferromagnetic electrode materials for magnetic tunnel junctions, because of their high spin polarization. We, therefore, investigated the micromagnetic properties in a prototypical thin film system comprising two different Heusler phases Co{sub 2}MnSi (CMS) and Co{sub 2}FeSi (CFS) separated by a MgO barrier. The magnetic microstructure was investigated by X-ray photoemission electron microscopy (XPEEM). We find a strong influence of the Heusler phase formation process on the magnetic domain patterns. SiO{sub 2}/V/CMS/MgO/CFS and SiO{sub 2}/V/CFS/MgO/CMS trilayer structures exhibit a strikingly different magnetic behavior, which is due to pinhole coupling through the MgO barrier and a strong thickness dependence of the magnetic ordering in Co{sub 2}MnSi.

378

X-ray magnetic diffraction of ferromagnets with synchrotron radiation  

X-ray magnetic diffraction experiment of ferromagnets that utilizes elliptically polarized synchrotron radiation is presented. First we have reviewed shortly historical backgrounds and theoretical aspects of the experiment. We have presented how the magnetic form factors are measured and are separated into the spin-moment component and the orbital-moment component in this experiment. Peculiar features of the polarization factor of this experiment have been explained. We have introduced two examples of the experiment. One is the measurement of the spin-magnetic form factor of SmAl sub 2 with white X-rays from a bending magnet at the Photon Factory. The other is the measurement of the orbital-magnetic form factor of Holmium Iron Garnets with monochromatic X-rays from an undulator at the SPring-8. Finally we summarize the article and show some future prospects of this experiment. (author)

379

The emergence of spin electronics in data storage.  

Electrons have a charge and a spin, but until recently these were considered separately. In classical electronics, charges are moved by electric fields to transmit information and are stored in a capacitor to save it. In magnetic recording, magnetic fields have been used to read or write the information stored on the magnetization, which 'measures' the local orientation of spins in ferromagnets. The picture started to change in 1988, when the discovery of giant magnetoresistance opened the way to efficient control of charge transport through magnetization. The recent expansion of hard-disk recording owes much to this development. We are starting to see a new paradigm where magnetization dynamics and charge currents act on each other in nanostructured artificial materials. Ultimately, 'spin currents' could even replace charge currents for the transfer and treatment of information, allowing faster, low-energy operations: spin electronics is on its way. PMID:17972936

380

Magnetic chitosan composite particles: Evaluation of thorium and uranyl ion adsorption from aqueous solutions  

Magnetic chitosan composite particles with 40@mm average size and 24emu/g saturation magnetization obtained by an in situ procedure were evaluated as a new low-cost adsorbent for radioactive wastewater decontamination. Sorbent characterization by SEM, EDX, FTIR and magnetization measurements proved that the target ions were bound and their surface distribution was uniform. The 18emu/g magnetization of the metal loaded particles was high enough to ensure their easy magnetic field separation and recovery. The parameters influencing the sorption process were optimized with respect to sorbent mass, target ion concentration and contact time. The material under study had superior adsorption capacity both for uranyl (666.67mg/g) and thorium (312.50mg/g) ions when compared to other low-cost adsorb...

 
 
 
 
381

Experimental observation of the optical spin transfer torque  

The spin transfer torque is a phenomenon in which angular momentum of a spin polarized electrical current entering a ferromagnet is transferred to the magnetization. The effect has opened a new research field of electrically driven magnetization dynamics in magnetic nanostructures and plays an important role in the development of a new generation of memory devices and tunable oscillators. Optical excitations of magnetic systems by laser pulses have been a separate research field the aim of which is to explore magnetization dynamics at short timescales and enable ultrafast spintronic devices. We report the experimental observation of the optical spin transfer torque, predicted theoretically several years ago, building the bridge between these two fields of spintronics research. In a pump-an...

382

Evidence for coexistence of exchange bias and exchange spring effects in oxidized Co nanocluster assembled films  

We present the observation of a double hysteresis loop behavior in oxidized Co nanocluster assembled films. These films consist of ferromagnetic Co clusters of about 2 nm diameter, embedded in a thin antiferromagnetic CoO matrix. Magnetization measurements after zero field cooling from 300 to 5 K show this double loop behavior, with remanent magnetization of the sample determining the point of loop separation. Such magnetization behavior is related to the presence of two ferromagnetic parts with antiparallel orientations of their magnetization vectors. While the loop shifts are provided via the exchange bias mechanism, the alignment of randomly oriented magnetization vectors of Co clusters in either of two directions suggests the presence of an exchange spring effect in the system.

383

Synthesis and biochemical properties of fluorescent/magnetic bifunctional starch particles  

Magnetic starch particles (MSPs) were synthesized in water-in-oil microemulsion at room temperature. MSPs were characterized by transmission electron microscopy (TEM), Fourier transform infrared spectrometry (FTIR), zeta potential system, thermogravimetric analysis (TGA) and vibrating sample magnetometry (VSM). The average diameter of the MSPs was 220 nm, dispersed with well-proportioned size and magnetic resonance, the saturation magnetization was 3.64 A?m2/kg. MSP was coated with poly-L-lysine (PLL), and then the surface of PLL-MSP was combined with fluorescein isothiocynate (FITC). Results show that fluorescent/magnetic starch particles (FMSPs) are of stable photo-bleaching capability compared with free FITC, with low bio-toxicity and certain function of magnetic separation. It is expec...

384

Effect of a strong magnetic field on a laser plasma produced from a solid target in a gaseous atmosphere  

The effect of a magnetic field on the dynamics of the development of a laser plasma produced from a target at different pressures of the ambient gas has been investigated with the aid of a streak camera. The velocity of propagation of a laser-supported detonation wave in a magnetic field of intensity H=170 kOe turned out to be higher than in the H=0 case. The presence of a magnetic field leads to a more efficient generation of x rays by the laser plasma from the focal region. It has been found that a radially-confined, long-lived, hot plasma is formed in a magnetic field along the optical axis. The possibility in principle of separating with the aid of a strong magnetic field plasma formations with different parameters is demonstrated.

385

Inductive magnetization of low-temperature ordered L1{sub 0}-FePt with CoAg underlayer  

The feasibility of controlling film microstructure and nanocomposition of FePt film with various compositions of the CoAg underlayer by ion beam sputtering accompanied by an external magnetic field was performed. The characteristic of phase separation of the CoAg underlayer was employed to induce an inductive magnetism region which reduced the annealing temperature acquired for L1{sub 0}-FePt. The segregation of Co atoms could influence the corresponding magnetic properties of FePt. After annealing at 400 degree sign C, the FePt/CoAg films deposited under the magnetic field showed a larger coercivity (H{sub c}=5 kOe) than that of the film deposited without a magnetic field (H{sub c}=0.4 kOe)

386

Layer-resolved real space imaging of domain wall interactions in magnetic tunnel junctions  

We have performed a layer-resolved, microscopic study of interactions between domain walls in two magnetic layers separated by a non-magnetic one, using high-resolution x-ray photoemission electron microscopy. Domain walls in the hard magnetic Co layer of a Co/Al2O3/FeNi trilayer with in-plane uniaxial anisotropy strongly modify the local magnetisation direction in the soft magnetic FeNi layer. Co domain walls parallel to the easy magnetisation axis induce `quasi-walls' in an initially saturated FeNi layer. Charged Co domain walls that are tilted with respect to the easy magnetisation axis favour a local antiparallel alignment of the magnetisation directions in the two magnetic layers.

387

Euler-Lagrange models with complex currents of three-phase electrical machines  

A Lagrangian formulation with complex currents is developed and yields a direct and simple method for modeling three-phases permanent-magnet and induction machines. The Lagrangian is the sum of the mechanical kinetic energy and of the magnetic energy. This magnetic energy is expressed in terms of rotor angle, complex stator and rotor currents. Such Lagrangian setting is a precious guide for modeling space-harmonics and saturation effects. A complexification procedure is applied here in order to derive the Euler-Lagrange equations with complex stator and rotor currents. Such complexification process avoids the usual separation into real and imaginary parts and simplifies notably the calculations. Via simple modification of magnetic energies we derive non-trivial dynamical models describing permanent-magnet machines with both saturation and saliency, and induction machines with both saturation and space harmonics.

388

Magnetic Visions: Mapping Cosmic Magnetism with LOFAR and SKA  

The origin of magnetic fields in the Universe is an open problem in astrophysics and fundamental physics. "Cosmic Magnetism" has been accepted as Key Science Project both for the Low Frequency Array (LOFAR, under construction) and the planned Square Kilometre Array (SKA). At low frequencies LOFAR and SKA will allow to map the structure of weak magnetic fields in the outer regions and halos of galaxies, in galaxy clusters and in the Milky Way. High-resolution polarization observations at high frequencies with the SKA will trace magnetic fields in the disks and central regions of galaxies in unprecedented detail. All-sky surveys of Faraday rotation measures (RM) towards polarized background sources will be used to model the structure and strength of the magnetic fields in the Milky Way, the interstellar medium of galaxies and the intergalactic medium. The new method of "RM Synthesis", applied to spectro-polarimetric data cubes, will separate RM components from different distances and allow 3-D "Faraday tomograp...

389

Analysis of high gradient magnetic field effects on distribution of nanoparticles injected into pulsatile blood stream  

Magnetic nanoparticles are widely used in a wide range of applications including data storage materials, pharmaceutical industries as magnetic separation tools, anti-cancer drug carriers and micro valve applications. The purpose of the current study is to investigate the effect of a non-uniform magnetic field on bio-fluid (blood) with magnetic nanoparticles. The effect of particles as well as mass fraction on flow field and volume concentration is investigated. The governing non-linear differential equations, concentration and Navier–stokes are coupled with the magnetic field. To solve these equations, a finite volume based code is developed and utilized. A real pulsatile velocity is utilized as inlet boundary condition. This velocity is extracted from an actual experimental data. ...

390

Highly ordered magnetic multilayer Ni/Cu nanowires  

Highly ordered nanowires with multilayer of Ni/Cu, have been successfully prepared by pulsed chemical electrodeposition into nanoporous alumina membrane. The diameter (ranging from 30 to 100 nm) of wires can be easily controlled by pore size of alumina. The applied potential and the duration of each potential square pulse determine the thickness of the metal layers. The nanowires have been characterized by transmission electron microscopy (TEM), magnetic force microscopy (MFM), and vibrating sample magnetometer (VSM) measurements. From the result of MFM analysis, the magnetic multilayer nanowire indicates unique magnetic property. The MFM images indicate that every ferromagnetic layer separated by Cu layer was present as single-domain magnet. The results are demonstrated that this type of nanowires has a potential to the application of magnetic nanodevices. (copyright 2006 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

391

Motion control of a magnetically levitated microrobot using magnetic flux measurement  

Recent advancements in micro/nano domain technologies have led to a renewed interest in ultra-high resolution magnetic-based actuation mechanisms. This paper deals with the development of a novel research-made magnetic microrobotic station (MMS) with promising potential in biological/biomedical applications. The MMS consists of two separate basic components: a magnetic drive unit and a microrobot. The magnetic drive unit produces and regulates the magnetic field for non-contact propelling of the microrobot in an enclosed environment. Our previous research findings have reported that the MMS should be equipped with high accuracy laser sensors for the position determination of the microrobot in the workspace. However, the laser positioning techniques can be used only in highly transparent en...

392

Human-assisted virtual reality for a magnetic-haptic micromanipulation platform  

This paper deals with the development of a virtual reality interface (VRI) for a magnetic-haptic micromanipulation platform (MHMP) (Mehrtash et?al. in IEEE/ASME Trans Mechatron 16(3):459?469, 2011). Our previously developed MHMP has shown a great deal of promise in non-contact micromanipulations. This micromanipulation platform concerns the integration of magnetic actuation technology and a bilateral macro?micro teleoperation. The MHMP has two separate stations: one magnetic microrobotic station and one haptic. The magnetic microrobotic station manipulates micro-sized objects based on the commands from the haptic station. The haptic station uses bilateral communication with the magnetic microrobotic station to allow a human operator the feeling of a micro-domain environment. In this paper,...

393

Swarm - An Earth Observation Mission investigating Geospace  

The Swarm mission was selected as the 5th mission in ESA's Earth Explorer Programme in 2004. This mission aims at measuring the Earth's magnetic field with unprecedented accuracy. This will be done by a constellation of three satellites, where two will fly at lower altitude, measuring the gradient of the magnetic field, and one satellite will fly at higher altitude. The measured magnetic field is the sum of many contributions including both magnetic fields and currents in the Earth's interior and electrical currents in Geospace. In order to separate all these sources electric field and plasma measurements will also be made to complement the primary magnetic field measurements. Together these will allow the deduction of information on a series of solid earth processes responsible for the cr...

394

Magnetic Nanospheres-based Electrochemical Immunoassay Amplified by Hyperbranched Polymer Conjugate  

A novel ultra-sensitive, magnetic nanospheres-based immunoassay method using hyperbranched polymer (HBP) conjugated Hepatitis B secondary antibody labeled with horseradish peroxidase (HRP) for signal amplification was proposed. Magnetic nanosphere functionalized with carboxyl group was activated with EDC/NHS, and then Hepatitis B surface antibody (HBsAb) was covalently immobilized on the surface. Hepatitis B secondary antibody labeled with HRP was covalently linked to the HBP. The HBsAb-modified magnetic nanosphere could capture the HBsAg when it was incubated with HBsAg. Then the HBP conjugate was added, and a sandwich immunocomplex formed on the surface of magnetic nanospheres, which was then magnetically separated from sample solution. The HRP could catalyze the reaction between 2-amino...

395

Magnetic nanotubes  

A magnetic nanotube includes bacterial magnetic nanocrystals contacted onto a nanotube which absorbs the nanocrystals. The nanocrystals are contacted on at least one surface of the nanotube. A method of fabricating a magnetic nanotube includes synthesizing the bacterial magnetic nanocrystals, which have an outer layer of proteins. A nanotube provided is capable of absorbing the nanocrystals and contacting the nanotube with the nanocrystals. The nanotube is preferably a peptide bolaamphiphile. A nanotube solution and a nanocrystal solution including a buffer and a concentration of nanocrystals are mixed. The concentration of nanocrystals is optimized, resulting in a nanocrystal to nanotube ratio for which bacterial magnetic nanocrystals are immobilized on at least one surface of the nanotubes. The ratio controls whether the nanocrystals bind only to the interior or to the exterior surfaces of the nanotubes. Uses include cell manipulation and separation, biological assay, enzyme recovery, and biosensors.

396

New High Performance Magnet Structures for Bead Based MolecularSeparation  

New High Performance Magnet Structures for Bead Based Molecular Separation David Humphries Lawrence Berkeley National Laboratory, D.O.E. Joint Genome Institute Abstract High performance Hybrid magnetic separation technology is under continuing development at the D.O.E. Joint Genome Institute and Lawrence Berkeley National Laboratory for general laboratory and high throughput automated applications. This technology has broad applicability for molecular separation in genomics, proteomics and other areas. It s applicability ranges from large and small scale microtiter plate and flow separation processes to single molecule DNA manipulation. It is currently an enabling purification technology for very high throughput production sequencing at the D.O.E. Joint Genome Institute. This technology incorporates hybrid magnetic structures that combine linear permanent magnet material and ferromagnetic material to produce significantly higher fields and gradients than those of currently available commercial devices. These structures incorporate ferromagnetic poles that can be easily shaped to produce complex field distributions for specialized applications. The higher maximum fields and strong gradients of the hybrid structures result in greater holding forces on magnetized targets that are being processed as well as faster extraction. Current development versions of these magnet plates have exhibited fields in excess of 1.0 tesla and gradients approaching 1000.0 tesla/meter. Second generation Hybrid magnet plates have now been developed for both 384 and 96-well applications. This technology is currently being made available to industry through the Tech Transfer Department at Lawrence Berkeley National Laboratory. This work was performed under the auspices of the US Department of Energy's Office of Science, Biological and Environmental Research Program and the by the University of California, Lawrence Livermore National Laboratory under Contract No. W-7405-Eng-48, Lawrence Berkeley National Laboratory under contract No. DE-AC03-6SF00098 and Los Alamos National Laboratory under contract No. W-7405-ENG-36.

397

Characterisation and Prediction of Phase Separation in Hot-Melt Extruded Solid Dispersions: A Thermal, Microscopic and NMR Relaxometry Study  

Purpose To develop novel analytical approaches for identifying both miscibility and phase separation in hot-melt extruded formulations. Methods Felodipine-Eudragit? E PO solid dispersions were prepared using hot-melt extrusion. The fresh and aged formulations were characterised using scanning electron microscopy, differential scanning calorimetry, heat capacity (Cp) measurements using modulated temperature DSC and nuclear magnetic resonance relaxometry. Results The solubility of the drug in polymer was predicted as being ?10% w/w using a novel model proposed in this study. Freshly prepared HME formulations were found to show no evidence for phase separation despite drug loadings greatly in excess of this figure. Conventional DSC showed limitations in directly detecting phase separation. Ho...

398

The origin of the phase separation in partially deuterated $\\kappa$-(ET)$_2$Cu[N(CN)$_2$]Br studied by infrared magneto-optical imaging spectroscopy  

The direct observation of the phase separation between the metallic and insulating states of 75 %-deuterated $\\kappa$-(ET)$_2$Cu[N(CN)$_2$]Br ($d33$) using infrared magneto-optical imaging spectroscopy is reported, as well as the associated temperature, cooling rate, and magnetic field dependencies of the separation. The distribution of the center of spectral weight ($$) of $d33$ did not change under any of the conditions in which data were taken and was wider than that of the non-deuterated material. This result indicates that the inhomogenity of the sample itself is important as part of the origin of the metal - insulator phase separation.

399

Beam--plasma discharge in crossed electric and magnetic fields  

An experimental study has been made of a steady beam--plasma discharge in a radial electric field crossed with a longitudinal magnetic field. At a certain power level of the electron beam, if the working-gas pressure is between 10/sup -4/ and 10/sup -3/ torr, a steady, fully ionized plasma is produced. The rotation of this plasma can be exploited for separation of elements and isotopes. Experiments on the separation of binary mixtures of noble gases and their isotopes are reported. A spectroscopic determination of the plasma rotation velocity and the ion temperature is also reported. The separation mechanism is interpreted theoretically.

400

Giant negative magneto-resistance in non-magnetic quantum dot arrays in the nearest-neighbor hopping conduction  

We propose a new mechanism of negative magnetoresistance in non-magnetic quantum dot arrays or granular materials in which electron transport in dominated by hopping between two nearest-neighbor clusters. We study the dependence of magnetoresistance on temperature and separation between neighboring clusters. At a small separation we find a negative magnetoresistance at low temperatures and it changes over to a positive value as temperature increases. For a fixed temperature, magnetoresistance changes from negative to positive when the cluster separation increases. The change of magnetoresistance {delta}R/R can be more than 80 % at low temperatures.

 
 
 
 
401

Small Medial Meniscocapsular Separations: A Potential Cause of Chronic Medial-Side Knee Pain  

PurposeTo describe clinical characteristics, surgical findings, and functional outcome after arthroscopic repair of a unique type of meniscocapsular separation. MethodsWe retrospectively reviewed office charts, magnetic resonance imaging (MRI) scans, operative reports, and arthroscopic images of 6 patients who underwent surgery between January 2007 and May 2009, in whom a medial meniscocapsular separation measuring less than 5 mm in length was identified and treated. Inclusion criteria were medial-side knee pain unresponsive to nonoperative management, negative MRI findings, and an isolated meniscocapsular separation injury detected on arthroscopy and repaired with 1 stitch. Patients were contacted and completed questionnaires that included subjective International Knee Documentation Commi...

402

55Mn NMR study of the effect of a constant magnetic field on the phase separation of the ferromagnetic phase in manganites  

The 55Mn NMR studies of nano-sized and polycrystalline La1 ? x Ca x MnO3 samples have been performed. It has been shown that a decrease in the average size of the nanoparticles leads to the disappearance of the phase separation of the ferromagnetic phase, which is likely a general property of manganites. The studies in constant magnetic fields have demonstrated that the phase separation under consideration occurs within domains rather than as a result of the separation of the samples into domains and domains walls.

403

Phase separator safety valve blow-off.  

The fast discharge of the CMS solenoid leads to a pressure rise in the phase separator. On August 28th, a fast discharge was triggered at a current level of 19.1 kA. The pressure in the phase separator increased up to the set pressure of the safety valve and some helium was discharged. In consequence of this and prevoious similar observations the liquid helium level in the phase separator has been reduced from 60% to 50% and later to 45% in order to reduce the helium inventory in the magnet.

404

Study on comprehensive utilization of secondary resources  

In light of the properties on process mineralogy of the old tailings in a certain copper mine in the People`s Republic of China, a new process of combined reagent and stepwise flotation is applied in which the flotation of copper sulfides is followed by the flotation of copper oxides. Recoveries of copper and associated gold and silver have been greatly increased. The tailings obtained were subjected to the gravitational separation-magnetic separation process to recover iron minerals. Tailings from iron separation are taken as fillers and sent to the pit underground. Thus, the secondary resources are comprehensively utilized.

405

On Poor Separation in Magnetically Driven Shock Tube  

Observations made at steady-state running conditions in a magnetically driven shock tube, with parallel-plate electrodes, showed that for a given discharge voltage, sufficient separation between the shock and the current-sheet occurred only at relatively high discharge pressures. As a comparison, poor separations were also noted in conventional diaphragm-type shock tubes running at low initial pressures. It is demonstrated that the observed poor separation can be explained by a mass leakage, instead of through the wall boundary layer, but through the current-sheet itself.

406

Magnetic mineralogy of heavy metals-contaminated soils  

Soils around mine and in urban areas are often contaminated by heavy metals derived from industrial and human activities [1, 2]. These contaminated soils are often characterized by a magnetic enhancement on topsoils. Many studies demonstrated that there are significant correlations between heavy metals and various magnetic parameters in contaminated soils, indicating a strong affinity of heavy metals to magnetic minerals. The magnetic particles in contaminated soils were separated by a magnetic separation technique. The rock magnetism, XRD, field emission scanning electron microscopy equiped with an energy-dispersive X-ray analyzer (FESEM/EDX) were used to characterize their magnetic mineralogy. Results of XRD analysis indicated that the magnetic particles separated from heavy metal-contaminated soils are composed of quartz, magnetite, and hematite. Based on the X-ray diffraction peak intensity, the Fe3O4 was identified as the predominant magnetic mineral phase. The high-temperature magnetization (Ms-T) curves of magnetic particles extracted from contaminated soils show a sharp Ms decrease at about 580C (the Curie temperature of magnetite), suggesting that magnetite is the dominant magnetic carrier. The hysteresis loops of contaminated soils are closed at about 100-200 mT which is consistent with the presence of a dominant ferrimagnetic mineral phase. The FESEM analysis showed a great variety of shapes of magnetic particles in contaminated soils. The most common morphology are observed in the form of spherules, with the sizes ranging from 20 to 100 um. The chemical composition of magnetic particles consist mainly of Fe, Si, Al, and Ca with minor heavy metal elements (Cu, Zn, Hg, and Cr). The semi-quantitative Fe content identified by FESEM/EDX ranged from 40 to 90%. Combined studies of rock magnetism, XRD, and FESEM/EDX indicated that magnetic mineral phases responsible for the magnetic enhancement of contaminated soils are anthropogenic origin which are coarse-grained multi-domain (MD) ferrimagnetic minerals. These spherical magnetic particles in contaminated soils are most likely related to airborne particles from coal combusition and industrial activities. Coal burning, metallurgical and industrial dusts contain a significant fraction of ferrimagnetic minerals. The magnetic particles in fly ash from coal-burning power plant have a typical spherical morphology, ranging from 10 to 100 ?m. Vehicle emissions have been suggested to be another source of magnetic particles. These anthropogenic ferrimagnetic mineral phases are directly responsible for the magnetic enhancement in the contaminated soils. Therefore, the strong magnetic signature in contaminated soils can be used as an effective tool for identifying pollution sources and quantifying pollution level of heavy metals. Acknowledgements: This research was supported by National Nature Science Foundation of China (No. 41171182 and 40971131) and the Ph.D. Programs Foundation of Ministry of Education of China (20090101110088). [1] Lu, S.G. & Bai, S.Q. (2006) J. Appl. Geophys., 60, 1-12. [2] Lu, S.G., Bai, S.Q. & Xue, Q.F. (2007) Geophys. J. Inter., 171, 568-580.

407

Magnetically modulated nanosystems: a unique drug-delivery platform.  

Magnetic nanoparticles are attractive targets owing to their unique characteristics that are not shared by bulk materials. Magnetic particles, ranging from nanometer-sized to 1 microm in size, are being used in an increasing number of medical applications. The important properties of magnetic particles for medical applications are nontoxicity, biocompatiblilty, injectability and high-level accumulation in the target tissue or organ. Magnetic nanoparticles modified with organic molecules have been widely used for biotechnological and biomedical applications as their properties can be magnetically controlled by applying an external magnetic field. They offer high potential for numerous biomedical applications, such as cell separation, automated DNA extraction, gene targeting, drug delivery, MRI and hyperthermia. When coated with, for example, an antibody, they can be applied in highly sensitive immunoassays or small substance recoveries. Furthermore, a novel application of magnetic nanoparticles and magnetic forces for tissue engineering, termed 'magnetic force-based tissue engineering' has been proposed. Particular attention had been paid to the preparation methods that allow the synthesis of particles of nearly uniform size and shape. PMID:19839815

408

Towards quantitative magnetic force microscopy: theory and experiment  

We introduce a simple and effective model of a commercial magnetic thin-film sensor for magnetic force microscopy (MFM), and we test the model employing buried magnetic dipoles. The model can be solved analytically in the half-space in front of the sensor tip, leading to a simple 1/R dependence of the magnetic stray field projected to the symmetry axis. The model resolves the earlier issue as to why the magnetic sensors cannot be described reasonably by a restricted multipole expansion as in the point pole approximation: the point pole model must be extended to incorporate a ‘lower-order’ pole, which we term ‘pseudo-pole’. The near-field dependence (?R-1) turns into the well-known and frequently used dipole behavior (?R-3) if the separation, R, exceeds the height of the sensor. Using magnetic nanoparticles (average diameter 18 nm) embedded in a SiO cover as dipolar point probes, we show that the force gradient-distance curves and magnetic images fit almost perfectly to the proposed model. The easy axis of magnetization of single nanoparticles is successfully deduced from these magnetic images. Our model paves the way for quantitative MFM, at least if the sensor and the sample are independent.

409

Layered Molecule-Based Magnets Formed by Decamethylmetallocenium Cations and Two-Dimensional Bimetallic Complexes [MIIRuIII(ox)3]-(MII=Mn, Fe, Co, Cu and Zn; ox=oxalate)  

A new series of hybrid organometallic-inorganic layered magnets with formula [ZIIICp*2] [MIIRuIII(ox)3] (ZIII=Co and Fe; MII=Mn, Fe, Co, Cu, and Zn; ox=oxalate: Cp*=pentamethylcyclopentadienyl) has been prepared. All of these compounds are isostructural to the previously reported [ZIIICp*2] [MIIMIII(ox)3] (MIII=Cr, Fe) series and crystallize in the monoclinic space group C2/m, as found by powder X-ray diffraction analysis. They are novel examples of magnetic materials formed by bimetallic oxalate-based extended layers separated by layers of organometallic cations. The magnetic properties of all these compounds have been investigated (ac and dc magnetic susceptibilities and field dependence of the isothermal magnetization at 2 K). In particular, it has been found that FeII and CoII derivatives behave as magnets with ordering temperatures of 12.8 and 2.8 K, respectively, while no long-range magnetic ordering has been detected down to 2 K in the MnII and CuII derivatives. The magnetic ordering in the FeII derivatives has been confirmed through Mössbauer spectroscopy. This technique has also made it possible to observe the spin polarization of the paramagnetic [FeCp*2]+ units caused by the internal magnetic field created by the bimetallic layers in the ordered state.

410

Conical Bearingless Motor/Generators  

Motor/generators based on conical magnetic bearings have been invented as an improved alternative to prior such machines based, variously, on radial and/or axial magnetic bearings. Both the present and prior machines are members of the class of so-called bearingless or self bearing (in the sense of not containing mechanical bearings) rotary machines. Each motor/generator provides both a torque and force allowing it to either function as a motor and magnetic bearing or a generator and magnetic bearing concurrently. Because they are not subject to mechanical bearing wear, these machines have potentially long operational lives and can function without lubrication and over wide ranges of speed and temperature that include conditions under which lubricants would become depleted, degraded, or ineffective and mechanical bearings would fail. The figure shows three typical configurations of conical bearingless motor/generators. The main elements of each motor/generator are concentric rotor and stator portions having conically tapered surfaces facing each other across a gap. Because a conical motor/generator imposes both radial and axial magnetic forces, it acts, in effect, as a combination of an axial and a radial magnetic bearing. Therefore, only two conical motor/generators - one at each end of a rotor - are needed to effect complete magnetic leviation of the rotor, whereas previously, it was necessary to use a combination of an axial and a radial magnetic bearing at each end of the rotor to achieve complete magnetic levitation and a separate motor to provide torque.

411

Metallic multilayers and magneto-optical recording; Nano sekiso kinzokumaku to hikari jiki kiroku  

It has become possible to produce very thin magnetic metal films, as thin as 0.05{mu}m in case of magnetic recording medium and 0.02{mu}m in case of magneto-optical recording medium, and studies are under way for the development of an advanced super-thin film not thicker than 10nm. This report describes recent developments in material research taking reference particularly to the enhancement of magneto-optical medium recording density. Such a medium is required to have various characteristics in view of the write/read principle that the medium follows. For example, while a high-density magnetic recording medium uses aggregates of magnetically (exchange interaction) separated microscopic single magnetic domain particulates, a magneto-optical recording medium uses a continuous medium strongly bonded together by magnetism in the exchange operation. The latter, because it uses vertically magnetized films, may be enhanced in density without being greatly affected by the opposite magnetic field. It is hoped that nano-scale multilayer films, such as magnetic super-resolution multilayer films, Pt/Co laminations, and Nd-based amorphous laminations will contribute to the enhancement of recording density. 8 refs., 5 figs.

412

Possible Existence of Magnetic Polaron in Nearly Ferromagnetic Semiconductor ?-US2  

We studied the magnetic properties of the paramagnet ?-US2 with an orthorhombic crystal structure by measuring its magnetization, magnetic susceptibility, specific heat, and electrical resistivity under magnetic field and pressure. The 5f-crystalline electric field (CEF) scheme was determined from the experimental results: a singlet in the ground state and a pseudo-doublet in the first excited state, separated by 85 and 91 K from the ground state. The insulating resistivity markedly changes to a metallic one under a high pressure of 8 GPa similarly to that of the semimetallic Ising-type ferromagnet UTeS with a Curie temperature TC=87 K. A resistivity anomaly was also observed in the temperature dependence of the resistivity under pressure, most likely corresponding to ferromagnetic ordering. From these experimental results, it was concluded that ?-US2 is in the vicinity of ferromagnetic ordering at ambient pressure. Furthermore, we found that the easy-axis magnetization at low fields for H||[001] consists of a linear magnetization based on the 5f-CEF scheme and a ferromagnetic-like magnetization with a saturated moment of 0.042 ?B/U. The latter magnetization was analyzed on the basis of the ferromagnetic cluster and discussed from the viewpoint of the magnetic polaron.   

413

Cluster glass magnetism in the phase-separated Nd2/3Ca1/3MnO3 perovskite  

A detailed study of the low-temperature magnetic state and the relaxation in the phase-separated colossal magnetoresistance Nd2/3Ca1/3MnO3 perovskite has been carried out. Clear experimental evidence of the cluster-glass magnetic behavior of this compound has been revealed. Well defined maxima in the in-phase linear ac susceptibility ??(T) were observed, indicative of the magnetic glass transition at Tg˜60 K. Strongly divergent zero-field-cooled and field-cooled static magnetizations and frequency dependent ac susceptibility are evident of the glassy-like magnetic state of the compound at low temperatures. The frequency dependence of the cusp temperature Tmax of the ??(T) susceptibility was found to follow the critical slowing down mechanism. The Cole-Cole analysis of the dynamic susceptibility at low temperature has shown extremely broad distribution of relaxation times, indicating that spins are frozen at "macroscopic" time scale. Slow relaxation in the zero-field-cooled magnetization has been experimentally revealed. The obtained results do not agree with a canonical spin-glass state and indicate a cluster glass magnetic state of the compound below Tg, associated with its antiferromagnetic-ferromagnetic nano-phase segregated state. It was found that the relaxation mechanisms below the cluster glass freezing temperature Tg and above it are strongly different. Magnetic field up to about ?0H˜0.4 T suppresses the glassy magnetic state of the compound.

414

Anisotropy of the Curie temperature in ultrathin epitaxial Fe(001) wire arrays  

According to Mermin and Wagner long-range ferromagnetic order in isotropic 2D systems with short-range magnetic interactions is destroyed by spin fluctuations at any temperature T>0. Curie temperatures, T{sub C}, above 200 K in single atomic layers can be understood by considering magnetic anisotropies and long-range dipolar interactions. The relevance of dipolar interaction was verified in ultrathin Fe(001) dot arrays epitaxially grown on GaAs(001) by variation of dot diameter and dot separation. By assuming that magnetization fluctuations in space and time close to T{sub C} are partially suppressed by combined exchange and dipolar interactions in the same way as purely spatial magnetization fluctuations in polycrystalline films (''magnetization ripple''), the result of a Green's function approach predicts that T{sub C} should be higher in a long wire magnetized perpendicular to the wire axis compared to a parallel magnetization and to a circular dot. This was confirmed by exploiting the strong uniaxial interface magnetic anisotropy in Fe/GaAs(001). Compared to the extended film a reduction of T{sub C} by 3% was observed for perpendicular magnetization versus 8% for the parallel case; for a dot with the same dimension the reduction was indeed the sum of both, i.e.11%. This means that in epitaxial ultrathin ferromagnetic wires the Curie temperature is indeed anisotropic.

415

Analysis of high gradient magnetic field effects on distribution of nanoparticles injected into pulsatile blood stream  

Magnetic nanoparticles are widely used in a wide range of applications including data storage materials, pharmaceutical industries as magnetic separation tools, anti-cancer drug carriers and micro valve applications. The purpose of the current study is to investigate the effect of a non-uniform magnetic field on bio-fluid (blood) with magnetic nanoparticles. The effect of particles as well as mass fraction on flow field and volume concentration is investigated. The governing non-linear differential equations, concentration and Navier-stokes are coupled with the magnetic field. To solve these equations, a finite volume based code is developed and utilized. A real pulsatile velocity is utilized as inlet boundary condition. This velocity is extracted from an actual experimental data. Three percent nanoparticles volume concentration, as drug carrier, is steadily injected in an unsteady, pulsatile and non-Newtonian flow. A power law model is considered for the blood viscosity. The results show that during the systole section of the heartbeat when the blood velocity increases, the magnetic nanoparticles near the magnetic source are washed away. This is due to the sudden increase of the hydrodynamic force, which overcomes the magnetic force. The probability of vein blockage increases when the blood velocity reduces during the diastole time. As nanoparticles velocity injection decreases (longer injection time) the wall shear stress (especially near the injection area) decreases and the retention time of the magnetic nanoparticles in the blood flow increases.

416

Experimental and theoretical studies of hydroxyl-induced magnetism in TiO nanoclusters.  

A main challenge in understanding the defect ferromagnetism in dilute magnetic oxides is the direct experimental verification of the presence of a particular kind of defect and distinguishing its magnetic contributions from other defects. The magnetic effect of hydroxyls on TiO nanoclusters has been studied by measuring the evolution of the magnetic moment as a function of moisture exposure time, which increases the hydroxyl concentration. Our combined experiment and density-functional theory (DFT) calculations show that as dissociative water adsorption transforms oxygen vacancies into hydroxyls, the magnetic moment shows a significant increase. DFT calculations show that the magnetic moment created by hydroxyls arises from 3d orbitals of neighboring Ti sites predominantly from the top and second monolayers. The two nonequivalent hydroxyls contribute differently to the magnetic moment, which decreases as the separation of hydroxyls increases. This work illustrates the essential interplay among defect structure, local structural relaxation, charge redistribution, and magnetism. The microscopic differentiation and clarification of the specific roles of each kind of intrinsic defect is critical for the future applications of dilute magnetic oxides in spintronic or other multifunctional materials. PMID:23132145

417

Dual Magnetic Separator for TRI$\\mu$P  

The TRI$\\mu$P facility, under construction at KVI, requires the production and separation of short-lived and rare isotopes. Direct reactions, fragmentation and fusion-evaporation reactions in normal and inverse kinematics are foreseen to produce nuclides of interest with a variety of heavy-ion beams from the superconducting cyclotron AGOR. For this purpose, we have designed, constructed and commissioned a versatile magnetic separator that allows efficient injection into an ion catcher, i.e., gas-filled stopper/cooler or thermal ionizer, from which a low energy radioactive beam will be extracted. The separator performance was tested with the production and clean separation of $^{21}$Na isotopes, where a beam purity of 99.5% could be achieved. For fusion-evaporation products, some of the features of its operation as a gas-filled recoil separator were tested.

418

Evaporation residue collection efficiencies and position spectra of the Dubna gas-filled recoil separator  

The focal-plane position spectra and collection efficiencies of the Dubna gas-filled recoil separator at the U400 cyclotron used to separate evaporation residues of complete fusion reaction products are described. The separator consists of a 23 deg. -dipole magnet and a quadrupole doublet and is filled with hydrogen at a pressure of about 1 Torr. After passing through the time-of-flight system, the separated evaporation residues are collected in a 120 mm centre dot 40 mm position-sensitive semiconductor detector at the focal plane. Depending on the asymmetry of the projectile, target combinations, the measured collection efficiencies were 3-45%, with suppression factors exceeding 10 sup 1 sup 5 and 10 sup 4 for beam and target-like particles, respectively. The ANAMARI code that is used to determine the separator settings is described and its predictions for the evaporation residue position spectra and collection efficiencies are compared with experimental data.

419

Modelling the Electromagnetic Separation of Non-metallic Particles from Liquid Metal Flowing through a Two-stage Multichannel  

A two-stage multichannel was designed to increase the efficiency of separating non-metallic particles from liquid metal flowing through an alternating magnetic field. Numerical method was developed to calculate the particle concentration and separation efficiency of a zinc melt containing dross particles and verified by the experimental results. The distribution of particle concentration and axial fluid velocity changed significantly due to the added walls in the sub-channel, resulting in an abrupt increase in the residence time of the inner bulk melt with high particle concentrations and a remarkable increase in particle separation efficiency when flowing through the single-channel to sub-channels. A multistage and multichannel arrangement is hence recommended for further increase in the separation efficiency of an electromagnetic separator.   

420

Production of Stable Aqueous Dispersions of Carbon Nanotubes ...  

amorphous carbon, the use of magnetic separation tech- niques to remove .... fraction #'s measured during fractionation of methyl-~ cyclodextrin .... a suitable level below its CMC will also ensure adequate ... (i.e. hydrogen bonding, molecular aggregation) it is pre- .... a 0.2 ,um cellulose acetate filter to remove any particulate ...

 
 
 
 
421

Charged two-dimensional magnetoexciton and two-mode squeezed vacuum states  

A novel unitary transformation of the Hamiltonian that allows one to partially separate the center-of-mass motion for charged electron-hole systems in a magnetic field is presented. The two-mode squeezed oscillator states that appear at the intermediate stage of the transformation are used for constructing a trial wave function of a two-dimensional (2D) charged magnetoexciton.

422

(c) Structure and Aft) tlons  

unclassif ied. (See ANSI-239.18) ...... tem—in the solar magnetic field, in explosive solar flares, possibly at inter- planetary current sheets ..... trino detection devices capable of sensing low-energy neutrinos produced in the separate and ..... E-region current densities, ionospheric conductivities, Joule heating rates, ion-neutral ...

423

Separation of the Magnetic Field into External and?Internal Parts  

The magnetic field of a planet or a planetary moon contains contributions from a?variety of sources in the environment of the body (external sources) and its interior (internal sources). This chapter describes different methods that have been developed for the separation of external and internal source contributions, and their application to selected planets and one of Jupiter?s moons, Ganymede.

424

Recovery of Rare Metals from the Sludge of Samarium-Cobalt Magnetic Alloy by a Chemical Vapor Transporting Method  

A dry process using chemical vapor transporting technique along temperature gradient was investigated for the recovery and recycling of rare metals from the sludge of Sm-Co binary alloys. For the permanent magnetic alloy sludge of Sm2Co17, the Sm and Co elements were effectively separated in the form of anhydrous chlorides with the purity higher than 99%.   

425

Readout From Iconic Memory and Selective Spatial Attention Involve Similar Neural Processes  

Iconic memory and spatial attention are often considered separately, but they may have functional similarities. Here we provide functional magnetic resonance imaging evidence for some common underlying neural effects. Subjects judged three visual stimuli in one hemifield of a bilateral array compris...

426

Analysis of phase separation by thermal aging in duplex stainless steels by magnetic methods  

The phase separation in ferrite phase of duplex stainless steel is the primary cause of thermal aging embrittlement of the LWR primary pressure boundary components. In this study the phase separation of simulated duplex stainless steel was detected by Mossbauer spectroscopy and magnetic property analysis by VSM (Vibrating Specimen Magnetometer). The simulated duplex stainless steels, Fe-Cr binary, Fe-Cr-Ni Temary, and Fe-Cr-Ni-Si quaternary alloys, were aged at 370 and 400 deg C up to 5,340 hours. It was observed from Mossbauer spectra analysis that internal magnetic field increases with aging time and from VSM that the specific saturation magnetization and Curie temperature increase with aging time. These results are indicative that phase separation into Fe-rich region and Cr-rich region is caused by thermal aging in the temperature range of 370 - 400 deg C. In cases specimens containing Ni, the increase of specific saturation magnetization is much higher. This implies that Ni seems to promote Fe-Cr interdiffusion, which accelerates the phase separation into Fe-rich {alpha} phase and Cr-rich {alpha}` phase. (author).

427

The M3D-C1 Approach to Simulating 3D 2-fluid Magnetohydrodynamics in Magnetic Fusion Experiments  

A new approach for solving the 3D MHD equations in a strongly magnetized toroidal plasma is presented which uses high-order 2D finite elements with C1 continuity. The vector fields use a physics-based decomposition. An efficient implicit time advance separates the velocity and field advance. ITAPS (SCOREC) adaptivity software and TOPS solvers are used.

428

Materials and Molecular Research Division annual report 1980  

Progress made in the following research areas is reported: materials sciences (metallurgy and ceramics, solid state physics, materials chemistry); chemical sciences (fundamental interactions, processes and techniques); nuclear sciences; fossil energy; advanced isotope separation technology; energy storage; magnetic fusion energy; and nuclear waste management.

429

Thiourea leaching of gold bearing mine wastes from Madjarovo processing plant in SE Bulgaria  

Flotation tailings derived from processing of complex sulphide gold-bearing ores have been repropcessed by means of thiourea leaching. Before leaching takes place the materials has been subjected to magnetic separation, flotattion and hydrocloric leaching. An environmental and economic benefits coul...

430

INTERACTING QUANTUM SPIN CHAINS  

A brief review of recent advances in neutron scattering studies of low-dimensional quantum magnets is followed by a particular example. The separation of single-particle and continuum states in the weakly-coupled S = l/2 chains system BaCu{sub 2}Si{sub 2}O{sub 7} is described in some detail.

431

Interplay between ferromagnetism and superconductivity in tunneling currents  

We study tunneling currents in a model consisting of two non-unitary ferromagnetic spin-triplet superconductors separated by a thin insulating layer. We find a novel interplay between ferromagnetism and superconductivity, manifested in the Josephson effect. This offers the possibility of tuning dissipationless currents of charge and spin in a well-defined manner by adjusting the magnetization direction on either side of the junction.

432

Phase Separation, Magnetism and Superconductivity in Rutheno-Cuprates  

The properties of the superconducting ferromagnets RuSr2(Gd/Eu)Cu2O8 and RuSr2(Ln/Ce)2Cu2O10 are reviewed. The problem of coexistence and competition between magnetic and superconducting states is discussed. A model of phase separation into ferromagnetic and anti-ferromagnetic structures is proposed.

433

Modification and characterization of polystyrene-based magnetic microspheres and comparison with albumin-based magnetic microspheres  

Polystyrene- and albumin-based magnetic microspheres for red blood cell separation were modified and characterized by scanning electron and atomic force microscopy. Albumin microspheres show higher coupling efficiency with the protein, and protein-modified albumin microspheres bind the red blood cells more efficiently than the polystyrene-based microspheres.

434

Development of a highly magnetic iron sulphide for metal uptake and magnetic separation  

Microbial iron sulphide (FeS) is a well-known absorbent for heavy metals which has the potential to be used in biomagnetic separation. This paper illustrates that highly magnetic FeS can be produced from bioreactors which are continually switched between batch and continuous culture modes. Cadmium metal uptake studies highlight the sulphide absorbent properties of the FeS produced.

435

Magnetic testing probe  

A cylindrical eddy current tube testing probe is disclosed. Current flow in dual electromagnetic coils separated by an eddy current sensing coil is so directed that magnetic fields of the electromagnet coils have components extending in opposite directions axially of the tested tube and components extending radially of the tube which add in the region of the eddy current sensing coil.

436

I-F starting method with smooth transition to EMF based motion-sensorless vector control of PM synchronous motor/generator  

This paper proposes a novel hybrid motion- sensorless control system for permanent magnet synchronous motors (PMSM) using a new robust start-up method called I-f control, and a smooth transition to emf-based vector control. The I-f method is based on separate control of id, iq currents with the refe...

437

International Congress on Glass XII  

A total of 158 papers are included under nine headings: structure and glass formation; optical properties; electrical and magnetic properties; mechanical properties and relaxation; mass transport; chemical durability and surfaces; nucleation; crystallization; and glass ceramics; processing; and automatic controls. Separate abstracts were prepared for eight papers; four of the remaining papers had been processed previously for the data base. (DLC)

438

Polyvinyl-alcohol-based magnetic beads for rapid and efficient separation of specific or unspecific nucleic acid sequences  

The versatile application of polyvinyl-alcohol-based magnetic M-PVA beads is demonstrated in the separation of genomic DNA, sequence specific nucleic acid purification, and binding of bacteria for subsequent DNA extraction and detection. It is shown that nucleic acids can be obtained in high yield and purity using M-PVA beads, making sample preparation efficient, fast and highly adaptable for automation processes.

439

Comparison of analytical and semi-preparative columns for high-performance liquid chromatography-solid-phase extraction-nuclear magnetic resonance  

The application of analytical and semi-preparative columns in reversed-phase liquid chromatography-solid-phase extraction-nuclear magnetic resonance (HPLC-SPE-NMR) was compared. The work was aiming at separating a higher sample amount in a single run and in this way to reduce the necessary NMR measu...

440

Studies of nonlinear and chaotic phenomena in solid state systems  

This thesis contains three sections discussing different areas. Spin wave interactions in iron garnets are described in section one. Mathematical analysis of a magnetic oscillator is presented in section two. In the final section, the source of noise in Josephson Junctions is investigated. The three sections are indexed separately. (JDH)

 
 
 
 
441

MRF agent based segmentation: Application to MRI brain scans  

Abstract. The Markov Random Field (MRF) probabilistic framework is classically introduced for a robust segmentation of Magnetic Resonance Imaging (MRI) brain scans. Most MRF approaches handle tissues segmentation via global model estimation. Structure segmentation is then carried out as a separate t...

442

Sources of polarized ions and atoms  

In this presentation we discuss methods of producing large quantities of polarized atoms and ions (Stern-Gerlach separation, optical pumping, and spin-exchange) as well as experimental methods of measuring the degree of polarization of atomic systems. The usefulness of polarized atoms in probing the microscopic magnetic surface properties of materials will also be discussed. 39 refs., 5 figs., 2 tabs.

443

Materials and Molecular Research Division. Annual report 1981  

Progress is reported in the areas of materials sciences, chemical sciences, nuclear sciences, fossil energy, advanced (laser) isotope separation technology, energy storage, superconducting magnets, and nuclear waste management. Work for others included phase equilibria for coal gasification products and ..beta..-alumina electrolytes for storage batteries. (DLC)

444

Preparing municipal solid waste for composting  

Processing procedures described are size reduction, air classification, screening and magnetic separation. Size reduction is the single most used and costliest of the unit processes involved. Non-compostable contaminants must be removed prior to screening. The cost of processing increases as the quality of the compost increases. One potential processing scheme that the authors consider technically reliable and economically practical is described. 6 references.

445

Dynamic and hysteresis losses  

A measuring procedure has been developed to determine the hysteresis loss as function of the magnetizing frequency. It was applied to single crystal frames of iron-silicon and tape wound cores of that alloy and metallic glasses. Actually the hysteresis loss energy is frequency dependent and to an extent that must not be neglected if the dynamic loss shall be separated.

446

Magnetic field in the Lobachevsky space and related integrable systems  

Various possibilities to define analogs of the uniform magnetic field in the Lobachevsky space are considered using different coordinate systems in this space. Quantum mechanical problem of motion in the defined fields is also treated. Variables in the Schr?dinger equation are separated and diagonal operators are found. For some cases, exact solutions are obtained.

447

RF Potential Formation in Electronegative Plasma Column under a Magnetic Field  

The experimental results on the radial RF potential formation in electronegative plasma with an applied axial magnetic field are reported by comparing the results of the electropositive plasma. The successful control of plasma potential has been established in a wide range of potential values even lower than the potential of the grounded chamber wall by biasing both the separation grid and the end plate.   

448

Magnetic Oscillation of Optical Phonon in Graphene  

The frequency shift and broadening of long-wavelength optical phonons due to interactions with electrons are calculated in a monolayer graphene in magnetic fields. The broadening is resonantly enhanced and the frequency shift exhibits a rapid change when the phonon energy becomes the energy separation of Landau levels between which optical transitions are allowed.   

449

Plasma centrifuge  

Mass separation in magnetized, highly ionized, rotating metal plasmas is described. Plasma rotation velocities up to 7.4 x 10/sup 3/ m/sec with centrifugal enrichment of up to a factor of 2 for /sup 65/Cu were measured. Such enrichments are significantly in excess of values reported earlier.

450

Polychlorodibenzo-p-dioxin and polychlorodibenzo-furan removal and destruction.  

This report provides a short summary of technologies used to destroy or separate dioxins/furans from environmental samples. It is meant as a resource for developing a technology employing magnetic particles as an engineering vehicle for large-scale, cost-effective destruction of dioxins/furans in fresh waters or sludges/soils.

451

ANALYSIS OF DYNAMICS IN MAGNETOTELLURIC DATA BY USING THE FISHER-SHANNON METHOD ANALYSIS OF DYNAMICS IN MAGNETOTELLURIC DATA BY USING THE FISHER-SHANNON METHOD  

The Fisher-Shannon information (FS) plane, defined by the Fisher information measure and the Shannon entropy power, is used to investigate the complex dynamics of magnetotelluric data of three stations in Taiwan. In the FS plane the electric and magnetic components are significantly separated, chara...

452

Morphological evaluation of atrioventricular septal defects by magnetic resonance imaging.  

Twelve patients aged between 2 weeks and 22 months (median 6 weeks) with atrioventricular septal defects were examined with a 1.5 T, whole body, magnetic resonance imaging system. Ten patients had a common atrioventricular orifice (complete defect) while two patients had separate right and left valv...

453

Die weltraumqualifizierte Datenakquisition des Übergangsstrahlungsdetektors im AMS-02 Experiment auf der Internationalen Raumstation. The Space Qualified Data Acquisition for the Transition Radiation Detector of the AMS-02 Experiment on the International Space Station  

The transition radiation detector (TRD) of the Alpha Magnetic Spectrometer (AMS-02) for cosmic rays allows a separation of positrons and protons and will be operated on the International Space Station for three years. Its space qualified readout electronics, developed and operated under responsibili...

454

The SPS beam lines to the West Hall  

The proton beam arriving from bottom is cut into three parts by the special steel septum magnets, seen in the centre, and then focussed onto the targets just out the sight on the top. The beam line near the right hand wall carries an RF-separated beam to BEBC from a target located deep in the TT60 tunnel. (Annual Report 1976 p. 116)

455

Vectorial magnetometry using magnetooptic Kerr effect including first- and second-order contributions for thin ferromagnetic films  

A new combination of different vectorial magnetometry techniques using magnetooptic Kerr effect is described. The processing of the experimental data contains the separation of linear and quadratic parts of the magnetization curves and determination of all three components of the magnetizat...

456

Magnetic separation using high-T{sub c} superconductors  

A magnetic separator with an iron return circuit that employs a high-T{sub c} superconducting coil has been built on a small scale. This type of separator, using an iron yoke, has been used by the mineral industry for many years and there appears to be an opportunity for the retrofitting of superconducting coils into existing machines to run them much more cheaply and closer to saturation. This paper describes the design requirements of such an apparatus when a high-T{sub c} superconducting coil is used to generate ampere-turns instead of a resistive one, and in particular the necessity to limit the magnetic stray field at the coil below the critical values. The strong anisotropy of the critical current characteristics with respect to the direction of the magnetic field of the present high-T{sub c} tapes imposes the consideration of two load lines, one for the axial field and one for the radial field at the solenoid. From this analysis the radial component, perpendicular to the tape surface and hence in the low J{sub c} direction, determines the upper limit for the operating current at 77 K. The analysis has been carried out using a 3D finite element package to model the apparatus and to calculate magnetic fields in the air gap of the separator and on the coil windings. The performance of the separator has been tested at 77 K. (author)

457

Recursive filtering and edge closing : two primary tools for 3d edge detection  

This paper deals with edge detection in 3d images such as scanner, magnetic resonance (NMR), or spatio-temporal data. We propose an unified formalism form 3d edge detection using optimal, recursive and separable filters recently introduced for 2d edge detection. Then we obtain some efficient 3d edge...

458

Calorimetric investigation of the low temperature excitations of Pr 3+ ions in the amorphous matrix La80Au20  

We present specific heat measurements between 0.3 K and 10 K, in magnetic fields up to 7 teslas, on three amorphous PrxLa80- xAu20 alloys, with x ? 10. The various component contributions to the specific heat have been separated and analysed. The crystal field ground state of the Pr3+ ions is shown ...

459

Spatial fluctuations and localisation effects in optical characteristics of p-doped GaN films  

We report the observation of several intense satellite lines in the emission of p-GaN excited at 325 nm with separations suggesting a multiple LO phonon-related process. The observed phenomenon is interpreted as hot exciton luminescence enhanced by potential fluctuations and localisation. Using optically detected magnetic resonance and photoluminescence kinetics we explore the compensation processes underpinning these localisation effects. (orig.)

460

Hyperfine and Optical Barium Ion Qubits  

State preparation, qubit rotation, and high fidelity readout are demonstrated for two separate \\baseven qubit types. First, an optical qubit on the narrow 6S$_{1/2}$ to 5D$_{5/2}$ transition at 1.76 $\\mu$m is implemented. Then, leveraging the techniques developed there for readout, a ground state hyperfine qubit using the magnetically insensitive transition at 8 GHz is accomplished.

 
 
 
 
461

2 3  

tube. sorption spectrum for 5 keV electrons. (b Magnetic. Ab field separation between the two resonances such as in ..... a = Pvc. C frequency et momentum P. It determines the amount of selective .... an evacuated microwave cavity resonator. All but a ..... The collector current necessary to support a self sustained oscillation ...

462

Recovery of the molybdenum catalyst for fossil fuel hydrogenation  

The composition and the properties of molybdenum-containing residues remaining after catalytic hydrogenation of coals and bitumen were studied. The chemical and the mineralogical composition of the products and the forms of molybdenum compounds were established. The techniques of concentration of molybdenum compounds (flotation, magnetic separation, and oxidative sublimation of MoO3) were considered.

463

A perturbation finite element method for efficiently calculating skin and proximity effects in any conductive material  

A perturbation finite element method for solving eddy current problems in two separate steps is developed for considering conductive and magnetic materials subject to strong skin and proximity effects. The proposed method al-lows to efficiently and accurately determine the current den-sity distribut...

464

Influence of a static magnetic field on the detected atomic velocity distribution in an optically pumped cesium beam frequency standard.  

Irregularities of the microwave Ramsey patterns in an optically pumped cesium atomic beam frequency standards with a sharp angle incidence detecting laser beam have been diagnosed. They arise from a separated two-peak detected velocity distribution, which is caused by static magnetic fields. Experimentally measured results and theoretical analysis of this phenomenon are presented in this paper. PMID:14561038

465

Single-Round, Multiplexed Antibody Mimetic Design through mRNA Display.  

In a single round: By combining the high-efficiency enrichment through the continuous-flow magnetic separation (CFMS) technique with the analytical power of next-generation sequencing, the generation of antibody mimetics with a single round of mRNA display is made possible. This approach eliminates iterative selection cycles and provides a path to fully automated ligand generation. PMID:23125174

466

Different Magnetic Properties for Diastereomers of Alkoxide-bridged (?-Diketonato)ruthenium(III) Binuclear Complexes  

Symmetric alkoxide-bridged diruthenium complexes [{Ru(acac)2}2(?-OMe)2], which are obtained when [Ru(acac)2(CH3CN)2] reacts in methanol, can be separated into two diastereomers by column chromatography, and these diastereomers are found to exhibit different magnetic properties despite their structural similarities.   

467

He$sup 3$-NUCLEI IN THE PRIMARY COSMIC RADIATION  

The ratio He/sup 3//(He/sup 3/ + He/sup 4/) was determined in two highaltitude balloon flights carried out about a year apart. A constant sagitta scattering scheme used for mass separation is described. A table shows results for each flight calculated on both energy/nucleon and magnetic rigidity bases. (A.G.W.)

468

Separation of magnetic fractions from coal by magnetic separation method. Paper no. IGEC-1-041  

The application of the magnetic separation method in the process of cleaning of the coal and the effect of the particular size of coal on the method was investigated in this study. The method is based on the fact that coal is weakly diamagnetic, while most of the minerals present are weakly to moderately paramagnetic. In the experimental studies, Manisa and Can lignites which have three different particular sizes (-1500+1000, -1000+500, -500+100 micron) were used. For the particular size of -1500+1000 micron, the magnetic fraction which was separated from Can lignite contained 24 % pyritic sulfur which was less than that of the ground coal. The amount of pyritic sulfur increased in the non-magnetic fraction of Manisa coal. The ash content of non-magnetic fraction which was separated from the particular size of -1000+500 micron of the Manisa coal reduced 20 %, while the value of calorie of coal was enhanced 15 % according to the ground coal. The amount of ash reduction in the non-magnetic fractions of Can lignites was slightly increased along with the value of calorie of coal was a little enhanced. (author)

469

Application of high gradient magnetic separation principles to magnetic drug targeting  

A hypothetical magnetic drug targeting system, utilizing high gradient magnetic separation (HGMS) principles, was studied theoretically using FEMLAB simulations. This new approach uses a ferromagnetic wire placed at a bifurcation point inside a blood vessel and an externally applied magnetic field, to magnetically guide magnetic drug carrier particles (MDCP) through the circulatory system and then to magnetically retain them at a target site. Wire collection (CE) and diversion (DE) efficiencies were defined and used to evaluate the system performance. CE and DE both increase as the strength of the applied magnetic field (0.3-2.0 T), the amount of ferromagnetic material (iron) in the MDCP (20-100%) and the size of the MDCP (1-10 {mu}m radius) increase, and as the average inlet velocity (0.1-0.8 m s{sup -1}), the size of the wire (50-250 {mu}m radius) and the ratio (4-10) of the parent vessel radius (0.25-1.25 mm radius) to wire radius decrease. The effect of the applied magnetic field direction (0 deg. and 90 deg. ) on CE and DE was minimal. Under these plausible conditions, CEs as high as 70% were obtained, with DEs reaching only 30%; however, when the MDCPs were allowed to agglomerate (4-10 {mu}m radius), CEs and DEs of 100% were indeed achieved. These results reveal that this new magnetic drug targeting approach for magnetically collecting MDCPs at a target site, even in arteries with very high velocities, is feasible and very promising; this new approach for magnetically guiding MDCPs through the circulatory system is also feasible but more limited. Overall, this study shows that magnetic drug targeting, based on HGMS principles, has considerable promise as an effective drug targeting tool with many potential applications.

470

Application of high gradient magnetic separation principles to magnetic drug targeting  

A hypothetical magnetic drug targeting system, utilizing high gradient magnetic separation (HGMS) principles, was studied theoretically using FEMLAB simulations. This new approach uses a ferromagnetic wire placed at a bifurcation point inside a blood vessel and an externally applied magnetic field, to magnetically guide magnetic drug carrier particles (MDCP) through the circulatory system and then to magnetically retain them at a target site. Wire collection (CE) and diversion (DE) efficiencies were defined and used to evaluate the system performance. CE and DE both increase as the strength of the applied magnetic field (0.3-2.0T), the amount of ferromagnetic material (iron) in the MDCP (20-100%) and the size of the MDCP (1-10?m radius) increase, and as the average inlet velocity (0.1-0.8ms-1), the size of the wire (50-250?m radius) and the ratio (4-10) of the parent vessel radius (0.25-1.25mm radius) to wire radius decrease. The effect of the applied magnetic field direction (0° and 90°) on CE and DE was minimal. Under these plausible conditions, CEs as high as 70% were obtained, with DEs reaching only 30%; however, when the MDCPs were allowed to agglomerate (4-10?m radius), CEs and DEs of 100% were indeed achieved. These results reveal that this new magnetic drug targeting approach for magnetically collecting MDCPs at a target site, even in arteries with very high velocities, is feasible and very promising; this new approach for magnetically guiding MDCPs through the circulatory system is also feasible but more limited. Overall, this study shows that magnetic drug targeting, based on HGMS principles, has considerable promise as an effective drug targeting tool with many potential applications.

471

Environmental friendly crush-magnetic separation technology for recycling metal-plated plastics from end-of-life vehicles.  

Metal-plated plastics (MPP), which are important from the standpoint of aesthetics or even performance, are increasingly employed in a wide variety of situations in the automotive industry. Serious environmental problems will be caused if they are not treated appropriately. Therefore, recycling of MPP is an important subject not only for resource recycling but also for environmental protection. This work represents a novel attempt to deal with the MPP. A self-designed hammer crusher was used to liberate coatings from the plastic substrate. The size distribution of particles was analyzed and described by the Rosin-Ramml